CN108148464A - Phototropic wall pastes special environment protection ink preparation process - Google Patents
Phototropic wall pastes special environment protection ink preparation process Download PDFInfo
- Publication number
- CN108148464A CN108148464A CN201810121069.8A CN201810121069A CN108148464A CN 108148464 A CN108148464 A CN 108148464A CN 201810121069 A CN201810121069 A CN 201810121069A CN 108148464 A CN108148464 A CN 108148464A
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- CN
- China
- Prior art keywords
- alcohol
- finished product
- ink
- phototropic
- fused
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
- C09D11/033—Printing inks characterised by features other than the chemical nature of the binder characterised by the solvent
Abstract
The invention discloses phototropic walls to paste special environment protection ink preparation process, and preparation method is as follows：It is 35 to be fused into PVB resin with alcohols solvent weight ratio according to alcohol：65 ratio weighs alcohol and is fused into PVB resin and alcohols solvent, and the two is added in reaction kettle, at 35 DEG C, keeps the temperature 6 hours, dissolving becomes translucent resin solution；It is 15 according to coloring pigment, resin solution and pigment binder weight ratio：55：30 ratio mixes three, is dispersed with stirring 55 minutes in the blender that rotating speed is 800 revs/min, semi-finished product mill base is made；It will be fully ground in sand mill by the above-mentioned semi-finished product mill base being dispersed with stirring, the colloidal liquid of fineness≤10 micron be made；Antistatic agent, dispersant, adhesion promoter, mineral oil, vegetable oil and gel are successively added in above-mentioned colloidal liquid, is sufficiently stirred modulation, obtains the molten ink finished product of no benzene alcohol.Using the solution of the present invention, wall patch ink special that is environment friendly and pollution-free and realizing sensitization discoloration can be prepared.
Description
Technical field
The present invention relates to ink preparation processes, and in particular to a kind of phototropic wall pastes special environment protection ink preparation process.
Background technology
With the prevalence that wall pastes, more and more people's selection decorates wall using wall patch, the coloring of conventional wall patch
Ink generally comprises the stronger noxious material of the volatility such as a large amount of organic solvent, particularly toluene, dimethylbenzene, makes for a long time
With in the process, a large amount of toluene, dimethylbenzene etc. can volatilize or remain on wall, not only can cause environmental pollution, to people
Body health will also result in harm, in addition, with the variation of light irradiating angle and intensity, the quality that can also influence ink is shown.
Invention content
In view of the deficiency of background technology, the technical problems to be solved by the invention be to provide it is a kind of prepare it is environment friendly and pollution-free and
Realize the preparation process of the wall patch ink special of sensitization discoloration.
For this purpose, the present invention is realized using following scheme：
Phototropic wall pastes special environment protection ink preparation process, it is characterised in that：The ink is made of the raw material of following parts by weight：
Dry powder kaolin 2~7%, coloring pigment 3~8%, pigment binder 10~15%, alcohol are fused into PVB resin 50~65%, and alcohols is molten
Agent 15~35%, mineral oil 1~3%, vegetable oil 3~7%, gel 0. 5~3. 0%, adhesion promoter 0. 1~2. 0% resist
Electrostatic agent 0.1~1%, dispersant 0.3~2%, the photic compound 10~20% of spiropyran derivatives；
Preparation method is as follows：
(1) it is 35 to be fused into PVB resin with alcohols solvent weight ratio according to alcohol：65 ratio weigh alcohol be fused into PVB resin and
The two is added in reaction kettle by alcohols solvent, at 32-55 DEG C, keeps the temperature 5~8 hours, dissolving becomes translucent resin solution；
(2) it is 15 according to coloring pigment, resin solution and pigment binder weight ratio：55：30 ratio mixes three, is turning
Semi-finished product mill base is made to be dispersed with stirring 45~60 minutes in 600-1300 revs/min of blender in speed；
(3) it will be fully ground in sand mill by the above-mentioned semi-finished product mill base being dispersed with stirring, the glue of fineness≤10 micron be made
Shape liquid；
(4) antistatic agent, dispersant, adhesion promoter, mineral oil, vegetable oil are successively added in above-mentioned colloidal liquid and is coagulated
Glue is sufficiently stirred modulation, obtains the molten ink finished product of no benzene alcohol；
(5) filter filtering is put into above-mentioned ink finished product, after filtering out ingredient of the fineness more than 10 microns, product packaging is entered
Library.
The coloring pigment is ultramarine blue or iron oxide red or toluidine red.
The adhesion promoter is polyethyleneimine.
It is fused into based on PVB resin as a result of with alcohol, alcohols solvent, coloring pigment substep add in, the compound conjunction of multistep
Into, repeatedly stirring, dispersion, the technique being fully ground solve the problems, such as serious containing benezene substance and its residual solution in ink,
Product is made to comply fully with international hygiene standards and environmental requirement.Product drying is rapid, noresidue solution, free from extraneous odour, printing sample
Gloss is good, and pattern color is bright-coloured.
In addition, due to adding dry powder kaolin, the suspension of ink is efficiently modified, prevents pigment sedimentation, due to adding in
Gel and adhesion promoter effectively improve the contrast ratio and scrub resistance of ink, photic due to adding spiropyran derivatives
Compound, there are photochromisms for the photic compound of spiropyran derivatives, are excited by external condition, it may occur that closed loop
Body SP structures are to the reversible transition process of open loop body MC structures so that the illumination condition that wall is attached to varying strength issues third contact of a total solar or lunar eclipse discoloration
Variation so that the color of wall patch is more gorgeous.
Specific embodiment
Phototropic wall disclosed by the invention pastes special environment protection ink preparation process, it is characterised in that：The ink is by following
The raw material composition of parts by weight：Dry powder kaolin 2~7%, coloring pigment 3~8%, wherein pigment binder 10~15%, coloring pigment
For ultramarine blue or iron oxide red or toluidine red, alcohol is fused into PVB resin 50~65%, alcohols solvent 15~35%, and mineral oil 1~
3%, vegetable oil 3~7%, gel 0. 5~3. 0%, adhesion promoter 0. 1~2. 0%, adhesion promoter is polyethylene
Imines, antistatic agent 0.1~1%, dispersant 0.3~2%, the photic compound 10~20% of spiropyran derivatives；
Preparation method is as follows：
(1) it is 35 to be fused into PVB resin with alcohols solvent weight ratio according to alcohol：65 ratio weigh alcohol be fused into PVB resin and
The two is added in reaction kettle by alcohols solvent, at 32-55 DEG C, keeps the temperature 5~8 hours, dissolving becomes translucent resin solution；
(2) it is 15 according to coloring pigment, resin solution and pigment binder weight ratio：55：30 ratio mixes three, is turning
Semi-finished product mill base is made to be dispersed with stirring 45~60 minutes in 600-1300 revs/min of blender in speed；
(3) it will be fully ground in sand mill by the above-mentioned semi-finished product mill base being dispersed with stirring, the glue of fineness≤10 micron be made
Shape liquid；
(4) antistatic agent, dispersant, adhesion promoter, mineral oil, vegetable oil are successively added in above-mentioned colloidal liquid and is coagulated
Glue is sufficiently stirred modulation, obtains the molten ink finished product of no benzene alcohol；
(5) filter filtering is put into above-mentioned ink finished product, after filtering out ingredient of the fineness more than 10 microns, product packaging is entered
Library.
Wherein coloring pigment is ultramarine blue or iron oxide red or toluidine red.
Wherein adhesion promoter is polyethyleneimine.
Claims (3)
1. phototropic wall pastes special environment protection ink preparation process, it is characterised in that：The ink by following parts by weight raw material group
Into：Dry powder kaolin 2~7%, coloring pigment 3~8%, pigment binder 10~15%, alcohol are fused into PVB resin 50~65%, alcohol
Class solvent 15~35%, mineral oil 1~3%, vegetable oil 3~7%, gel 0. 5~3. 0%, adhesion promoter 0. 1~2.
0%, antistatic agent 0.1~1%, dispersant 0.3~2%, the photic compound 10~20% of spiropyran derivatives；
Preparation method is as follows：
(1) it is 35 to be fused into PVB resin with alcohols solvent weight ratio according to alcohol：65 ratio weigh alcohol be fused into PVB resin and
The two is added in reaction kettle by alcohols solvent, at 32-55 DEG C, keeps the temperature 5~8 hours, dissolving becomes translucent resin solution；
(2) it is 15 according to coloring pigment, resin solution and pigment binder weight ratio：55：30 ratio mixes three, is turning
Semi-finished product mill base is made to be dispersed with stirring 45~60 minutes in 600-1300 revs/min of blender in speed；
(3) it will be fully ground in sand mill by the above-mentioned semi-finished product mill base being dispersed with stirring, the glue of fineness≤10 micron be made
Shape liquid；
(4) antistatic agent, dispersant, adhesion promoter, mineral oil, vegetable oil are successively added in above-mentioned colloidal liquid and is coagulated
Glue is sufficiently stirred modulation, obtains the molten ink finished product of no benzene alcohol；
(5) filter filtering is put into above-mentioned ink finished product, after filtering out ingredient of the fineness more than 10 microns, product packaging is entered
Library.
2. phototropic wall as described in claim 1 pastes special environment protection ink preparation process, which is characterized in that the coloring face
Expect for ultramarine blue or iron oxide red or toluidine red.
3. phototropic wall as described in claim 1 pastes special environment protection ink preparation process, which is characterized in that the adhesive force
Accelerating agent is polyethyleneimine.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810121069.8A CN108148464A (en) | 2018-02-07 | 2018-02-07 | Phototropic wall pastes special environment protection ink preparation process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810121069.8A CN108148464A (en) | 2018-02-07 | 2018-02-07 | Phototropic wall pastes special environment protection ink preparation process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108148464A true CN108148464A (en) | 2018-06-12 |
Family
ID=62457042
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810121069.8A Withdrawn CN108148464A (en) | 2018-02-07 | 2018-02-07 | Phototropic wall pastes special environment protection ink preparation process |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108148464A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111253861A (en) * | 2020-03-25 | 2020-06-09 | 江苏纽克莱涂料有限公司 | High-temperature multi-color-changing irreversible temperature indicating coating for petrochemical equipment and preparation method thereof |
| CN116515345A (en) * | 2023-06-02 | 2023-08-01 | 安徽普米阳新材料有限公司 | Preparation method for producing printing ink |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1810895A (en) * | 2005-09-09 | 2006-08-02 | 诸城市腾霞油墨有限公司 | Environment protection plastic printing ink and its prepn |
| CN101033393A (en) * | 2003-07-01 | 2007-09-12 | 光学转变公司 | Photochromic compounds |
| CN101087836A (en) * | 2004-12-24 | 2007-12-12 | 西巴特殊化学品控股有限公司 | Coating compositions for marking substrates |
| CN103013224A (en) * | 2012-12-27 | 2013-04-03 | 茂名阪田油墨有限公司 | Planographic printing ink containing high-concentration kaolin and preparation method thereof |
| CN103666090A (en) * | 2012-08-30 | 2014-03-26 | 广东广乐包装材料股份有限公司 | Alcohol-soluble environment-friendly printing ink for tipping paper and preparation method thereof |
| CN107075287A (en) * | 2014-09-12 | 2017-08-18 | 多米诺英国有限公司 | Ink composite |
-
2018
- 2018-02-07 CN CN201810121069.8A patent/CN108148464A/en not_active Withdrawn
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101033393A (en) * | 2003-07-01 | 2007-09-12 | 光学转变公司 | Photochromic compounds |
| CN101087836A (en) * | 2004-12-24 | 2007-12-12 | 西巴特殊化学品控股有限公司 | Coating compositions for marking substrates |
| CN1810895A (en) * | 2005-09-09 | 2006-08-02 | 诸城市腾霞油墨有限公司 | Environment protection plastic printing ink and its prepn |
| CN103666090A (en) * | 2012-08-30 | 2014-03-26 | 广东广乐包装材料股份有限公司 | Alcohol-soluble environment-friendly printing ink for tipping paper and preparation method thereof |
| CN103013224A (en) * | 2012-12-27 | 2013-04-03 | 茂名阪田油墨有限公司 | Planographic printing ink containing high-concentration kaolin and preparation method thereof |
| CN107075287A (en) * | 2014-09-12 | 2017-08-18 | 多米诺英国有限公司 | Ink composite |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111253861A (en) * | 2020-03-25 | 2020-06-09 | 江苏纽克莱涂料有限公司 | High-temperature multi-color-changing irreversible temperature indicating coating for petrochemical equipment and preparation method thereof |
| CN111253861B (en) * | 2020-03-25 | 2021-10-22 | 江苏纽克莱涂料有限公司 | High-temperature multi-color-changing irreversible temperature indicating coating for petrochemical equipment and preparation method thereof |
| CN116515345A (en) * | 2023-06-02 | 2023-08-01 | 安徽普米阳新材料有限公司 | Preparation method for producing printing ink |
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| PB01 | Publication | ||
| PB01 | Publication | ||
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| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20180612 |