CN108114679B - Magnetization reaction system for aliphatic sulfonate water reducer - Google Patents

Magnetization reaction system for aliphatic sulfonate water reducer Download PDF

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Publication number
CN108114679B
CN108114679B CN201711418484.1A CN201711418484A CN108114679B CN 108114679 B CN108114679 B CN 108114679B CN 201711418484 A CN201711418484 A CN 201711418484A CN 108114679 B CN108114679 B CN 108114679B
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reaction
barrel body
liquid feeding
support
reaction barrel
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CN108114679A (en
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胡勇
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Yingde Junguan New Material Co ltd
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Yingde Junguan New Material Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/087Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/005Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the outlet side being of particular interest
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094Jackets

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention discloses an aliphatic sulfonate water reducer magnetization reaction system, which comprises a reaction barrel body, wherein a stirring motor is fixed at the middle position of the upper surface of the reaction barrel body, a supporting frame is arranged at the bottom of the reaction barrel body, the bottom end of the stirring motor is connected with a stirring shaft, three stirring blades are equidistantly arranged on the stirring shaft, one side of the supporting frame is connected with a first bracket, and a first liquid adding hopper and a third liquid adding hopper are arranged at the position of the upper surface of the reaction barrel body, which is close to the stirring motor.

Description

Magnetization reaction system for aliphatic sulfonate water reducer
Technical Field
The invention belongs to the technical field of water reducer production, and particularly relates to an aliphatic sulfonate water reducer magnetization reaction system.
Background
The water reducing agent is a concrete additive capable of reducing the mixing water consumption under the condition of maintaining the slump constant of concrete, and mostly belongs to anionic surfactants, such as lignosulfonate, naphthalene sulfonate formaldehyde polymer and the like, and the water reducing agent has a dispersing effect on cement particles after being added into the concrete mixture, can improve the workability, reduce the unit water consumption and improve the fluidity of the concrete mixture; or reduce the unit cement consumption and save cement.
However, the magnetization reaction system of the aliphatic sulfonate water reducer in the current market still has certain defects in the process of manufacturing the water reducer, for example, manual liquid adding is performed during reaction manufacturing, the error is large, quantitative liquid adding cannot be performed, the working strength of workers is large, the working efficiency is low, in addition, the fluidity of a mixed solution is poor, blockage is easy to occur during liquid discharging, and the water reducer is inconvenient to rapidly discharge.
Disclosure of Invention
The invention aims to provide an aliphatic sulfonate water reducer magnetization reaction system, which solves the problems that the manual liquid adding is large in error, quantitative liquid adding cannot be performed during reaction and manufacture, the working intensity of workers is high, the working efficiency is low, in addition, the fluidity of mixed solution is poor, the mixed solution is easy to block during liquid discharging, and the quick discharge of the water reducer is inconvenient.
In order to achieve the above purpose, the present invention provides the following technical solutions: the magnetization reaction system of the aliphatic sulfonate water reducer comprises a reaction barrel body, wherein a stirring motor is fixed at the middle position of the upper surface of the reaction barrel body, a support frame is arranged at the bottom of the reaction barrel body, the bottom end of the stirring motor is connected with a stirring shaft, three stirring blades are equidistantly arranged on the stirring shaft, one side of the support frame is connected with a first bracket, one side of the support frame, which is opposite to the first bracket, is connected with a second bracket, a first liquid adding hopper and a third liquid adding hopper are arranged at the position of one side, which is close to the stirring motor, of the upper surface of the reaction barrel body, a water inlet pipe and a second liquid adding hopper are arranged at one side, which is opposite to the first liquid adding hopper and the third liquid adding hopper, the first liquid adding hopper is positioned at the front side of the third liquid adding hopper, electromagnetic valves are arranged inside the connecting positions of the first liquid adding hopper, the water inlet pipe, the second liquid adding hopper and the third liquid adding hopper and the reaction barrel body, the pressure discharge valve is arranged at the lower position of one side of the reaction barrel body close to the water inlet pipe, the heat insulation layer is arranged on the inner wall of the reaction barrel body, the heating layer is arranged in the heat insulation layer, the electric heating blocks are equidistantly arranged in the heating layer, three guide plates are symmetrically arranged at the two sides of the bottom of the inside of the reaction barrel body, the middle position of the bottom end of the reaction barrel body is connected with the blanking pipe, the blanking gate is arranged at the upper half section of the blanking pipe, the circulating water pump is arranged on the upper surface of the first bracket, the magnetizer is fixed at the position of the upper surface of the first bracket close to the rear side of the circulating water pump, the water outlet end of the magnetizer is connected with the top of the reaction barrel body through the conveying pipe, the controller is arranged on the upper surface of the second bracket, the temperature controller is arranged in the second bracket, the electric heating block is electrically connected with the temperature controller, the stirring motor, the magnetizing machine, the circulating water pump and the electromagnetic valve are electrically connected with the controller, and the temperature controller and the controller are electrically connected with an external power supply.
Preferably, the water inlet end of the circulating water pump is connected with the bottom of the reaction barrel body through a pipeline, and the water outlet end of the circulating water pump is connected with the water inlet of the magnetizer through a pipeline.
Preferably, the first bracket is of an L-shaped structure, and the second bracket is of an F-shaped structure.
Preferably, the inclination angle of the deflector is 15 °.
Preferably, the circulating water pump is fixedly connected with the first bracket through bolts.
Compared with the prior art, the invention has the beneficial effects that:
(1) According to the invention, the electromagnetic valves are arranged, when the electromagnetic valve is manufactured, a worker can control the electromagnetic valves in the first liquid adding hopper, the water inlet pipe, the second liquid adding hopper and the third liquid adding hopper to be opened through the controller, the sulfonating agent, water, ketone compounds and aldehyde compounds required in the reaction are respectively added into the reaction barrel body through the first liquid adding hopper, the water inlet pipe, the second liquid adding hopper and the third liquid adding hopper, and when a certain amount of sulfonating agent is added, the electromagnetic valves in the first liquid adding hopper, the water inlet pipe, the second liquid adding hopper and the third liquid adding hopper can be closed through the controller by the worker, so that the purpose of automatic liquid adding is achieved, the automatic quantitative liquid adding of a reaction system is further realized, the manual liquid adding error is avoided, the quality of the water reducer is ensured, the working strength of the worker is reduced, and the working efficiency of the worker is improved.
(2) According to the invention, the guide plate is arranged, and in the reaction manufacturing process of the water reducer, the guide plate plays a role in guiding the solution by utilizing the inclination of the guide plate by 15 degrees, so that the flow state of the solution is changed, the fluidity of the mixed solution is enhanced, the quick discharge of the water reducer from the blanking pipe is promoted, the blanking pipe is prevented from being blocked, the quick discharge of the water reducer is facilitated, and the reaction manufacturing efficiency of the water reducer is improved.
Drawings
FIG. 1 is a schematic diagram of the structure of the present invention;
FIG. 2 is a right side view of the present invention;
FIG. 3 is a left side view of the present invention;
FIG. 4 is a left side view of the present invention;
in the figure: 1-a stirring motor; 2-a first liquid adding hopper; 3-stirring the leaves; 4-a conveying pipe; 5-a magnetizer; 6-a first bracket; 7-a circulating water pump; 8-blanking gate; 9-blanking pipe; 10-a deflector; 11-a supporting frame; 12-temperature controller; 13-a second bracket; 14-a controller; 15-an electric heating block; 16-a heating layer; 17-a heat insulation layer; 18-a reaction barrel; 19-a pressure relief valve; 20-stirring shaft; 21-a water inlet pipe; 22-electromagnetic valve; 23-a second liquid adding hopper; 24-a third liquid adding hopper.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Referring to fig. 1-4, the present invention provides a technical solution: the magnetization reaction system of the aliphatic sulfonate water reducer comprises a reaction barrel 18, a stirring motor 1 is fixed at the middle position of the upper surface of the reaction barrel 18 for realizing uniform mixing of various solutions and promoting solution reaction, the stirring motor 1 adopts a GS0075A driving motor, a support frame 11 is arranged at the bottom of the reaction barrel 18, the bottom end of the stirring motor 1 is connected with a stirring shaft 20, three stirring blades 3 are equidistantly arranged on the stirring shaft 20, one side of the support frame 11 is connected with a first bracket 6, one side of the support frame 11 opposite to the first bracket 6 is connected with a second bracket 13, a first liquid adding hopper 2 and a third liquid adding hopper 24 are arranged at the position of the upper surface of the reaction barrel 18, which is close to one side of the stirring motor 1, a water inlet pipe 21 and a second liquid adding hopper 23 are arranged at one side of the upper surface of the reaction barrel 18 opposite to the first liquid adding hopper 2 and the third liquid adding hopper 24, the first liquid adding hopper 2 is positioned at the front side of the third liquid adding hopper 24, the water inlet pipe 21 is positioned at the front side of the second liquid adding hopper 23, the electromagnetic valves 22 are arranged in the connection parts of the first liquid adding hopper 2, the water inlet pipe 21, the second liquid adding hopper 23 and the third liquid adding hopper 24 and the reaction barrel 18, the pressure discharging valve 19 is arranged at the position, close to the lower part of the water inlet pipe 21, of one side of the reaction barrel 18, the heat insulating layer 17 is arranged on the inner wall of the reaction barrel 18, the heating layer 16 is arranged in the heat insulating layer 17, the electric heating blocks 15 are equidistantly arranged in the heating layer 16, the electric heating blocks 15 are electrified and heated under the control of the temperature controller 12, the rapid reaction of solution is ensured, the three guide plates 10 are symmetrically arranged at the two sides of the bottom of the inside of the reaction barrel 18, the blanking pipe 9 is connected at the middle position of the bottom end of the reaction barrel 18, the blanking gate 8 is arranged at the upper half section of the blanking pipe 9, the circulating water pump 7 is arranged on the upper surface of the first bracket 6, and the magnetization machine 5 is fixed on the upper surface of the first bracket 6 near the rear side position of the circulating water pump 7, the magnetization machine 5 is electrified under the control of the controller 14 to generate a magnetic field, a solution flows through the magnetic field to generate physical change so as to achieve the effect of solution magnetization, the water outlet end of the magnetization machine 5 is connected with the top of the reaction barrel 18 through the conveying pipe 4, the controller 14 is mounted on the upper surface of the second bracket 13, the model of the controller 14 is NUC120, the temperature controller 12 is mounted in the second bracket 13, the temperature controller 12 adopts a Sdc35 temperature controller, the electric heating block 15 is electrically connected with the temperature controller 12, and the stirring motor 1, the magnetization machine 5, the circulating water pump 7 and the electromagnetic valve 22 are electrically connected with the controller 14, and the temperature controller 12 and the controller 14 are electrically connected with an external power supply.
In order to realize that the circulating water pump 7 drives the mixed solution to flow for magnetization, in this embodiment, preferably, the water inlet end of the circulating water pump 7 is connected with the bottom of the reaction barrel 18 through a pipeline, and the water outlet end of the circulating water pump 7 is connected with the water inlet of the magnetization machine 5 through a pipeline.
In order to facilitate the fixing of the components by the first bracket 6 and the second bracket 13, in this embodiment, it is preferable that the first bracket 6 has an L-shaped structure and the second bracket 13 has an F-shaped structure.
In order to achieve the effect of the baffle 10 as a baffle, in this embodiment, the inclined angle of the baffle 10 is preferably 15 °.
In order to facilitate stable operation of the circulating water pump 7, in this embodiment, it is preferable that the circulating water pump 7 is fixedly connected to the first bracket 6 by bolts.
Working principle: when the invention is used, a worker firstly turns on an external power supply and turns on a power supply of the equipment through the controller 14, at the moment, the equipment starts to work, then turns on the water inlet electromagnetic valve 22 through the controller 14, external water is added into the reaction barrel 18 through the water inlet pipe 21, when the external water is added, the worker turns off the water inlet electromagnetic valve 22 through the controller 14, then turns on the electromagnetic valve 22 in the first liquid adding hopper 2 through the controller 14, the sulfonating agent is added into the reaction barrel 18 through the first liquid adding hopper 2, when the sulfonating agent is added, the worker turns off the electromagnetic valve 22 in the first liquid adding hopper 2 through the controller 14 to realize quantitative liquid adding, meanwhile, the stirring motor 1 works under the control of the controller 14 and rotates under the control of the stirring blade 3 through the stirring shaft 20 to stir the solution in the reaction barrel 18, the solution mixing reaction is promoted, after a certain time, the worker controls the circulating water pump 7 to work and rotate through the controller 14 to pump out the reaction solution in the reaction barrel 18 and conveys the reaction solution to the magnetizer 5 through a pipeline, the magnetizer 5 is electrified under the control of the controller 14 to generate a magnetic field, the solution flows through the magnetic field to generate physical change so as to achieve the purpose of magnetizing the solution, after the solution is magnetized, the solution is conveyed into the reaction barrel 18 through the conveying pipe 4, at the moment, the worker opens the electromagnetic valve 22 in the second liquid adding hopper 23 through the controller 14 to quantitatively add the ketone compound into the reaction barrel 18 through the second liquid adding hopper 23, meanwhile, the worker controls the electric heating block 15 in the heating layer 16 through the temperature controller 12 to carry out electrified heating, when the electric heating block is heated to a certain temperature, the ketone compound in the reaction barrel 18 carries out sulfonation reflux reaction, after a certain time of reaction, the worker opens the electromagnetic valve 22 in the third liquid adding hopper 24 through the controller 14, the aldehyde compound is added into the reaction barrel 18 through the third liquid adding hopper 24, meanwhile, a worker controls the electric heating block 15 to continuously heat through the temperature controller 12, when the electric heating block is heated to the temperature required by solution reaction, the aldehyde compound and the mixed solution are uniformly mixed for reaction under the stirring action of the stirring blade 3, after a certain period of reaction, the worker pulls the blanking gate 8 to discharge the aliphatic sulfonate water reducer reacted in the reaction barrel 18 through the blanking pipe 9, namely, magnetization reaction manufacturing of the aliphatic sulfonate water reducer is completed, in the water reducer reaction manufacturing process, the guide plate 10 plays a role in guiding the solution, the solution state is changed, and the quick discharge of the water reducer through the blanking pipe 9 is promoted.
Although embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (1)

1. Aliphatic sulfonate water-reducing agent magnetization reaction system, including reaction staving (18), its characterized in that: the utility model discloses a reaction tank, including reaction tank (18) and reaction tank, stirring motor (1) is fixed in intermediate position department of reaction tank (18) upper surface, and support frame (11) is installed to the bottom of reaction tank (18), the bottom of stirring motor (1) is connected with (mixing) shaft (20), and three stirring leaf (3) are installed to the equidistance on (mixing) shaft (20), one side of support frame (11) is connected with first support (6), and one side of support frame (11) for first support (6) is connected with second support (13), one side department that reaction tank (18) upper surface is close to (stirring) motor (1) installs first liquid feeding fill (2) and third liquid feeding fill (24), and reaction tank (18) upper surface is for one side of first liquid feeding fill (2) and third liquid feeding fill (24) installs inlet tube (21) and second fill (23), first liquid feeding fill (2) are located the front side of third liquid feeding fill (24), inlet tube (21) are located the front side of second fill (23), first liquid feeding fill (21), second liquid feeding fill (24) are all provided with the electromagnetic valve (18) and are all connected with reaction tank (18), the utility model discloses a reaction barrel body (18), including reaction barrel body (18), heat-insulating layer (17), heating layer (16), three guide plates (10) are installed to the inside equidistance of heating layer (16), the bottom bilateral symmetry in reaction barrel body (18) is provided with three guide plates (10), and the intermediate position department of reaction barrel body (18) bottom is connected with unloading pipe (9), unloading floodgate (8) are installed to the upper half section of unloading pipe (9), circulating water pump (7) are installed to the upper surface of first support (6), and the rear side position department that the upper surface of first support (6) is close to circulating water pump (7) is fixed with magnetizer (5), the water outlet end of magnetizer (5) is connected with the top of reaction barrel body (18) through conveyer pipe (4), upper surface mounting controller (14) of second support (13), and second support (13), electric motor (12), temperature controller (12) and electric connection (14) are all installed to magnetizer (14) and electric connection (12), the temperature controller (12) and the controller (14) are electrically connected with an external power supply;
the water inlet end of the circulating water pump (7) is connected with the bottom of the reaction barrel body (18) through a pipeline, and the water outlet end of the circulating water pump (7) is connected with the water inlet of the magnetizer (5) through a pipeline;
the first bracket (6) is of an L-shaped structure, and the second bracket (13) is of an F-shaped structure;
the inclination angle of the guide plate (10) is 15 degrees;
the circulating water pump (7) is fixedly connected with the first bracket (6) through bolts.
CN201711418484.1A 2017-12-25 2017-12-25 Magnetization reaction system for aliphatic sulfonate water reducer Active CN108114679B (en)

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CN108114679B true CN108114679B (en) 2024-02-13

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110368883A (en) * 2019-06-21 2019-10-25 枣阳市金鹏化工有限公司 A kind of reaction kettle producing organosilicon

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN204365190U (en) * 2015-01-07 2015-06-03 昌吉市力和精细化工厂 High performance water reducing agent of polyocarboxy acid production system
CN205379900U (en) * 2016-03-16 2016-07-13 四川恒泽建材有限公司 Automatic liquid agitating unit that mixes of water -reducing agent
CN205391354U (en) * 2016-02-27 2016-07-27 李金斌 Traditional chinese medicine decocting machine
CN206526745U (en) * 2017-03-07 2017-09-29 吉安民辉新型材料有限公司 For producing the energy-saving automatic batch mixing stirred tank of water reducer
CN207786569U (en) * 2017-12-25 2018-08-31 英德市竣冠新型材料有限公司 Aliphatic sulfonate water-reducing agent magnetizes reaction system

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN204365190U (en) * 2015-01-07 2015-06-03 昌吉市力和精细化工厂 High performance water reducing agent of polyocarboxy acid production system
CN205391354U (en) * 2016-02-27 2016-07-27 李金斌 Traditional chinese medicine decocting machine
CN205379900U (en) * 2016-03-16 2016-07-13 四川恒泽建材有限公司 Automatic liquid agitating unit that mixes of water -reducing agent
CN206526745U (en) * 2017-03-07 2017-09-29 吉安民辉新型材料有限公司 For producing the energy-saving automatic batch mixing stirred tank of water reducer
CN207786569U (en) * 2017-12-25 2018-08-31 英德市竣冠新型材料有限公司 Aliphatic sulfonate water-reducing agent magnetizes reaction system

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