CN108115789A - A kind of windmill palm vine material low-melting alloy enhances method of modifying - Google Patents

A kind of windmill palm vine material low-melting alloy enhances method of modifying Download PDF

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Publication number
CN108115789A
CN108115789A CN201711390265.7A CN201711390265A CN108115789A CN 108115789 A CN108115789 A CN 108115789A CN 201711390265 A CN201711390265 A CN 201711390265A CN 108115789 A CN108115789 A CN 108115789A
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China
Prior art keywords
rattan
vine material
windmill palm
palm vine
windmill
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CN201711390265.7A
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CN108115789B (en
Inventor
汪佑宏
季必超
薛夏
王鹏程
张利萍
刘亚梅
张辉
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Anhui Agricultural University AHAU
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Anhui Agricultural University AHAU
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/02Processes; Apparatus
    • B27K3/0242Processes; Apparatus using melt impregnation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/001Heating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/007Treating of wood not provided for in groups B27K1/00, B27K3/00 using pressure
    • B27K5/0075Vacuum
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K9/00Chemical or physical treatment of reed, straw, or similar material
    • B27K9/002Cane, bamboo

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Forests & Forestry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Chemical And Physical Treatments For Wood And The Like (AREA)

Abstract

The invention discloses a kind of windmill palm vine material low-melting alloys to enhance method of modifying, refers to a kind of rattan furniture, rattan craftwork, the technical field of rattan article processing technology, step includes:By windmill palm vine material gas is dry be processed into required size after be put into large beaker, tin bismuth cadmium alloy block is placed on windmill palm vine material, it is put into together in vacuum drying chamber after the small beaker equipped with weight is pressed in thereon again, it vacuumizes to exclude the air in windmill palm vine material internal voids, heating is completely melt the tin bismuth cadmium alloy block, it releases vacuum state and recovers that the tin bismuth cadmium alloy block in molten condition to an atmospheric pressure, is made to impregnate under external and internal pressure difference effect in the gap inside windmill palm vine material.The method of the invention causes density and parallel-to-grain compressive strength of windmill palm vine material etc. all to improve a lot, it solves the problems, such as that the easily rupturable damage of windmill palm vine material low value rattan core during processing and utilization, deformation are easily replied, extends cane furniture, rattan article, the service life of rattan craftwork.

Description

A kind of windmill palm vine material low-melting alloy enhances method of modifying
Technical field
The present invention relates to a kind of rattan furniture, rattan craftwork, the technical fields of rattan article processing technology more particularly to one Kind windmill palm vine material low-melting alloy enhancing method of modifying.
Background technology
Rattan is monocotyledon, belongs to Palmae, saves rattan subfamily, saves rattan same clan plant, is weight in Tropical forests treasure-house The green non-timber resource recycled want, multiduty, renewable, natural distributed is in the torrid zone in the Eastern Hemisphere and its proximity Domain, the whole world share 13 categories more than 600 and plant, and there be 3 category, 42 kind of 26 mutation in China.
Rattan stem is commonly called as rattan, and long reachable over one hundred rice, mostly milky or ecru are naturally pure and fresh, with wood, bamboo wood phase Compare, be manufacture rattan furniture, rattan craftwork, rattan because having many advantages, such as flexible, ventilative, light and handy, low heat conductivity, biodegradable The high-quality environment-friendly materials of product etc.;In addition, rattan furniture because appearance it is elegant, it is beautiful and generous, get close to nature, have very high ornamental Property, practicability and commercial value.
But due to secondary growth of the windmill palm vine material without timber, the center pillar inside rattan peel is mainly distributed by vascular bundle Wherein, parenchyma cell, which is divided into, is distributed between vascular bundle;Its vascular bundle, conduit are gradually increased to rattan core size by rattan peel, divided simultaneously Cloth is gradually sparse, this unique non-uniform construction features, causes that its density is small, intensity is low and extremely uneven on cross section The shortcomings of even, influences the service life of the various products of windmill palm vine material;Remaining Rattan rattan core after rattan peel is especially peelled off, substantially On be difficult to be applied.Dipping thermosetting resin is commonly used in the prior art, and reinforcing modification, but these are carried out to windmill palm vine material Common thermosetting resin limits the use scope of modified windmill palm vine material and its product because containing the unwanted volatiles such as formaldehyde; And during impregnation, though heating is conducive to the dipping of resin, the curing of part resin will also result in simultaneously, influence To the amount of impregnating of resin, it is ineffective to ultimately result in reinforcing modification.In conclusion currently used enhancing modification drop Low competitiveness of the rattan material in fields such as Furniture manufactures, significant limitation is brought to the use of rattan material;In addition, because of timber knot Structure is relatively uniform, material is naturally easily consistent after processing;And monocotyledon windmill palm vine material does not have the secondary growth of timber, Center pillar inside rattan peel mainly by vascular bundle distribution wherein, parenchyma cell is divided into and is distributed between vascular bundle;While its vascular bundle, Conduit gradually increases by rattan peel to rattan core size, it is gradually sparse to be distributed, this unique non-uniform construction features, cause its The shortcomings of extremely uneven on cross section, and containing inclusions such as a large amount of thyloses in conduit, therefore handle more to be totally different from Timber.
The content of the invention
It is an object of the invention to overcome the deficiencies of the prior art and provide a kind of enhancings of windmill palm vine material low-melting alloy to change Property method, to solve windmill palm vine material during processing and utilization, because density is low, intensity is low, cracky, the technology easily replied of deformation Problem improves the added value of windmill palm vine material, extends cane furniture, rattan article, the service life of rattan craftwork.
The present invention is achieved by the following technical solutions:
A kind of windmill palm vine material low-melting alloy enhances method of modifying, comprises the following steps:
Step 1, by windmill palm vine material gas is dry be processed into required size after be put into large beaker, tin bismuth cadmium alloy block is placed on It on windmill palm vine material, then is put into together in vacuum drying chamber after the small beaker equipped with weight is pressed in thereon, vacuumizes to exclude palm fibre Air in palmitic acid rattan material internal voids;
Step 2, the heating large beaker release vacuum state and recover extremely to the tin bismuth cadmium alloy block is completely melt One atmospheric pressure makes the tin bismuth cadmium alloy block in molten condition be impregnated under external and internal pressure difference effect in windmill palm vine material In the gap in portion;
Step 3 is cleaned before the tin bismuth cadmium alloy block in molten condition cures in the windmill palm vine material surface The tin bismuth cadmium alloy block in molten condition, then the windmill palm vine material impregnated by the tin bismuth cadmium alloy block is put into dry It is cooled to room temperature in dry device.
Further, windmill palm vine material is the white core rattan of low value after removal rattan peel in the step 1, the tin bismuth cadmium alloy block Fusing point is 103 DEG C, and the vacuum degree after vacuumizing is 0.093MPa.
Further, the temperature heated in the step 2 be 105 DEG C, when impregnating it is a length of 6 it is small when.
Further, cooling time is 10 days in the step 3.
Further, the vacuum degree after the step 1 vacuumizes is 0.093MPa.
The present invention has the following advantages compared with prior art:The present invention provides a kind of enhancings of windmill palm vine material low-melting alloy Method of modifying, this method utilize the negative pressure generated under vacuum state, are not required to miscellaneous equipment and provide impressed pressure, and investment is small, and Alloy injection rate is big;In a heated condition by the tin bismuth cadmium alloy injection windmill palm vine material of melting, heating temperature is not high, can keep The original color and luster of rattan material;Using ambient temperature curing, windmill palm vine material is solved during processing and utilization to reach, because density is small, strong It spends low, cracky, the technical barrier that deformation is easily replied, improves the added value of windmill palm vine material, extend cane furniture, rattan system Product, rattan craftwork service life purpose.
Specific embodiment
It elaborates below to the embodiment of the present invention, the present embodiment is carried out lower based on the technical solution of the present invention Implement, give detailed embodiment and specific operating process, but protection scope of the present invention is not limited to following implementation Example.
Embodiment 1
1st, test material
(1) preparation of windmill palm vine material:
Several gas of white core rattan for choosing removal rattan peel are done, and obtain windmill palm vine material;Windmill palm vine material is processed growth 30mm's Test specimen is several, spare.
(2) alloy prepares:
Fusing point is that 103 DEG C of tin bismuth cadmium alloy is purchased from market.
2nd, the enhancing modification of alloy and the measure of rate of body weight gain
(1) the white core rattan test specimen after gas is done is divided into two groups after being polished with sand paper and numbers respectively, and one of which weighs up just Beginning mass M1, as the modified modification test specimen of enhancing (another ergin material compares the control test specimen of experiment);
(2) the modification test specimen to be enhanced is placed in large beaker, the tin bismuth cadmium alloy block that fusing point is 103 DEG C is placed on it On, then be put into together in vacuum drying chamber after the small beaker equipped with weight is pressed in thereon, while another ergin material is compared The control test specimen of experiment is also placed in vacuum drying chamber;0.093MPa is evacuated to exclude in windmill palm vine material internal voids Air;It is then heated to 105 DEG C and is completely melt to alloy, then release vacuum and recover the alloy for an atmospheric pressure, making melting It is impregnated under the conditions of a nearly atmospheric pressure, 105 DEG C in the gap inside windmill palm vine material;Rattan is taken out after impregnating 6 hours Material cleans the molten state alloy on its surface before alloy curing, with compareing after test specimen is put into is cooled to room temperature in drier together, Weigh up modification test specimen treated the mass M of enhancing0;.
(3) rate of body weight gain of the modification test specimen of enhancing is calculated
3rd, density and parallel-to-grain compressive strength calculate
(1) the control test specimen being cooled to room temperature in drier is taken out into half, while the modification test specimen of enhancing is also taken out, Its absolute dry mass M is weighed up respectively0
It puts it into again in the beaker equipped with tap water until being dipped to sinking, measures its diameter R, height H;
Basic density
(2) the control test specimen being cooled to room temperature in drier is taken out the other half, while the modification test specimen of enhancing is also taken Go out, weigh up its diameter R respectively1
Maximal destruction power P when measuring it on mechanics test-run a machine in rift grain resistance to compressionmax
By formulaParallel-to-grain compressive strength (MPa) is calculated, the results are shown in Table 1:
1 white core rattan alloy of table enhances modified test result
White core rattan is after the tin bismuth cadmium alloy that fusing point is 103 DEG C enhances modification, and basic density is by control test specimen 0.334g/cm3Increase to modified test specimen 1.219g/cm3, basic density increases 3.65 times, amplification is up to 265.24% (and mesh It is preceding that density after treating of wood is only capable of to increase by 50% or so);And parallel-to-grain compressive strength is also increased by the 42.889MPa of control test specimen To the 76.454MPa of modified test specimen, parallel-to-grain compressive strength also increases to original 1.78 times, and amplification is also up to 78.26%.
From the point of view of result of the test, Rattan is close after the tin bismuth cadmium alloy that fusing point is 103 DEG C enhances modification Degree, parallel-to-grain compressive strength have the increase of highly significant, this intensity for increasing windmill palm vine material, extend palm rattan furniture, The service life of rattan article, rattan craftwork, the added value for improving windmill palm vine material are all highly effective.

Claims (5)

1. a kind of windmill palm vine material low-melting alloy enhances method of modifying, which is characterized in that comprises the following steps:
Step 1, by windmill palm vine material gas is dry be processed into required size after be put into large beaker, tin bismuth cadmium alloy block is placed on palm It on rattan material, then is put into together in vacuum drying chamber after the small beaker equipped with weight is pressed in thereon, vacuumizes to exclude Rattan Air in material internal voids;
Step 2, the heating large beaker release vacuum state and recover to one to the tin bismuth cadmium alloy block is completely melt Atmospheric pressure makes the tin bismuth cadmium alloy block in molten condition be impregnated under external and internal pressure difference effect inside windmill palm vine material In gap;
Step 3 is cleaned before the tin bismuth cadmium alloy block in molten condition cures in the place on the windmill palm vine material surface In the tin bismuth cadmium alloy block of molten condition, the windmill palm vine material impregnated by the tin bismuth cadmium alloy block is then put into drier In be cooled to room temperature.
A kind of 2. windmill palm vine material low-melting alloy enhancing method of modifying according to claim 1, which is characterized in that the step Windmill palm vine material is the white core rattan of low value after removal rattan peel in rapid 1, and the fusing point of the tin bismuth cadmium alloy block is 103 DEG C, after vacuumizing Vacuum degree be 0.093MPa.
A kind of 3. windmill palm vine material low-melting alloy enhancing method of modifying according to claim 2, which is characterized in that the step The temperature heated in rapid 2 be 105 DEG C, when impregnating it is a length of 6 it is small when.
A kind of 4. windmill palm vine material low-melting alloy enhancing method of modifying according to claim 3, which is characterized in that the step Cooling time is 10 days in rapid 3.
5. enhancing method of modifying according to a kind of any windmill palm vine material low-melting alloy of Claims 1 to 4, feature exists In the vacuum degree after the step 1 vacuumizes is 0.093MPa.
CN201711390265.7A 2017-12-21 2017-12-21 A kind of windmill palm vine material low-melting alloy enhancing method of modifying Active CN108115789B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109333715A (en) * 2018-11-08 2019-02-15 福建农林大学 A kind of method of the co-melting system collaboration heat treatment improved wood of inorganic salts-metal

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20020045057A1 (en) * 2000-10-16 2002-04-18 Guritza Dennis A. Stenoprophiluric matrices, and methods of making and using the same
CN101745952A (en) * 2009-12-22 2010-06-23 何光临 Modification method of soft timber and special device
CN104210000A (en) * 2014-09-11 2014-12-17 安徽农业大学 Embrittlement-prevention treatment method for palm rattan materials
CN104476648A (en) * 2014-11-27 2015-04-01 天津市耐特家具有限公司 Process method for improving solid wood furniture plate performance

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20020045057A1 (en) * 2000-10-16 2002-04-18 Guritza Dennis A. Stenoprophiluric matrices, and methods of making and using the same
CN101745952A (en) * 2009-12-22 2010-06-23 何光临 Modification method of soft timber and special device
CN104210000A (en) * 2014-09-11 2014-12-17 安徽农业大学 Embrittlement-prevention treatment method for palm rattan materials
CN104210000B (en) * 2014-09-11 2016-06-08 安徽农业大学 A kind of anti-embrittlement processing method of windmill palm vine material
CN104476648A (en) * 2014-11-27 2015-04-01 天津市耐特家具有限公司 Process method for improving solid wood furniture plate performance

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
何云晓等: "《园林建筑材料实用教程》", 30 September 2015, 东南大学 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109333715A (en) * 2018-11-08 2019-02-15 福建农林大学 A kind of method of the co-melting system collaboration heat treatment improved wood of inorganic salts-metal
CN109333715B (en) * 2018-11-08 2021-02-02 福建农林大学 Method for modifying wood through synergistic heat treatment of inorganic salt-metal eutectic system

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