CN108203551A - A kind of method prepared by alkali resistance disperse dye composition - Google Patents
A kind of method prepared by alkali resistance disperse dye composition Download PDFInfo
- Publication number
- CN108203551A CN108203551A CN201611179951.5A CN201611179951A CN108203551A CN 108203551 A CN108203551 A CN 108203551A CN 201611179951 A CN201611179951 A CN 201611179951A CN 108203551 A CN108203551 A CN 108203551A
- Authority
- CN
- China
- Prior art keywords
- disperse
- mass fraction
- alkali resistance
- dye composition
- disperse dye
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0033—Blends of pigments; Mixtured crystals; Solid solutions
- C09B67/0041—Blends of pigments; Mixtured crystals; Solid solutions mixtures containing one azo dye
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
- D06P3/54—Polyesters using dispersed dyestuffs
Landscapes
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Abstract
The present invention discloses a kind of method prepared by alkali resistance disperse dye composition, belongs to technical field of dye.It is according to weight fraction ratio：35 mass fraction of disperse violet is 40%~60%, and disperse red 60 mass fraction is 20%~30%, and Disperse Red 343 mass fraction is 15%~30%, and 76 mass fraction of disperse red is 1%~5%, and surplus is auxiliary agent.The dye composite of the present invention while original dyestuff performance is retained, can improve the alkaline resistance properties of dyestuff.It effectively solves in polyester fabric stamp industry, realizes terylene etching and carried out while stamp, simplify the technological process of production, reduce the labor intensity of Workshop Production worker.
Description
Technical field
The present invention relates to a kind of preparation methods of alkali resistance disperse dye composition, belong to technical field of dye.
Background technology
The burn-out printing of conventional fabrics is poor using the acidproof or alkaline resistance properties of fiber, with acid or alkali removal one of which fibre
The processing method of dimension, since the alkali resistance of disperse dyes is not good enough.The poor-performing of particularly resistance to sodium hydroxide, therefore cannot obtain
The printing quality of colored etching.The rotten suede in part is first mostly carried out with alkali using white polyester flannelette, is obtained in concave-convex matte, then pass through
Dyeing or stamp.The present invention improves the alkali resistance of disperse dyes, effectively solves in polyester fabric stamp industry, it is rotten to realize terylene
Flower simplifies the technological process of production, reduces the labor intensity of Workshop Production worker with being carried out while stamp.While dyestuff
The raising of utilization rate and time processing success rate, has not only simplified production cost, reduces the dosage of highly basic, also reduces " three
It is useless " discharge, be conducive to environmental protection.The fabric of high-quality terylene etching special efficacy Disperse Printing processing, has excellent
Soaping fastness etc. takes fastness ability, meets the pursuit of people's high-quality life.
Invention content
In view of the deficiencies of the prior art, it is a primary object of the present invention to provide a kind of alkali resistance disperse dye composition
Preparation method.
To realize aforementioned invention purpose, the technical solution that the present invention takes is as follows：
A kind of alkali resistance disperse dye composition, which is characterized in that consisting of 35 mass fraction of disperse violet for 40%~
60%, disperse red 60 mass fraction is 20%~30%, and Disperse Red 343 mass fraction is 15%~30%, 76 mass of disperse red
Score is 1%~5%, and surplus is auxiliary agent.
The auxiliary agent is lignosulfonates and naphthyl sulphonic acids salt quality score 2:1 mixture.
The alkali resistance disperse dye composition, which is characterized in that the preparation of the composition includes the following steps：
Each component is added according to aforementioned proportion, particlized processing, spray drying are crushed under the existence condition of water, and add in dispersion
Agent stirs 1.5h in grinder blending equipment, obtains finished product after oven drying again.
The oven drying places into 100 DEG C of baking ovens first to dry 15min in 60 DEG C and bakes 5min.
Alkali resistance disperse dye composition prepared by this method can be in the dye bath higher than normal dyeing alkalinity 20% smoothly
The dyeing to fabric is completed, dye-uptake is high, and uniformity is good, is generated without apparent precipitation.
Embodiment
A kind of alkali resistance disperse dye composition is prepared, respectively mixes following component, 35 mass fraction of disperse violet is
50%, disperse red 60 mass fraction is 20%, and Disperse Red 343 mass fraction is 15%, and 76 mass fraction of disperse red is 5%, wood
Mahogany sulfonate is 6.7%, and naphthyl sulphonic acids salt is 3.3%, forms beauty's dye composition.It is weighed according to said components proportioning
Each component is matched, and sized particlesization processing, the step is ground by sand for abrasive media, grinds filter sand
Son.Oven drying is spray-dried or be put into, oven drying is put into and includes first passing through 60 DEG C of prebake 15min, then place into 100
DEG C bake 5min.And add in dispersant and stirred 1.5 hours in blending equipment, dry-mixed spelling is carried out under conditions of less than 30 DEG C,
Finished product after mixing.In use, taking finished product 1g, be scattered in 200g cold water, taken after being sufficiently stirred after l0mL with 90mL
Water is uniformly mixed, and is adjusted pH value to 5 with dilute acetic acid solution, is put into 5g polyester fibers and is dyed, obtain the dyeing and weaving object of red color.
Dyestuff prepared by the present invention can be dyed in pH ranges 4.5-8.0, and dyestuff dye-uptake is high, good level-dyeing property, dyeability
It is excellent.4 grades of fabric sublimation reliability after dyeing, 4 grades of washing fastness, 4 grades of fastness to rubbing.
Claims (4)
1. a kind of alkali resistance disperse dye composition, which is characterized in that consisting of 35 mass fraction of disperse violet for 40%~
60%, disperse red 60 mass fraction is 20%~30%, and Disperse Red 343 mass fraction is 15%~30%, 76 mass of disperse red
Score is 1%~5%, and surplus is auxiliary agent.
2. according to the alkali resistance disperse dye composition described in claim 1, which is characterized in that the auxiliary agent is lignin
Sulfonate and naphthyl sulphonic acids salt quality score 2:1 mixture.
3. the alkali resistance disperse dye composition as described in claim 1-2, it is characterised in that the preparation of the composition
Include the following steps：Each component is added according to aforementioned proportion, particlized processing is crushed under the existence condition of water, spraying is dry
It is dry, and add in dispersant and stir 1.5h in grinder blending equipment, again finished product is obtained after oven drying.
4. alkali resistance disperse dye composition as described in claim 3, it is characterised in that the oven drying is first 60
15min is dried in DEG C, places into 100 DEG C of baking ovens and bakes 5min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611179951.5A CN108203551A (en) | 2016-12-20 | 2016-12-20 | A kind of method prepared by alkali resistance disperse dye composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611179951.5A CN108203551A (en) | 2016-12-20 | 2016-12-20 | A kind of method prepared by alkali resistance disperse dye composition |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108203551A true CN108203551A (en) | 2018-06-26 |
Family
ID=62601936
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611179951.5A Pending CN108203551A (en) | 2016-12-20 | 2016-12-20 | A kind of method prepared by alkali resistance disperse dye composition |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108203551A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109629254A (en) * | 2018-12-28 | 2019-04-16 | 常州安达环保科技有限公司 | A kind of nano-dispersed dye paste and preparation method thereof suitable for terylene printing and dyeing |
-
2016
- 2016-12-20 CN CN201611179951.5A patent/CN108203551A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109629254A (en) * | 2018-12-28 | 2019-04-16 | 常州安达环保科技有限公司 | A kind of nano-dispersed dye paste and preparation method thereof suitable for terylene printing and dyeing |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104790226B (en) | Anti-staining dyeing method of polyamide-cotton fabric | |
| CN103740136B (en) | A kind of high fastness disperses bright blue dye composite | |
| CN102618079A (en) | Disperse dye composite, dyeing method and preparation method for disperse dye composite | |
| CN105803828A (en) | Disperse/activated one-emulsion paste printing dye and printing technology thereof | |
| CN102618078A (en) | Disperse dye composition, dyeing method and preparation method of disperse dye composition | |
| CN107476081B (en) | Dyeing and finishing process of polyester fiber-cellulose fiber mixed textile | |
| CN109233337B (en) | Black dye composition and dye product | |
| CN102677486B (en) | Formaldehyde-free pigment printing covering white slurry, preparation method and application thereof | |
| CN105908534A (en) | process for dyeing viscose yarns on bobbins | |
| CN102618080A (en) | Disperse dye composition, dyeing method and preparation method of disperse dye composition | |
| CN103450705B (en) | Snow top dye and preparation method thereof | |
| CN102675916B (en) | Nano disperse black combined dye and preparation method thereof | |
| CN103469618B (en) | A kind of without urea printing with reactive dye mill base, manufacture method and dyeing method | |
| CN104945953A (en) | Alkali-resistant fast-dyeing disperse dye and preparation method thereof | |
| CN108203551A (en) | A kind of method prepared by alkali resistance disperse dye composition | |
| CN107326704B (en) | Leveling agent for cotton and preparation method thereof | |
| CN102888129B (en) | Disperse dye composition and applications thereof | |
| CN107298875A (en) | A kind of economic and environment-friendly type disperse dyes | |
| CN104447429B (en) | Environment protection acidic can pulling color Yellow dye compound, application and synthetic method | |
| CN106758321A (en) | A kind of disperse dyes alkalescence stamp composite paste material mill base and preparation method thereof and textile printing process | |
| CN102653635A (en) | Printing black disperse dyes | |
| CN104343022A (en) | Fluorescent dye and preparation method and application thereof | |
| CN105385192A (en) | Green and environment-friendly red reactive dye composite | |
| CN108976844B (en) | Red reactive dye composition and dye product | |
| CN108395734A (en) | A kind of dye for fabrics composition that water-wash resistance is strong |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20180626 |