CN108148954A - The heat treatment process of bolt - Google Patents

The heat treatment process of bolt Download PDF

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Publication number
CN108148954A
CN108148954A CN201611105083.6A CN201611105083A CN108148954A CN 108148954 A CN108148954 A CN 108148954A CN 201611105083 A CN201611105083 A CN 201611105083A CN 108148954 A CN108148954 A CN 108148954A
Authority
CN
China
Prior art keywords
nitrate
quenched
bolt
hours
sodium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611105083.6A
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Chinese (zh)
Inventor
曲立辉
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Qingdao Xiaomi Star Electronic Technology Co Ltd
Original Assignee
Qingdao Xiaomi Star Electronic Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Qingdao Xiaomi Star Electronic Technology Co Ltd filed Critical Qingdao Xiaomi Star Electronic Technology Co Ltd
Priority to CN201611105083.6A priority Critical patent/CN108148954A/en
Publication of CN108148954A publication Critical patent/CN108148954A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/18Hardening; Quenching with or without subsequent tempering
    • C21D1/19Hardening; Quenching with or without subsequent tempering by interrupted quenching
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/56General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering characterised by the quenching agents
    • C21D1/60Aqueous agents
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/0093Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for screws; for bolts

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Heat Treatment Of Articles (AREA)

Abstract

The invention discloses a kind of heat treatment process of bolt, include the following steps:1) pending bolt is preheated 45 hours, 360 370 DEG C of preheating furnace furnace temperature;2) Carburization Treatment;3) 56 hours are kept the temperature in 600 620 DEG C of salt bath furnace again to be quenched;4) first stage quenches, and salt made from earth containing a comparatively high percentage of sodium chloride is used at the uniform velocity to be quenched to 500 510 DEG C with 50 55 DEG C/min, the nitrate quenching agent presses 2 for potassium nitrate and sodium nitrate:The quenching medium of 1 mass ratio mixing;5) second stage quenches, and is quenched to 100 110 DEG C using salt made from earth containing a comparatively high percentage of sodium chloride constant temperature, the nitrate quenching agent presses 1 for potassium nitrate and sodium nitrate:The quenching medium of 2 mass ratio mixing;6) phase III quenches, and 230 235 DEG C are quenched to using 200 205 DEG C of hot water;7) the tempering furnace inside holding again at 300 305 DEG C is air-cooled to room temperature after 8 10 hours.The heat treatment process of bolt provided by the invention, the bolt contraction percentage of area obtained is small, and fit rate improves, and rejection rate reduces, and avoids using the Cyanides penetration enhancer being harmful to human body and environment.

Description

The heat treatment process of bolt
Technical field
The present invention relates to the heat treatment process of bolt.
Background technology
The treatment process of the high bolt of intensity is the techniques such as Q-tempering to be added to be handled, and adopt using carburizing or cyaniding With the 850-900 DEG C of heat preservation full annealing technique of 10 hours, but using the technique productions bolt in quenching the contraction percentage of area Larger, deformation rate is big, and low with the fit rate of nut, rejection rate is sometimes more than 10%.
Invention content
The purpose of the present invention is to provide a kind of heat treatment process of bolt, the bolt contraction percentage of area obtained is small, matches Conjunction rate improves, and rejection rate reduces, and avoids using the Cyanides penetration enhancer being harmful to human body and environment.
To achieve the above object, the technical scheme is that a kind of heat treatment process of bolt is designed, including walking as follows Suddenly:
1) pending bolt is preheated 4-5 hours, 360-370 DEG C of preheating furnace furnace temperature;
2) Carburization Treatment;
3) it keeps the temperature 5-6 hours in 600-620 DEG C of salt bath furnace again to be quenched, saline solution is using a concentration of 80-90g/L's Potassium chloride, the sodium sulphate of a concentration of 200-210g/L, the potassium nitrate of a concentration of 100-110g/L and a concentration of 180-190g/L The mixed solution of sodium chloride;
4) first stage quenches, and salt made from earth containing a comparatively high percentage of sodium chloride is used at the uniform velocity to be quenched to 500-510 DEG C with 50-55 DEG C/min, the nitrate quenching Agent presses 2 for potassium nitrate and sodium nitrate:The quenching medium of 1 mass ratio mixing;
5) second stage quenches, and is quenched to 100-110 DEG C using salt made from earth containing a comparatively high percentage of sodium chloride constant temperature, the nitrate quenching agent is potassium nitrate and nitre Sour sodium presses 1:The quenching medium of 2 mass ratio mixing;
6) phase III quenches, and 230-235 DEG C is quenched to using 200-205 DEG C of hot water;
7) the tempering furnace inside holding again at 300-305 DEG C is air-cooled to room temperature after 8-10 hours.
The advantages of the present invention are:A kind of heat treatment process of bolt, bolt section obtained are provided Shrinking percentage is small, and fit rate improves, and rejection rate reduces, and avoids using the Cyanides penetration enhancer being harmful to human body and environment.
Specific embodiment
With reference to embodiment, the specific embodiment of the present invention is further described.Following embodiment is only used for more Add and clearly demonstrate technical scheme of the present invention, and be not intended to limit the protection scope of the present invention and limit the scope of the invention.
The technical solution that the present invention is embodied is:A kind of heat treatment process of 1 bolt of embodiment, includes the following steps:
1) pending bolt is preheated 4 hours, 360 DEG C of preheating furnace furnace temperature;
2) Carburization Treatment;
3) 5 hours are kept the temperature in 600 DEG C of salt bath furnace again to be quenched, saline solution using a concentration of 80g/L potassium chloride, dense Spend the mixed solution of the sodium chloride of the sodium sulphate for 200g/L, the potassium nitrate of a concentration of 100g/L and a concentration of 180g/L;
4) first stage quenches, and salt made from earth containing a comparatively high percentage of sodium chloride is used at the uniform velocity to be quenched to 500 DEG C with 50 DEG C/min, the nitrate quenching agent is nitre Sour potassium and sodium nitrate press 2:The quenching medium of 1 mass ratio mixing;
5) second stage quenches, and is quenched to 100 DEG C using salt made from earth containing a comparatively high percentage of sodium chloride constant temperature, the nitrate quenching agent is potassium nitrate and sodium nitrate By 1:The quenching medium of 2 mass ratio mixing;
6) phase III quenches, and 230 DEG C are quenched to using 200 DEG C of hot water;
7) the tempering furnace inside holding again at 300 DEG C is air-cooled to room temperature after 8 hours.
Embodiment 2
A kind of heat treatment process of bolt, includes the following steps:
1) pending bolt is preheated 5 hours, 370 DEG C of preheating furnace furnace temperature;
2) Carburization Treatment;
3) 6 hours are kept the temperature in 620 DEG C of salt bath furnace again to be quenched, saline solution using a concentration of 90g/L potassium chloride, dense Spend the mixed solution of the sodium chloride of the sodium sulphate for 210g/L, the potassium nitrate of a concentration of 110g/L and a concentration of 190g/L;
4) first stage quenches, and salt made from earth containing a comparatively high percentage of sodium chloride is used at the uniform velocity to be quenched to 510 DEG C with 55 DEG C/min, the nitrate quenching agent is nitre Sour potassium and sodium nitrate press 2:The quenching medium of 1 mass ratio mixing;
5) second stage quenches, and is quenched to 110 DEG C using salt made from earth containing a comparatively high percentage of sodium chloride constant temperature, the nitrate quenching agent is potassium nitrate and sodium nitrate By 1:The quenching medium of 2 mass ratio mixing;
6) phase III quenches, and 235 DEG C are quenched to using 205 DEG C of hot water;
7) the tempering furnace inside holding again at 305 DEG C is air-cooled to room temperature after 10 hours.
Embodiment 3
A kind of heat treatment process of bolt, includes the following steps:
1) pending bolt is preheated 4.5 hours, 365 DEG C of preheating furnace furnace temperature;
2) Carburization Treatment;
3) 5.5 hours are kept the temperature in 610 DEG C of salt bath furnace again to be quenched, saline solution using a concentration of 85g/L potassium chloride, The mixed solution of the sodium chloride of the sodium sulphate of a concentration of 204g/L, the potassium nitrate of a concentration of 107g/L and a concentration of 183g/L;
4) first stage quenches, and salt made from earth containing a comparatively high percentage of sodium chloride is used at the uniform velocity to be quenched to 504 DEG C with 52 DEG C/min, the nitrate quenching agent is nitre Sour potassium and sodium nitrate press 2:The quenching medium of 1 mass ratio mixing;
5) second stage quenches, and is quenched to 105 DEG C using salt made from earth containing a comparatively high percentage of sodium chloride constant temperature, the nitrate quenching agent is potassium nitrate and sodium nitrate By 1:The quenching medium of 2 mass ratio mixing;
6) phase III quenches, and 232 DEG C are quenched to using 203 DEG C of hot water;
7) the tempering furnace inside holding again at 301 DEG C is air-cooled to room temperature after 9 hours.
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art For member, without departing from the technical principles of the invention, several improvements and modifications can also be made, these improvements and modifications Also it should be regarded as protection scope of the present invention.

Claims (1)

1. the heat treatment process of bolt, which is characterized in that include the following steps:
1) pending bolt is preheated 4-5 hours, 360-370 DEG C of preheating furnace furnace temperature;
2) Carburization Treatment;
3) it keeps the temperature 5-6 hours in 600-620 DEG C of salt bath furnace again to be quenched, saline solution uses the chlorination of a concentration of 80-90g/L The chlorination of potassium, the sodium sulphate of a concentration of 200-210g/L, the potassium nitrate of a concentration of 100-110g/L and a concentration of 180-190g/L The mixed solution of sodium;
4) first stage quenches, and salt made from earth containing a comparatively high percentage of sodium chloride is used at the uniform velocity to be quenched to 500-510 DEG C with 50-55 DEG C/min, the nitrate quenching agent is Potassium nitrate and sodium nitrate press 2:The quenching medium of 1 mass ratio mixing;
5) second stage quenches, and is quenched to 100-110 DEG C using salt made from earth containing a comparatively high percentage of sodium chloride constant temperature, the nitrate quenching agent is potassium nitrate and sodium nitrate By 1:The quenching medium of 2 mass ratio mixing;
6) phase III quenches, and 230-235 DEG C is quenched to using 200-205 DEG C of hot water;
7) the tempering furnace inside holding again at 300-305 DEG C is air-cooled to room temperature after 8-10 hours.
CN201611105083.6A 2016-12-05 2016-12-05 The heat treatment process of bolt Pending CN108148954A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611105083.6A CN108148954A (en) 2016-12-05 2016-12-05 The heat treatment process of bolt

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611105083.6A CN108148954A (en) 2016-12-05 2016-12-05 The heat treatment process of bolt

Publications (1)

Publication Number Publication Date
CN108148954A true CN108148954A (en) 2018-06-12

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611105083.6A Pending CN108148954A (en) 2016-12-05 2016-12-05 The heat treatment process of bolt

Country Status (1)

Country Link
CN (1) CN108148954A (en)

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WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20180612

WD01 Invention patent application deemed withdrawn after publication