CN108176118A - For the vacuum filter of insoluble sulfur separation of solid and liquid - Google Patents

For the vacuum filter of insoluble sulfur separation of solid and liquid Download PDF

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Publication number
CN108176118A
CN108176118A CN201810162594.4A CN201810162594A CN108176118A CN 108176118 A CN108176118 A CN 108176118A CN 201810162594 A CN201810162594 A CN 201810162594A CN 108176118 A CN108176118 A CN 108176118A
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CN
China
Prior art keywords
solid
distributing trough
washing lotion
insoluble sulfur
liquid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201810162594.4A
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Chinese (zh)
Other versions
CN108176118B (en
Inventor
陈锡林
陈杰
顾蓉英
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
WUXI HUASHENG RUBBER TECHNICAL CO Ltd
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WUXI HUASHENG RUBBER TECHNICAL CO Ltd
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Priority to CN201810162594.4A priority Critical patent/CN108176118B/en
Publication of CN108176118A publication Critical patent/CN108176118A/en
Application granted granted Critical
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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D33/00Filters with filtering elements which move during the filtering operation
    • B01D33/15Filters with filtering elements which move during the filtering operation with rotary plane filtering surfaces
    • B01D33/17Filters with filtering elements which move during the filtering operation with rotary plane filtering surfaces with rotary filtering tables
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D33/00Filters with filtering elements which move during the filtering operation
    • B01D33/44Regenerating the filter material in the filter
    • B01D33/46Regenerating the filter material in the filter by scrapers, brushes nozzles or the like acting on the cake-side of the filtering element
    • B01D33/466Regenerating the filter material in the filter by scrapers, brushes nozzles or the like acting on the cake-side of the filtering element scrapers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D33/00Filters with filtering elements which move during the filtering operation
    • B01D33/80Accessories
    • B01D33/82Means for pressure distribution

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Filtration Of Liquid (AREA)

Abstract

The present invention provides the vacuum filters for insoluble sulfur separation of solid and liquid, can improve and filter effect, solid-liquid separation efficiency, reduce scale cost of investment, the manufacturing cost of insoluble sulfur entirety, and ensure the suction filtration of soluble sulfur, separating effect.The vacuum filter, including housing, blanking scraper plate, driving mechanism and filter mechanism, housing is equipped with feed slurry inlet, washing lotion import, balanced gas import, solid outlet and mother liquor suction filtration mouth, it filters mechanism and includes suction filtering tube, filtering table and case, filtering table is closed together in the upper end opening of case to form compartment, for compartment Integral sealing in housing, compartment, other end connection mother liquor suction filtration mouth are stretched into suction filtering tube one end, it is characterised in that:Filtering table is driven by driving mechanism realizes rotation, is provided with slurry distributing trough, washing lotion distributing trough and blanking scraper plate above filtering table, slurry distributing trough connects corresponding feed slurry inlet, washing lotion import with washing lotion distributing trough.

Description

For the vacuum filter of insoluble sulfur separation of solid and liquid
Technical field
The present invention relates to the process equipments prepared for insoluble sulfur, and in particular to for insoluble sulfur separation of solid and liquid Vacuum filter.
Background technology
It is acted on for the vacuum filter of insoluble sulfur separation of solid and liquid by insoluble sulfur solid and carbon disulfide liquid And be dissolved in carbon disulfide liquid have soluble sulfur carry out separation of solid and liquid, divided by the way of vacuum filtration From, good separating effect, and powdered insoluble sulfur can be obtained, crushing operation of the later stage to insoluble sulfur filter cake is avoided, Technique can be simplified.
The existing vacuum filter for insoluble sulfur separation of solid and liquid uses intermittent operation, will contain first insoluble Property sulphur, soluble sulfur and carbon disulfide slurry quantify in implanter body after, disconnect slurry supply, then filter, finally The filter cake that insoluble sulfur is formed is struck off, is collected.To consider integrated artistic efficiency, the injection rate of each slurry all compared with Greatly, the filter cake of the insoluble sulfur of generation is thicker, and filter cake is thicker not only to be influenced to filter efficiency, solid-liquid separation efficiency, and then influence The scale cost of investment of insoluble sulfur entirety, manufacturing cost, and can not ensure the suction filtration of soluble sulfur, separation effect Fruit.
Invention content
Filter that effect is poor, scale cost of investment for the vacuum filter for being currently used for insoluble sulfur separation of solid and liquid The technical issues of height, production cost are high, the separating effect of soluble sulfur is poor, the present invention provides consolidate for insoluble sulfur The vacuum filter of liquid separation, can improve and filter effect, solid-liquid separation efficiency, and the scale for reducing insoluble sulfur entirety is thrown Cost, manufacturing cost are provided, and ensures the suction filtration of soluble sulfur, separating effect.
Its technical solution is such, for the vacuum filter of insoluble sulfur separation of solid and liquid, is scraped including housing, blanking Plate, driving mechanism and filter mechanism, the housing be equipped with feed slurry inlet, washing lotion import, balanced gas import, solid outlet and Mother liquor suction filtration mouth, the suction filtration mechanism include suction filtering tube, filtering table and case, and the filtering table is closed together in the case Upper end opening to form compartment, the compartment Integral sealing in housing, described suction filtering tube one end stretch into the compartment, The other end connects the mother liquor suction filtration mouth, it is characterised in that:The filtering table is driven by the driving mechanism and realizes rotation, institute It states and slurry distributing trough, washing lotion distributing trough and the blanking scraper plate is provided with above filtering table, the slurry distributing trough and described wash The connection of liquid the distributing trough corresponding feed slurry inlet, washing lotion import.
Further, the slurry distributing trough is equipped with 1, and the washing lotion distributing trough is equipped with 1 ~ 3, the slurry distributing trough The filtering table center arrangement is surrounded with 1 ~ 3 washing lotion distributing trough.
Further, the two side that the slurry distributing trough and/or the washing lotion distributing trough are radially extended along filtering table Top be placed with tooth form overflow port respectively.
Further, it is equipped with the solid outlet below the blanking scraper plate.
Further, the mother liquor suction filtration mouth of the suction filtering tube and the housing is sealed by bedding and padding seal box coordinates, described Bedding and padding seal box includes box body, airtight and watertight padding, sealing plate and filters connector, and the suction filtering tube is stretched in the box body, the box Filled with airtight and watertight padding between body and the suction filtering tube, the box body lower end is convexly equipped with the flange for supporting the airtight and watertight padding, institute It states cassette upper end and is covered with the pressure ring for being pressed the airtight and watertight padding, the suction filtration fitting end is equipped with skirt section, and the skirt section is arranged In the pressure ring periphery and with the box body be located at the position of pressure ring axle box or housing be located at mother liquor suction filtration mouth circumferential direction position it is close Sealing is determined, and the suction filtration connector is connected with the suction filtering tube.
Further, fixed frame is fixed in the housing, the fixed frame is located above the filtering table, the blanking Scraper plate, the slurry distributing trough, the washing lotion distributing trough are fixedly connected respectively with the fixed frame.
Further, the housing includes upper shell and lower housing, and the upper shell passes through flange with lower housing stitching portion Structure connects.
Further, the driving mechanism includes motor and speed reducer, the motor, speed reducer and the case company of transmission successively Connect, the speed reducer is set to below the enclosure interior, the speed reducer and the position that the motor drive is connect with it is described Housing seal connects.
Further, the case is tapered pyramidal structure from top to bottom, the speed reducer under the case End is sequentially connected.
Further, visor, headlamp, pressure vacuum gauge, safety inspection mouth and flush pipe, institute are additionally provided on the housing Flush pipe is stated for being rinsed to the visor.
Further, the motor is explosion-proof variable frequency motor, and the speed reducer is disk feeder speed reducer, described Headlamp is explosion-proof lamp;The explosion-proof lamp, visor are all provided with there are two and are symmetrically fixed on the upper part of the housing both sides, wherein one A explosion-proof lamp and a visor are located at top at solid outlet.
Further, the position that the vacuum filter is contacted with slurry, balanced gas, washing lotion uses stainless steel Matter.
Further, the filtering table is made of filter cloth, support mesh and the stent set from top to bottom, and the filter cloth passes through In on the support mesh, the stent, the support mesh is punching net or bar shaped net for press strip press fitting, and the filter cloth is chemical fibre Cloth, metal or the combination of sintered metal mesh formula.
The present invention is realized by driving mechanism driving and turned by the way that the filtering table for filtering mechanism is set as rotational structure Dynamic, scraper is stationary structure so that the filter cake for the insoluble sulfur being formed on filtering table can continuously strike off by scraper, It collects so that the filter cake of insoluble sulfur maintains relatively thin thickness, and corresponding slurry can realize continuous feed with washing lotion, Avoid balanced gas fill or collect repeatedly and carbon disulfide with balanced gas collect caused by be lost in, and then improve filter effect Fruit, solid-liquid separation efficiency reduce scale cost of investment, the manufacturing cost of insoluble sulfur entirety, and relatively thin filter cake is thick Degree ensures suction filtration, the separating effect of soluble sulfur.
Description of the drawings
Fig. 1 is the structural diagram of the present invention.
Fig. 2 is the structure diagram of the bedding and padding seal box of the present invention.
Specific embodiment
As shown in Figure 1 and Figure 2, for the vacuum filter of insoluble sulfur separation of solid and liquid, including housing 1, blanking scraper plate 3, Driving mechanism and suction filtration mechanism, housing 1 is equipped with and feed slurry inlet, washing lotion import, balanced gas import, solid outlet and mother liquor The corresponding slurry connector 4 of suction filtration mouth, washing lotion connector 5, balanced gas connector 6, anchor tip 7 and suction filtration connector 8, filter machine Structure includes suction filtering tube 9, filtering table 10, case 11 and vacuum pump(Vacuum pump is not shown, is existing conventional techniques), filtering Disk 10 is closed together in the upper end opening of case 11 to form compartment 12, and 12 Integral sealing of compartment is in housing 1, suction filtering tube Compartment 12 is stretched into 9 one end, the other end connects mother liquor suction filtration mouth, and the lower end of driving mechanism and case 11 is sequentially connected to drive Filter disc 10 realizes rotation, and 10 top of filtering table is provided with slurry distributing trough 13, washing lotion distributing trough 14 and blanking scraper plate, slurry cloth Slot 13 is equipped with 1, and washing lotion distributing trough 14 is equipped with 1 ~ 3, and slurry distributing trough 13 and 1 ~ 3 washing lotion distributing trough 14 surround filtering table 10 Center arrangement, slurry distributing trough and washing lotion distributing trough 14 connect corresponding feed slurry inlet, washing lotion import by pipeline 15 respectively, under Expect to be equipped with solid outlet below scraper plate.Slurry uniform distribution removes carbon disulfide by suction filtration, is dissolved in two on filtering table 10 The soluble sulfur of nitric sulfid, insoluble sulfur remaines in 10 top of filtering table, and passes through washing lotion under the rotation of filtering table 10 The cleaning area that distributing trough 14 is formed, to be cleaned to insoluble sulfur, it is ensured that purity, the number of washing lotion distributing trough 14 can basis Actual demand is configured, and is contacted blanking scraper plate when the filter cake that insoluble sulfur is formed reaches certain thickness, is scraped by blanking The inclined bevel of scraping of plate lower end is scraped off and is fallen into solid outlet, and then collects;During being somebody's turn to do, slurry is continuous charging, no Dissolubility sulphur continuously to scrape off collection, avoid because blanking valve is frequently opened in conventional batch operating process, fill repeatedly and Collect balanced gas(Nitrogen, carbon disulfide gas)Caused production efficiency reduces, and to accomplish scale production, while avoids frequency It is numerous to open nitrogen escape, the increase of nitrogen usage amount that blanking valve causes,.
It arranges respectively on the top of two side that slurry distributing trough 13 and/or washing lotion distributing trough 14 are radially extended along filtering table 10 There is tooth form overflow port 16, prevent from causing cloth uneven because the top position overflow of side wall is not horizontal, it is ensured that along 10 diameter of filtering table To the uniform distribution in direction.
The mother liquor suction filtration mouth of suction filtering tube 9 and housing 1 is sealed by bedding and padding seal box to be coordinated, and bedding and padding seal box includes box body 17th, airtight and watertight padding 18, sealing plate and suction filtration connector, suction filtering tube 9 are stretched in box body 17, are filled between box body 17 and suction filtering tube 9 Airtight and watertight padding 18,17 lower end of box body are convexly equipped with the flange of bearing seal filler 18, and 17 upper end of box body is covered with press fitting airtight and watertight padding 18 pressure ring 19 filters fitting end and is equipped with skirt section 20, and skirt section 20 is sheathed on 19 periphery of pressure ring and is located at pressure ring 19 with box body 17 The position sealing of axle box is fixed, and is filtered connector and is connected with suction filtering tube 9, real by airtight and watertight padding 18 between suction filtering tube 9 and box body 17 Existing dynamic sealing filters the skirt section 20 of connector and 17 static seal of box body, and then effectively ensures the sealing effect of junction, prevents from balancing Gas is escaped, and due to carbon disulfide gas explosion limit wider range, can improve the explosion-proof performance of device.
Fixed frame is fixed in housing 1, fixed frame is located at 10 top of filtering table, blanking scraper plate, slurry distributing trough, washing lotion cloth Hopper 14 is fixedly connected respectively with fixed frame.
Housing 1 includes upper shell 1a and lower housing 1b, and upper shell 1a is connected with lower housing 1b stitching portions by flange arrangement 2 It connects;Driving mechanism includes motor 26 and speed reducer 27, and motor 26, speed reducer 27 and case 11 are sequentially connected successively, and speed reducer is set 1 lower inside of housing is placed in, the position that speed reducer is connect with motor drive is tightly connected with housing 1, since driving mechanism is set In 10 lower section of filtering table, convenient for the maintenance of filtering table 10.
Case 11 is pyramidal structure tapered from top to bottom, convenient for the collection of filtrate.
Visor 21, headlamp 22, pressure vacuum gauge 23, safety inspection mouth 24 and flush pipe 25 are additionally provided on housing 1, is rinsed Pipe 25 is used to be rinsed visor 21;Motor is explosion-proof variable frequency motor, and speed reducer is disk feeder speed reducer, headlamp 22 be explosion-proof lamp;Explosion-proof lamp, visor 21 are all provided with there are two and are symmetrically fixed on 1 top both sides of housing, one of explosion-proof lamp It is located at top at solid outlet with a visor 21.
The position that vacuum filter is contacted with slurry, balanced gas, washing lotion uses stainless steel.
Filtering table is made of filter cloth, support mesh and the stent set from top to bottom, filter cloth by press strip be pressed in support mesh, On stent, support mesh is punching net or bar shaped net, and filter cloth is chemical fiber cloth, metal or sintered metal mesh formula combine.
In Fig. 1,28 be the leakage fluid dram for being set to lower housing lower part, is excluded convenient for the carbon disulfide of condensation, 29 be support foot.

Claims (10)

1. for the vacuum filter of insoluble sulfur separation of solid and liquid, including housing, blanking scraper plate, driving mechanism and machine is filtered Structure, the housing are equipped with feed slurry inlet, washing lotion import, balanced gas import, solid outlet and mother liquor suction filtration mouth, the suction filtration Mechanism includes suction filtering tube, filtering table and case, and the filtering table is closed together in the upper end opening of the case and is separated with being formed Room, the compartment Integral sealing is in housing, and the compartment is stretched into described suction filtering tube one end, the other end connects the mother liquor Suction filtration mouth, it is characterised in that:The filtering table is driven by the driving mechanism realizes rotation, is provided with above the filtering table Slurry distributing trough, washing lotion distributing trough and the blanking scraper plate, the slurry distributing trough connect accordingly with the washing lotion distributing trough The feed slurry inlet, washing lotion import.
2. the vacuum filter according to claim 1 for insoluble sulfur separation of solid and liquid, it is characterised in that:The material It starches distributing trough and is equipped with 1, the washing lotion distributing trough is equipped with 1 ~ 3, and the slurry distributing trough and 1 ~ 3 washing lotion distributing trough enclose Around the filtering table center arrangement.
3. the vacuum filter according to claim 1 or 2 for insoluble sulfur separation of solid and liquid, it is characterised in that:Institute It states the top of two side that slurry distributing trough and/or the washing lotion distributing trough are radially extended along filtering table and is placed with tooth form respectively and overflow Head piece.
4. the vacuum filter according to claim 1 for insoluble sulfur separation of solid and liquid, it is characterised in that:Under described Expect to be equipped with the solid outlet below scraper plate.
5. the vacuum filter according to claim 1 for insoluble sulfur separation of solid and liquid, it is characterised in that:The pumping The mother liquor suction filtration mouth of chimney filter and the housing is sealed by bedding and padding seal box to be coordinated, and the bedding and padding seal box includes box body, sealing Filler, sealing plate and suction filtration connector, the suction filtering tube are stretched in the box body, are filled between the box body and the suction filtering tube Airtight and watertight padding, the box body lower end are convexly equipped with the flange for supporting the airtight and watertight padding, and the cassette upper end is covered with described in press fitting The pressure ring of airtight and watertight padding, it is described suction filtration fitting end be equipped with skirt section, the skirt section be sheathed on the pressure ring periphery and with the box Body is located at the position of pressure ring axle box or housing is located at the position sealing of mother liquor suction filtration mouth circumferential direction and fixes, the suction filtration connector with it is described Suction filtering tube connects.
6. the vacuum filter according to claim 1 for insoluble sulfur separation of solid and liquid, it is characterised in that:The shell It is fixed with fixed frame in vivo, the fixed frame is located above the filtering table, the blanking scraper plate, the slurry distributing trough, institute Washing lotion distributing trough is stated to be fixedly connected with the fixed frame respectively.
7. the vacuum filter according to claim 1 for insoluble sulfur separation of solid and liquid, it is characterised in that:The shell Body includes upper shell and lower housing, and the upper shell is connect with lower housing stitching portion by flange arrangement;
The driving mechanism includes motor and speed reducer, and the motor, speed reducer and compartment are sequentially connected successively, the deceleration Machine is set to below the enclosure interior, and the position that the speed reducer is connect with the motor drive connects with the housing seal It connects.
8. the vacuum filter according to claim 7 for insoluble sulfur separation of solid and liquid, it is characterised in that:The cover Shell is pyramidal structure tapered from top to bottom, and the lower end of the speed reducer and the case is sequentially connected.
9. the vacuum filter according to claim 7 for insoluble sulfur separation of solid and liquid, it is characterised in that:The shell Visor, headlamp, pressure vacuum gauge, safety inspection mouth and flush pipe are additionally provided on body, the flush pipe is used for the visor It is rinsed.
10. the vacuum filter according to claim 9 for insoluble sulfur separation of solid and liquid, it is characterised in that:It is described Motor is explosion-proof variable frequency motor, and the speed reducer is disk feeder speed reducer, and the headlamp is explosion-proof lamp;It is described explosion-proof Lamp, visor are all provided with there are two and are symmetrically fixed on the upper part of the housing both sides, and one of explosion-proof lamp and a visor are located at Top at solid outlet;
The position that the vacuum filter is contacted with slurry, balanced gas, washing lotion uses stainless steel.
CN201810162594.4A 2018-02-26 2018-02-26 Vacuum filter for insoluble sulfur solid-liquid separation Active CN108176118B (en)

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CN108176118B CN108176118B (en) 2023-12-05

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109896504A (en) * 2019-04-11 2019-06-18 无锡华盛橡胶新材料科技股份有限公司 For the continuous separation of wet production insoluble sulfur, dry system
CN109911864A (en) * 2019-04-11 2019-06-21 无锡华盛橡胶新材料科技股份有限公司 System for the screening of wet production insoluble sulfur, crushing, de-oiling
CN109970033A (en) * 2019-04-11 2019-07-05 无锡华盛橡胶新材料科技股份有限公司 Separation of solid and liquid, the system of precipitation for the oil-filled insoluble sulfur of wet production
CN111773803A (en) * 2020-06-18 2020-10-16 四川润邦利泰科技有限公司 Automatic rapid solid-liquid separation device and application method
CN112371069A (en) * 2020-10-23 2021-02-19 无锡市张华医药设备有限公司 Continuous reaction, crystallization, filtration, washing, drying system
CN112370843A (en) * 2020-10-23 2021-02-19 无锡市张华医药设备有限公司 Closed continuous filtering washing machine
CN112973243A (en) * 2021-03-04 2021-06-18 浙江环森环境科技有限公司 Filtering device for industrial wastewater purification and use method thereof
CN115253457A (en) * 2022-08-23 2022-11-01 三门峡义翔铝业有限公司 Flat disc filter and filtering method thereof

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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109896504A (en) * 2019-04-11 2019-06-18 无锡华盛橡胶新材料科技股份有限公司 For the continuous separation of wet production insoluble sulfur, dry system
CN109911864A (en) * 2019-04-11 2019-06-21 无锡华盛橡胶新材料科技股份有限公司 System for the screening of wet production insoluble sulfur, crushing, de-oiling
CN109970033A (en) * 2019-04-11 2019-07-05 无锡华盛橡胶新材料科技股份有限公司 Separation of solid and liquid, the system of precipitation for the oil-filled insoluble sulfur of wet production
CN109911864B (en) * 2019-04-11 2023-09-01 无锡华盛橡胶新材料科技股份有限公司 System for screening, crushing and deoiling for wet production of insoluble sulfur
CN111773803A (en) * 2020-06-18 2020-10-16 四川润邦利泰科技有限公司 Automatic rapid solid-liquid separation device and application method
CN112371069A (en) * 2020-10-23 2021-02-19 无锡市张华医药设备有限公司 Continuous reaction, crystallization, filtration, washing, drying system
CN112370843A (en) * 2020-10-23 2021-02-19 无锡市张华医药设备有限公司 Closed continuous filtering washing machine
CN112371069B (en) * 2020-10-23 2023-08-29 无锡市张华医药设备有限公司 Continuous reaction, crystallization, filtration, washing and drying system
CN112973243A (en) * 2021-03-04 2021-06-18 浙江环森环境科技有限公司 Filtering device for industrial wastewater purification and use method thereof
CN115253457A (en) * 2022-08-23 2022-11-01 三门峡义翔铝业有限公司 Flat disc filter and filtering method thereof

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