CN108126645A - A kind of reaction kettle of good antiscale property, the sufficient successive reaction of mixing - Google Patents

A kind of reaction kettle of good antiscale property, the sufficient successive reaction of mixing Download PDF

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Publication number
CN108126645A
CN108126645A CN201810096961.5A CN201810096961A CN108126645A CN 108126645 A CN108126645 A CN 108126645A CN 201810096961 A CN201810096961 A CN 201810096961A CN 108126645 A CN108126645 A CN 108126645A
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CN
China
Prior art keywords
reaction kettle
leaf
reaction
kettle
mixing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810096961.5A
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Chinese (zh)
Inventor
柏兆钰
汪根钟
洪文辉
王丽霞
吴夫根
景志华
吴立新
汝萍
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Danyang Is With Safe Chemical Machinery Co Ltd
Original Assignee
Danyang Is With Safe Chemical Machinery Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Danyang Is With Safe Chemical Machinery Co Ltd filed Critical Danyang Is With Safe Chemical Machinery Co Ltd
Priority to CN201810096961.5A priority Critical patent/CN108126645A/en
Publication of CN108126645A publication Critical patent/CN108126645A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/0013Controlling the temperature of the process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/002Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00054Controlling or regulating the heat exchange system
    • B01J2219/00056Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00058Temperature measurement
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00054Controlling or regulating the heat exchange system
    • B01J2219/00056Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00058Temperature measurement
    • B01J2219/00063Temperature measurement of the reactants
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/0009Coils

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)

Abstract

The invention discloses a kind of good antiscale properties, mix the reaction kettle of sufficient successive reaction, the present invention is by changing the feeding manner of material, using tangential feed, and branch is in two orientation of reactor, reaction kettle wall is continuously rinsed with heating tube, feeding temperature is minimum, it can directly be contacted again with heating surface, improve heating effect, material in reactor temperature is made to be more nearly the temperature of reaction, improve reaction efficiency, it is combined using the paddle of various ways, material is made not move in a certain way in a kettle, material is made to form disordered motion, reduce centrifugal action, make particle or the big material of gravity reduces Long Term Contact with heating surface, and avoid the fouling of material;Mixing is more abundant simultaneously, improves the efficiency of reaction, and using the equipment of the present invention, fouling reduces more than 90%, and accurately controlling for temperature and being uniformly mixed for material, reactivity improves 5%.

Description

A kind of reaction kettle of good antiscale property, the sufficient successive reaction of mixing
Technical field
The present invention relates to the reaction kettles of a kind of good antiscale property, the sufficient successive reaction of mixing, belong to reaction kettle equipment and technology neck Domain.
Background technology
Currently used reaction kettle agitating mode is vane type, paddle formula;In the case of Stirring, material turns over up and down It moves and under the action of the centrifugal force, material will appear centrifugation, and the appearance for making gravity big is centrifuged closer to reaction kettle wall;It is and anti- Answering kettle is heated by reaction kettle wall or by the inner coil pipe of stomach wall, and the big material of such gravity easily contacts high temperature for a long time Heating surface.When particularly liquid is reacted with granular material and in the case of the easy fouling of material that gravity is big, reaction kettle is more Easy fouling, due to the shortcomings that mixing is uneven, and reaction effect is poor, and yield is low.
For the present invention in view of the above problems, providing the reaction kettle of a kind of good antiscale property, the sufficient successive reaction of mixing, realization is automatic Good antiscale property, and cause reaction kettle in material be more fully mixed.
Invention content
To achieve the above object, the present invention provides following technical solution:A kind of good antiscale property mixes sufficient successive reaction Reaction kettle including reaction kettle ontology, heating tube assembly, feeding assembly and stirs leaf component, on the outside of the reaction kettle ontology End, which is provided with, stirs leaf drive component, and the output terminal for stirring leaf drive component stretches into be stirred described in the reaction kettle body interior driving Leaf component rotates, and the heating tube assembly winding is in the inside of the reaction kettle ontology, which is characterized in that
The feeding assembly is arranged by the way of tangential feed, and the feeding assembly is distributed in two sides of reaction kettle Position, continuously to be rinsed to the inner wall of reaction kettle ontology and heating tube assembly, the leaf component that stirs includes a variety of agitations What mode was stirred stirs leaf group, so that material is made to form disordered motion in a kettle, reduces centrifugal action.
Further, preferably, it is described stir leaf group include above stir leaf, leaf is stirred in centre and under stir leaf;
Wherein, leaf is stirred on described and is arranged on the upper end for stirring rachis, and it is described on stir the shape and structure structure of leaf and be set as so that material exists Movement is advanced downwardly in stirring;
The centre stirs leaf and is arranged on the middle and lower part for stirring rachis, and the centre is stirred the shape and structure structure of leaf and is set as so that material exists It boosts in stirring movement;
Leaf is stirred under described and is arranged on the lower end of stirring rachis and positioned at bottom in the reaction kettle, and it is described under stir the shape and structure of leaf Structure is set as the movement so that material is boosted in stirring.
Further, preferably, the feeding assembly includes feed distributor flange one, feed distributor flange two and connects Guide pipe is connect, the distributor flange one, feed distributor flange two are symmetrically arranged at the both upper ends thereof of the reaction kettle, Respective feed distributor, the feed distributor are all connected on the feed distributor flange one and feed distributor flange two On be provided with charging hole, the feed distributor flange one, feed distributor flange two stretch into the side setting of reaction kettle inner wall There is the connection guide pipe of curved bend head.
Further, it is described to stir leaf electricity preferably, the leaf drive component that stirs includes stirring leaf motor, stent and retarder Machine is fixed on the reaction kettle upper end using the stent, and the output terminal for stirring leaf motor connects the retarder, described to subtract Rachis is stirred described in the output terminal connection of fast device.
Further, preferably, the material outlet pressure of the charging hole is 4kg/cm2, and the material of charging hole enters Cause material and pipe, 45 degree of the angle of kettle wall during reaction kettle.
Further, preferably, the heating tube assembly is using steam-heating pipe, the upper end of the reaction kettle be provided with The steam inlet flange of steam-heating pipe connection, the lower end of the reaction kettle be provided with connect with steam-heating pipe it is hydrophobic Outlet(discharge) flange.
Further, preferably, the output terminal of the retarder by shaft coupling connect described in stir rachis.
Further, preferably, the heating tube of the heating tube assembly is arranged in the reaction kettle by the way of spiral It is internal.
Compared with prior art, the beneficial effects of the invention are as follows:
(1)The design of feeding assembly:The present invention specially devises reaction kettle feeding assembly, by changing the feeding manner of material, Using tangential feed, and branch is continuously rinsed reaction kettle wall with heating tube, into material temperature in two orientation of reactor It spends minimum, and can directly be contacted with heating surface, improve heating effect, material in reactor temperature is made to be more nearly reaction Temperature improves reaction efficiency.
(2)The design of paddle;The present invention is combined using the paddles of various ways, does not make material in a kettle not It moves in a certain way, material is made to form disordered motion;Reduce centrifugal action, make particle or the big material of gravity reduce and plus The Long Term Contact in hot face, and avoid the fouling of material;Mixing is more abundant simultaneously;Improve the efficiency of reaction.
(3)By the present invention in that with the temperature of each position in detection reaction kettle, the temperature of Temperature Difference Ratio routine successive reaction kettle Difference reduces more than 60%, and the temperature of reaction is more prone to control, and improves the efficiency of reaction.
(4)Fouling condition:The present invention reaction kettle can use in multiple industries, especially for glycerine, biodiesel, The original reactors such as DOP need to clean weekly once, and the present invention can solve the problems, such as that this needs often cleans.
(5)It was verified that using the equipment of the present invention, fouling reduces more than 90%.
(6)The accurately controlling for temperature of reaction kettle and being uniformly mixed for material, reactivity of the present invention can at least improve 5%。
Description of the drawings
Fig. 1 be a kind of good antiscale property of the present invention, the sufficient successive reaction of mixing reaction kettle overall structure diagram;
Fig. 2 be a kind of good antiscale property of the present invention, the sufficient successive reaction of mixing reaction kettle feed distributor structure diagram;
Wherein, 1, stir leaf motor, 2, stent, 3, retarder, 4, reaction kettle ontology, 5, stir rachis, 6, on stir leaf, 7, centre stirs Leaf, 8, under stir leaf, 9, steam inlet flange, 10, hydrophobic outlet(discharge) flange, 11, feed distributor flange one, 12, feed distributor Flange two, 13, connection guide pipe, 14, shaft coupling, 15, feed distributor, 16, charging hole.
Specific embodiment
Below in conjunction with the attached drawing in the embodiment of the present invention, the technical solution in the embodiment of the present invention is carried out clear, complete Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, those of ordinary skill in the art are obtained every other without making creative work Embodiment shall fall within the protection scope of the present invention.
- 2 are please referred to Fig.1, the present invention provides a kind of technical solution:A kind of good antiscale property mixes the anti-of sufficient successive reaction Kettle is answered, including reaction kettle ontology 4, heating tube assembly, feeding assembly and stirs leaf component, the outer upper ends of the reaction kettle ontology It is provided with and stirs leaf drive component, the output terminal for stirring leaf drive component stretches into and stirs leaf described in the reaction kettle body interior driving Component rotates, and the heating tube assembly winding uses tangential feed in the inside of the reaction kettle ontology, the feeding assembly Mode is arranged, and the feeding assembly is distributed in two orientation of reaction kettle, so that the inner wall to reaction kettle ontology is with adding Heat pipe assembly is continuously rinsed, and the leaf component that stirs stirs leaf group including what a variety of agitation modes were stirred, to make object Material forms disordered motion in a kettle, reduces centrifugal action.
In the present embodiment, as a kind of preferable Combination Design waterproof of paddle group, the leaf group of stirring includes above stirring Leaf 6, centre stir leaf 7 and under stir leaf 8;Wherein, leaf 6 is stirred on described and is arranged on the upper end for stirring rachis 5, and it is described on stir the shape of leaf 6 Shape structure structure is set as so that material advances downwardly movement in stirring;The centre stirs leaf 7 and is arranged on the middle and lower part for stirring rachis, and The shape and structure structure that leaf 7 is stirred in the centre is set as the movement so that material is boosted in stirring;It leaf 8 is stirred under described is arranged on and stir The lower end of rachis 5 and the bottom in the reaction kettle, and it is described under stir the shape and structure structure of leaf 8 and be set as so that material is stirring In boost movement.For the type of drive of paddle, in the present embodiment, the leaf drive component that stirs includes stirring leaf motor 1st, stent 2 and retarder 3, the leaf motor 1 that stirs is fixed on the reaction kettle upper end using the stent 2, described to stir leaf motor 1 Output terminal connect the retarder 3, the output terminal of the retarder 3 using shaft coupling 14 connect described in stir rachis 5.
As more preferably embodiment, as shown in Figure 1, the feeding assembly includes feed distributor flange 1, charging point Cloth device flange 2 12 and connection guide pipe 13, the distributor flange 1, feed distributor flange 2 12 are symmetrically arranged It is all connected in the both upper ends thereof of the reaction kettle, the feed distributor flange 1 and feed distributor flange 2 12 respectively Feed distributor 15, be provided with charging hole 16, the feed distributor flange one, feed distributor on the feed distributor The side that flange two stretches into reaction kettle inner wall is provided with the connection guide pipe 13 of curved bend head.
Wherein, by long-term experiment with it was verified that as best feed pressure, the material outlet of the charging hole Pressure is 4kg/cm2, and the material of charging hole when entering reaction kettle so that material and pipe, 45 degree of the angle of kettle wall.
As shown in Figure 1, in the present embodiment, using steam-heating pipe, the upper end of the reaction kettle is set the heating tube assembly The steam inlet flange 9 being connect with the steam-heating pipe is equipped with, the lower end of the reaction kettle is provided with to be connected with steam-heating pipe The hydrophobic outlet(discharge) flange 10 connect.In order to ensure heating uniformity, the heating tube for heating tube assembly cloth by the way of spiral It puts inside the reaction kettle.
The present invention is by changing the feeding manner of material, and using tangential feed, and branch is in two orientation of reactor, right Reaction kettle wall is continuously rinsed with heating tube, and feeding temperature is minimum, and can directly be contacted with heating surface, improves heating Effect makes material in reactor temperature be more nearly the temperature of reaction, improves reaction efficiency.The present invention is by using a variety of sides The paddle of formula is combined, and material is made not move in a certain way in a kettle, and material is made to form disordered motion;It reduces Centrifugal action, makes particle or the big material of gravity reduces Long Term Contact with heating surface, and avoids the fouling of material;It mixes simultaneously More fully;Improve the efficiency of reaction.
By using the temperature of each position in detection reaction kettle, the temperature difference of Temperature Difference Ratio routine successive reaction kettle reduces More than 60%;The temperature of reaction is more prone to control, and improves the efficiency of reaction, and using the equipment of the present invention, fouling reduces More than 90%, accurately controlling for temperature and being uniformly mixed for material, reactivity improves 5%.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace And modification, the scope of the present invention is defined by the appended.

Claims (8)

1. a kind of reaction kettle of good antiscale property, the sufficient successive reaction of mixing, including reaction kettle ontology, heating tube assembly, charging Component and leaf component is stirred, the outer upper ends of the reaction kettle ontology, which are provided with, stirs leaf drive component, the leaf drive component that stirs Output terminal stretches into and the rotation of leaf component is stirred described in the reaction kettle body interior driving, and the heating tube assembly winding is in the reaction The inside of kettle ontology, which is characterized in that
The feeding assembly is arranged by the way of tangential feed, and the feeding assembly is distributed in two sides of reaction kettle Position, continuously to be rinsed to the inner wall of reaction kettle ontology and heating tube assembly, the leaf component that stirs includes a variety of agitations What mode was stirred stirs leaf group, so that material is made to form disordered motion in a kettle, reduces centrifugal action.
2. the reaction kettle of a kind of good antiscale property according to claim 1, the sufficient successive reaction of mixing, it is characterised in that:Institute State stir leaf group include above stir leaf, leaf is stirred in centre and under stir leaf;
Wherein, leaf is stirred on described and is arranged on the upper end for stirring rachis, and it is described on stir the shape and structure structure of leaf and be set as so that material exists Movement is advanced downwardly in stirring;
The centre stirs leaf and is arranged on the middle and lower part for stirring rachis, and the centre is stirred the shape and structure structure of leaf and is set as so that material exists It boosts in stirring movement;
Leaf is stirred under described and is arranged on the lower end of stirring rachis and positioned at bottom in the reaction kettle, and it is described under stir the shape and structure of leaf Structure is set as the movement so that material is boosted in stirring.
3. the reaction kettle of a kind of good antiscale property according to claim 1, the sufficient successive reaction of mixing, it is characterised in that:Institute Feeding assembly is stated to include feed distributor flange one, feed distributor flange two and connect guide pipe, the distributor flange one, Feed distributor flange two is symmetrically arranged at the both upper ends thereof of the reaction kettle, the feed distributor flange one and charging Respective feed distributor is all connected on distributor flange two, charging hole, the charging point are provided on the feed distributor The side that cloth device flange one, feed distributor flange two stretch into reaction kettle inner wall is provided with the connection guide pipe of curved bend head.
4. the reaction kettle of a kind of good antiscale property according to claim 2, the sufficient successive reaction of mixing, it is characterised in that:Institute State and stir leaf drive component and include stirring leaf motor, stent and retarder, it is described stir leaf motor using the stent be fixed on it is described instead Kettle upper end is answered, the output terminal for stirring leaf motor connects the retarder, rachis is stirred described in the output terminal connection of the retarder.
5. the reaction kettle of a kind of good antiscale property according to claim 3, the sufficient successive reaction of mixing, it is characterised in that:Institute The material outlet pressure of charging hole is stated as 4kg/cm2, and when material of charging hole enters reaction kettle causes material and pipe, kettle wall 45 degree of angle.
6. the reaction kettle of a kind of good antiscale property according to claim 1, the sufficient successive reaction of mixing, it is characterised in that:Institute Heating tube assembly is stated using steam-heating pipe, the upper end of the reaction kettle be provided with the steam that the steam-heating pipe is connect into Mouth flange, the lower end of the reaction kettle is provided with the hydrophobic outlet(discharge) flange being connect with steam-heating pipe.
7. the reaction kettle of a kind of good antiscale property according to claim 4, the sufficient successive reaction of mixing, it is characterised in that:Institute State the output terminal of retarder by shaft coupling connect described in stir rachis.
8. the reaction kettle of a kind of good antiscale property, the sufficient successive reaction of mixing according to claim 1-7 any one, special Sign is:The heating tube of the heating tube assembly is arranged in by the way of spiral inside the reaction kettle.
CN201810096961.5A 2018-01-31 2018-01-31 A kind of reaction kettle of good antiscale property, the sufficient successive reaction of mixing Pending CN108126645A (en)

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Application Number Priority Date Filing Date Title
CN201810096961.5A CN108126645A (en) 2018-01-31 2018-01-31 A kind of reaction kettle of good antiscale property, the sufficient successive reaction of mixing

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Application Number Priority Date Filing Date Title
CN201810096961.5A CN108126645A (en) 2018-01-31 2018-01-31 A kind of reaction kettle of good antiscale property, the sufficient successive reaction of mixing

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112969528A (en) * 2018-11-14 2021-06-15 巴斯夫欧洲公司 Process for producing superabsorbers

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101890327A (en) * 2010-08-09 2010-11-24 朱荣 Preparation method of distributor of reaction tank nozzle
US20110178254A1 (en) * 2008-09-18 2011-07-21 Toyo Engineering Corporation Apparatus for manufacturing polymer resin, polymerization vessel, and method for manufacturing polymer resin
CN202683196U (en) * 2012-06-27 2013-01-23 安庆市中天石油化工有限公司 Reaction kettle with feeding system for scouring
CN206652498U (en) * 2017-04-21 2017-11-21 青海快驴电动汽车科技有限公司 A kind of reactor for being used to prepare micron order threadiness nickel oxalate
CN207981172U (en) * 2018-01-31 2018-10-19 丹阳同泰化工机械有限公司 A kind of reaction kettle of good antiscale property, the sufficient successive reaction of mixing

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20110178254A1 (en) * 2008-09-18 2011-07-21 Toyo Engineering Corporation Apparatus for manufacturing polymer resin, polymerization vessel, and method for manufacturing polymer resin
CN101890327A (en) * 2010-08-09 2010-11-24 朱荣 Preparation method of distributor of reaction tank nozzle
CN202683196U (en) * 2012-06-27 2013-01-23 安庆市中天石油化工有限公司 Reaction kettle with feeding system for scouring
CN206652498U (en) * 2017-04-21 2017-11-21 青海快驴电动汽车科技有限公司 A kind of reactor for being used to prepare micron order threadiness nickel oxalate
CN207981172U (en) * 2018-01-31 2018-10-19 丹阳同泰化工机械有限公司 A kind of reaction kettle of good antiscale property, the sufficient successive reaction of mixing

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112969528A (en) * 2018-11-14 2021-06-15 巴斯夫欧洲公司 Process for producing superabsorbers

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