CN108165340A - A kind of preparation method of functionalization graphene lube oil additive for reducing cost - Google Patents
A kind of preparation method of functionalization graphene lube oil additive for reducing cost Download PDFInfo
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- CN108165340A CN108165340A CN201810114071.2A CN201810114071A CN108165340A CN 108165340 A CN108165340 A CN 108165340A CN 201810114071 A CN201810114071 A CN 201810114071A CN 108165340 A CN108165340 A CN 108165340A
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- functionalization graphene
- oil additive
- lube oil
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M125/00—Lubricating compositions characterised by the additive being an inorganic material
- C10M125/02—Carbon; Graphite
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M163/00—Lubricating compositions characterised by the additive being a mixture of a compound of unknown or incompletely defined constitution and a non-macromolecular compound, each of these compounds being essential
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/04—Elements
- C10M2201/041—Carbon; Graphite; Carbon black
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/06—Metal compounds
- C10M2201/062—Oxides; Hydroxides; Carbonates or bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/10—Compounds containing silicon
- C10M2201/102—Silicates
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/02—Hydroxy compounds
- C10M2207/021—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/281—Esters of (cyclo)aliphatic monocarboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/06—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings
- C10M2215/064—Di- and triaryl amines
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/28—Amides; Imides
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/72—Extended drain
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Lubricants (AREA)
Abstract
The present invention relates to technical field of lubricating oil, and in particular to a kind of preparation method of functionalization graphene lube oil additive for reducing cost.11~28 parts of base oil, 3~10 parts of graphene are added in blender and be stirred；1~6 part of silicate, 2~7 parts of calcium mahogany sulfonate, 3~8 parts of boronation polyisobutene succinimide, 1~5 part of terpinol are added in step 1, are stirred；3~8 parts of di-iron trioxide, 2~6 parts of methyl oleate, 1~4 part of antioxidant, 3~7 parts of anti-wear agent are added in step 2, heating stirring, obtain to reduce the functionalization graphene lube oil additive of cost.A kind of preparation method of functionalization graphene lube oil additive for reducing cost of the present invention, simple production process, conveniently is cost-effective, can effectively improve the abrasive resistance of lubricating oil, enhances lubricating oil bearing capacity, and service life extends.
Description
Technical field
The present invention relates to technical field of lubricating oil, and in particular to a kind of functionalization graphene lubricating oil for reducing cost adds
Add the preparation method of agent.
Background technology
A kind of lubricating oil oil product very high as important, technology content, application range is very extensive, nearly all
Machinery field will use.The value volume and range of product of China's lube product is constantly increasing, but product quality and class and hair
China's lubricating oil industry compels when being compared up to country and also there is very big gap, therefore improved product quality, improve product specification
Being essential will.
Lubricating oil is generally made of base oil and additive two parts.The quality of base oil is the basic of lubricating oil, addition
The marrow of lubricating oil when the quality and performance of agent, the quality and performance of additive and the ratio of addition directly influence lubricating oil
Performance.As a kind of novel nano-material, graphene is applied to have what Conventional nano particle did not had in lubricating oil
Many advantages.The friction coefficient of graphene in itself is close to zero, and lubricants performance is outstanding, and two-dimensional structure physicochemical properties are steady
It is fixed, there is the heat conductivility of superelevation, proportion is small, and easily carries out a variety of modifications, can solve nanometer additive long-time stability
Problem.
Therefore, it using novel nano-material graphene as lube oil additive, develops with good abrasion resistance, Gao Cheng
Loading capability, the lubricating oil to mechanical surface with certain repair function, form a series of new lubrication product, are lube product
Height of quickly being marched toward by low side sits up straight out contribution.
Invention content
The overcome the deficiencies in the prior art during purpose of the present invention and provide it is a kind of reduce cost functionalization graphene profit
The preparation method of oil additive, simple production process, conveniently is cost-effective, can effectively improve the abrasive resistance of lubricating oil,
Enhance lubricating oil bearing capacity, service life extends.
A kind of preparation method of functionalization graphene lube oil additive for reducing cost, includes the following steps：
11~28 parts of base oil, 3~10 parts of graphene in parts by weight, are added in blender and are stirred by step 1；
Step 2 in parts by weight, adds in 1~6 part of silicate, 2~7 parts of calcium mahogany sulfonate, boronation polyisobutene fourth in step 1
3~8 parts of imidodicarbonic diamide, 1~5 part of terpinol, are stirred；
Step 3 in parts by weight, by 3~8 parts of di-iron trioxide, 2~6 parts of methyl oleate, 1~4 part of antioxidant, anti-wear agent 3
~7 parts are added in step 2, heating stirring, obtain to reduce the functionalization graphene lube oil additive of cost；
As being further improved for foregoing invention, antioxidant described in step 3 is secondary aromatic amine.
As being further improved for foregoing invention, mixing speed is 100~300rpm in step 1.
As being further improved for foregoing invention, mixing speed is 300~500rpm in step 2.
As being further improved for foregoing invention, heating temperature is 40~80 DEG C in step 3.
As being further improved for foregoing invention, mixing speed is 200~400rpm in step 3.
The invention has the advantages that：A kind of functionalization graphene lubricating oil addition for reducing cost of the present invention
The preparation method of agent, simple production process, conveniently is cost-effective, can effectively improve the abrasive resistance of lubricating oil, make lubricating oil
Bearing capacity enhances, and service life extends.
Specific embodiment
Embodiment 1
A kind of preparation method of functionalization graphene lube oil additive for reducing cost, includes the following steps：
11 parts of base oil, 3 parts of graphene in parts by weight, are added in blender and are stirred by step 1；
Step 2 in parts by weight, it is sub- to add in 1 part of silicate, 2 parts of calcium mahogany sulfonate, boronation polyisobutene succinyl in step 1
3 parts of amine, 1 part of terpinol, are stirred；
Step 3 is added to step in parts by weight, by 3 parts of di-iron trioxide, 2 parts of methyl oleate, 1 part of antioxidant, 3 parts of anti-wear agent
In 2, heating stirring obtains to reduce the functionalization graphene lube oil additive of cost；
Antioxidant described in step 3 is secondary aromatic amine.
Mixing speed is 100rpm in step 1.
Mixing speed is 300rpm in step 2.
Heating temperature is 40 DEG C in step 3.
Mixing speed is 200rpm in step 3.
Embodiment 2
A kind of preparation method of functionalization graphene lube oil additive for reducing cost, includes the following steps：
12 parts of base oil, 4 parts of graphene in parts by weight, are added in blender and are stirred by step 1；
Step 2 in parts by weight, it is sub- to add in 2 parts of silicate, 3 parts of calcium mahogany sulfonate, boronation polyisobutene succinyl in step 1
4 parts of amine, 2 parts of terpinol, are stirred；
Step 3 is added to step in parts by weight, by 4 parts of di-iron trioxide, 3 parts of methyl oleate, 2 parts of antioxidant, 4 parts of anti-wear agent
In 2, heating stirring obtains to reduce the functionalization graphene lube oil additive of cost；
Antioxidant described in step 3 is secondary aromatic amine.
Mixing speed is 150rpm in step 1.
Mixing speed is 350rpm in step 2.
Heating temperature is 45 DEG C in step 3.
Mixing speed is 250rpm in step 3.
Embodiment 3
A kind of preparation method of functionalization graphene lube oil additive for reducing cost, includes the following steps：
27 parts of base oil, 9 parts of graphene in parts by weight, are added in blender and are stirred by step 1；
Step 2 in parts by weight, it is sub- to add in 5 parts of silicate, 6 parts of calcium mahogany sulfonate, boronation polyisobutene succinyl in step 1
7 parts of amine, 4 parts of terpinol, are stirred；
Step 3 is added to step 2 in parts by weight, by 7 parts of di-iron trioxide, 5 parts of methyl oleate, 3 parts anti-oxidant, 6 parts of anti-wear agent
In, heating stirring obtains to reduce the functionalization graphene lube oil additive of cost；
Antioxidant described in step 3 is secondary aromatic amine.
Mixing speed is 250rpm in step 1.
Mixing speed is 450rpm in step 2.
Heating temperature is 75 DEG C in step 3.
Mixing speed is 350rpm in step 3.
Embodiment 4
A kind of preparation method of functionalization graphene lube oil additive for reducing cost, includes the following steps：
26 parts of base oil, 8 parts of graphene in parts by weight, are added in blender and are stirred by step 1；
Step 2 in parts by weight, it is sub- to add in 4 parts of silicate, 5 parts of calcium mahogany sulfonate, boronation polyisobutene succinyl in step 1
6 parts of amine, 3 parts of terpinol, are stirred；
Step 3 is added to step in parts by weight, by 6 parts of di-iron trioxide, 4 parts of methyl oleate, 2 parts of antioxidant, 5 parts of anti-wear agent
In 2, heating stirring obtains to reduce the functionalization graphene lube oil additive of cost；
Antioxidant described in step 3 is secondary aromatic amine.
Mixing speed is 200rpm in step 1.
Mixing speed is 400rpm in step 2.
Heating temperature is 70 DEG C in step 3.
Mixing speed is 300rpm in step 3.
Embodiment 5
A kind of preparation method of functionalization graphene lube oil additive for reducing cost, includes the following steps：
28 parts of base oil, 10 parts of graphene in parts by weight, are added in blender and are stirred by step 1；
Step 2 in parts by weight, it is sub- to add in 6 parts of silicate, 7 parts of calcium mahogany sulfonate, boronation polyisobutene succinyl in step 1
8 parts of amine, 5 parts of terpinol, are stirred；
Step 3 is added to step in parts by weight, by 8 parts of di-iron trioxide, 6 parts of methyl oleate, 4 parts of antioxidant, 7 parts of anti-wear agent
In 2, heating stirring obtains to reduce the functionalization graphene lube oil additive of cost；
Antioxidant described in step 3 is secondary aromatic amine.
Mixing speed is 300rpm in step 1.
Mixing speed is 500rpm in step 2.
Heating temperature is 80 DEG C in step 3.
Mixing speed is 400rpm in step 3.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
All any modification, equivalent and improvement made within refreshing and principle etc., should all be included in the protection scope of the present invention.
Claims (5)
1. a kind of preparation method of functionalization graphene lube oil additive for reducing cost, it is characterised in that：Including following
Step：
11~28 parts of base oil, 3~10 parts of graphene in parts by weight, are added in blender and are stirred by step 1；
Step 2 in parts by weight, adds in 1~6 part of silicate, 2~7 parts of calcium mahogany sulfonate, boronation polyisobutene fourth in step 1
3~8 parts of imidodicarbonic diamide, 1~5 part of terpinol, are stirred；
Step 3 in parts by weight, by 3~8 parts of di-iron trioxide, 2~6 parts of methyl oleate, 1~4 part of antioxidant, anti-wear agent 3
~7 parts are added in step 2, heating stirring, obtain to reduce the functionalization graphene lube oil additive of cost；
Antioxidant described in step 3 is secondary aromatic amine.
2. the preparation method of functionalization graphene lube oil additive according to claim 1 for reducing cost, special
Sign is：Mixing speed is 100~300rpm in step 1.
3. the preparation method of functionalization graphene lube oil additive according to claim 1 for reducing cost, special
Sign is：Mixing speed is 300~500rpm in step 2.
4. the preparation method of functionalization graphene lube oil additive according to claim 1 for reducing cost, special
Sign is：Heating temperature is 40~80 DEG C in step 3.
5. the preparation method of functionalization graphene lube oil additive according to claim 1 for reducing cost, special
Sign is：Mixing speed is 200~400rpm in step 3.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810114071.2A CN108165340A (en) | 2018-02-05 | 2018-02-05 | A kind of preparation method of functionalization graphene lube oil additive for reducing cost |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810114071.2A CN108165340A (en) | 2018-02-05 | 2018-02-05 | A kind of preparation method of functionalization graphene lube oil additive for reducing cost |
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| CN108165340A true CN108165340A (en) | 2018-06-15 |
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| CN201810114071.2A Pending CN108165340A (en) | 2018-02-05 | 2018-02-05 | A kind of preparation method of functionalization graphene lube oil additive for reducing cost |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114561241A (en) * | 2022-01-21 | 2022-05-31 | 辽宁国瑞新能科技有限公司 | Nano graphene extreme pressure antiwear repair additive |
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| US20110003721A1 (en) * | 2006-01-12 | 2011-01-06 | Haiping Hong | Carbon nanoparticle-containing nanofluid |
| US20110046027A1 (en) * | 2009-08-19 | 2011-02-24 | Aruna Zhamu | Nano graphene-modified lubricant |
| CN104342238A (en) * | 2014-09-30 | 2015-02-11 | 赖婷婷 | Lubricant additive and preparation method thereof |
| CN105038907A (en) * | 2015-08-05 | 2015-11-11 | 苏州赛斯德工程设备有限公司 | Preparation method of lubricant oil additive |
| CN106893619A (en) * | 2017-01-07 | 2017-06-27 | 江苏广源发石墨烯纳米科技有限公司 | Graphene lubricating oil intelligence additive |
| CN107057813A (en) * | 2017-05-02 | 2017-08-18 | 秦继恩 | A kind of graphene lube oil additive, preparation method, purposes and the lubricating oil comprising it |
| CN107312600A (en) * | 2017-07-06 | 2017-11-03 | 广西柳工机械股份有限公司 | Graphene composite lube additive and preparation method thereof |
| CN107513457A (en) * | 2017-09-14 | 2017-12-26 | 辽宁兰晶科技有限公司 | A kind of transmission system of electric automobile special oil and preparation method thereof |
-
2018
- 2018-02-05 CN CN201810114071.2A patent/CN108165340A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20110003721A1 (en) * | 2006-01-12 | 2011-01-06 | Haiping Hong | Carbon nanoparticle-containing nanofluid |
| US20110046027A1 (en) * | 2009-08-19 | 2011-02-24 | Aruna Zhamu | Nano graphene-modified lubricant |
| CN104342238A (en) * | 2014-09-30 | 2015-02-11 | 赖婷婷 | Lubricant additive and preparation method thereof |
| CN105038907A (en) * | 2015-08-05 | 2015-11-11 | 苏州赛斯德工程设备有限公司 | Preparation method of lubricant oil additive |
| CN106893619A (en) * | 2017-01-07 | 2017-06-27 | 江苏广源发石墨烯纳米科技有限公司 | Graphene lubricating oil intelligence additive |
| CN107057813A (en) * | 2017-05-02 | 2017-08-18 | 秦继恩 | A kind of graphene lube oil additive, preparation method, purposes and the lubricating oil comprising it |
| CN107312600A (en) * | 2017-07-06 | 2017-11-03 | 广西柳工机械股份有限公司 | Graphene composite lube additive and preparation method thereof |
| CN107513457A (en) * | 2017-09-14 | 2017-12-26 | 辽宁兰晶科技有限公司 | A kind of transmission system of electric automobile special oil and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114561241A (en) * | 2022-01-21 | 2022-05-31 | 辽宁国瑞新能科技有限公司 | Nano graphene extreme pressure antiwear repair additive |
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Application publication date: 20180615 |
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