CN108124993A - A kind of pure folium cortex eucommiae Fu-brick tea oral liquid and preparation method thereof - Google Patents
A kind of pure folium cortex eucommiae Fu-brick tea oral liquid and preparation method thereof Download PDFInfo
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- CN108124993A CN108124993A CN201810006860.4A CN201810006860A CN108124993A CN 108124993 A CN108124993 A CN 108124993A CN 201810006860 A CN201810006860 A CN 201810006860A CN 108124993 A CN108124993 A CN 108124993A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/06—Treating tea before extraction; Preparations produced thereby
- A23F3/14—Tea preparations, e.g. using additives
Abstract
The invention discloses a kind of pure folium cortex eucommiae Fu-brick tea oral liquids and preparation method thereof, after folium cortex eucommiae decatize, pile fermentation, are inoculated with the coronoid process dissipate capsule bacterium spore manually cultivated, then after being molded and floating is dried, folium cortex eucommiae Fu-brick tea is prepared；Folium cortex eucommiae Fu-brick tea is extracted by water logging, vacuum concentration, vacuum spray drying, obtained soluble concrete powder, it is filling to obtain pure folium cortex eucommiae Fu brick oral liquids after mixed accessories and water, and after homogeneous, sterilizing.Pure folium cortex eucommiae oral liquid prepared by the present invention, raw material is pure folium cortex eucommiae, it is fragrant with the distinctive faint scent of folium cortex eucommiae Fu-brick tea kneading folium cortex eucommiae and coronoid process dissipate capsule bacterium bacterium, Cortex Eucommiae peculiar fragrance is pure, alcohol and tempting, there is fatigue-relieving, improve the immunity of the human body, while be also the health beverages of a breeding taste.
Description
Technical field
The invention belongs to tea processing field, and in particular to a kind of method that Fu-brick tea oral liquid is prepared using folium cortex eucommiae.
Background technology
Fu-brick tea category black tea, also referred to as fermented tea first ancestor have aid digestion weight-reducing and supplement each biostearin, trace element
Deng.First piece of Fu-brick tea, which is recorded, according to history records is born in Xianyang Jingyang County.The Fu-brick tea produced at present, shape brick face is smooth,
Corner angle are clearly demarcated, and thickness is consistent, and floating is generally luxuriant, and Fu brick teas face is dark brown or yellowish-brown.During bubble drink, it is desirable that Tang Hong is not turbid,
Fragrant clear not thick, rich not puckery, mouth strength is strong, endures repeated infusions, and specially requires that coronoid process dissipate capsule bacterium in brick is generally luxuriant, it is dry smell have it is colored clear
It is fragrant.With this coronoid process dissipate capsule bacterium classes of golden flower Fu tea bubble drink when, the fragrance of a flower can be incorporated among millet paste, be turned into tea flavour and more
Mellow micro-puckery, it is pure it is not thick, mouthfeel is powerful.In addition golden flower can also be effectively facilitated adjusting metabolism, reducing blood lipid, conditioning intestines
Stomach plays health care and pathology prevention effect.
Contain lactones, coumarin, alkaloid, polysaccharide, reduced sugar, organic acid, protein, amino acid and Cortex Eucommiae in folium cortex eucommiae
The ingredients such as glue, wherein active ingredient have：Pinoresinol diglucoside, Aucubin, chlorogenic acid, gutta-percha, ajugoside, Du
Secondary glucoside, Kaempferol, caffeic acid, tartaric acid, reduced sugar, chromocor compound, alkaloid etc., have blood pressure lowering, weight-reducing, anti-aging,
Filling liver kidney and other effects.There are Eucommia Tea and series beverage now on the market at present, wherein Eucommia Tea is finished using conventional green tea
Stir-frying technique is made, and is the problem of industry is applied：Folium cortex eucommiae has careless fishy smell, bitter taste and astringent taste in itself so that existing
Some Eucommia Teas and the drink that is prepared according to folium cortex eucommiae the generally existing grass fishy smell in mouthfeel the defects of, limit Eucommia Tea with
And the popularization and application of related folium cortex eucommiae beverage Industry.And at present generally use in folium cortex eucommiae process add in ozone or its
His chemical substance is made a return journey the method for weeding fishy smell, ineffective and complex process, of high cost, is limited it and is widely applied.
Invention content
The purpose of the present invention is to provide a kind of folium cortex eucommiae Fu brick speed oral liquids and preparation method thereof prepared by folium cortex eucommiae,
Any tea component is not added in raw material, but the technique processing folium cortex eucommiae that Fu-brick tea is used to prepare, become the outer of brick tea
Shape, while by Fu tea zymotechniques, eliminate the original astringent taste of folium cortex eucommiae and bitter taste, finally prepare and obtain folium cortex eucommiae Fu-brick tea
Oral liquid so that mouthfeel is better than common Cortex Eucommiae drink.
The technical solution adopted by the present invention is as follows：
A kind of pure folium cortex eucommiae Fu-brick tea oral liquor, it is characterised in that：Using the coronoid process dissipate capsule bacterium manually cultivated
Bacteria suspension is made in conidia powder；Cortex Eucommiae culture solution will be obtained after folium cortex eucommiae water logging, according to ratio from less to more, gradually added in institute
In the bacteria suspension stated, coronoid process dissipate capsule bacterium is carried out after gradually taming, folium cortex eucommiae Fu-brick tea inoculation liquid is prepared, is seeded to Cortex Eucommiae
In leaf Fu-brick tea embryo material；With after floating drying, folium cortex eucommiae Fu-brick tea is prepared, by Cortex Eucommiae in repressed molding to Fu-brick tea embryo material again
Soluble concrete powder, mixing beta-cyclodextrin, sorb is made by water logging extraction, vacuum concentration, vacuum spray drying in leaf Fu-brick tea
After sugar alcohol and candy sugar powder and water, and after homogeneous, sterilizing, pure folium cortex eucommiae Fu bricks are prepared according to oral liquid preparing process and take orally
Liquid.
In a kind of above-mentioned pure folium cortex eucommiae Fu-brick tea oral liquor, the preparation method of folium cortex eucommiae Fu-brick tea is including following
Step：
【2.1】The preparation of Cortex Eucommiae culture solution
Cortex Eucommiae culture solution is prepared by nutritional agents is added in after fresh folium cortex eucommiae or Folium Eucommiae water logging, gives over to spare；
【2.2】Coronoid process dissipate capsule bacterium obtains
The appropriate coronoid process dissipate capsule bacterium conidia powder manually cultivated is taken, is put into the aseptic bottle containing sterile water, bacterium is made
Suspension is for use；
【2.3】Coronoid process dissipate capsule bacterium is tamed
To step【2.2】Bacteria suspension according to ratio from less to more, gradually add in step【2.1】Cortex Eucommiae culture
Liquid after often adding in a Cortex Eucommiae culture solution, is cultivated 2-5 days at 25-30 DEG C, carries out coronoid process dissipate capsule bacterium domestication；
【2.4】The preparation of folium cortex eucommiae Fu-brick tea inoculation liquid
By step【2.3】The base fluid containing bacteria suspension and Cortex Eucommiae culture solution after domestication is placed in shake in shaking table and trains
It supports, cultivation temperature is 28 DEG C -30 DEG C, cultivates 15-20 days, obtains final Cortex Eucommiae Fu tea bacterium solutions, prepares and gives birth to as Cortex Eucommiae Fu tea
Inoculation liquid in production；
【2.5】Folium cortex eucommiae decatize and pile fermentation
By fresh folium cortex eucommiae high temperature steaming or Folium Eucommiae raw material water spray after high temperature steaming, steam temperature for 100 DEG C-
120 DEG C, when decatize, is 1-5 minutes a length of, carries out concentration accumulation, pile fermentation time 3.5-5 hours, temperature in heap after decatize immediately
Control is at 75 DEG C -80 DEG C；
【2.6】The preparation of folium cortex eucommiae Fu-brick tea embryo material
Folium cortex eucommiae after pile fermentation is added into step【2.1】Cortex Eucommiae culture solution so that Cortex Eucommiae leaf water content 20%-40% it
Between, after stirring again by steam engine carry out decatize softening, 100 DEG C -107 DEG C of steam temperature, time 5-10 second, and
Folium cortex eucommiae Fu-brick tea embryo material is made；
【2.7】It is inoculated with coronoid process dissipate capsule bacterium spore
The folium cortex eucommiae mixing embryo material that high temperature steaming softened will be again passed by uniformly to spread out, cooled to room temperature, sprinkling
Step【2.4】Inoculation liquid, be then pressed into brick；
【2.8】Floating is dried
Folium cortex eucommiae brick is sent into drying chamber, controls its temperature and humidity, carries out floating；Floating is finished after aeration-drying to obtain the final product
To folium cortex eucommiae Fu-brick tea finished product.
In a kind of above-mentioned pure folium cortex eucommiae Fu-brick tea oral liquor, step【2.1】In nutritional agents for NaCl,
NH4NO3, sucrose, MgSO4、K2HPO4, according to NaCl:NH4NO3:Sucrose:MgSO4:K2HPO4:Water is 32:33:20:40:41:
1000 weight ratio mixed configuration.
In a kind of above-mentioned pure folium cortex eucommiae Fu-brick tea oral liquor, step【2.3】In coronoid process dissipate capsule bacterium domestication, for the first time
The Cortex Eucommiae culture solution of addition is 0.05-0.1 times of bacteria suspension volume, and the Cortex Eucommiae culture solution that last time adds in is bacteria suspension volume
10-50 times, centre addition number be 3-10 times.
In a kind of above-mentioned pure folium cortex eucommiae Fu-brick tea oral liquor, step【2.8】Middle floating drying steps are：
First, floating 7-10 days under the conditions of 25-35 DEG C, humidity 65-85%；
2nd, floating 3-4 days under the conditions of 30-35 DEG C, humidity 45-65%；
3rd, it dry 5-6 days or naturally dries to folium cortex eucommiae Fu-brick tea water content at 35-50 DEG C and reaches 10-14%, as
Finished product folium cortex eucommiae Fu-brick tea.
In a kind of above-mentioned pure folium cortex eucommiae Fu-brick tea oral liquor, the folium cortex eucommiae Fu-brick tea using deionized water into
Row water logging is extracted, and folium cortex eucommiae Fu-brick tea is 1 according to mass ratio with water:10~20 mixing, are rapidly heated to 100 DEG C, drop after five minutes
To 70~85 DEG C, constant temperature 1 hour.
In a kind of above-mentioned pure folium cortex eucommiae Fu-brick tea oral liquor, during the vacuum concentration vacuum degree for 0.05~
0.1MPa, the temperature of vacuum concentration is 45~60 DEG C.
In a kind of above-mentioned pure folium cortex eucommiae Fu-brick tea oral liquor, vacuum degree during vacuum spray drying for 0.06~
0.09MPa, 10~30min of drying time.
In a kind of above-mentioned pure folium cortex eucommiae Fu-brick tea oral liquor, auxiliary material is beta-cyclodextrin, D-sorbite and rock sugar
Powder, mixing weight ratio are extract powder：Beta-cyclodextrin：D-sorbite：Candy sugar powder=6~10：20~25：0.3~0.45：30~
45。
A kind of pure folium cortex eucommiae Fu-brick tea oral liquid, is prepared according to the method described above.
The advantageous effects that the present invention has are as follows：
1st, pure folium cortex eucommiae Fu-brick tea oral liquid quality prepared by the present invention has individual style, folium cortex eucommiae Fu-brick tea kneading Du
The distinctive faint scent of Zhong Ye and coronoid process dissipate capsule bacterium bacterium are fragrant, it is instant after color and luster it is reddish brown it is bright, Cortex Eucommiae peculiar fragrance is pure, alcohol and tempting,
There is fatigue-relieving, improve the immunity of the human body, while be also the health-care tea beverage of a breeding taste.
2nd, pure folium cortex eucommiae Fu-brick tea oral liquid of the invention does not contain any tea component, but is pressed using pure Folium Eucommiae
It is prepared according to Fu tea techniques, using technological processes such as decatize, pile fermentation, floatings, has effectively removed bitter taste, the astringent taste of folium cortex eucommiae
With careless fishy smell, the mouthfeel of Eucommia Tea and drink is improved, simultaneously because the coronoid process dissipate capsule bacterium spore employed in Fu tea techniques connects
Kind, more add the aid digestion and weight losing function that Fu-brick tea has.
3rd, the present invention is in the preparation of folium cortex eucommiae Fu-brick tea, using in the bacteria suspension to coronoid process dissipate capsule bacterium, by low concentration to high
Concentration is gradually added into the scheme of Cortex Eucommiae culture solution, realizes the domestication culture of coronoid process dissipate capsule bacterium.Since coronoid process dissipate capsule bacterium is growth
It is made to generate the strain of golden flower made of conventional tealeaves on Fu-brick tea, and the folium cortex eucommiae Fu tea of the present invention is pressed using pure folium cortex eucommiae
It is prepared according to the technique of Fu tea, itself is simultaneously free of any tealeaves composition.It is well known that self-contained chlorogenic acid of folium cortex eucommiae etc.
Antibacterial medicinal component can inhibit the growth of coronoid process dissipate capsule bacterium spore, therefore in order to enable coronoid process dissipate capsule bacterium can be numerous in folium cortex eucommiae
It grows, therefore employs the process for gradually cultivating domestication, according to being gradually added into the culture solution containing Cortex Eucommiae in bacteria suspension so that coronoid process
Bulk bacteria gradually adapt to the environment of Cortex Eucommiae culture solution, finally realize common coronoid process dissipate capsule bacterium spore in pure folium cortex eucommiae Fu-brick tea
On culture and maturation, and floating is luxuriant.
4th, fresh leaf not only may be used as raw material in folium cortex eucommiae Fu-brick tea and its beverage of the invention, can also use
Prepared by veteran leaf, improve raw material sources.
Specific embodiment
To make the objectives, technical solutions, and advantages of the present invention clearer, the present invention is done with reference to embodiment
It is further to be described in detail.Here, the illustrative embodiments of the present invention and their descriptions are used to explain the present invention, but it is not intended as pair
The restriction of the present invention.
Embodiment 1
A kind of preparation method of pure folium cortex eucommiae Fu-brick tea oral liquid of the present invention, includes the following steps：
(1) acquisition of folium cortex eucommiae
Pick the folium cortex eucommiae of the annual 7-10 months, natural air drying dries or drying system drying, and water content is 10%, drying
Temperature be 65 DEG C, put with Polywoven Bag be placed in it is spare at aeration-drying.
(2) preliminary treatment of folium cortex eucommiae
Folium cortex eucommiae is cleaned up, with cutter be divided into the directly upper round as a ball screening and choosing impurity elimination of slice or whole leaf to get
Cortex Eucommiae leaf raw material.
(3) preparation of Cortex Eucommiae culture solution
The smalls folium cortex eucommiae that sieve round as a ball in step (2) leaks down is leached into Cortex Eucommiae juice, is added according to per kilogram Folium Eucommiae
20 kilograms of water is obtained in 70-100 DEG C of leaching of water temperature.NaCl, NH are added in leaching liquid4NO3, sucrose, MgSO4、K2HPO4Make
For nutritional agents, and according to NaCl:NH4NO3:Sucrose:MgSO4:K2HPO4:Water is 32:33:20:40:41:1000 weight ratio is mixed
Configuration is closed, Cortex Eucommiae culture solution is made, is given over to follow-up spare.
(4) coronoid process dissipate capsule bacterium obtains
Good coronoid process dissipate capsule bacterium conidia powder is bought on the market, is taken and is put into the aseptic bottle containing sterile water in right amount
In, it is for use that bacteria suspension is made.
(5) coronoid process dissipate capsule bacterium is tamed
In the bacteria suspension of step (4), according to ratio from less to more, the Cortex Eucommiae culture solution of step (3) is gradually added in, according to
The secondary volume ratio according to opportunistic pathogen suspension and Cortex Eucommiae culture solution is respectively 1:0.05、1:0.5、1:2、1:5、1:10 ratio adds in,
It after often adding in a Cortex Eucommiae culture solution, is cultivated 2 days at 25 DEG C, when coronoid process dissipate capsule bacterium growth is vigorous, that is, completes domestication.
(6) preparation of Cortex Eucommiae Fu tea inoculation liquid
The base fluid containing bacteria suspension and Cortex Eucommiae culture solution after step (5) is tamed is placed in shake culture in shaking table, cultivates
Temperature is 28 DEG C, rotating speed 200r/min, cultivates 15 days, obtains final Cortex Eucommiae Fu tea bacterium solutions, prepares and gives birth to as Cortex Eucommiae Fu tea
Inoculation liquid in production.
(7) decatize, pile fermentation
After the processed Cortex Eucommiae leaf raw material water spray of step (2), high temperature steaming when detection water content reaches 20%, decatize temperature
It is 100 DEG C to spend, a length of 5 minutes during decatize；Eucommia ulmoides Oliv. leaves after decatize are accumulated immediately, the processing capacity of foundation folium cortex eucommiae,
Concentrate accumulation.Heap is 2 meters high, pile fermentation time 3.5 hours, and temperature control is at 75 DEG C -80 DEG C in heap.If it should be turned over immediately during more than 80 DEG C
Heap radiates.Folium cortex eucommiae after pile fermentation, Appearance color become the consistent yellowish-brown of color and luster by different variegated of the depth, endoplasm flavour by
Not mature grass fishy smell becomes mellow fragranced.Decatize and pile fermentation make folium cortex eucommiae fully soften, and remove peculiar smell, effectively remove Cortex Eucommiae
The careless fishy smell of leaf, while by physic-chemical changes complicated in hydrothermal promotion folium cortex eucommiae blade.
(8) mixing of folium cortex eucommiae embryo material and Cortex Eucommiae leaf sap
Folium cortex eucommiae after pile fermentation is precisely weighed, after determining folium cortex eucommiae embryo material weight, the Cortex Eucommiae culture of addition step (3)
Liquid, between adjustment Cortex Eucommiae leaf water content 20-40%, (usually according in every 500g folium cortex eucommiaes embryo material plus Cortex Eucommiae culture solution 200g),
It stirs, carries out decatize softening, 100 DEG C of steam temperature again by steam engine, folium cortex eucommiae mixing was made in 5 seconds time
Embryo material.
(9) it is inoculated with coronoid process dissipate capsule bacterium spore
It will uniformly be spread out by the folium cortex eucommiae mixing embryo material that decatize softened, cooled to room temperature softens according to decatize
The weight of folium cortex eucommiae mixing embryo material afterwards, the Cortex Eucommiae Fu tea inoculation liquids of sprinkling step (6), fountain height are inoculated with reference to general Fu tea
Depending on technique.
(10) pressed sizing
Inoculation coronoid process is dissipated to the folium cortex eucommiae embryo material of cystospore bacterium, mold is packed into after weighing as required, is pressed into tea brick type.
(11) floating is dried
Cortex Eucommiae brick is sent into drying chamber, it is edge-on on shelf.The spacing of brick is 2 centimetres, using indirect heating, is sent out
Flower culture, this process are divided into floating phase, the phase of raising flowers and dry phase three phases, complete within 20 days altogether, wherein sending out bloom temperature
25 DEG C, relative humidity 75%, 10 days time；Support 30 DEG C of bloom temperature, relative humidity 45%, 4 days time；Dry 6 days phases, temperature
35 DEG C, the method that natural drying can also be used, until Cortex Eucommiae brick tea includes water when being reduced to 6%-14%, as folium cortex eucommiae Fu bricks
Tea finished product.
(12) medicinal extract extracts
Deionized water is added in folium cortex eucommiae Fu-brick tea finished product and carries out water logging extraction, leaching liquid is through being concentrated in vacuo, vacuum spraying
It is dry, obtain folium cortex eucommiae Fu-brick tea soluble concrete.When wherein folium cortex eucommiae Fu-brick tea is extracted using deionized water, folium cortex eucommiae Fu bricks
The mass ratio of tea and water is 1:10~20, folium cortex eucommiae Fu-brick tea and deionized water are placed in stainless steel extractor in proportion, rapidly
100 DEG C are warming up to, is down to 70~85 DEG C after five minutes, constant temperature 1 hour.During vacuum concentration vacuum degree be 0.05~0.1MPa, vacuum
The temperature of concentration is 45~60 DEG C.Vacuum degree during vacuum spray drying is 0.06~0.09MPa, and power is 3~6KW, dry
10~30min of time.
(13) prepared by oral liquid
By folium cortex eucommiae Fu-brick tea medicinal extract, beta-cyclodextrin, D-sorbite, candy sugar powder, according to extract powder：Beta-cyclodextrin：Sorb
Sugar alcohol：Candy sugar powder=6：20：0.3：In 30 weight ratio accurate weighing merging stainless steel blend tank, the pure water of 44 parts of addition,
It keeps being sufficiently stirred under the conditions of 80 DEG C of constant temperature, until beta-cyclodextrin, D-sorbite, candy sugar powder are completely dissolved, lighter color palm fibre is sparkling and crystal-clear
It is bright.
By prepared feed liquid, the plate filter through precision not less than 200 mesh filters, then through vacuum outgas, homogenizer
The homogeneous under 60Pt pressure is pumped into high-temperature sterilization tank, using 115 ± 2 DEG C of sterilizations, keeps 20min.Again through filling, inspection, packet
It fills, enter warehouse for finished product.
Embodiment 2
(1) acquisition of folium cortex eucommiae
It picks the 7-10 months without the neat folium cortex eucommiae in insect pest, blade face every year.
(2) preliminary treatment of folium cortex eucommiae
Folium cortex eucommiae is cleaned up, with cutter be divided into the directly upper round as a ball screening and choosing impurity elimination of slice or whole leaf to get
Cortex Eucommiae leaf raw material.
(3) preparation of Cortex Eucommiae culture solution
The smalls folium cortex eucommiae that sieve round as a ball in step (2) leaks down is leached into Cortex Eucommiae juice, is added according to per kilogram Folium Eucommiae
20 kilograms of water is obtained in 70-100 DEG C of leaching of water temperature.NaCl, NH are added in leaching liquid4NO3, sucrose, MgSO4、K2HPO4Make
For nutritional agents, and according to NaCl:NH4NO3:Sucrose:MgSO4:K2HPO4:Water is 32:33:20:40:41:1000 weight ratio is mixed
Configuration is closed, Cortex Eucommiae culture solution is made, is given over to follow-up spare.
(4) coronoid process dissipate capsule bacterium obtains
Good coronoid process dissipate capsule bacterium conidia powder is bought on the market, is taken and is put into the aseptic bottle containing sterile water in right amount
In, it is for use that bacteria suspension is made.
(5) coronoid process dissipate capsule bacterium is tamed
In the bacteria suspension of step (4), according to ratio from less to more, the Cortex Eucommiae culture solution of step (3) is gradually added in, according to
The secondary volume ratio according to opportunistic pathogen suspension and Cortex Eucommiae culture solution is respectively 1:0.1、1:0.5、1:2、1:5、1:10、1:50 ratio adds
Enter, after often adding in a Cortex Eucommiae culture solution, cultivated 2 days at 25 DEG C, when coronoid process dissipate capsule bacterium growth is vigorous, that is, complete domestication.
(6) preparation of Cortex Eucommiae Fu tea inoculation liquid
The base fluid containing bacteria suspension and Cortex Eucommiae culture solution after step (5) is tamed is placed in shake culture in shaking table, cultivates
Temperature is 28 DEG C, rotating speed 200r/min, cultivates 20 days, obtains final Cortex Eucommiae Fu tea bacterium solutions, prepares and gives birth to as Cortex Eucommiae Fu tea
Inoculation liquid in production.
(7) decatize, pile fermentation
The processed Cortex Eucommiae leaf raw material of step (2) is subjected to high temperature steaming, steam temperature is 120 DEG C, a length of 1 point during decatize
Clock；Eucommia ulmoides Oliv. leaves after decatize are accumulated immediately, according to the processing capacity of folium cortex eucommiae, concentrate accumulation.Heap is 2 meters high, during pile fermentation
Between 5 hours, in heap temperature control at 75 DEG C -80 DEG C.It if should the heat dissipation of turning immediately during more than 80 DEG C.Folium cortex eucommiae after pile fermentation, outside
Shape and color pool becomes the consistent yellowish-brown of color and luster by different variegated of the depth, and endoplasm flavour becomes mellow fragrance by not mature careless fishy smell
Taste.Decatize and pile fermentation make folium cortex eucommiae fully soften, and remove peculiar smell, effectively remove the careless fishy smell of folium cortex eucommiae, while by hydro-thermal
Effect promotes physic-chemical changes complicated in folium cortex eucommiae blade.
(8) mixing of folium cortex eucommiae embryo material and Cortex Eucommiae leaf sap
Folium cortex eucommiae after pile fermentation is precisely weighed, after determining folium cortex eucommiae embryo material weight, the Cortex Eucommiae culture of addition step (3)
Liquid between adjustment Cortex Eucommiae leaf water content 20-40% (usually according in every 500g folium cortex eucommiaes embryo material plus Cortex Eucommiae culture solution 200g), fills
Divide and stir evenly, carry out decatize softening, 107 DEG C of steam temperature again by steam engine, folium cortex eucommiae mixing embryo was made in 10 seconds time
Material.
(9) it is inoculated with coronoid process dissipate capsule bacterium spore
It will uniformly be spread out by the folium cortex eucommiae mixing embryo material that decatize softened, cooled to room temperature softens according to decatize
The weight of folium cortex eucommiae mixing embryo material afterwards, the Cortex Eucommiae Fu tea inoculation liquids of sprinkling step (6), fountain height are inoculated with reference to general Fu tea
Depending on technique.
(10) pressed sizing
Inoculation coronoid process is dissipated to the folium cortex eucommiae embryo material of cystospore bacterium, mold is packed into after weighing as required, is pressed into tea brick type.
(11) floating is dried
Cortex Eucommiae brick is sent into drying chamber, it is edge-on on shelf.The spacing of brick is 2 centimetres, using indirect heating, is sent out
Flower culture, this process are divided into floating phase, the phase of raising flowers and dry phase three phases, complete within 15 days altogether, wherein sending out bloom temperature
35 DEG C, relative humidity 85%, 7 days time；Support 35 DEG C of bloom temperature, relative humidity 65%, 3 days time；Dry 5 days phases, temperature
50 DEG C, the method that natural drying can also be used, until Cortex Eucommiae brick tea includes water when being reduced to 6%-14%, as folium cortex eucommiae Fu bricks
Tea finished product.
(12) medicinal extract extracts
Deionized water is added in folium cortex eucommiae Fu-brick tea finished product and carries out water logging extraction, leaching liquid is through being concentrated in vacuo, vacuum spraying
It is dry, obtain folium cortex eucommiae Fu-brick tea soluble concrete.When wherein folium cortex eucommiae Fu-brick tea is extracted using deionized water, folium cortex eucommiae Fu bricks
The mass ratio of tea and water is 1:10~20, folium cortex eucommiae Fu-brick tea and deionized water are placed in stainless steel extractor in proportion, rapidly
100 DEG C are warming up to, is down to 70~85 DEG C after five minutes, constant temperature 1 hour.During vacuum concentration vacuum degree be 0.05~0.1MPa, vacuum
The temperature of concentration is 45~60 DEG C.Vacuum degree during vacuum spray drying is 0.06~0.09MPa, and power is 3~6KW, dry
10~30min of time.
(13) prepared by oral liquid
By folium cortex eucommiae Fu-brick tea medicinal extract, beta-cyclodextrin, D-sorbite, candy sugar powder, according to extract powder：Beta-cyclodextrin：Sorb
Sugar alcohol：Candy sugar powder=10：25：0.45：In 45 weight ratio accurate weighing merging stainless steel blend tank, 20 parts pure of addition
Water keeps being sufficiently stirred under the conditions of 80 DEG C of constant temperature, until beta-cyclodextrin, D-sorbite, candy sugar powder are completely dissolved, lighter color palm fibre is sparkling and crystal-clear
It is transparent.
By prepared feed liquid, the plate filter through precision not less than 200 mesh filters, then through vacuum outgas, homogenizer
The homogeneous under 60Pt pressure is pumped into high-temperature sterilization tank, using 115 ± 2 DEG C of sterilizations, keeps 30min.Again through filling, inspection, packet
It fills, enter warehouse for finished product.
Folium cortex eucommiae Fu-brick tea and folium cortex eucommiae Fu-brick tea oral liquid has been prepared according to embodiment 1,2 respectively, and has invited 9 people
Tasting group has carried out tasting evaluation, obtains that the results are shown in table below.
Claims (10)
1. a kind of pure folium cortex eucommiae Fu-brick tea oral liquor, it is characterised in that：Using the coronoid process dissipate capsule bacterium spore manually cultivated
Bacteria suspension is made in sub- powder；Cortex Eucommiae culture solution will be obtained after folium cortex eucommiae water logging, according to ratio from less to more, gradually added in described
Bacteria suspension in, to coronoid process dissipate capsule bacterium carry out gradually tame after, folium cortex eucommiae Fu-brick tea inoculation liquid is prepared, is seeded to folium cortex eucommiae
In Fu-brick tea embryo material；With after floating drying, folium cortex eucommiae Fu-brick tea is prepared, by folium cortex eucommiae in repressed molding to Fu-brick tea embryo material again
Soluble concrete powder, mixing beta-cyclodextrin, sorbose is made by water logging extraction, vacuum concentration, vacuum spray drying in Fu-brick tea
After alcohol and candy sugar powder and water, and after homogeneous, sterilizing, pure folium cortex eucommiae Fu bricks are prepared according to oral liquid preparing process and take orally
Liquid.
A kind of 2. pure folium cortex eucommiae Fu-brick tea oral liquor according to claim 1, which is characterized in that Du
The preparation method of Zhong Ye Fu-brick teas includes the following steps：
【2.1】The preparation of Cortex Eucommiae culture solution
Cortex Eucommiae culture solution is prepared by nutritional agents is added in after fresh folium cortex eucommiae or Folium Eucommiae water logging, gives over to spare；
【2.2】Coronoid process dissipate capsule bacterium obtains
The appropriate coronoid process dissipate capsule bacterium conidia powder manually cultivated is taken, is put into the aseptic bottle containing sterile water, bacteria suspension is made
For use；
【2.3】Coronoid process dissipate capsule bacterium is tamed
To step【2.2】Bacteria suspension according to ratio from less to more, gradually add in step【2.1】Cortex Eucommiae culture solution, often
It after adding in a Cortex Eucommiae culture solution, is cultivated 2-5 days at 25-30 DEG C, carries out coronoid process dissipate capsule bacterium domestication；
【2.4】The preparation of folium cortex eucommiae Fu-brick tea inoculation liquid
By step【2.3】The base fluid containing bacteria suspension and Cortex Eucommiae culture solution after domestication is placed in shake culture in shaking table, training
It is 28 DEG C -30 DEG C to support temperature, cultivates 15-20 days, obtains final Cortex Eucommiae Fu tea bacterium solutions, prepares in production and connects as Cortex Eucommiae Fu tea
Kind liquid；
【2.5】Folium cortex eucommiae decatize and pile fermentation
By high temperature steaming after fresh folium cortex eucommiae high temperature steaming or Folium Eucommiae raw material water spray, steam temperature is 100 DEG C -120
DEG C, when decatize, is 1-5 minutes a length of, carries out concentration accumulation, pile fermentation time 3.5-5 hours, temperature control in heap after decatize immediately
System is at 75 DEG C -80 DEG C；
【2.6】The preparation of folium cortex eucommiae Fu-brick tea embryo material
Folium cortex eucommiae after pile fermentation is added into step【2.1】Cortex Eucommiae culture solution so that between Cortex Eucommiae leaf water content 20%-40%,
Decatize softening, 100 DEG C -107 DEG C of steam temperature, time 5-10 second are carried out again by steam engine after stirring, and is made
Into folium cortex eucommiae Fu-brick tea embryo material；
【2.7】It is inoculated with coronoid process dissipate capsule bacterium spore
The folium cortex eucommiae mixing embryo material that high temperature steaming softened will be again passed by uniformly to spread out, cooled to room temperature sprays step
【2.4】Inoculation liquid, be then pressed into brick；
【2.8】Floating is dried
Folium cortex eucommiae brick is sent into drying chamber, controls its temperature and humidity, carries out floating；Floating is shut out after finishing aeration-drying
Zhong Ye Fu-brick tea finished products.
3. a kind of pure folium cortex eucommiae Fu-brick tea oral liquor according to claim 1, it is characterised in that：Step
【2.1】In nutritional agents be NaCl, NH4NO3, sucrose, MgSO4、K2HPO4, according to NaCl:NH4NO3:Sucrose:MgSO4:
K2HPO4:Water is 32:33:20:40:41:1000 weight ratio mixed configuration.
4. a kind of pure folium cortex eucommiae Fu-brick tea oral liquor according to claim 1, it is characterised in that：Step
【2.3】In coronoid process dissipate capsule bacterium domestication, the Cortex Eucommiae culture solution added in for the first time is 0.05-0.1 times of bacteria suspension volume, and last time adds
The Cortex Eucommiae culture solution entered is 10-50 times of bacteria suspension volume, and the number of centre addition is 3-10 times.
5. a kind of pure folium cortex eucommiae Fu-brick tea oral liquor according to claim 1, it is characterised in that：Step
【2.8】Middle floating drying steps are：
【5.1】Floating 7-10 days under the conditions of 25-35 DEG C, humidity 65-85%；
【5.2】Floating 3-4 days under the conditions of 30-35 DEG C, humidity 45-65%；
【5.3】Dry 5-6 days or naturally dry to folium cortex eucommiae Fu-brick tea water content at 35-50 DEG C and reach 10-14%, as into
Product folium cortex eucommiae Fu-brick tea.
6. a kind of pure folium cortex eucommiae Fu-brick tea oral liquor according to claim 1, it is characterised in that：The Cortex Eucommiae
Leaf Fu-brick tea carries out water logging extraction using deionized water, and folium cortex eucommiae Fu-brick tea is 1 according to mass ratio with water:10~20 mixing, soon
Speed is warming up to 100 DEG C, is down to 70~85 DEG C after five minutes, constant temperature 1 hour.
7. a kind of pure folium cortex eucommiae Fu-brick tea oral liquor according to claim 1, it is characterised in that：The vacuum
Vacuum degree is 0.05~0.1MPa during concentration, and the temperature of vacuum concentration is 45~60 DEG C.
8. a kind of pure folium cortex eucommiae Fu-brick tea oral liquor according to claim 1, it is characterised in that：Vacuum spraying
Vacuum degree when dry is 0.06~0.09MPa, 10~30min of drying time.
9. a kind of pure folium cortex eucommiae Fu-brick tea oral liquor according to claim 1, it is characterised in that：Auxiliary material for β-
Cyclodextrin, D-sorbite and candy sugar powder, mixing weight ratio are extract powder：Beta-cyclodextrin：D-sorbite：Candy sugar powder=6~10：
20~25：0.3~0.45：30~45.
10. a kind of pure folium cortex eucommiae Fu-brick tea oral liquid, it is characterised in that：It is prepared according to one of the arbitrary methods of claim 1-9
It forms.
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