CN108192552A - A kind of flame-proof antibiotic polyurethane glass glue - Google Patents

A kind of flame-proof antibiotic polyurethane glass glue Download PDF

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Publication number
CN108192552A
CN108192552A CN201711444646.9A CN201711444646A CN108192552A CN 108192552 A CN108192552 A CN 108192552A CN 201711444646 A CN201711444646 A CN 201711444646A CN 108192552 A CN108192552 A CN 108192552A
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Prior art keywords
parts
flame
glass glue
proof antibiotic
mixture
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CN201711444646.9A
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Chinese (zh)
Inventor
端连友
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Tianchang Mexico Glass Building Materials Co Ltd
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Tianchang Mexico Glass Building Materials Co Ltd
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Priority to CN201711444646.9A priority Critical patent/CN108192552A/en
Publication of CN108192552A publication Critical patent/CN108192552A/en
Withdrawn legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J175/00—Adhesives based on polyureas or polyurethanes; Adhesives based on derivatives of such polymers
    • C09J175/04—Polyurethanes
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/02—Non-macromolecular additives
    • C09J11/04—Non-macromolecular additives inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/02—Non-macromolecular additives
    • C09J11/06—Non-macromolecular additives organic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/08—Macromolecular additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20—Oxides; Hydroxides
    • C08K3/22—Oxides; Hydroxides of metals
    • C08K2003/221—Oxides; Hydroxides of metals of rare earth metal
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20—Oxides; Hydroxides
    • C08K3/22—Oxides; Hydroxides of metals
    • C08K2003/2217—Oxides; Hydroxides of metals of magnesium
    • C08K2003/222—Magnesia, i.e. magnesium oxide
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/32—Phosphorus-containing compounds
    • C08K2003/321—Phosphates
    • C08K2003/322—Ammonium phosphate
    • C08K2003/323—Ammonium polyphosphate
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/02—Flame or fire retardant/resistant

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Adhesives Or Adhesive Processes (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

The invention discloses a kind of flame-proof antibiotic polyurethane glass glue, raw material includes by weight：50 60 parts of base polyurethane prepolymer for use as, 8 15 parts of plasticizer, 2 10 parts of diatomite, 3 20 parts of talcum powder, 3 15 parts of lanthana, 3 16 parts of montmorillonite, 15 parts of carbon nanotube, 18 parts of galapectite, 1 2.5 parts of antioxidant, 0.3 1.2 parts of ultra-violet absorber, 0.1 0.35 parts of thixotropic agent, 0.1 0.5 parts of catalyst, 25 parts of antiseptic, 3 14 parts of fire retardant；The fire retardant is hydroxymethyl phenyl phosphinic acids, the mixture of polyimide modified magnesium hydroxide, three (neopentyl glycol phosphate phosphorus methylene) amine, polyphosphoric acid amine；The antiseptic is curcumin, the mixture of Citrated chitosan, 8 oxyquinolines, dandelion polyphenol, ε poly-D-lysines, glycine zine, zinc lactate.

Description

A kind of flame-proof antibiotic polyurethane glass glue
Technical field
The present invention relates to glass cement technical field more particularly to a kind of flame-proof antibiotic polyurethane glass glue.
Background technology
Glass cement is that various glass are carried out material that is be bonded and sealing with other base materials, is broadly divided into silicone adhesive and poly- ammonia Two major class of ester gum.Polyurethane is a kind of high molecular material, wide, adaptable, resistance to its manufactured glass cement performance adjustable extent Biological aging, moderate cost are widely used in numerous industries such as upholstery, construction industry, transportation industry.But polyurethane conduct has Machine object, anti-flammability are not fine, while do not have antibiotic property yet, and with its manufactured glass cement, there are anti-flammability and antibiotic property are poor The defects of, limit the application of glass cement.
Invention content
Technical problems based on background technology, the present invention propose a kind of flame-proof antibiotic polyurethane glass glue, glue Knotting strength is high, quick solidifying, excellent fireproof performance, and antibiotic property is strong.
A kind of flame-proof antibiotic polyurethane glass glue proposed by the present invention, raw material include by weight：Base polyurethane prepolymer for use as 50-60 parts, 8-15 parts of plasticizer, 2-10 parts of diatomite, 3-20 parts of talcum powder, 3-15 parts of lanthana, 3-16 parts of montmorillonite, carbon receives 1-5 parts of mitron, 1-2.5 parts of antioxidant, 0.3-1.2 parts of ultra-violet absorber, 0.1-0.35 parts of thixotropic agent, is urged at 1-8 parts of galapectite 0.1-0.5 parts of agent, 2-5 parts of antiseptic, 3-14 parts of fire retardant；
Wherein, the fire retardant is hydroxymethyl phenyl phosphinic acids, polyimide modified magnesium hydroxide, three (neopentyl glycol phosphorus Acid esters-phosphorus-methylene) amine, polyphosphoric acid amine mixture；
The antiseptic for curcumin, Citrated chitosan, 8-hydroxyquinoline, dandelion polyphenol, ε-poly-D-lysine, The mixture of glycine zine, zinc lactate.
Preferably, the plasticizer for chlorinated paraffin, ethylene-butyl acrylate copolymer, 5- hydroxyl dodecanoic acids glyceride, Tetraoctyl 1,2,4,5-benzenetetra-carboxylate is 3-10 by weight：5-12：1-4：The mixture of 3-15.
Preferably, the antioxidant is antioxidant 1010.
Preferably, the ultra-violet absorber is benzophenone tetracarboxylic dianhydride, 2- (bis- tertiary amyls of 2'- hydroxyls -3', 5'- Phenyl) benzotriazole, ultra-violet absorber UV234 by weight be 2-10:4-8:The mixture of 3-14.
Preferably, the thixotropic agent is aerosil.
Preferably, the catalyst is dibutyl tin laurate.
Preferably, hydroxymethyl phenyl phosphinic acids, polyimide modified magnesium hydroxide, three (neopentyl glycol phosphates-phosphorus-Asia Methyl) amine, polyphosphoric acid amine weight ratio be 4-10：4-16：3-9：5-10.
Preferably, curcumin, Citrated chitosan, 8-hydroxyquinoline, dandelion polyphenol, ε-poly-D-lysine, sweet ammonia Sour zinc, zinc lactate weight ratio be 3-10：3-9：4-10：4-18：5-10：5-9：3-10.
Flame-proof antibiotic polyurethane glass glue of the present invention, with hydroxymethyl phenyl phosphinic acids, polyimide modified hydrogen-oxygen Change magnesium, three (neopentyl glycol phosphate-phosphorus-methylene) amine, polyphosphoric acid amine cooperation as in fire retardant, with system diatomite, Lanthana, montmorillonite, carbon nanotube, galapectite cooperation, excellent fire-retardant of imparting glass cement while glass cement intensity is improved Property；With curcumin, Citrated chitosan, 8-hydroxyquinoline, dandelion polyphenol, ε-poly-D-lysine, glycine zine, zinc lactate Cooperation plays best synergistic effect, assigns glass cement excellent antibiotic property as antiseptic.
Specific embodiment
In the following, technical scheme of the present invention is described in detail by specific embodiment.
Embodiment 1
A kind of flame-proof antibiotic polyurethane glass glue proposed by the present invention, raw material include by weight：Base polyurethane prepolymer for use as 60 parts, 8 parts of plasticizer, 10 parts of diatomite, 3 parts of talcum powder, 15 parts of lanthana, 3 parts of montmorillonite, 5 parts of carbon nanotube, galapectite 1 Part, 2.5 parts of antioxidant, 0.3 part of ultra-violet absorber, 0.35 part of thixotropic agent, 0.1 part of catalyst, 5 parts of antiseptic, fire retardant 3 Part；
Wherein, the fire retardant is hydroxymethyl phenyl phosphinic acids, polyimide modified magnesium hydroxide, three (neopentyl glycol phosphorus Acid esters-phosphorus-methylene) amine, polyphosphoric acid amine mixture；
The antiseptic for curcumin, Citrated chitosan, 8-hydroxyquinoline, dandelion polyphenol, ε-poly-D-lysine, The mixture of glycine zine, zinc lactate.
Embodiment 2
A kind of flame-proof antibiotic polyurethane glass glue proposed by the present invention, raw material include by weight：Base polyurethane prepolymer for use as 50 parts, 15 parts of plasticizer, 2 parts of diatomite, 20 parts of talcum powder, 3 parts of lanthana, 16 parts of montmorillonite, 1 part of carbon nanotube, galapectite 8 Part, 1 part of antioxidant, 1.2 parts of ultra-violet absorber, 0.1 part of thixotropic agent, 0.5 part of catalyst, 2 parts of antiseptic, 14 parts of fire retardant；
Wherein, the fire retardant is hydroxymethyl phenyl phosphinic acids, polyimide modified magnesium hydroxide, three (neopentyl glycol phosphorus Acid esters-phosphorus-methylene) amine, polyphosphoric acid amine mixture；
The antiseptic for curcumin, Citrated chitosan, 8-hydroxyquinoline, dandelion polyphenol, ε-poly-D-lysine, The mixture of glycine zine, zinc lactate.
Embodiment 3
A kind of flame-proof antibiotic polyurethane glass glue proposed by the present invention, raw material include by weight：Base polyurethane prepolymer for use as 58 parts, 10 parts of plasticizer, 8.7 parts of diatomite, 5 parts of talcum powder, 13 parts of lanthana, 5 parts of montmorillonite, 2 parts of carbon nanotube, galapectite 2 parts, 2.3 parts of antioxidant, 0.5 part of ultra-violet absorber, 0.3 part of thixotropic agent, 0.15 part of catalyst, 4.3 parts of antiseptic, fire retardant 5 parts；
Wherein, the fire retardant is hydroxymethyl phenyl phosphinic acids, polyimide modified magnesium hydroxide, three (neopentyl glycol phosphorus Acid esters-phosphorus-methylene) amine, polyphosphoric acid amine mixture, and hydroxymethyl phenyl phosphinic acids, polyimide modified magnesium hydroxide, three (neopentyl glycol phosphate-phosphorus-methylene) amine, polyphosphoric acid amine weight ratio be 4：16：3：10；
The antiseptic for curcumin, Citrated chitosan, 8-hydroxyquinoline, dandelion polyphenol, ε-poly-D-lysine, The mixture of glycine zine, zinc lactate, and curcumin, Citrated chitosan, 8-hydroxyquinoline, dandelion polyphenol, ε-poly Lysine, glycine zine, zinc lactate weight ratio be 3：9：4：4：10：5：10；
The plasticizer is chlorinated paraffin, ethylene-butyl acrylate copolymer, 5- hydroxyl dodecanoic acids glyceride, equal benzene four Sour four monooctyl esters are 3 by weight：12：1：15 mixture；
The antioxidant is antioxidant 1010；
The ultra-violet absorber is benzophenone tetracarboxylic dianhydride, 2- (bis- tertiary amyl phenyl of 2'- hydroxyls -3', 5'-) benzene And triazole, ultra-violet absorber UV234 are 2 by weight:8:3 mixture；
The thixotropic agent is aerosil；
The catalyst is dibutyl tin laurate.
Embodiment 4
A kind of flame-proof antibiotic polyurethane glass glue proposed by the present invention, raw material include by weight：Base polyurethane prepolymer for use as 52 parts, 13 parts of plasticizer, 4 parts of diatomite, 17 parts of talcum powder, 6 parts of lanthana, 12 parts of montmorillonite, 3 parts of carbon nanotube, galapectite 7 Part, 1.6 parts of antioxidant, 1 part of ultra-violet absorber, 0.15 part of thixotropic agent, 0.4 part of catalyst, 2.6 parts of antiseptic, fire retardant 12 Part；
Wherein, the fire retardant is hydroxymethyl phenyl phosphinic acids, polyimide modified magnesium hydroxide, three (neopentyl glycol phosphorus Acid esters-phosphorus-methylene) amine, polyphosphoric acid amine mixture, and hydroxymethyl phenyl phosphinic acids, polyimide modified magnesium hydroxide, three (neopentyl glycol phosphate-phosphorus-methylene) amine, polyphosphoric acid amine weight ratio be 10：4：9：5；
The antiseptic for curcumin, Citrated chitosan, 8-hydroxyquinoline, dandelion polyphenol, ε-poly-D-lysine, The mixture of glycine zine, zinc lactate, and curcumin, Citrated chitosan, 8-hydroxyquinoline, dandelion polyphenol, ε-poly Lysine, glycine zine, zinc lactate weight ratio be 10：3：10：18：5：9：3；
The plasticizer is chlorinated paraffin, ethylene-butyl acrylate copolymer, 5- hydroxyl dodecanoic acids glyceride, equal benzene four Sour four monooctyl esters are 10 by weight：5：4：3 mixture；
The antioxidant is antioxidant 1010；
The ultra-violet absorber is benzophenone tetracarboxylic dianhydride, 2- (bis- tertiary amyl phenyl of 2'- hydroxyls -3', 5'-) benzene And triazole, ultra-violet absorber UV234 are 10 by weight:4:14 mixture；
The thixotropic agent is aerosil；
The catalyst is dibutyl tin laurate.
Embodiment 5
A kind of flame-proof antibiotic polyurethane glass glue proposed by the present invention, raw material include by weight：Base polyurethane prepolymer for use as 55 parts, 12 parts of plasticizer, 7 parts of diatomite, 13 parts of talcum powder, 8 parts of lanthana, 12 parts of montmorillonite, 2 parts of carbon nanotube, galapectite 5 Part, 2 parts of antioxidant, 1 part of ultra-violet absorber, 0.3 part of thixotropic agent, 0.25 part of catalyst, 3 parts of antiseptic, 11 parts of fire retardant；
Wherein, the fire retardant is hydroxymethyl phenyl phosphinic acids, polyimide modified magnesium hydroxide, three (neopentyl glycol phosphorus Acid esters-phosphorus-methylene) amine, polyphosphoric acid amine mixture, and hydroxymethyl phenyl phosphinic acids, polyimide modified magnesium hydroxide, three (neopentyl glycol phosphate-phosphorus-methylene) amine, polyphosphoric acid amine weight ratio be 7：11：5：8；
The antiseptic for curcumin, Citrated chitosan, 8-hydroxyquinoline, dandelion polyphenol, ε-poly-D-lysine, The mixture of glycine zine, zinc lactate, and curcumin, Citrated chitosan, 8-hydroxyquinoline, dandelion polyphenol, ε-poly Lysine, glycine zine, zinc lactate weight ratio be 7：5：8：12：7：6：8；
The plasticizer is chlorinated paraffin, ethylene-butyl acrylate copolymer, 5- hydroxyl dodecanoic acids glyceride, equal benzene four Sour four monooctyl esters are 7 by weight：11：3：12 mixture；
The antioxidant is antioxidant 1010；
The ultra-violet absorber is benzophenone tetracarboxylic dianhydride, 2- (bis- tertiary amyl phenyl of 2'- hydroxyls -3', 5'-) benzene And triazole, ultra-violet absorber UV234 are 8 by weight:5:12 mixture；
The thixotropic agent is aerosil；
The catalyst is dibutyl tin laurate.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto, Any one skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (8)

1. a kind of flame-proof antibiotic polyurethane glass glue, which is characterized in that its raw material includes by weight：Base polyurethane prepolymer for use as 50- 60 parts, 8-15 parts of plasticizer, 2-10 parts of diatomite, 3-20 parts of talcum powder, 3-15 parts of lanthana, 3-16 parts of montmorillonite, carbon nanometer 1-5 parts of pipe, 1-8 parts of galapectite, 1-2.5 parts of antioxidant, 0.3-1.2 parts of ultra-violet absorber, 0.1-0.35 parts of thixotropic agent, catalysis 0.1-0.5 parts of agent, 2-5 parts of antiseptic, 3-14 parts of fire retardant；
Wherein, the fire retardant for hydroxymethyl phenyl phosphinic acids, polyimide modified magnesium hydroxide, three (neopentyl glycol phosphate- Phosphorus-methylene) amine, polyphosphoric acid amine mixture；
The antiseptic is curcumin, Citrated chitosan, 8-hydroxyquinoline, dandelion polyphenol, ε-poly-D-lysine, sweet ammonia The mixture of sour zinc, zinc lactate.
2. flame-proof antibiotic polyurethane glass glue according to claim 1, which is characterized in that the plasticizer for chlorinated paraffin, Ethylene-butyl acrylate copolymer, 5- hydroxyl dodecanoic acids glyceride, tetraoctyl 1,2,4,5-benzenetetra-carboxylate are 3-10 by weight：5-12：1- 4：The mixture of 3-15.
3. flame-proof antibiotic polyurethane glass glue according to claim 1 or claim 2, which is characterized in that the antioxidant is antioxidant 1010。
4. according to any one of the claim 1-3 flame-proof antibiotic polyurethane glass glue, which is characterized in that the ultraviolet light is inhaled Receipts agent is benzophenone tetracarboxylic dianhydride, 2- (bis- tertiary amyl phenyl of 2'- hydroxyls -3', 5'-) benzotriazole, ultra-violet absorber UV234 is 2-10 by weight:4-8:The mixture of 3-14.
5. according to any one of the claim 1-4 flame-proof antibiotic polyurethane glass glue, which is characterized in that the thixotropic agent is Aerosil.
6. according to any one of the claim 1-5 flame-proof antibiotic polyurethane glass glue, which is characterized in that the catalyst is Dibutyl tin laurate.
7. according to any one of the claim 1-6 flame-proof antibiotic polyurethane glass glue, which is characterized in that hydroxymethyl phenyl Phosphonic acids, polyimide modified magnesium hydroxide, three (neopentyl glycol phosphate-phosphorus-methylene) amine, polyphosphoric acid amine weight ratio be 4- 10：4-16：3-9：5-10.
8. according to any one of the claim 1-7 flame-proof antibiotic polyurethane glass glue, which is characterized in that curcumin, lemon Acidified chitosan, 8-hydroxyquinoline, dandelion polyphenol, ε-poly-D-lysine, glycine zine, zinc lactate weight ratio be 3-10： 3-9：4-10：4-18：5-10：5-9：3-10.
CN201711444646.9A 2017-12-27 2017-12-27 A kind of flame-proof antibiotic polyurethane glass glue Withdrawn CN108192552A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109880574A (en) * 2019-03-06 2019-06-14 温州包鹿新材料有限公司 Antibacterial flame-retardant modified glass glue and preparation method thereof

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101402845A (en) * 2008-11-11 2009-04-08 北京市化学工业研究院 Process for producing flame-proof fluid sealant for construction

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101402845A (en) * 2008-11-11 2009-04-08 北京市化学工业研究院 Process for producing flame-proof fluid sealant for construction

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
国家食品安全风险评估中心等: "《食品安全国家标准汇编 通用标准》", 31 March 2014, 中国人口出版社 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109880574A (en) * 2019-03-06 2019-06-14 温州包鹿新材料有限公司 Antibacterial flame-retardant modified glass glue and preparation method thereof
CN109880574B (en) * 2019-03-06 2021-09-17 广东华成新材料有限公司 Antibacterial flame-retardant modified glass cement and preparation method thereof

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