CN108219532B - Energy-saving and emission-reducing high strength fluid disperse dyes and preparation method thereof and application - Google Patents
Energy-saving and emission-reducing high strength fluid disperse dyes and preparation method thereof and application Download PDFInfo
- Publication number
- CN108219532B CN108219532B CN201711428524.0A CN201711428524A CN108219532B CN 108219532 B CN108219532 B CN 108219532B CN 201711428524 A CN201711428524 A CN 201711428524A CN 108219532 B CN108219532 B CN 108219532B
- Authority
- CN
- China
- Prior art keywords
- disperse
- disperse dyes
- emission
- saving
- energy
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0001—Post-treatment of organic pigments or dyes
- C09B67/0002—Grinding; Milling with solid grinding or milling assistants
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0033—Blends of pigments; Mixtured crystals; Solid solutions
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/008—Preparations of disperse dyes or solvent dyes
- C09B67/0082—Preparations of disperse dyes or solvent dyes in liquid form
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
- D06P3/54—Polyesters using dispersed dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/82—Textiles which contain different kinds of fibres
- D06P3/8204—Textiles which contain different kinds of fibres fibres of different chemical nature
- D06P3/8276—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing ester groups
Abstract
Public affairs of the present invention are related to a kind of energy-saving and emission-reducing high strength fluid disperse dyes and preparation method thereof and application, and the liquid disperse dyes are suitable for dyeing and the stamp of textile dyeing, especially terylene and its blended fabric.Total weight of the liquid disperse dyes based on the liquid disperse dyes, including following component: one or more disperse dyes original dyestuff total weight percents are 36%~50%, the auxiliary agent that weight percent is 4.1%~11%, 45%~55% water that weight percent is；The weight ratio of the auxiliary agent and disperse dyes original dyestuff is 0.1~0.25:1.This kind of liquid disperse dyes are cheap, energy-saving and emission-reduction, dye strength height, good fluidity, be not easy to precipitate, dyeing residual liquid coloration is shallow, COD is low, every fastness ability is excellent.
Description
Technical field
It is described the present invention relates to a kind of energy-saving and emission-reducing high strength fluid disperse dyes and preparation method thereof and application
Liquid disperse dyes are coloured suitable for synthetic fibers, especially the dyeing of terylene and its blended fabric and stamp.
Background technique
In recent years, as environmental problem is got worse, country is higher and higher to the requirement in terms of environmental protection, to textile printing and dyeing row
The regulation of industry is also increasingly stringenter, and there is an urgent need to the high-intensitive dyestuffs of energy-saving and emission-reduction for textile printing and dyeing enterprises.
Liquid dyes are to develop to process dosage form than faster dyestuff in recent years, since it is easy with production method, uses
The advantages that dyeability can be improved in easy to operate, energy-saving and emission-reduction, and by the great attention of printing and dyeing mill, development speed is very fast.
Liquid dyes are prepared with following features: 1, liquid dyes do not need the process such as dry, granulation, molding, therefore
Process equipment greatly simplifies, and production process is obviously shortened；2, the storage stability of liquid dyes is poor, is easy to produce precipitating, because
This requires reasonable selection dispersant with high efficiency and other matched addition auxiliary agents, more needs to the formulating of commodity, preparation process
It keeps on improving；3, it needs using advanced microemulsified, pulverize dispersion suspended substance processing technology, for water-insoluble dye
Material, can also produce and process stable liquid dyes dispersion by wet type superfine communication technique；4, it is particularly suitable for dispersion dye
The production and processing of material reduces impurity so that disperse dyes be made further to be purified processing, improves purity.
Liquid disperse dyes have following items basic demand: 1, the dispersion of liquid should be more stable, can be in longer-term
Time lower storage；2, there is good mobility, pump conveying can be used, can toppled over；3, it is easy at normal temperature or in cold water
It disperses or dissolves, it can or blending miscible with similar or other dyestuffs；4, noxious material is free of, PH is neutrality；5, it should mention as far as possible
High dye strength；6, a variety of dyeing and printing process are applicable to.
The advantages of liquid disperse dyes: 1, good application performance uses always powder in printing and dyeing industry for a long time
Shape, granular dyes, when sizing mixing or preparing dye liquor, dyestuff dust is most troubling problem, not only influences environment, hinders labor
Dynamic protection, and be often attached on the apparatus of ingredient or suspend in the dye liquor foam of preparation.Big not be dispersed or dissolved
The grain dyestuff that dyestuff, especially solubility are small, dispersion performance is poor, wettability and dispersion performance are all poor, are easy mutually to cohere
At agglomerate, it is easy that fabric is made to form fault in dyeing, influences product quality.And the above problem is substantially not present in liquid dyes,
The generation of dyeing defect can be significantly reduced.2, migration phenomenon is reduced, the migration of dyestuff is a problem deserving of attention, dyestuff
Migration degree is related with perhaps various factors.It is again mainly related with the content of auxiliary agent in dyestuff.It is related studies have shown that many points
Powder, wetting agent have the tendency that increasing dyestuff occurs migration.In liquid dyes processing formula, due to dispersing agent dosage compared with
Solid fraction dyestuff substantially reduce (as soon as correspond generally to liquid dyes five/or less), so also effectively reducing dyeing
Migration degree when post-process treatment: 3, can be improved dye-uptake, and some non-water soluble dyes, especially disperse dyes are washed in dye
When synthetic fibre or other synthetic fibers, grain fineness is important.Usual powdery, granular dyes are needed after being pulverized by drying process,
This just inevitably makes partial particulate generate cohesion, dispersion performance decline.Therefore, solid fraction dyestuff is thick compared with the particle of liquid dyes
Greatly, same amount of powder dye and liquid dyes hot melt dye terylene, as a result, upper dye of the liquid dyes than powder dye
Rate is high, and maximum differential can reach 50% or more sometimes.And hot melt when dyeing powder dye be also easy to produce fault, and liquid dyes
It but can be to avoid such problems；4, liquid dyes reduce production cost, and liquid dyes compare with solid fraction dyestuff, do not need drying
Process, also do not need dry grinding and dry blending process: this just substantially reduces the technological process of production.Drying is one in production
Highly energy-consuming operating process eliminates drying and just saves production cost, in addition, with water instead of part of auxiliary in liquid dyes
Use, largely also reduce cost of material, thus liquid dyes can be effectively reduced dyestuff cost of material and
Production cost；5, the COD in dyeing residual liquid is reduced, the dye dispersant as used in liquid dyes and other auxiliary agents are relatively
Few, allowing for COD content in dyeing residual liquid naturally reduces；6, the coloration for reducing dyeing residual liquid, due to liquid dyes dye uptake
Higher than powder dye, dyestuff remaining in raffinate is less after dyeing, and the coloration of raffinate is substantially reduced；7, with present labour city
The increased costs of field, more and more printing and dyeing enterprises have used automation process equipment, and liquid disperse dyes are particularly suitable for automatic
Change metering, obtains a large amount of application therewith.
The former dyestuff weight percent control range of liquid disperse dyes on existing market is 17.9%~36%, auxiliary agent
Weight percent control range is 4.5%~14.4%, auxiliary agent and former dyestuff weight percent control range are 0.25~0.4:
1, there are liquid dyes low strength, in application, there are a little limitations for printing and dyeing mill, and auxiliary agent content is higher, the color of raffinate after dyeing
Degree abs value, COD are higher, and there are no the purposes for really realizing optimal energy-saving and emission-reduction.
Summary of the invention
The present invention in view of the shortcomings of the prior art, provide a kind of cheap, energy-saving and emission-reduction, dye strength height, good fluidity,
It is not easy the liquid disperse dyes precipitated, dyeing residual liquid coloration is shallow, COD is low, every fastness ability is excellent.
In order to solve the above-mentioned technical problem, the present invention is addressed by following technical proposals: energy-saving and emission-reducing is high-intensitive
Liquid disperse dyes, based on the total weight of the liquid disperse dyes, including following component: one or more disperse dyes original dyes
Expect total weight percent be 36%~50%, weight percent be 4.1%~11% auxiliary agent, weight percent be 45%~
55% water；The weight ratio of the auxiliary agent and disperse dyes original dyestuff is 0.1~0.25:1.
In above-mentioned technical proposal, it is preferred that the disperse dyes original dyestuff is disperse orange 288, disperse orange 30, disperse orange
31, disperse orange 61, Red-1 200 45, Red-1 200 53, Red 167, disperse blue 54, Disperse Blue-56, disperse blue 60, disperse blue
73, disperse blue 77, Disperse Blue-79, disperse blue 165, disperse blue 183:1, disperse blue 291, disperse blue 291:1, disperse violet 93, point
Dissipate one of purple 93:1 or a variety of combinations.
In above-mentioned technical proposal, it is preferred that the weight ratio of the auxiliary agent and disperse dyes original dyestuff is 0.2~0.25:1.
In above-mentioned technical proposal, it is preferred that the auxiliary agent be dye dispersant or be dye dispersant with emulsifier, help
Stain, non-ionic dispersing agent, the anti-condensation poly- agent of anti-precipitating, anticorrosion and bactericidal agent, defoaming agent, antifreezing agent, chelating agent, polyalcohol, oneself
Lactams, hydroxyethyl cellulose, ethylenediamine polyethers, combination one or more in anhydrous sodium sulphate.
In above-mentioned technical proposal, it is preferred that the dye dispersant is lignin 83A, lignin 85A, methyl naphthalene sulfonic acid
One or more combination in formaldehyde condensation products, benzyl naphthalene sulfonic acid-formaldehyde condensation product.
In above-mentioned technical proposal, it is preferred that the solid content of the energy-saving and emission-reducing high strength fluid disperse dyes is 45%
~55%.
The present invention also provides the preparation methods of energy-saving and emission-reducing high strength fluid disperse dyes in the present invention, will be a kind of or more
Kind disperse dyes original dyestuff, auxiliary agent and water carry out mixed processing with sand mill or grinder in proportion, and liquid disperse dyes are made.
The present invention also provides energy-saving and emission-reducing high strength fluid disperse dyes according to the present invention to be used for textile dyeing
Purposes.
Preferably, the fabric is terylene and its blended fabric.
The present invention also provides a kind of fabrics, and the energy-saving and emission-reducing high strength fluid disperse dyes carry out through the invention
Dyeing and stamp are made.
Compared with prior art, the present invention having the following beneficial effects: energy-saving and emission-reducing high intensity liquid provided by the invention
Body disperse dyes are cheap, energy-saving and emission-reduction, dye strength height, good fluidity, be not easy to precipitate, dyeing residual liquid coloration is shallow, COD
Low, every fastness ability is excellent.
Specific embodiment
Present invention is further described in detail With reference to embodiment: the dispersion of energy-saving and emission-reducing high strength fluid
Dyestuff, based on the total weight of the liquid disperse dyes, including following component: one or more disperse dyes original dyestuff total weights
Percentage is 36%~50%, the auxiliary agent that weight percent is 4.1%~11%, 45%~55% water that weight percent is；
The weight ratio of the auxiliary agent and disperse dyes original dyestuff is 0.1~0.25:1.
The disperse dyes original dyestuff can be disperse orange 288, disperse orange 30, disperse orange 31, disperse orange 61, disperse red
145, Red-1 200 53, Red 167, disperse blue 54, Disperse Blue-56, disperse blue 60, disperse blue 73, disperse blue 77, disperse blue
79, one of disperse blue 165, disperse blue 183:1, disperse blue 291, disperse blue 291:1, disperse violet 93, disperse violet 93:1 or
A variety of combinations is also possible to other dyestuffs of same type.
The weight ratio of the auxiliary agent and disperse dyes original dyestuff is 0.2~0.25:1
The auxiliary agent is dye dispersant or is dye dispersant and emulsifier, dyeing auxiliaries, non-ionic dispersing agent, prevents
Precipitate anti-flocculating agent, anticorrosion and bactericidal agent, defoaming agent, antifreezing agent, chelating agent, polyalcohol, caprolactam, hydroxyethyl cellulose, second
One or more combination in diamine polyether, anhydrous sodium sulphate.
Anticorrosion and bactericidal agent is sodium benzoate, sodium nitrite, and chelating agent is EDTA and adjusts the sodium carbonate etc. of PH.
The dye dispersant is lignin 83A, lignin 85A, condensation compound of methyl naphthalene sulfonic acid and formaldehyde (such as diffusant
MF), combination one or more in benzyl naphthalene sulfonic acid-formaldehyde condensation product (such as dispersing agent CNF).
The solid content of the energy-saving and emission-reducing high strength fluid disperse dyes is 45%~55%.
The present invention also provides the preparation methods of energy-saving and emission-reducing high strength fluid disperse dyes, by one or more dispersions
Dyestuff original dyestuff, auxiliary agent and water carry out mixed processing with sand mill or grinder in proportion, and liquid disperse dyes are made.
The present invention also provides energy-saving and emission-reducing high strength fluid disperse dyes according to the present invention to be used for textile dyeing
Purposes.The fabric is terylene and its blended fabric.
The present invention also provides a kind of fabrics, and the energy-saving and emission-reducing high strength fluid disperse dyes carry out through the invention
Dyeing and stamp are made.
In following examples, the present invention selects disperse orange 288, disperse orange 30, disperse orange 31, disperse orange 61, dispersion
Red 145, Red-1 200 53, Red 167, disperse blue 54, Disperse Blue-56, disperse blue 60, disperse blue 73, disperse blue 77, disperse blue
79, one of disperse blue 165, disperse blue 183:1, disperse blue 291, disperse blue 291:1, disperse violet 93 or a variety of random mixing
With and auxiliary agent and water in the ratio blending of table 1 after, carrying out grinding distribution with sand mill, that a kind of energy-saving and emission-reducing is made is high-intensitive
Liquid disperse dyes.
The disperse dyes original dyestuff and auxiliary agent are known compound and can buy on the market, or can be by
Existing method preparation.
Table 1: the formula table of each embodiment.
Comparative example 1: 162.50 grams of water are added in 55.00 grams of disperse dyes original dyestuffs, 32.50 grams of dispersing agent MFs, with sand milling
Machine carries out grinding distribution, and liquid disperse dyes are made.
Comparative example 2: 161.50 grams of water are added in 43.50 grams of disperse dyes original dyestuffs, 43.50 grams of dispersing agent CNFs, with sand milling
Machine carries out grinding distribution, and liquid disperse dyes are made.
The liquid disperse dyes of embodiment 1 and comparative example 1-2 are tested for the property.The specific test method is as follows: weighing
The liquid disperse dyes and commercially available powder dye of 1.0 grams of embodiment 1-11 and comparative example 1-2 are respectively placed in the water of 500Om1
In, disperse dyes suspension is made.It draws 50m1 disperse dyes suspension to mix with the water of 50m1, adjusts dye bath pH with acetic acid
To 5,60 DEG C are then warming up to, while being respectively put into 2g polyester fiber and carrying out high-temperature pressure dyeing, is warming up to 130 in 35 minutes
DEG C, 45 minutes are kept the temperature, 80 DEG C of samplings are cooled to.
Observe cloth specimen coloured light and using side specified in GB/T6688-2008
Method surveys its dye strength, surveys it with ultraviolet-uisible spectrophotometer UV-2550
Dyeing residual liquid is used in the coloration abs value that wavelength is 380-750nm
One dichromate titration of GB11914-89 COD measures its dyeing residual liquid
COD, data measured are shown in Table 2.
Table 2: the detection data table of each embodiment and comparative example.
As shown in Table 2, compared with comparative example 1-2, the time for occurring precipitating obtains the liquid disperse dyes of embodiment 1-11
Extend, to transport and using bringing great convenience.And the liquid disperse dyes of embodiment 1-11 and comparative example 1-2 with
And powder dye is compared, dyeing residual liquid coloration is shallow, COD is low, more environmentally-friendly.
Claims (10)
1. energy-saving and emission-reducing high strength fluid disperse dyes, it is characterised in that: the total weight based on the liquid disperse dyes, packet
Include following component: one or more disperse dyes original dyestuff total weight percents be 39.9%~50%, weight percent be 5%~
10.5% auxiliary agent, 45%~54% water that weight percent is；The weight ratio of the auxiliary agent and disperse dyes original dyestuff is 0.1~
0.25: 1。
2. energy-saving and emission-reducing high strength fluid disperse dyes as described in claim 1, it is characterised in that: the disperse dyes are former
Dyestuff is disperse orange 288, disperse orange 30, disperse orange 31, disperse orange 61, Red-1 200 45, Red-1 200 53, Red 167, dispersion
Indigo plant 54, Disperse Blue-56, disperse blue 60, disperse blue 73, disperse blue 77, Disperse Blue-79, disperse blue 165, disperse blue 183:1, dispersion
One of indigo plant 291, disperse blue 291:1, disperse violet 93, disperse violet 93:1 or a variety of combinations.
3. energy-saving and emission-reducing high strength fluid disperse dyes as described in claim 1, it is characterised in that: the auxiliary agent and dispersion
The weight ratio of dyestuff original dyestuff is 0.2~0.25:1.
4. energy-saving and emission-reducing high strength fluid disperse dyes as described in claim 1, it is characterised in that: the auxiliary agent is dyestuff
Dispersing agent is dye dispersant and emulsifier, dyeing auxiliaries, non-ionic dispersing agent, the anti-condensation poly- agent of anti-precipitating, antisepsis and sterilization
Agent, defoaming agent, antifreezing agent, chelating agent, polyalcohol, caprolactam, hydroxyethyl cellulose, ethylenediamine polyethers, one in anhydrous sodium sulphate
Kind or a variety of combinations.
5. energy-saving and emission-reducing high strength fluid disperse dyes as claimed in claim 4, it is characterised in that: the dye dispersant
It is one or more in lignin 83A, lignin 85A, condensation compound of methyl naphthalene sulfonic acid and formaldehyde, benzyl naphthalene sulfonic acid-formaldehyde condensation product
Combination.
6. energy-saving and emission-reducing high strength fluid disperse dyes as described in claim 1, it is characterised in that: the energy-saving and emission-reducing
The solid content of high strength fluid disperse dyes is 45%~55%.
7. the preparation method of energy-saving and emission-reducing high strength fluid disperse dyes as claimed in any one of claims 1 to 6, special
Sign is: one or more disperse dyes original dyestuffs, auxiliary agent and water are subjected to mixed processing with sand mill or grinder in proportion,
Liquid disperse dyes are made.
8. the use that energy-saving and emission-reducing high strength fluid disperse dyes as claimed in any one of claims 1 to 6 are used for textile dyeing
On the way.
9. the purposes of energy-saving and emission-reducing high strength fluid disperse dyes as claimed in claim 8, it is characterised in that: the fabric
For terylene and its blended fabric.
10. a kind of fabric, it is characterised in that: high-strength by using energy-saving and emission-reducing as claimed in any one of claims 1 to 6
Degree liquid disperse dyes carry out dyeing and stamp is made.
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711428524.0A CN108219532B (en) | 2017-12-26 | 2017-12-26 | Energy-saving and emission-reducing high strength fluid disperse dyes and preparation method thereof and application |
| PCT/CN2018/000135 WO2019127611A1 (en) | 2017-12-26 | 2018-04-10 | Energy-saving and emission-reducing high-strength liquid disperse dye, preparation method therefor, and application thereof |
| BR112019014281A BR112019014281A2 (en) | 2017-12-26 | 2018-04-10 | high-strength dispersed liquid dye of the energy-saving and pollution-reducing type, its manufacturing process and its use process |
| KR1020197009789A KR20190084030A (en) | 2017-12-26 | 2018-04-10 | Energy saving and pollutant-abatement type high-strength liquid disperse dyes, manufacturing method and use method |
| JP2019518104A JP2020506247A (en) | 2017-12-26 | 2018-04-10 | High-strength liquid disperse dye with low energy-saving emission and its production method and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711428524.0A CN108219532B (en) | 2017-12-26 | 2017-12-26 | Energy-saving and emission-reducing high strength fluid disperse dyes and preparation method thereof and application |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108219532A CN108219532A (en) | 2018-06-29 |
| CN108219532B true CN108219532B (en) | 2019-07-05 |
Family
ID=62648872
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711428524.0A Active CN108219532B (en) | 2017-12-26 | 2017-12-26 | Energy-saving and emission-reducing high strength fluid disperse dyes and preparation method thereof and application |
Country Status (5)
| Country | Link |
|---|---|
| JP (1) | JP2020506247A (en) |
| KR (1) | KR20190084030A (en) |
| CN (1) | CN108219532B (en) |
| BR (1) | BR112019014281A2 (en) |
| WO (1) | WO2019127611A1 (en) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109054442A (en) * | 2018-09-17 | 2018-12-21 | 佛山市禅城区诺高环保科技有限公司 | A kind of preparation method of environment-friendly high-intensity liquid disperse dyes |
| CN110218466A (en) * | 2019-07-04 | 2019-09-10 | 九江富达实业有限公司 | A kind of superhigh intensity disperse dyes and preparation method thereof and application |
| CN110183874A (en) * | 2019-07-11 | 2019-08-30 | 浙江双冠染料有限公司 | A kind of red disperse dyes composition |
| CN111138886B (en) * | 2019-12-26 | 2021-05-04 | 东华大学 | Liquid disperse dye and preparation method and application thereof |
| CN111535051A (en) * | 2020-05-29 | 2020-08-14 | 西安工程大学 | Dyeing method of TPU (thermoplastic polyurethane) type 3D (three-dimensional) printing garment fabric |
| CN111549544B (en) * | 2020-05-29 | 2023-04-07 | 西安工程大学 | Dyeing method of ABS type 3D printing garment fabric |
| CN111849200A (en) * | 2020-07-14 | 2020-10-30 | 浙江博澳新材料股份有限公司 | 250% -360% strength disperse turquoise blue dye and preparation method thereof |
| CN112480711A (en) * | 2020-12-11 | 2021-03-12 | 九江富达实业有限公司 | Preparation method and application of high-strength disperse brilliant blue dye |
| CN112778796B (en) * | 2021-01-07 | 2023-05-12 | 浙江万丰化工股份有限公司 | Energy-saving emission-reducing high-stability liquid disperse dye and preparation method and application thereof |
| CN112981983A (en) * | 2021-04-01 | 2021-06-18 | 浙江大能纺织印染有限公司 | Liquid disperse dye capable of reducing COD (chemical oxygen demand) discharge and preparation method and dyeing method thereof |
| CN115197584A (en) * | 2021-04-12 | 2022-10-18 | 福建莱得化工科技有限公司 | Liquid disperse dye beneficial to preventing skinning and preparation method thereof |
| CN114213870A (en) * | 2021-12-27 | 2022-03-22 | 维昂(山东)纺织科技有限公司 | High-exhaustion-rate liquid disperse dye and preparation method and application thereof |
| CN114525044A (en) * | 2021-12-28 | 2022-05-24 | 浙江龙盛染料化工有限公司 | Sol type liquid disperse dye, preparation and application thereof |
| CN116041980A (en) * | 2022-12-27 | 2023-05-02 | 浙江欧亚数码科技有限公司 | Disperse liquid dye for continuous hot melt dyeing of polyester |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104448933A (en) * | 2014-12-31 | 2015-03-25 | 浙江闰土股份有限公司 | Red liquid disperse dye and preparation method and usage thereof |
| CN104497631A (en) * | 2014-12-31 | 2015-04-08 | 浙江闰土股份有限公司 | Blue liquid disperse dye and preparation method and application thereof |
| CN104530763A (en) * | 2014-12-31 | 2015-04-22 | 浙江闰土染料有限公司 | Blue liquid disperse dye and preparation method and application thereof |
| CN104530762A (en) * | 2014-12-31 | 2015-04-22 | 浙江闰土染料有限公司 | Orange liquid disperse dye and preparation method and application thereof |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102558908B (en) * | 2011-12-31 | 2014-08-13 | 浙江博澳染料工业有限公司 | Compound high-strength disperse dye |
| CN104710840B (en) * | 2013-12-31 | 2016-10-12 | 江苏吉华化工有限公司 | A kind of dispersion red dye composition |
| CN105585876B (en) * | 2015-12-31 | 2018-05-25 | 浙江闰土股份有限公司 | A kind of disperse dye composition, disperse dyes and its preparation method and application |
| CN106009775B (en) * | 2016-05-23 | 2017-07-07 | 杭州欣阳三友精细化工有限公司 | A kind of disperse dye composition, the preparation method and applications of weathering color fastness high |
| CN106752084A (en) * | 2016-12-31 | 2017-05-31 | 浙江博澳染料工业有限公司 | A kind of Novel disperse dyestuff composition and its preparation method and application |
-
2017
- 2017-12-26 CN CN201711428524.0A patent/CN108219532B/en active Active
-
2018
- 2018-04-10 JP JP2019518104A patent/JP2020506247A/en active Pending
- 2018-04-10 KR KR1020197009789A patent/KR20190084030A/en not_active Application Discontinuation
- 2018-04-10 BR BR112019014281A patent/BR112019014281A2/en not_active Application Discontinuation
- 2018-04-10 WO PCT/CN2018/000135 patent/WO2019127611A1/en active Application Filing
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104448933A (en) * | 2014-12-31 | 2015-03-25 | 浙江闰土股份有限公司 | Red liquid disperse dye and preparation method and usage thereof |
| CN104497631A (en) * | 2014-12-31 | 2015-04-08 | 浙江闰土股份有限公司 | Blue liquid disperse dye and preparation method and application thereof |
| CN104530763A (en) * | 2014-12-31 | 2015-04-22 | 浙江闰土染料有限公司 | Blue liquid disperse dye and preparation method and application thereof |
| CN104530762A (en) * | 2014-12-31 | 2015-04-22 | 浙江闰土染料有限公司 | Orange liquid disperse dye and preparation method and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2019127611A1 (en) | 2019-07-04 |
| KR20190084030A (en) | 2019-07-15 |
| BR112019014281A2 (en) | 2020-04-28 |
| CN108219532A (en) | 2018-06-29 |
| JP2020506247A (en) | 2020-02-27 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN108219532B (en) | Energy-saving and emission-reducing high strength fluid disperse dyes and preparation method thereof and application | |
| CN100503740C (en) | Dispersed black dye composition | |
| CN101798472B (en) | Black and blue disperse dye composition | |
| CN101792615A (en) | Environment-friendly dark blue and black series compound disperse dye and production method thereof | |
| CN101735664B (en) | Disperse scarlet dye composition | |
| CN102344695B (en) | Composite dye composition, composite disperse dye and preparation method thereof | |
| CN100558822C (en) | A kind of disperse dye composition | |
| CN100422270C (en) | Composite disperse red dye composition | |
| CN105255216A (en) | Disperse dye composition, disperse dye as well as preparation method and application of disperse dye | |
| CN110373043A (en) | It is a kind of blue to black disperse dye composition and dye preparations | |
| CN104530763B (en) | Blue liquid disperse dyes and its preparation method and purposes | |
| CN105255215A (en) | Disperse dye composition, disperse dye as well as preparation method and application of disperse dye | |
| CN103589190A (en) | Disperse red dye composition | |
| CN109705618A (en) | A kind of dispersion bright red dye composite and dye preparations | |
| CN104448933B (en) | Red liquid disperse dyes and its preparation method and purposes | |
| CN104650621B (en) | Disperse dye composition, disperse dyes and its production and use | |
| CN104945954B (en) | A kind of dispersion red dye composition and dye preparations | |
| CN101275039A (en) | Disperse orange dye composition | |
| CN104530761B (en) | Red liquid disperse dyes and its preparation method and purposes | |
| CN104497631B (en) | Blue liquid disperse dyes and its preparation method and purposes | |
| TW202100666A (en) | Energy saving and pollutant reducing type high-strength liquid dispersion dye, manufacturing method thereof and using method thereof | |
| CN104530764B (en) | Yellow liquid disperse dyes and its preparation method and purposes | |
| CN104530760B (en) | Red liquid disperse dyes and its preparation method and purposes | |
| CN104448929B (en) | Grey disperse dye compound, disperse dye and preparation method and usage of disperse dye | |
| CN105001672B (en) | A kind of orange disperse dye composition, disperse dyes and its production and use |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address |
Address after: 312300, No. three, No. 3, Shangyu economic and Technological Development Zone, Hangzhou Bay, Shangyu District, Zhejiang, Shaoxing Patentee after: Zhejiang Bo'ao new materials Co., Ltd Address before: 312369, No. three, No. 3, Shangyu economic and Technological Development Zone, Hangzhou Bay, Zhejiang, Shaoxing, China Patentee before: ZHEJIANG BOAO DYESTUFF INDUSTRY Co.,Ltd. |
|
| CP03 | Change of name, title or address |