CN108142768A - A kind of solid particle and its production method based on combined spicebush leaf - Google Patents
A kind of solid particle and its production method based on combined spicebush leaf Download PDFInfo
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- CN108142768A CN108142768A CN201711143032.7A CN201711143032A CN108142768A CN 108142768 A CN108142768 A CN 108142768A CN 201711143032 A CN201711143032 A CN 201711143032A CN 108142768 A CN108142768 A CN 108142768A
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The present invention provides a kind of granules and its production method based on combined spicebush leaf.Belong to beverage technology field.Include the following steps：A, beverage stoste is extracted, and combined spicebush leaf, cassia seed, fructus cannabis, brush-cherry seed, ginseng and red yeast rice difference refluxing extraction obtain extracting solution, it is concentrated in vacuo after said extracted liquid is mixed, concentrate is obtained, B, microencapsulation add embedding medium in concentrate, Homogenizing pump homogeneous is used under 20 40MPa, obtain homogenizing fluid, C, spray drying, the Sucralose of addition 0.025wt% in homogenizing fluid, it is spray-dried after stirring evenly, obtains the granule based on combined spicebush leaf.The present invention realizes new resource food using combined spicebush leaf as product of the primary raw material research and development with lipid-reducing function --- concrete application of the combined spicebush leaf on functional food.
Description
Technical field
The invention belongs to drink extractive technique fields, are related to a kind of solid particle and its producer based on combined spicebush leaf
Method.
Background technology
Theory in terms of all being described in herbal and pharmacopeia that there are many China in relation to diet conservancy, there is abundant health food
Raw material.According to foreign study achievement, many foods with hypolipemic function are found that, wherein with the main of effect for reducing blood fat
Ingredient has dietary fiber, polypeptide, aliphatic acid, phytosterol, phenolic compound and polysaccharose substance etc., it is often edible can be with
Have the function that prevent hyperlipidemia.
In recent years, functional beverage market development was very swift and violent.The U.S. possesses the world's largest drinks market,
The functional beverage that market is related to has sports drink, energy drink, calcium-fortified beverage, fortified water etc..Functional beverage is in America and Europe
The development in market is more and more prosperous, and the development of the Asian-Pacific area also can not be ignored.Cradle of the Japan as functional beverage, total sales volume
The U.S. is only second to, occupies the second in the world.China is staple market of the functional beverage in the Asian-Pacific area in addition to Japan.China has
Cooking culture of extensive knowledge and profound scholarship, the theory of " integration of drinking and medicinal herbs " is through among the daily life of common people.Guangdong and Guangxi Provinces area it is old
The common people began to drink medicinal herb tea made of various herbal medicine and rhizome before more than 1000 years, for dispelling cold, dehumidifying, relieving summer-heat etc..Chinese work
Industry metaplasia production drinks start from the eighties.It can be seen that drinks have become the bright spot of beverage market, Chinese drinks market
It has begun to start.In future, the Main way of key technology innovation of the whole world in functional beverage production is function factor
Separation and purification technique, function factor detection technique (Fast Detection Technique), raw material and the pseudo- technology of product inspection and function factor
Stabilization technology etc..
Chinese medicine is the rarity in China, but to the utilization of Chinese medicine, is confined to its medical value mostly, in the market few medicines
Homologous drink is eaten to occur.
Invention content
The purpose of the present invention is regarding to the issue above and defect, provide a kind of life of the solid particle based on combined spicebush leaf
Production method.
It is a further object of the present invention to provide a kind of granules based on combined spicebush leaf.
In order to achieve the above objectives, present invention employs following technical proposals：
The production method of a kind of solid particle based on combined spicebush leaf, which is characterized in that include the following steps：
A, beverage stoste is extracted,
Combined spicebush leaf adds in 90% ethyl alcohol of 10 times of weight, and twice, each 1hr filters to obtain extracting solution to refluxing extraction,
The mixture of cassia seed, fructus cannabis and brush-cherry seed, adds in 10 times of weight waters, and refluxing extraction 1hr filters to obtain extraction
Liquid,
Ginseng adds in 70% ethyl alcohol of 10 times of weight, refluxing extraction 2 times, and each 1.5hr filters to obtain extracting solution,
Red yeast rice adds 10 times of amount water, and twice, each 2hr filters to obtain extracting solution to refluxing extraction,
It is concentrated in vacuo after said extracted liquid is mixed, obtains concentrate,
B, microencapsulation,
Embedding medium is added in concentrate, with Homogenizing pump homogeneous under 20-40MPa, obtains homogenizing fluid,
C, it is spray-dried,
The Sucralose of 0.025wt% is added in homogenizing fluid, is spray-dried, is obtained based on combined spicebush leaf after stirring evenly
The granule of body.
In the production method of the above-mentioned solid particle based on combined spicebush leaf, the embedding medium is maltodextrin,
Addition is the 2% of concentrate weight, the combined spicebush leaf, cassia seed, fructus cannabis, brush-cherry seed ginseng and red yeast rice weight ratio
It is followed successively by 1:10:10:8:5:1, in step C, also in homogenizing fluid added with combined spicebush leaf weight 40% aloe powder and with crow
The grain size of the equiponderant dendrobium officinale powder of medicine leaf, the aloe powder and dendrobium officinale powder is between 100-200 mesh.
In the production method of the above-mentioned solid particle based on combined spicebush leaf, solid content is 8- in the concentrate
15wt%, temperature concentrated in vacuo are 60-80 DEG C, vacuum degree 0.065-0.07MPa, and the homogenizing temperature is 75-80 DEG C,
The sterilization temperature is 98 DEG C, time 30s.
In the production method of the above-mentioned solid particle based on combined spicebush leaf, the extraction of step A is in extraction mechanism
It carries out, the extraction mechanism includes extraction canister assembly, extraction canister assembly connection extracting solution temporary storage tank, the extraction
There are four canister assemblies, and each canister assembly top part of extracting is not connected with extracting solution supply assembly, and the extraction canister assembly includes
Extractor, extractor top are equipped with return duct, return duct connection condenser inlet, condensator outlet connection extractor side
Wall, the extraction pot bottom are equipped with filter residue filter plate, filter residue filter plate connection extraction pump, extraction pump connection extracting solution
Temporary storage tank, extracting solution temporary storage tank pump connection inspissator by No.1, and the inspissator connects UHT sterilizers, institute with No. two pumps
No. three pumps of the UHT sterilizers stated connect homogeneous liquid storage tank, and the homogeneous liquid storage tank connects Homogenizing pump with No. four pumps, described
Homogenizing pump connects transfer storage tank, and transfer storage tank passes through high pressure by No. five pump connection spraying liquid storage tanks, the spraying liquid storage tank
Pump connection spray drying tower.
In the production method of the above-mentioned solid particle based on combined spicebush leaf, between condensator outlet and extractor
If there are one U-shaped dip tube, the return duct is in being vertically arranged, and the condenser is in horizontally disposed.
In the production method of the above-mentioned solid particle based on combined spicebush leaf, the extracting solution supply assembly includes
Water tank and ethanol storage tank, water tank water pump connect extracting solution supplying tank, and the ethanol storage tank is pumped with ethyl alcohol to be connected
Extracting solution supplying tank is connect, extracting solution supplying tank extraction supply pump connection extractor top, the water supply pump is with carrying
The pipeline between liquid supplying tank is taken to be equipped with first flowmeter, is set on the pipeline between ethyl alcohol pump and extracting solution supplying tank
There is second flowmeter.
In the production method of the above-mentioned solid particle based on combined spicebush leaf, homogeneous is equipped at the top of the Homogenizing pump
Feeding cylinder, the outlet connection homogenization buffer cylinder of Homogenizing pump, the homogenization buffer cylinder are located above homogenous charge cylinder, and in homogeneous
The first valve is equipped between dsah-pot and homogenous charge cylinder.
In the production method of the above-mentioned solid particle based on combined spicebush leaf, described No. four pumps pass through the second valve
Homogenous charge cylinder is connected, No. four pumps also connect homogenizing fluid tank top by third valve, and homogeneous pump discharge passes through the 4th respectively
Valve and the 5th valve connection homogenization buffer cylinder and transfer storage tank, described No. five pumps pass through the 6th valve and the 7th valve respectively
Connection spraying liquid storage tank and transfer storage tank.
In the production method of the above-mentioned solid particle based on combined spicebush leaf, the spray drying tower includes tower
Body, the tower body side wall are connected with hot wind air intake assembly, and air-out component is connected at the top of the tower body, spray is equipped in tower body
Mist component, spray assembly connection high-pressure pump, the hot wind air intake assembly include air-heater and connect air-heater
Heater, the heater connect main blast pipe, main blast pipe connecting side blast pipe, side blast pipe connection tower body side wall, institute
The main blast pipe stated is also associated with voltage stabilizing disk, and the voltage stabilizing disk is located above spray assembly, and the voltage stabilizing disk is equipped with
Several steady wind outlets, towards tower body bottom, the spray assembly includes the nozzle being located in tower body, high for steady wind outlet
Press pump connects nozzle, and the nozzle is located at the lower section of voltage stabilizing disk, and the air-out component includes the outlet air at the top of connection tower body
Pipe, discharge pipe connection dust suction pond.
It is entitled according to made from above-mentioned production method to enjoy thin solid particle and its producer based on combined spicebush leaf
Method.
Compared with prior art, the invention has the advantages that：
Using combined spicebush leaf as product of the primary raw material research and development with lipid-reducing function, new resource food is realized --- the root of three-nerved spicebush
Concrete application of the leaf on functional food.Blood fat is reduced in line with qi-regulating, defaecation ease constipation as the main purpose, makes this product formula
Selected raw material plays maximum effect.
The effect of in this product ingredient by capsule of nanoization generate new function and new features, as solubility improve,
Storage-stable enhancing, the enhancing of function targeting, Controlled release, bioactivity improves, bioavailability improves.
The extraction of combined spicebush leaf particle drink, concentration, homogeneous to a whole set of continuous production being spray-dried are realized, especially
Homogenizing effect is good, is capable of the mouthfeel and quality of the guarantee particle drink of maximum purity.
It using different material corresponding extraction respectively, both prevents from malfunctioning, can also improve production efficiency, while extractant is carried out
The method of situ configuration can utilize extractant, prevent extractant from wasting to greatest extent；Homogenizing effect is good, homogeneous uniform, energy
The small molecule being evenly distributed, so as to create conditions for the drink of production high-quality.
Spray-drying process dust yield is few, and dust can be adsorbed substantially, and environmental pollution is small；In spray process
In, the dust of larger particles can fall back to bottom of towe, and byproduct can be used as after screening, carries out secondary recovery utilization, from
And improve product yield.
In the drying chamber by green logical beverage stoste after atomization, in the contact with hot-air, moisture rapid vaporization obtains
Dry solid powder.The active constituent of the Chinese herbal medicines such as combined spicebush leaf is remained to greatest extent, and product has full of nutrition, flavor
, there is very big market value in the features such as unique.
Part is illustrated to embody by further advantage, target and the feature of the present invention by following, and part will also be by this
The research and practice of invention and be understood by the person skilled in the art.
Description of the drawings
Fig. 1 is the structure diagram of extraction mechanism.
Fig. 2 is the structure diagram of spray drying tower.
Fig. 3 is the structure diagram of voltage stabilizing disk.
In figure, extraction canister assembly 101, extracting solution temporary storage tank 102, extracting solution supply assembly 103, extractor 104, heat exchange
Chuck 104a, return duct 105, condenser 106, filter residue filter plate 107, extraction pump 108, U-shaped dip tube 109, water tank 110,
Ethanol storage tank 111, water pump 112, extracting solution supplying tank 113, ethyl alcohol pump 114, extraction supply pump 115, first flowmeter 116, the
Two flowmeters 117, No.1 pump 118,119, No. two pumps 120 of inspissator, UHT sterilizers 121, No. three pumps 122, homogeneous liquid storage tanks
123rd, No. four pump 124, Homogenizing pump 125, homogenous charge cylinder 126, homogenization buffer cylinder 127, the first valve 128, the second valve 129,
Third valve 130,131, No. five pumps 132 of transfer storage tank, spraying liquid storage tank 133, spray drying tower 134, air-out component 200, tower
Body 201, hot wind air intake assembly 202, spray assembly 203, air-heater 204, heater 205, main blast pipe 206, side blast pipe
207th, voltage stabilizing disk 208, steady wind outlet 209, high-pressure pump 211, nozzle 212, filter plate 213, suction tube 214, discharge pipe 215, dust suction
Pond 216, horn mouth 217, secondary filter pond 218, check valve 219, screen pipe 220, volume damper 221.
Specific embodiment
A kind of production method of solid particle based on combined spicebush leaf, includes the following steps：
A, beverage stoste is extracted,
Combined spicebush leaf adds in 90% ethyl alcohol of 10 times of weight, and twice, each 1hr filters to obtain extracting solution to refluxing extraction, pine torch,
The mixture of fructus cannabis and brush-cherry seed adds in 10 times of weight waters, and refluxing extraction 1hr filters to obtain extracting solution, and ginseng adds in 10 times of weights
70% ethyl alcohol of amount, refluxing extraction 2 times, each 1.5hr filter to obtain extracting solution, and red yeast rice adds 10 times of amount water, refluxing extraction two
Secondary, each 2hr filters to obtain extracting solution, is concentrated in vacuo after said extracted liquid is mixed, obtains concentrate,
It will be appreciated by those skilled in the art that refluxing extraction mentioned above 2 times, refers to every time with the extraction of 10 times of weight
A part of extracting solution is filtered to obtain in agent after having extracted every time, No. 2 times extracting solution merges, and during refluxing extraction, liquid keeps slightly boiling
State,
B, microencapsulation adds embedding medium in concentrate, with Homogenizing pump homogeneous under 20-40MPa, obtains homogenizing fluid,
C, it is spray-dried,
The Sucralose of 0.025wt% is added in homogenizing fluid, is spray-dried, is obtained based on combined spicebush leaf after stirring evenly
The granule of body.
Embedding medium is maltodextrin, and addition is the 2% of concentrate weight, the combined spicebush leaf, cassia seed, fructus cannabis,
The weight ratio of brush-cherry seed ginseng and red yeast rice is followed successively by 1:10:10:8:5:1, in step C, added with crow also in homogenizing fluid
The aloe powder of medicine leaf weight 40% and with the equiponderant dendrobium officinale powder of combined spicebush leaf, the aloe powder and dendrobium officinale powder
Grain size is between 100-200 mesh.
Solid content is 8-15wt% in concentrate, and temperature concentrated in vacuo is 60-80 DEG C, vacuum degree 0.065-0.07MPa,
The homogenizing temperature is 75-80 DEG C, and the sterilization temperature is 98 DEG C, time 30s.
The extraction of step A carries out in extraction mechanism, as shown in Figure 1, extraction mechanism includes extraction canister assembly 101, it is described
Extraction canister assembly 101 connect extracting solution temporary storage tank 102, there are four the extraction canister assemblies 101, each extracts canister assembly
101 tops are connected separately with extracting solution supply assembly 103, and the extraction canister assembly 101 includes extractor 104, and described carries
104 top of tank is taken to be equipped with return duct 105, return duct 105 connects 106 import of condenser, the outlet of condenser 106 connection extractor
104 side walls, 104 bottom of extractor are equipped with filter residue filter plate 107, and the connection extraction of filter residue filter plate 107 pump 108 is described
108 connection extracting solution temporary storage tanks 102 of extraction pump, extracting solution temporary storage tank 102 is described by 118 connection inspissators 119 of No.1 pump
No. two 120 connection UHT sterilizers 121 of pump of inspissator 119, the UHT sterilizers 121 connect homogeneous with No. three pumps 122
Liquid storage tank 123, the homogeneous liquid storage tank 123 is with No. four 124 connection Homogenizing pumps 125 of pump, dump in Homogenizing pump connection
Tank 131, transfer storage tank 131 pass through high-pressure pump by No. five 132 connection spraying liquid storage tanks 133 of pump, the spraying liquid storage tank 133
211 connection spray drying towers 134.
It will be appreciated by those skilled in the art that heater is provided on extractor 104, for exchanging heat, in this implementation
In example, 104 outer wall of extractor is equipped with heat exchange jacket 104a, and heat exchange jacket 104a can be passed through steam or conduction oil.
In the present embodiment, condenser 106 is shell and tube condenser or finned cooler, and filter residue filter plate 107 is with carrying
104 bottom of tank is taken removably to connect, and passes through sealing ring and is connected and sealed, the filter opening specification of filter residue filter plate 107 can root
It is selected according to process condition.
Four extraction canister assemblies 101 of the present embodiment correspond to the extraction of five leaves grass, cassia seed, fructus cannabis and brush-cherry seed respectively
Extraction, the extraction of ginseng, the extraction of red yeast rice, the material in each extractor 104 is constant always, avoids mixing, also favorably
In the operation for carrying out serialization.
In concrete operations, the material weighed up by technical recipe is respectively put into four extractors 104, is divided after the completion of extraction
It is not driven into extracting solution temporary storage tank 102 to store, the liquid of mixing is extracting solution, and material formula is not error-prone, and produces effect
Rate also significantly improves.
U-shaped dip tube 109 there are one exporting and set between extractor 104 in condenser 106.The U-shaped dip tube 109 is
Using the principle of water seal, the steam generated in extraction process is made directly not arrive condensator outlet, but by return duct 105 into
After entering into condenser condensation, then become liquid and be flowed into extractor 104 from U-shaped dip tube 109, realize that reflux repeatedly carries
It takes, so as to improve extraction efficiency.
In the present embodiment, return duct 105 is in being vertically arranged, and the condenser 106 is in horizontally disposed.
Extracting solution supply assembly 103 includes water tank 110 and ethanol storage tank 111, the water pump 112 of water tank 110
Extracting solution supplying tank 113 is connected, the ethanol storage tank 111 ethyl alcohol pumps 114 connection extracting solution supplying tanks 113, and described carries
The extraction supply pump 115 of liquid supplying tank 113 is taken to connect 104 top of extractor.
Pipeline between water supply pump 112 and extracting solution supplying tank 113 is equipped with first flowmeter 116, ethyl alcohol pump
Pipeline between 114 and extracting solution supplying tank 113 is equipped with second flowmeter 117.
Extracting solution due to being an extractor 104 is different, and the proportioning of mainly second alcohol and water is different, under normal conditions
It is to prepare to be that a proportioning tank is matched, but production cost so significantly rises, the present embodiment passes through extracting solution supplying tank 113
The ethanol solution of various concentration is respectively configured, is driven into respectively in different extractors 104, avoids the waste of extracting solution.
Extracting solution temporary storage tank 102 passes through 118 connection inspissator 119 of No.1 pump, No. two pumps 120 of the inspissator 119
Connect UHT sterilizers 121, the UHT sterilizers 121 No. three 122 connection homogeneous liquid storage tanks 123 of pump, the homogenizing fluid
No. four 124 connection Homogenizing pumps 125 of pump of storage tank 123.
It is well known that Homogenizing pump 125 is that macromolecular is sheared using the principle of high shear, small point is become
Son, however existing Homogenizing pump 125 is all to be passed straight back to feed end after discharging, the material for leading to feed end are stoste and
The mixture of clipped liquid, macromolecular and small molecule coexist in the mixture, are difficult to realize uniform homogenizing effect.
In the present embodiment, 125 top of Homogenizing pump is equipped with homogenous charge cylinder 126, and the outlet connection homogeneous of Homogenizing pump 125 delays
Cylinder 127 is rushed, the homogenization buffer cylinder 127 is located at 126 top of homogenous charge cylinder, and in homogenization buffer cylinder 127 and homogenous charge
The first valve 128 is equipped between cylinder 126.
Its principle is by the material in homogenous charge cylinder 126 first whole homogeneous to homogenization buffer cylinder 127, treats homogenous charge
When cylinder 126 is without material, then the material in homogenization buffer cylinder 127 is put into homogenous charge cylinder 126, realizes homogeneous again, according to
It is secondary analogize can realize multiple homogeneous, so as to fulfill perfectly homogenous effect.
No. four pumps 124 connect homogenous charge cylinder 126 by the second valve 129, and No. four pumps 124 also pass through third valve 130
123 top of homogeneous liquid storage tank is connected, Homogenizing pump 125 exports connects homogeneous by the 4th valve 135 and the 5th valve 136 respectively
Dsah-pot 127 and transfer storage tank 131, described No. five pumps 132 pass through the 6th valve 137 and the connection spray of the 7th valve 138 respectively
Spray film storage tank 133 and transfer storage tank 131.
The second valve 129 is closed, opens third valve 13, the material in 124 pairs of homogeneous liquid storage tanks 123 of No. four pumps can be passed through
Carry out self-loopa mixing.
The spray drying of step C is dried using spray drying tower, with reference to shown in Fig. 2 and Fig. 3, the spray drying tower
134 include tower body 201, and 201 side wall of tower body is connected with hot wind air intake assembly 202, and 201 top of tower body is connected with
Air-out component 200, tower body 201 is interior to be equipped with spray assembly 203, spray assembly connection high-pressure pump 211, the hot wind
Air intake assembly 202 includes air-heater 204 and connects the heater 205 of air-heater 204, the heater 205 connection master
Blast pipe 206, main 206 connecting side blast pipe 207 of blast pipe, side blast pipe 207 connect 201 side wall of tower body, the main air inlet
Pipe 206 is also associated with voltage stabilizing disk 208, and the voltage stabilizing disk 208 is located above spray assembly 203, on the voltage stabilizing disk 208
Equipped with several steady wind outlets 209, the steady wind exports 209 towards 201 bottom of tower body.
In the present embodiment, there is gap, voltage stabilizing disk 208 is one hollow between 201 inner wall of voltage stabilizing disk 208 and tower body
Disk body, the hot wind in main blast pipe 206 can enter in voltage stabilizing disk 208 and export 209 outlet air, writing style outlet 209 along steady wind
Air-out direction it is downward, and side blast pipe 207 enters hot wind in tower body 201 and is moved toward 201 top-direction of tower body, is moved through
Cheng Zhonghui drives the smaller dried dust of particle up to move, and moves to voltage stabilizing Pan208Chu, since steady wind exports 209 outlet air
It influences, wind speed weakens, and forms dust floating zone in voltage stabilizing disk 208, larger dust particles are settled, entered so as to reduce
Dust in air-out component 200.
Voltage stabilizing disk 208 is in disk form, and volume damper 221 is equipped between voltage stabilizing disk 208 and main blast pipe 206, described
Steady wind outlet 209 protrude from 208 lower surface of voltage stabilizing disk, and steady wind outlet 209 is gathered on voltage stabilizing disk 208.
Side blast pipe 207 can be directly connected to tower body, and junction is located at 203 lower section of spray assembly, preferred embodiment, side into
Air hose 207 is connect along the tangential direction of 201 side wall of tower body with tower body 201.
Spray assembly 203 includes the nozzle 212 being located in tower body 201, and high-pressure pump 211 connects nozzle, the nozzle
212 are located at the lower section of voltage stabilizing disk 208.
133 bottom of liquid storage tank spray with one piece of filter plate 213, the high-pressure pump 211 connects spraying with suction tube 214
Liquid storage tank 133, suction tube 214 are located at 213 top of filter plate.It is well known that high-pressure pump 211, which encounters solid, can be easy to cause inside
The abrasion of movement parts, therefore before high-pressure pump 211 is entered, spray liquid filtering is made using the method for natural subsidence, filter plate 213 plays
Barrier effect prevents bottom solid particle from entering in high-pressure pump 211.
Preferably, the distance between 214 bottom of suction tube and 213 upper surface of filter plate are 2-4cm.
In the present embodiment, air-out component 200 includes the discharge pipe 215 at 201 top of connection tower body, the discharge pipe 215
Connect dust suction pond 216.
Horn mouth 217 is formed after expanding on 215 bottom of discharge pipe, liquid is housed, and horn mouth 217 is located in dust suction pond 216
The ullage of liquid in dust suction pond 216 prevents liquid along horn mouth suck-back.
Dust suction pond 216 is the pond body of closing, and discharge pipe 215 is inserted into dust suction pond 216 and is tightly connected with dust suction pond 216,
216 top connection secondary filter pond 218 of dust suction pond.
Equipped with liquid in secondary filter pond 218, dust suction pond 216 is with secondary filter pond 218 by being equipped with check valve 219
Pipeline connects, and pipeline connection screen pipe 220, screen pipe 220 is located in secondary filter pond 218, the top extension of screen pipe 220
In to secondary filter pond 218 below the liquid level of liquid.Screen pipe 220 is inserted under liquid level, and dust is directly contacted with liquid to be inhaled
Attached, due to the setting of check valve 219, liquid will not be by suck-back to dust suction pond 216.
The material of extraction is respectively charged into four extractors 104.Pass through first flowmeter 116 and second flowmeter 117
Flow velocity and the time of water and ethyl alcohol are controlled, the ethanol solution of various concentration is obtained in extracting solution supplying tank 113, respectively by carrying
Supply pump 115 is taken to imported into four different extractors 104, extractor 104 is thermally formed reflux, four extractors 104
Return time is different.
After the completion of reflux, filtrate is evacuated to extracting solution temporary storage tank 102 with extraction pump 108 respectively and stored by four extractors.Again
Inspissator 119 is driven by No.1 pump 118 to concentrate, inspissator 119 is vacuum concentrator, and scraper-type inspissator or more may be selected
Inspissator is imitated, UHT sterilizers 121 are entered after concentration and are sterilized, later into homogeneous liquid storage tank 123, are realized by Homogenizing pump 125
Homogeneous in homogenizing process, sweetener or macromolecular coating agent can also be added in homogenous charge cylinder 126, forms micro- glue
Capsule after the completion of homogeneous, obtains drinks extraction liquid.
Drinks extraction liquid is deposited into transfer storage tank 131, is squeezed into spraying liquid storage tank 133 with No. five pumps 132, uses high pressure later
Pump 211 is squeezed into spray drying tower 134 and is spray-dried.
High-pressure pump 211 is sprayed extracting solution by nozzle 212, and air-heater 204, which works, heats wind by heater 205,
Heater can be electric heater or steam heater, and the hot wind part after heating enters tower body 201 from side blast pipe 207,
Another part is sprayed from steady wind outlet 209, and extracting solution encounters hot wind, is dried to particle.
For hot wind along discharge pipe 215 to horn mouth 217, part dust enters two by liquid adsorption along screen pipe 220 later
Secondary filtering ponds 218, dust achieve the effect that complete dedusting by liquid adsorption.
The present invention has following innovation：
1st, raw material is innovated：Combined spicebush leaf is comprehensively utilized, there is lipid-loweringing work(by primary raw material research and development of combined spicebush leaf
The product of energy, realizes new resource food --- concrete application of the root of three-nerved spicebush leaf on functional food.In line with qi-regulating, logical
Just ease constipation reduces blood fat as the main purpose, and the principle of medicine is selected according to dialectical legislation and with method, consults relevant Chinese medicine books
Several medicinal material usage histories are recorded, including《Compendium of Materia Medica》、《Chinese herbal medicine》、《People's Republic of China's spy's pharmacopeia》(2015 editions) etc.
It records, with reference to the effect of Chinese medicine modern pharmacology and pilot plant test data, raw material selected by this product formula is made to play maximum effect.
2nd, process innovation：Change traditional production technology, using water carry with alcohol extracting combined technology, high pressure homogenization technique,
Capsule of nano technology is concentrated in vacuo technology, spraying granulation technology, product quality detection technique etc. and carries out Integrated research and open
Hair, establishes green logical solid beverage production new technology and new process；Product color, the shape for making production are all good.In assurance function
It, can be with the release of control effect ingredient using the targeting and slow releasing function of capsule of nano technology while food quality
Rate achievees the effect that targeted release, improves its bioavailability, farthest plays its health-care efficacy.
3rd, products innovation：This product using combined spicebush leaf, ginseng, Radix Glycyrrhizae, red yeast rice, cassia seed, fructus cannabis, brush-cherry seed as formula and
Manufactured granule achievees the effect that reducing blood lipid by defaecation qi-regulating, easy to carry, and having improves sleep, improves immunity,
Antifatigue, vivotoxin is discharged in defaecation ease constipation, and product market prospects are had an optimistic view of.
4th, function innovation：The effect of in this product ingredient by capsule of nanoization generate new function and new features, such as
Solubility raising, storage-stable enhancing, the enhancing of function targeting, Controlled release, bioactivity improves, bioavailability improves
Deng.
Specific embodiment described herein is only an example for the spirit of the invention.Technology belonging to the present invention is led
The technical staff in domain can do various modifications or additions to described specific embodiment or replace in a similar way
In generation, however, it does not deviate from the spirit of the invention or beyond the scope of the appended claims.
Although be used more herein extraction canister assembly 101, extracting solution temporary storage tank 102, extracting solution supply assembly 103,
Extractor 104, heat exchange jacket 104a, return duct 105, condenser 106, filter residue filter plate 107, extraction pump 108, U-shaped dip tube
109th, water tank 110, ethanol storage tank 111, water pump 112, extracting solution supplying tank 113, ethyl alcohol pump 114, extraction supply pump 115, the
121, No. three flow meters 116, second flowmeter 117, No.1 pump 118,119, No. two pumps 120 of inspissator, UHT sterilizers pumps
122nd, 123, No. four pumps 124, Homogenizing pump 125, homogenous charge cylinder 126, homogenization buffer cylinder 127, the first valves of homogeneous liquid storage tank
128th, the second valve 129, third valve 130,131, No. five pumps 132 of transfer storage tank, spraying liquid storage tank 133, spray drying tower
134th, air-out component 200, tower body 201, hot wind air intake assembly 202, spray assembly 203, air-heater 204, heater 205, it is main into
Air hose 206, side blast pipe 207, voltage stabilizing disk 208, steady wind outlet 209, high-pressure pump 211, nozzle 212, filter plate 213, suction tube
214th, discharge pipe 215, dust suction pond 216, horn mouth 217, secondary filter pond 218, check valve 219, screen pipe 220, air quantity are adjusted
221 grade terms of valve, but it does not preclude the possibility of using other terms.The use of these items is only for more easily describe
With the essence for explaining the present invention；Any one of the additional limitations is construed as all to disagree with spirit of the present invention.
Claims (10)
1. the production method of a kind of solid particle based on combined spicebush leaf, which is characterized in that include the following steps：
A, beverage stoste is extracted,
Combined spicebush leaf adds in 90% ethyl alcohol of 10 times of weight, and twice, each 1hr filters to obtain extracting solution to refluxing extraction,
The mixture of cassia seed, fructus cannabis and brush-cherry seed adds in 10 times of weight waters, and refluxing extraction 1hr filters to obtain extracting solution,
Ginseng adds in 70% ethyl alcohol of 10 times of weight, refluxing extraction 2 times, and each 1.5hr filters to obtain extracting solution,
Red yeast rice adds 10 times of amount water, and twice, each 2hr filters to obtain extracting solution to refluxing extraction,
It is concentrated in vacuo after said extracted liquid is mixed, obtains concentrate,
B, microencapsulation,
Embedding medium is added in concentrate, with Homogenizing pump homogeneous under 20-40MPa, obtains homogenizing fluid,
C, it is spray-dried,
The Sucralose of 0.025wt% is added in homogenizing fluid, is spray-dried, is obtained based on combined spicebush leaf after stirring evenly
Granule.
A kind of 2. production method of solid particle based on combined spicebush leaf according to claim 1, which is characterized in that institute
The embedding medium stated be maltodextrin, addition be concentrate weight 2%, the combined spicebush leaf, cassia seed, fructus cannabis, Yu Li
Kindhearted person joins and the weight ratio of red yeast rice is followed successively by 1:10:10:8:5:1, in step C, combined spicebush leaf is added with also in homogenizing fluid
The aloe powder of weight 40% and with the equiponderant dendrobium officinale powder of combined spicebush leaf, the grain size of the aloe powder and dendrobium officinale powder
Between 100-200 mesh.
A kind of 3. production method of solid particle based on combined spicebush leaf according to claim 1, which is characterized in that institute
Solid content is 8-15wt% in the concentrate stated, and temperature concentrated in vacuo is 60-80 DEG C, vacuum degree 0.065-0.07MPa, described
Homogenizing temperature for 75-80 DEG C, the sterilization temperature is 98 DEG C, time 30s.
A kind of 4. production method of solid particle based on combined spicebush leaf according to claim 1, which is characterized in that step
The extraction of rapid A carries out in extraction mechanism, and the extraction mechanism includes extraction canister assembly (101), the extraction canister assembly
(101) connection extracting solution temporary storage tank (102), which is characterized in that there are four the extraction canister assemblies (101), each extractor
Extracting solution supply assembly (103) is connected separately at the top of component (101),
The extraction canister assembly (101) includes extractor (104), and return duct is equipped at the top of the extractor (104)
(105), return duct (105) connection condenser (106) import, condenser (106) outlet connection extractor (104) side wall are described
Extractor (104) bottom be equipped with filter residue filter plate (107), filter residue filter plate (107) connection extraction pump (108), described carries
Pump (108) is taken to connect extracting solution temporary storage tank (102),
Extracting solution temporary storage tank (102) pumps (118) by No.1 and connects inspissator (119), No. two pumps of the inspissator (119)
(120) connection UHT sterilizers (121), the UHT sterilizers (121) connect homogeneous liquid storage tanks (123) with No. three pumps (122),
The homogeneous liquid storage tank (123) No. four pump (124) connection Homogenizing pumps (125), Homogenizing pump connection transfer storage tank
(131), transfer storage tank (131) is led to by No. five pump (132) connection spraying liquid storage tanks (133), the spraying liquid storage tank (133)
Cross high-pressure pump (211) connection spray drying tower (134).
5. a kind of production method of solid particle based on combined spicebush leaf according to claim 4, which is characterized in that
U-shaped dip tube (109) there are one being set between condenser (106) outlet and extractor (104), the return duct (105) is in perpendicular
Straight setting, the condenser (106) is in horizontally disposed.
A kind of 6. production method of solid particle based on combined spicebush leaf according to claim 5, which is characterized in that institute
The extracting solution supply assembly (103) stated includes water tank (110) and ethanol storage tank (111), and the water tank (110) uses water pump
(112) connection extracting solution supplying tank (113), the ethanol storage tank (111) pump (114) connection extracting solution supplying tank with ethyl alcohol
(113), the extracting solution supplying tank (113) is connected with extraction supply pump (115) at the top of extractor (104), the water supply
Pump the pipeline between (112) and extracting solution supplying tank (113) and be equipped with first flowmeter (116), ethyl alcohol pump (114) and
Pipeline between extracting solution supplying tank (113) is equipped with second flowmeter (117).
A kind of 7. production method of solid particle based on combined spicebush leaf according to claim 6, which is characterized in that institute
Homogenous charge cylinder (126) is equipped at the top of the Homogenizing pump (125) stated, the outlet of Homogenizing pump (125) connects homogenization buffer cylinder (127),
The homogenization buffer cylinder (127) is above the homogenous charge cylinder (126), and in homogenization buffer cylinder (127) and homogenous charge cylinder
(126) the first valve (128) is equipped between.
A kind of 8. production method of solid particle based on combined spicebush leaf according to claim 7, which is characterized in that institute
No. four pumps (124) stated connect homogenous charge cylinder (126) by the second valve (129), and No. four pumps (124) also pass through third valve
(130) at the top of connection homogeneous liquid storage tank (123), Homogenizing pump (125) outlet passes through the 4th valve (135) and the 5th valve respectively
(136) connection homogenization buffer cylinder (127) and transfer storage tank (131), described No. five pumps (132) pass through the 6th valve respectively
(137) and the 7th valve (138) connects spraying liquid storage tank (133) and transfer storage tank (131).
A kind of 9. production method of solid particle based on combined spicebush leaf according to claim 8, which is characterized in that step
The spray drying of rapid C is dried using spray drying tower, and the spray drying tower (134) includes tower body (201), the tower body
(201) side wall is connected with hot wind air intake assembly (202), and air-out component (200), tower body are connected at the top of the tower body (201)
(201) spray assembly (203), spray assembly connection high-pressure pump (211), the hot wind air intake assembly are equipped in
(202) heater (205) including air-heater (204) and connection air-heater (204), the heater (205) connection master
Blast pipe (206), main blast pipe (206) connecting side blast pipe (207), side blast pipe (207) connection tower body (201) side wall, institute
The main blast pipe (206) stated is also associated with voltage stabilizing disk (208), and the voltage stabilizing disk (208) is on spray assembly (203)
Side, the voltage stabilizing disk (208) are equipped with several steady wind outlets (209), and the steady wind exports (209) towards tower body (201)
Bottom, the spray assembly (203) include the nozzle (212) being located in tower body (201), high-pressure pump (211) connection nozzle, institute
The nozzle (212) stated is positioned at the lower section of voltage stabilizing disk (208), and the air-out component (200) is including connecting at the top of tower body (201)
Discharge pipe (215), the discharge pipe (215) connection dust suction pond (216).
10. a kind of solid according to made from production method described in any one of claim 1-9 based on combined spicebush leaf
Grain.
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Application publication date: 20180612 |