CN108114679A - Aliphatic sulfonate water-reducing agent magnetizes reaction system - Google Patents

Aliphatic sulfonate water-reducing agent magnetizes reaction system Download PDF

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Publication number
CN108114679A
CN108114679A CN201711418484.1A CN201711418484A CN108114679A CN 108114679 A CN108114679 A CN 108114679A CN 201711418484 A CN201711418484 A CN 201711418484A CN 108114679 A CN108114679 A CN 108114679A
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China
Prior art keywords
water
liquid feeding
reaction
staving
reducing agent
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Granted
Application number
CN201711418484.1A
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Chinese (zh)
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CN108114679B (en
Inventor
胡勇
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City Jun Crown New Materials Co Ltd
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City Jun Crown New Materials Co Ltd
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Priority to CN201711418484.1A priority Critical patent/CN108114679B/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/087Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electric or magnetic energy
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/005Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the outlet side being of particular interest
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094Jackets

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The invention discloses aliphatic sulfonate water-reducing agents to magnetize reaction system,Including reacting staving,The middle position of the reaction staving upper surface is fixed with stirring motor,And the bottom of reaction staving is equipped with supporting rack,The bottom of the stirring motor is connected with agitating shaft,And equidistant on agitating shaft three paddles are installed,The one side of support frame as described above is connected with first support,The reaction staving upper surface is equipped with the first liquid feeding bucket and the 3rd liquid feeding bucket at a side position of stirring motor,The present invention is provided with solenoid valve,Realize reaction system automatic ration liquid feeding,It ensure that the quality of water-reducing agent,The working strength of worker is reduced simultaneously,Improve work task efficiency,There is provided deflectors,Change solution fluidised form,Enhance the mobility of mixed solution,Water-reducing agent is promoted quickly to be discharged by tremie pipe,Prevent blanking blockage,It is quickly discharged convenient for water-reducing agent,Improve the reaction producing efficiency of water-reducing agent.

Description

Aliphatic sulfonate water-reducing agent magnetizes reaction system
Technical field
The invention belongs to water-reducing agent production technical fields, and in particular to aliphatic sulfonate water-reducing agent magnetizes reaction system.
Background technology
Water-reducing agent is outside a kind of concrete that under conditions of maintaining concrete slump constant, can reduce mixing water amount Add agent, belong to anion surfactant mostly, there is lignosulfonates, naphthalene sulphonate formaldehyde polymer etc., add in concrete There is peptizaiton to cement granules after mixture, its workability can be improved, reduce unit consumption of water, improve concrete mix Mobility;Or unit cement consumption is reduced, save cement.
But aliphatic sulfonate water-reducing agent currently on the market magnetizes reaction system during water-reducing agent is made still There are it is certain the defects of, for example, artificial liquid feeding when reaction makes, error is big, it is impossible to carry out quantitative liquid feeding, and the work of worker is strong Degree is big, and work efficiency is low, in addition, mixed solution poor fluidity, when drain easily blocks, and is not easy to water-reducing agent and quickly arranges Go out.
The content of the invention
It is an object of the invention to provide aliphatic sulfonate water-reducing agents to magnetize reaction system, to solve above-mentioned background technology Artificial liquid feeding when the reaction of middle proposition makes, error are big, it is impossible to carry out quantitative liquid feeding, and the great work intensity of worker, work effect Rate is low, in addition, mixed solution poor fluidity, when drain easily blocks, and is not easy to the problem of water-reducing agent is quickly discharged.
To achieve the above object, the present invention provides following technical solution:Aliphatic sulfonate water-reducing agent magnetizes reaction system, Including reacting staving, the middle position of the reaction staving upper surface is fixed with stirring motor, and reacts the bottom peace of staving Equipped with supporting rack, the bottom of the stirring motor is connected with agitating shaft, and equidistant on agitating shaft is equipped with three paddles, institute The one side for stating supporting rack is connected with first support, and supporting rack is connected with second support compared with the one side of first support, described Reaction staving upper surface is equipped with the first liquid feeding bucket and the 3rd liquid feeding bucket at a side position of stirring motor, and reacts staving Upper surface is equipped with water inlet pipe and the second liquid feeding bucket, first liquid feeding compared with the one side of the first liquid feeding bucket and the 3rd liquid feeding bucket Bucket is located at the front side of the second liquid feeding bucket positioned at the front side of the 3rd liquid feeding bucket, the water inlet pipe, the first liquid feeding bucket, water inlet pipe, The inside of second liquid feeding bucket and the 3rd liquid feeding bucket and reaction staving junction is both provided with solenoid valve, and the reaction staving one side is leaned on The lower position of nearly water inlet pipe is equipped with purge valve, and is provided with thermal insulation layer on the inner wall of reaction staving, and thermal insulation layer is interior Portion is provided with heating layer, and the inside of the heating layer is equidistant to be equipped with several electrical heating blocks, inside the reaction container body Two bottom sides are symmetrical arranged there are three deflector, and the middle position for reacting staving bottom is connected with tremie pipe, the blanking The upper semisection of pipe is equipped with blanking lock, and the upper surface of the first support is equipped with water circulating pump, and first support upper surface is leaned on Magnetizer is fixed at the rearward position of nearly water circulating pump, the water outlet of the magnetizer passes through delivery pipe and the top of reaction staving Portion is connected, and the upper surface of the second support is equipped with controller, and the inside of second support is equipped with temperature controller, the electricity Heat block is electrically connected with temperature controller, and the stirring motor, magnetizer, water circulating pump and solenoid valve electrically connect with controller It connects, the temperature controller and controller are electrically connected with external power supply.
Preferably, the water inlet end of the water circulating pump is connected by pipeline with reaction staving bottom, and water circulating pump goes out Water end (W.E.) is connected by the water inlet of pipeline and magnetizer.
Preferably, the first support is L-type structure, and second support is F type structures.
Preferably, the angle of inclination of the deflector is 15 °.
Preferably, the water circulating pump is bolted to connection with first support.
Compared with prior art, the beneficial effects of the invention are as follows:
(1) present invention is provided with solenoid valve, and during making, worker can pass through controller control and open the first liquid feeding bucket, water inlet Solenoid valve inside pipe, the second liquid feeding bucket and the 3rd liquid feeding bucket, by sulfonating agent required when reacting, water, ketone compounds and Aldehyde compound is added by the first liquid feeding bucket, water inlet pipe, the second liquid feeding bucket and the 3rd liquid feeding bucket in reaction staving respectively, is added When entering a certain amount of, worker can be closed by controller inside the first liquid feeding bucket, water inlet pipe, the second liquid feeding bucket and the 3rd liquid feeding bucket Solenoid valve, to achieve the purpose that automatic liquid-feeding, and then realize reaction system automatic ration liquid feeding, avoid artificial liquid feeding error Greatly, it ensure that the quality of water-reducing agent, while reduce the working strength of worker, improve work task efficiency.
(2) present invention is provided with deflector, and water-reducing agent is reacted in manufacturing process, and deflector is right using its own 15 ° of inclination Solution plays the role of water conservancy diversion, changes solution fluidised form, enhances the mobility of mixed solution, and water-reducing agent is promoted quickly to be arranged by tremie pipe Go out, prevent blanking blockage, quickly discharged convenient for water-reducing agent, improve the reaction producing efficiency of water-reducing agent.
Description of the drawings
Fig. 1 is the structural diagram of the present invention;
Fig. 2 is the right view of the present invention;
Fig. 3 is the left view of the present invention;
Fig. 4 is the left view of the present invention;
In figure:1- stirring motors;2- the first liquid feeding buckets;3- paddles;4- delivery pipes;5- magnetizers;6- first supports;7- Water circulating pump;8- blanking locks;9- tremie pipes;10- deflectors;11- supporting racks;12- temperature controllers;13- second supports;14- is controlled Device;15- electrical heating blocks;16- heating layers;17- thermal insulation layers;18- reacts staving;19- purge valves;20- agitating shafts;21- water inlet pipes; 22- solenoid valves;23- the second liquid feeding buckets;The 3rd liquid feeding buckets of 24-.
Specific embodiment
Below in conjunction with the attached drawing in the embodiment of the present invention, the technical solution in the embodiment of the present invention is carried out clear, complete Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, those of ordinary skill in the art are obtained every other without making creative work Embodiment belongs to the scope of protection of the invention.
- 4 are please referred to Fig.1, the present invention provides a kind of technical solution:Aliphatic sulfonate water-reducing agent magnetizes reaction system, bag Reaction staving 18 is included, in order to realize that a variety of solution are uniformly mixed, promotes solution reaction, the centre position of 18 upper surface of reaction staving Place is fixed with stirring motor 1, and stirring motor 1 uses GS0075A driving motors, and the bottom for reacting staving 18 is equipped with supporting rack 11, the bottom of stirring motor 1 is connected with agitating shaft 20, and equidistant on agitating shaft 20 is equipped with three paddles 3, supporting rack 11 One side be connected with first support 6, and supporting rack 11 is connected with second support 13, reaction container compared with the one side of first support 6 18 upper surface of body is equipped with the first liquid feeding bucket 2 and the 3rd liquid feeding bucket 24 at a side position of stirring motor 1, and reacts staving 18 upper surfaces are equipped with 21 and second liquid feeding bucket 23 of water inlet pipe compared with the one side of the first liquid feeding bucket 2 and the 3rd liquid feeding bucket 24, the One liquid feeding bucket 2 is located at the front side of the 3rd liquid feeding bucket 24, and water inlet pipe 21 is located at the front side of the second liquid feeding bucket 23, the first liquid feeding bucket 2, into Water pipe 21, the second liquid feeding bucket 23 and the 3rd liquid feeding bucket 24 and the inside of 18 junction of reaction staving are both provided with solenoid valve 22, instead It answers 18 one side of staving that purge valve 19 is installed close to the lower position of water inlet pipe 21, and is provided on the inner wall of reaction staving 18 Thermal insulation layer 17, and thermal insulation layer 17 is internally provided with heating layer 16, the inside of heating layer 16 is equidistant be equipped with several electricity plus Heat block 15, electrical heating block 15 carry out electrified regulation in the control of temperature controller 12, ensure that solution fast reaction, react in staving 18 The two bottom sides in portion are symmetrical arranged there are three deflector 10, and the middle position for reacting 18 bottom of staving is connected with tremie pipe 9, The upper semisection of tremie pipe 9 is equipped with blanking lock 8, and the upper surface of first support 6 is equipped with water circulating pump 7, and 6 upper table of first support Face is fixed with magnetizer 5 at the rearward position of water circulating pump 7, and magnetizer 5 is powered under control of the controller 14 generates magnetic , solution flows through magnetic field, physical change occurs, to achieve the effect that solution magnetization, the water outlet of magnetizer 5 passes through delivery pipe 4 It is connected with the top for reacting staving 18, the upper surface of second support 13 is equipped with controller 14, the model of controller 14 NUC120, and the inside of second support 13 is equipped with temperature controller 12, temperature controller 12 use Sdc35 temperature controllers, electrical heating block 15 with Temperature controller 12 is electrically connected, and stirring motor 1, magnetizer 5, water circulating pump 7 and solenoid valve 22 are electrically connected with controller 14, temperature Device 12 and controller 14 is controlled to be electrically connected with external power supply.
In order to realize that water circulating pump 7 drives mixed solution flowing to be magnetized, in the present embodiment, it is preferred that water circulating pump 7 Water inlet end be connected by pipeline with reaction staving 18 bottom, and the water outlet of water circulating pump 7 by pipeline and magnetizer 5 into The mouth of a river connects.
For the ease of 13 fixed component of first support 6 and second support, in the present embodiment, it is preferred that first support 6 is L Type structure, second support 13 are F type structures.
In order to realize that deflector 10 plays the role of water conservancy diversion, in the present embodiment, it is preferred that the angle of inclination of deflector 10 is 15°。
For the ease of 7 steady operation of water circulating pump, in the present embodiment, it is preferred that water circulating pump 7 passes through with first support 6 Bolt is fixedly connected.
Operation principle:In the use of the present invention, worker first switches it on external power supply, and pass through controller 14 and open equipment Power supply, equipment start-up operation at this time, worker opens the solenoid valve 22 of water inlet by controller 14 again, by external water by water inlet pipe 21 It adds in reaction staving 18, when adding in a timing, worker is closed the solenoid valve 22 of water inlet by controller 14, then passes through control Device 14 processed opens the solenoid valve 22 inside the first liquid feeding bucket 2, and sulfonating agent is added by the first liquid feeding bucket 2 in reaction staving 18, When adding in a timing, worker is closed the solenoid valve 22 inside the first liquid feeding bucket 2 by controller 14, realizes quantitative liquid feeding, together When stirring motor 1 work under control of the controller 14 rotation, and pass through agitating shaft 20 and paddle 3 driven to rotate, with to reaction Solution is stirred in staving 18, promotes solution hybrid reaction, after a certain period of time, worker passes through 14 control loop of controller for reaction The work of water pump 7 rotates, and reaction solution in reaction staving 18 is extracted out, and by pipeline into magnetizer 5, magnetizer 5 exists It is powered under the control of controller 14 and generates magnetic field, solution flows through magnetic field and physical change occurs, to achieve the purpose that solution magnetization, magnetic After change, solution is input into through delivery pipe 4 in reaction staving 18, at this point, worker is opened by controller 14 inside the second liquid feeding bucket 23 Solenoid valve 22, ketone compounds are quantitatively added by the second liquid feeding bucket 23 in reaction staving 18, while worker passes through temperature controller Electrical heating block 15 in 12 control heating layers 16 carries out electrified regulation, when being heated to certain temperature, reacts ketone in staving 18 It closes object and carries out sulfonation reflux reaction, after a certain period of time, worker opens the electricity inside the 3rd liquid feeding bucket 24 by controller 14 for reaction Magnet valve 22 is added in aldehyde compound in reaction staving 18 by the 3rd liquid feeding bucket 24, while worker controls electricity by temperature controller 12 Heat block 15 continues to heat, and when being heated to solution reaction required temperature, aldehyde compound and mixed solution are in the stirring of paddle 3 Uniform hybrid reaction under effect, after a certain period of time, worker pulls blanking lock 8 for reaction, the fat of completion will be reacted in reaction staving 18 Fat race sulfonate water reducer is discharged by tremie pipe 9, that is, the magnetization reaction for completing aliphatic sulfonate water-reducing agent makes, and water-reducing agent is anti- It answers in manufacturing process, deflector 10 plays the role of solution water conservancy diversion, changes solution fluidised form, promotes water-reducing agent fast by tremie pipe 9 Speed discharge.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace And modification, the scope of the present invention is defined by the appended.

Claims (5)

1. aliphatic sulfonate water-reducing agent magnetizes reaction system, including reaction staving (18), it is characterised in that:The reaction staving (18) middle position of upper surface is fixed with stirring motor (1), and the bottom for reacting staving (18) is equipped with supporting rack (11), The bottom of the stirring motor (1) is connected with agitating shaft (20), and equidistant on agitating shaft (20) is equipped with three paddles (3), the one side of support frame as described above (11) is connected with first support (6), and supporting rack (11) is compared with the one side of first support (6) It is connected with second support (13), reaction staving (18) upper surface is equipped with the at a side position of stirring motor (1) One liquid feeding bucket (2) and the 3rd liquid feeding bucket (24), and staving (18) upper surface is reacted compared with the first liquid feeding bucket (2) and the 3rd liquid feeding The one side of bucket (24) is equipped with water inlet pipe (21) and the second liquid feeding bucket (23), and the first liquid feeding bucket (2) is located at the 3rd liquid feeding bucket (24) front side, the water inlet pipe (21) are located at the front side of the second liquid feeding bucket (23), the first liquid feeding bucket (2), water inlet pipe (21), the second liquid feeding bucket (23) and the 3rd liquid feeding bucket (24) and the inside of reaction staving (18) junction are both provided with solenoid valve (22), reaction staving (18) one side is equipped with purge valve (19), and reaction container close to the lower position of water inlet pipe (21) It is provided with thermal insulation layer (17) on the inner wall of body (18), and thermal insulation layer (17) is internally provided with heating layer (16), the heating layer (16) inside is equidistant to be equipped with several electrical heating blocks (15), and the internal two bottom sides of the reaction staving (18) are symmetrically set It puts there are three deflector (10), and the middle position for reacting staving (18) bottom is connected with tremie pipe (9), the tremie pipe (9) upper semisection is equipped with blanking lock (8), and the upper surface of the first support (6) is equipped with water circulating pump (7), and first Frame (6) upper surface is fixed with magnetizer (5) at the rearward position of water circulating pump (7), and the water outlet of the magnetizer (5) leads to Delivery pipe (4) is crossed with being connected at the top of reaction staving (18), the upper surface of the second support (13) is equipped with controller (14), and the inside of second support (13) is equipped with temperature controller (12), and the electrical heating block (15) electrically connects with temperature controller (12) It connects, the stirring motor (1), magnetizer (5), water circulating pump (7) and solenoid valve (22) are electrically connected with controller (14), institute Temperature controller (12) and controller (14) is stated to be electrically connected with external power supply.
2. aliphatic sulfonate water-reducing agent according to claim 1 magnetizes reaction system, it is characterised in that:The recirculated water The water inlet end for pumping (7) is connected by pipeline with reaction staving (18) bottom, and the water outlet of water circulating pump (7) passes through pipeline and magnetic The water inlet connection of change machine (5).
3. aliphatic sulfonate water-reducing agent according to claim 1 magnetizes reaction system, it is characterised in that:Described first Frame (6) is L-type structure, and second support (13) is F type structures.
4. aliphatic sulfonate water-reducing agent according to claim 1 magnetizes reaction system, it is characterised in that:The deflector (10) angle of inclination is 15 °.
5. aliphatic sulfonate water-reducing agent according to claim 1 magnetizes reaction system, it is characterised in that:The recirculated water Pump (7) is bolted to connection with first support (6).
CN201711418484.1A 2017-12-25 2017-12-25 Magnetization reaction system for aliphatic sulfonate water reducer Active CN108114679B (en)

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CN108114679B CN108114679B (en) 2024-02-13

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110368883A (en) * 2019-06-21 2019-10-25 枣阳市金鹏化工有限公司 A kind of reaction kettle producing organosilicon

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN204365190U (en) * 2015-01-07 2015-06-03 昌吉市力和精细化工厂 High performance water reducing agent of polyocarboxy acid production system
CN205379900U (en) * 2016-03-16 2016-07-13 四川恒泽建材有限公司 Automatic liquid agitating unit that mixes of water -reducing agent
CN205391354U (en) * 2016-02-27 2016-07-27 李金斌 Traditional chinese medicine decocting machine
CN206526745U (en) * 2017-03-07 2017-09-29 吉安民辉新型材料有限公司 For producing the energy-saving automatic batch mixing stirred tank of water reducer
CN207786569U (en) * 2017-12-25 2018-08-31 英德市竣冠新型材料有限公司 Aliphatic sulfonate water-reducing agent magnetizes reaction system

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN204365190U (en) * 2015-01-07 2015-06-03 昌吉市力和精细化工厂 High performance water reducing agent of polyocarboxy acid production system
CN205391354U (en) * 2016-02-27 2016-07-27 李金斌 Traditional chinese medicine decocting machine
CN205379900U (en) * 2016-03-16 2016-07-13 四川恒泽建材有限公司 Automatic liquid agitating unit that mixes of water -reducing agent
CN206526745U (en) * 2017-03-07 2017-09-29 吉安民辉新型材料有限公司 For producing the energy-saving automatic batch mixing stirred tank of water reducer
CN207786569U (en) * 2017-12-25 2018-08-31 英德市竣冠新型材料有限公司 Aliphatic sulfonate water-reducing agent magnetizes reaction system

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110368883A (en) * 2019-06-21 2019-10-25 枣阳市金鹏化工有限公司 A kind of reaction kettle producing organosilicon

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