CN108130248A - A kind of preparation method of cold water soap powder - Google Patents

A kind of preparation method of cold water soap powder Download PDF

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Publication number
CN108130248A
CN108130248A CN201810108349.5A CN201810108349A CN108130248A CN 108130248 A CN108130248 A CN 108130248A CN 201810108349 A CN201810108349 A CN 201810108349A CN 108130248 A CN108130248 A CN 108130248A
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CN
China
Prior art keywords
powder
saponification
cold water
machine
puffing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810108349.5A
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Chinese (zh)
Inventor
刘京文
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhongshan Mei Lian Clean Articles Co Ltd
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Zhongshan Mei Lian Clean Articles Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zhongshan Mei Lian Clean Articles Co Ltd filed Critical Zhongshan Mei Lian Clean Articles Co Ltd
Priority to CN201810108349.5A priority Critical patent/CN108130248A/en
Publication of CN108130248A publication Critical patent/CN108130248A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D10/00Compositions of detergents, not provided for by one single preceding group
    • C11D10/04Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
    • C11D10/042Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on anionic surface-active compounds and soap

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention discloses a kind of preparation methods of cold water soap powder, are characterized in that, include the following steps:Saponification:Using several alkali solid raw materials, in saponification machine after mixing, long-chain unsaturated fatty acid is added in, be stirred to uniform, after the abundant saponification of material, add in powder urea and carry out secondary mixing, mixed to substantially uniformity after material is secondary, blowing;It is broken:The lump material that will have been cooled down, is slowly added into crusher material being broken into fine granularity;It is puffing:Dried material is put into bulking machine, and dodecyl benzene sulfonic acid is slowly added under stirring, makes powder fully puffing;The beneficial effects of the invention are as follows:Not only dirt-removing power is stronger, but also soft fabric pro-skin after washing, while also can quickly be dissolved in cold water, and soap powder is not hurt hands more mildly in use, not hot.

Description

A kind of preparation method of cold water soap powder
Technical field
The invention belongs to daily use chemicals washing technology fields, and in particular to be a kind of preparation method of cold water soap powder.
Background technology
Primary raw material soap powder in terms of daily use chemicals washing at present, and soap powder be a kind of wash, the washing that protective function combines Product has the characteristics that natural, strong decontamination, easily ultralow bubble, rinsing, its active material is mainly aliphatic acid, but needs heat Water dissolution, though and the relatively slow detergency of solution rate can be with, fabric hardens after washing, without soft pro-skin effect, and washed It is hot and hinder hand in journey;It washes rear clothing harden, is airtight, not perspiring, often people need secondary washing.
Invention content
In order to solve the above technical problems, to provide a kind of not only decontamination again submissive by the present invention, it can be under cold water state quickly Dissolving, the softness of the clothing after washing can be made, breathe freely, perspire, wear the preparation method of comfortable cold water soap powder.
To achieve the above object, the technical solution adopted by the present invention is a kind of preparation method of cold water soap powder, and technology will Point is to include the following steps:
S1. saponification:Using several alkali solid raw materials, in saponification machine after mixing, long-chain unsaturated fatty acid is added in, is stirred It mixes and mixes to uniform, after the abundant saponification of material, add in powder urea and carry out secondary mixing, treat that material is secondary and mix to completely After even, blowing;
S2. it cools down:The good material of saponification is formed into lump material after cold front heavy rain;
S3. it crushes:The lump material that will have been cooled down, is slowly added into crusher material being broken into fine granularity;
S4. it crushes:Broken material is delivered continuously to feeding hole of pulverizer, is fallen after pulverizer is ground into powder material In designated position;
S5. it dries:The material that will be crushed, is extracted into vacuum drier, with 80 DEG C of circulating water heating drying machine, in 80 DEG C of temperature Drying 1 hour is vacuumized under degree, vacuum pressure reaches -0.08MP;
S6. it is puffing:Dried material is put into bulking machine, and dodecyl benzene sulfonic acid is slowly added under stirring, makes powder abundant It is puffing;
S7. it is sieved:Puffing good powder is sieved, into the white powder of appearance uniform through being pumped into sieving machine through 8 mesh screens.
S8. it packs:Be sieved the powder completed, and stitches packet after precise, is placed on snap-gauge.
Further, the alkali solid raw material of step S1 kinds includes 7% sodium soap, 8% enuatrol, 4% sulfonic acid Sodium, 25% sodium carbonate, 1% organized enzyme, 5% emulsifier, 1.5% softening agent, 3% water softener, 20% silicate, 10% 4A zeolites.
Further, the temperature of charge being stirred in step S1 is 90-100 DEG C, and it is 30 minutes to be stirred the time.
Further, lump material after cooling passes through aging in 24 hours in step S2.
The beneficial effects of the invention are as follows:Not only dirt-removing power is stronger, but also soft fabric pro-skin after washing, while in cold water In also can quickly dissolve, and soap powder is not hurt hands more mildly in use, it is not hot.
Description of the drawings
Fig. 1 is the process flow diagram of the present invention.
Specific embodiment
Explanation that the present invention will be further explained in the following with reference to the drawings and specific embodiments, but the guarantor of the present invention is not limited Protect range.
As shown in Figure 1, first, by 7% sodium soap, 8% enuatrol, 4% sodium sulfonate, 25% sodium carbonate, 1% The alkali solids such as organized enzyme, 5% emulsifier, 1.5% softening agent, 3% water softener, 20% silicate, 10% 4A zeolites are former Material after mixing, adds in the long-chain unsaturated fatty acid of metering in saponification machine, is stirred to uniform, had been stirred Cheng Zhong, the continuous heat release of meeting when temperature of charge slowly rises to 90 DEG C in saponification machine, mix 30 minutes, treat object at this temperature Expect to add after abundant saponification powder urea and carry out secondary mixing, temperature declines during secondary mixing, and secondary mixing treats object in 10 minutes After expecting substantially uniformity, blowing;
It is fallen on the conveyor belt when then, by the good material emptying of saponification, by cold front heavy rain, lump material after cooling passes through 24 After hour aging, the lump material that will cool down is slowly added into the crusher to run at high speed, and broken material afterwards is into fine granularity After fall in elevator hopper, the boosted machine of broken material is continuously transported to after feeding hole of pulverizer material through powder Broken machine crushes powdered, and powder material is exported in pulverizer through cyclone separator, is fallen behind designated position, is taken out by pumping material machine Into vacuum drier, with 80 DEG C of circulating water heating drying machine, 1 hour dry, vacuum pressure is vacuumized at a temperature of 80 DEG C Reach -0.08MP, drying is basically completed;
Subsequently, dried material being put into the interior circulating frame for preparing material elevator, boosted machine is extracted into bulking machine, Dodecyl benzene sulfonic acid is slowly added under stirring, makes powder fully puffing, alkalinity remaining in powder can be neutralized in puffing process Substance makes soap powder not hurt hands more mildly in use, not hot, and the powder of puffing completion is put into interior preparation material carries In the circulating frame of the machine of liter, the boosted machine of puffing good powder is pumped into sieving machine, is sieved through 8 mesh screens, into appearance uniform White powder.
Finally, by the powder completed that is sieved, with the packaging bag specified, packet is stitched after precise, is placed on snap-gauge.
Another embodiment of the present invention, by 7% sodium soap, 8% enuatrol, 4% sodium sulfonate, 25% sodium carbonate, 1% organized enzyme, 5% emulsifier, 1.5% softening agent, 3% water softener, 20% silicate, 10% 4A zeolites etc. alkalinity When solid material mixes in saponification machine, hydrophilic silicone oil and nonionic consistent lubricant and moisture control agent are added, it is to be mixed equal After even, add in the long-chain unsaturated fatty acid of metering, be stirred to uniform, during being stirred, can continuous heat release, treat When temperature of charge slowly rises to 100 DEG C in saponification machine, mix 30 minutes, added after the abundant saponification of material at this temperature Powder urea carries out secondary mixing, and temperature declines during secondary mixing, 10 minutes blowings after material substantially uniformity of secondary mixing.
It is obvious to a person skilled in the art that the present invention is not limited to the details of above-mentioned exemplary embodiment, Er Qie In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power Profit requirement rather than above description limit, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims Variation is included within the present invention, and any reference numeral in claim should not be considered as to the involved claim of limitation.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should It considers the specification as a whole, the technical solutions in each embodiment can also be properly combined, forms those skilled in the art The other embodiment being appreciated that.

Claims (4)

1. a kind of preparation method of cold water soap powder, which is characterized in that include the following steps:
S1. saponification:Using several alkali solid raw materials, in saponification machine after mixing, long-chain unsaturated fatty acid is added in, is stirred It mixes and mixes to uniform, after the abundant saponification of material, add in powder urea and carry out secondary mixing, treat that material is secondary and mix to completely Blowing after even;
S2. it cools down:The good material of saponification is formed into lump material after cold front heavy rain;
S3. it crushes:The lump material that will have been cooled down, is slowly added into crusher material being broken into fine granularity;
S4. it crushes:Broken material is delivered continuously to feeding hole of pulverizer, is fallen after pulverizer is ground into powder material In designated position;
S5. it dries:The material that will be crushed, is extracted into vacuum drier, with 80 DEG C of circulating water heating drying machine, in 80 DEG C of temperature Drying 1 hour is vacuumized under degree, vacuum pressure reaches -0.08MP;
S6. it is puffing:Dried material is put into bulking machine, and dodecyl benzene sulfonic acid is slowly added under stirring, makes powder abundant It is puffing;
S7. it is sieved:Puffing good powder is sieved, into the white powder of appearance uniform through being pumped into sieving machine through 8 mesh screens;
S8. it packs:Be sieved the powder completed, and stitches packet after precise, is placed on snap-gauge.
2. a kind of preparation method of cold water soap powder according to claim 1, it is characterised in that:The alkali of the step S1 kinds Property solid material includes 7% sodium soap, 8% enuatrol, 4% sodium sulfonate, 25% sodium carbonate, 1% organized enzyme, 5% Emulsifier, 1.5% softening agent, 3% water softener, 20% silicate, 10% 4A zeolites.
3. a kind of preparation method of cold water soap powder according to claim 1, it is characterised in that:It is stirred in the step S1 The temperature of charge of mixing is 90-100 DEG C, and it is 30 minutes to be stirred the time.
4. a kind of preparation method of cold water soap powder according to claim 1, it is characterised in that:It is cooled down in the step S2 Lump material afterwards passes through aging in 24 hours.
CN201810108349.5A 2018-02-02 2018-02-02 A kind of preparation method of cold water soap powder Pending CN108130248A (en)

Priority Applications (1)

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CN201810108349.5A CN108130248A (en) 2018-02-02 2018-02-02 A kind of preparation method of cold water soap powder

Publications (1)

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CN108130248A true CN108130248A (en) 2018-06-08

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109112020A (en) * 2018-10-17 2019-01-01 广州立白企业集团有限公司 A kind of instant soap flakes and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1101937A (en) * 1994-06-16 1995-04-26 赵勇 Neutral soap powder and producing process thereof
CN1135523A (en) * 1996-02-06 1996-11-13 赵勇 Concentrated spaonin powder and production method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1101937A (en) * 1994-06-16 1995-04-26 赵勇 Neutral soap powder and producing process thereof
CN1135523A (en) * 1996-02-06 1996-11-13 赵勇 Concentrated spaonin powder and production method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109112020A (en) * 2018-10-17 2019-01-01 广州立白企业集团有限公司 A kind of instant soap flakes and preparation method thereof
CN109112020B (en) * 2018-10-17 2020-12-22 广州立白企业集团有限公司 Instant soap flakes and preparation method thereof

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Application publication date: 20180608

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