CN108149474A - A kind of cold slurry of weaving and preparation method thereof - Google Patents

A kind of cold slurry of weaving and preparation method thereof Download PDF

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Publication number
CN108149474A
CN108149474A CN201611099980.0A CN201611099980A CN108149474A CN 108149474 A CN108149474 A CN 108149474A CN 201611099980 A CN201611099980 A CN 201611099980A CN 108149474 A CN108149474 A CN 108149474A
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Prior art keywords
weaving
yarn
cold slurry
yarn count
sizing
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CN201611099980.0A
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Chinese (zh)
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李志国
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Individual
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
    • D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/165—Ethers
    • D06M13/17—Polyoxyalkyleneglycol ethers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/402—Amides imides, sulfamic acids
    • D06M13/432—Urea, thiourea or derivatives thereof, e.g. biurets; Urea-inclusion compounds; Dicyanamides; Carbodiimides; Guanidines, e.g. dicyandiamides
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03—Polysaccharides or derivatives thereof
    • D06M15/05—Cellulose or derivatives thereof
    • D06M15/09—Cellulose ethers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/53—Polyethers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/35—Abrasion, pilling or fibrillation resistance
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/40—Reduced friction resistance, lubricant properties; Sizing compositions

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention discloses cold slurry of a kind of weaving and preparation method thereof, by number percentage, including：0.6% 0.9% CMC powder, 0.5% 1% antifoaming agent, 3% 4.5% attapulgite, 0.5% 1% urea, 1% 2% waterglass, 0.3% 0.45% JFC bleeding agents, 0.2% 0.3% 7 emulsions of AE0, the cold slurry of this weaving, it is pollution-free, odorlessness, it can make yarn count that there is good antistatic property, make yarn count wearability good, not pilling, it can also make yarn count adhesion, enhance the strength of yarn count, can be very good the filoplume of docile yarn count, make opening clear, weaving is allowed to be without fear of an attack from the rear, greatly reduces cost, improves production efficiency.

Description

A kind of cold slurry of weaving and preparation method thereof
Technical field
The present invention relates to a kind of slurry and preparation method thereof more particularly to the cold slurries of a kind of weaving and preparation method thereof.
Background technology
Warp sizing is the key link for weaving engineering, and the main purpose of sizing is to improve the wearability of yarn, reduces hair Plumage, the appropriate strength for increasing yarn, reduces degree of stretching, and to bear the mechanicals efforts that warp thread is subject in weaving process, improves yarn The weavability of line.
But the slurry of starching at present, slashing strength is inadequate, not wear-resisting, inadequate with fiber affinity, poor fluidity, to ring Border pollution is big.
Invention content
In view of the above problems, the invention discloses cold slurry of a kind of weaving and preparation method thereof, the cold slurry of this weaving, nothings Pollution, odorlessness can make yarn count have good antistatic property, make yarn count wearability good, not pilling can also make yarn count not Adhesion enhances the strength of yarn count, can be very good the filoplume of docile yarn count, makes opening clear, weaving is allowed to be without fear of an attack from the rear, greatly Cost is reduced greatly, improves production efficiency.
The present invention is in order to achieve the above object, using following scheme：
A kind of cold slurry of weaving, it is characterised in that：By number percentage, including：CMC powder, the 0.5%- of 0.6%-0.9% 1% antifoaming agent, the attapulgite of 3%-4.5%, 0.5%-1% urea, the waterglass of 1%-2%, 0.3%-0.45% The AE0-7 emulsions of JFC bleeding agents, 0.2%-0.3%.
The present invention also provides a kind of preparation methods for cold slurry of weaving, which is characterized in that is as follows：
1. adding in the water of 60%-80% in mixing cirtern, high, low speed blender is started,
2. adding in 0.6%-0.9%CMC powder, 30min is stirred, turns off high, low speed blender, 20 DEG C are impregnated 2h,
3. adding in 3%-4.5% attapulgites, the antifoaming agent of 0.5%-1%, 0.5%-1% urea, 20min is stirred,
4. 1%-2% waterglass, 0.3%-0.45%JFC bleeding agents, 0.2%-0.3%AE0-7 emulsions are added in, stirring 20min, mixing speed 700r/min turn off high, low speed blender, and water is filled in mixing cirtern, and 20 DEG C are impregnated 4h,
5. stir 30min, mixing speed 700r/min, with filter screen filtration to get.
Beneficial effects of the present invention：
The cold slurry of this weaving, pollution-free, odorlessness can make yarn count have good antistatic property, make yarn count wearability good, Not pilling can also make yarn count adhesion, enhance the strength of yarn count, can be very good the filoplume of docile yarn count, make opening clear It is clear, weaving is allowed to be without fear of an attack from the rear, greatly reduces cost, improves production efficiency.
Specific embodiment
The present invention is described further with reference to embodiment.
Embodiment 1:
(1) the cold slurry of weaving is prepared according to the following steps：
1. adding in 60% water in mixing cirtern, high, low speed blender is started,
2. adding in 0.6%CMC powder, 30min is stirred, turns off high, low speed blender, 20 DEG C are impregnated 2h,
3. adding in 3% attapulgite, 0.5% antifoaming agent, 0.5% urea, 20min is stirred,
4. adding in 1% waterglass, 0.3%JFC bleeding agents, 0.2%AE0-7 emulsions, 20min, mixing speed are stirred 700r/min turns off high, low speed blender, and water is filled in mixing cirtern, and 20 DEG C are impregnated 4h,
5. stir 30min, mixing speed 700r/min, with filter screen filtration to get.
(2) size film property test is carried out to the cold slurry of weaving prepared by above-mentioned steps：
1. serous coat makes
By 210mm*300mm, the serous coat plate that thick 5 ㎜ polished glass make adjusts horizontal.It is dipped in a small amount of water on glass plate, Then the tiling of the mylar of 0.3 ㎜ thickness on a glass, glass plate level is corrected with level meter, prepared by configuration above-mentioned steps 5% concentration cold slurry slurries 100ml.By slurries slowly on a glass, and with glass bar gently move back and forth, make slurries It is paved on a glass, after spontaneously drying film forming, carefully serous coat from glass plate is peeled, is put into climatic chamber inner equilibrium It is for use for 24 hours.
2. fracture strength and the elongation at break test of serous coat
Serous coat is cut into long 200mm, the bar-shaped sample of wide 5mm is placed in constant temperature and humidity room, in the item of relative humidity 40% It is balanced under part for 24 hours, then tests its ultimate strength and elongation at break on the grand HD021N electronics single yarn tester in Nantong, tried Sample accommodates distance 100mm, decrease speed 50mm/min, tests 10 times and is averaged, and it is 8.16% to measure than elongation at break, than Fracture strength is 742.2cN.mm-1。
3. the water solubility rate test of serous coat
Serous coat is cut into the strip of long 100 ㎜, wide 20 ㎜, a straight line mark is drawn in length direction middle, it then will slurry Film is immersed in 80 DEG C of water, when mark overlaps among horizontal plane and serous coat, then presses stopwatch termination timing, stopwatch show when Between for representing the water solubility rate of serous coat, during test, the lower weight quality of hanging of serous coat is 3.6g, and experiment 10 times is averaged, survey It is 30.2s to obtain water solubility rate.
(3) slurry viscosity heat stability testing
The adjustable funnel viscometer tested viscosity of TY821 types and viscosity stability are selected, modulation 800ml contains above-mentioned steps system The cold slurry slurries of 5% standby concentration, stirring frequency 120r/min, water bath with thermostatic control heating are raised to 95 DEG C, are surveyed per 30min primary viscous Degree, keeps the temperature 3h altogether, and it is 86.26% to measure viscosity thermal stability.
(4) slashing performance is tested
1. sizing hairiness is tested
The filoplume of more than the 3mm of raw yarn and sizing, each test yarns line length are tested on YG171 type filoplume testers respectively It spends for 1m, surveys 30 times altogether, take its average value, yarn is 30m/min by speed, and in biology microscope Microscopic observation raw yarn and slurry Longitudinal filoplume situation of yarn measures raw yarn as 12.6/m, and sizing is 5.86/m.
2. sizing wear resistant is tested
It embraces in Y113 types and is tested on power machine, test 30, sizing every time, calculate average value, test condition is 20 DEG C, yarn Line static tensile is 200cN, and grinding is 235cN from pressure, and it is 143 times/min to be ground unloaded round-trip rate, measures abrasion resistance, raw yarn It it is 7.36 times, sizing is 11.52 times.
3. the elongation of yarn and the test of slashing strength
The elongation of yarn and the strength of yarn are tested on the grand HD021N electronics single yarn tester in Nantong, and clamping opening spacing is 500mm, speed 500mm/min, every group of test 30 times, take its average value, measure raw yarn ultimate strength as 176.6cN, sizing Ultimate strength is 228.6cN；Raw yarn elongation is 1.32%, and the elongation of sizing is 2.68%.
4. sizing desizing rate is tested
According to the dry weight before desizing and after desizing, the desizing rate for measuring sizing is 10.15%.
Embodiment 2:
(1) the cold slurry of weaving is prepared according to the following steps：
1. adding in 80% water in mixing cirtern, high, low speed blender is started,
2. adding in 0.9%CMC powder, 30min is stirred, turns off high, low speed blender, 20 DEG C are impregnated 2h,
3. adding in 4.5% attapulgite, 1% antifoaming agent, 1% urea, 20min is stirred,
4. adding in 2% waterglass, 0.45%JFC bleeding agents, 0.3%AE0-7 emulsions, 20min, mixing speed are stirred 700r/min turns off high, low speed blender, and water is filled in mixing cirtern, and 20 DEG C are impregnated 4h,
5. stir 30min, mixing speed 700r/min, with filter screen filtration to get.
(2) size film property test is carried out to the cold slurry of weaving prepared by above-mentioned steps：
1. serous coat makes
By 210mm*300mm, the serous coat plate that thick 5 ㎜ polished glass make adjusts horizontal.It is dipped in a small amount of water on glass plate, Then the tiling of the mylar of 0.3 ㎜ thickness on a glass, glass plate level is corrected with level meter, prepared by configuration above-mentioned steps 5% concentration cold slurry slurries 100ml.By slurries slowly on a glass, and with glass bar gently move back and forth, make slurries It is paved on a glass, after spontaneously drying film forming, carefully serous coat from glass plate is peeled, is put into climatic chamber inner equilibrium It is for use for 24 hours.
2. fracture strength and the elongation at break test of serous coat
Serous coat is cut into long 200mm, the bar-shaped sample of wide 5mm is placed in constant temperature and humidity room, in the item of relative humidity 40% It is balanced under part for 24 hours, then tests its ultimate strength and elongation at break on the grand HD021N electronics single yarn tester in Nantong, tried Sample accommodates distance 100mm, decrease speed 50mm/min, tests 10 times and is averaged, and it is 9.28% to measure than elongation at break, than Fracture strength is 750.2cN.mm-1。
3. the water solubility rate test of serous coat
Serous coat is cut into the strip of long 100 ㎜, wide 20 ㎜, a straight line mark is drawn in length direction middle, it then will slurry Film is immersed in 80 DEG C of water, when mark overlaps among horizontal plane and serous coat, then presses stopwatch termination timing, stopwatch show when Between for representing the water solubility rate of serous coat, during test, the lower weight quality of hanging of serous coat is 3.6g, and experiment 10 times is averaged, survey It is 29.6s to obtain water solubility rate.
(4) slurry viscosity heat stability testing
The adjustable funnel viscometer tested viscosity of TY821 types and viscosity stability are selected, modulation 800ml contains above-mentioned steps system The cold slurry slurries of 5% standby concentration, stirring frequency 120r/min, water bath with thermostatic control heating are raised to 95 DEG C, are surveyed per 30min primary viscous Degree, keeps the temperature 3h altogether, and it is 86.26% to measure viscosity thermal stability.
(5) slashing performance is tested
1. sizing hairiness is tested
The filoplume of more than the 3mm of raw yarn and sizing, each test yarns line length are tested on YG171 type filoplume testers respectively It spends for 1m, surveys 30 times altogether, take its average value, yarn is 30m/min by speed, and in biology microscope Microscopic observation raw yarn and slurry Longitudinal filoplume situation of yarn measures raw yarn as 12.8/m, and sizing is 5.96/m.
2. sizing wear resistant is tested
It embraces in Y113 types and is tested on power machine, test 30, sizing every time, calculate average value, test condition is 20 DEG C, yarn Line static tensile is 200cN, and grinding is 235cN from pressure, and it is 143 times/min to be ground unloaded round-trip rate, measures abrasion resistance, raw yarn It it is 7.38 times, sizing is 11.68 times.
3. the elongation of yarn and the test of slashing strength
The elongation of yarn and the strength of yarn are tested on the grand HD021N electronics single yarn tester in Nantong, and clamping opening spacing is 500mm, speed 500mm/min, every group of test 30 times, take its average value, measure raw yarn ultimate strength as 178.6cN, sizing Ultimate strength is 228.6cN；Raw yarn elongation is 1.36%, and the elongation of sizing is 2.69%.
4. sizing desizing rate is tested
According to the dry weight before desizing and after desizing, the desizing rate for measuring sizing is 10.16%.

Claims (2)

1. a kind of cold slurry of weaving, it is characterised in that：By number percentage, including：CMC powder, the 0.5%-1% of 0.6%-0.9% Antifoaming agent, the attapulgite of 3%-4.5%, 0.5%-1% urea, the waterglass of 1%-2%, 0.3%-0.45% JFC The AE0-7 emulsions of bleeding agent, 0.2%-0.3%.
2. prepare a kind of method of cold slurry of weaving described in claim 1, it is characterised in that：Include the following steps,
1. adding in the water of 60%-80% in mixing cirtern, high, low speed blender is started,
2. adding in 0.6%-0.9%CMC powder, 30min is stirred, turns off high, low speed blender, 20 DEG C are impregnated 2h,
3. adding in 3%-4.5% attapulgites, the antifoaming agent of 0.5%-1%, 0.5%-1% urea, 20min is stirred,
4. 1%-2% waterglass, 0.3%-0.45%JFC bleeding agents, 0.2%-0.3%AE0-7 emulsions are added in, stirring 20min, mixing speed 700r/min turn off high, low speed blender, and water is filled in mixing cirtern, and 20 DEG C are impregnated 4h,
5. stir 30min, mixing speed 700r/min, with filter screen filtration to get.
CN201611099980.0A 2016-12-05 2016-12-05 A kind of cold slurry of weaving and preparation method thereof Pending CN108149474A (en)

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Application Number Priority Date Filing Date Title
CN201611099980.0A CN108149474A (en) 2016-12-05 2016-12-05 A kind of cold slurry of weaving and preparation method thereof

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CN108149474A true CN108149474A (en) 2018-06-12

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001048596A (en) * 1999-08-05 2001-02-20 Nippon Electric Glass Co Ltd Sizing agent and glass fiber coated with the agent
CN101658343A (en) * 2009-09-16 2010-03-03 蔡张林 Manufacturing method of silk garments
CN103898756A (en) * 2014-04-15 2014-07-02 苏州润弘贸易有限公司 Sizing method of textile slurry for dacron fabrics
CN103966848A (en) * 2014-05-20 2014-08-06 湖州福美达纺织有限公司 Size mixing process of ceiba or cotton blended yarn
CN104790211A (en) * 2015-04-17 2015-07-22 诸城市奥尼生物科技有限公司 Intermediate-temperature textile sizing method

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001048596A (en) * 1999-08-05 2001-02-20 Nippon Electric Glass Co Ltd Sizing agent and glass fiber coated with the agent
CN101658343A (en) * 2009-09-16 2010-03-03 蔡张林 Manufacturing method of silk garments
CN103898756A (en) * 2014-04-15 2014-07-02 苏州润弘贸易有限公司 Sizing method of textile slurry for dacron fabrics
CN103966848A (en) * 2014-05-20 2014-08-06 湖州福美达纺织有限公司 Size mixing process of ceiba or cotton blended yarn
CN104790211A (en) * 2015-04-17 2015-07-22 诸城市奥尼生物科技有限公司 Intermediate-temperature textile sizing method

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
刘森: "《纺织染概论》", 28 February 2004, 中国纺织出版社 *

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Application publication date: 20180612