CN108106967A - A kind of method for judging lithium ion battery glue dispersion effect - Google Patents

A kind of method for judging lithium ion battery glue dispersion effect Download PDF

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Publication number
CN108106967A
CN108106967A CN201611054825.7A CN201611054825A CN108106967A CN 108106967 A CN108106967 A CN 108106967A CN 201611054825 A CN201611054825 A CN 201611054825A CN 108106967 A CN108106967 A CN 108106967A
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CN
China
Prior art keywords
glue
wide
solid content
mouth bottle
dispersion effect
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Pending
Application number
CN201611054825.7A
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Chinese (zh)
Inventor
黄锐升
黄艳
李国敏
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shenzhen Green's Moral Ltd Energy Co
Huizhou University
Original Assignee
Shenzhen Green's Moral Ltd Energy Co
Huizhou University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shenzhen Green's Moral Ltd Energy Co, Huizhou University filed Critical Shenzhen Green's Moral Ltd Energy Co
Priority to CN201611054825.7A priority Critical patent/CN108106967A/en
Publication of CN108106967A publication Critical patent/CN108106967A/en
Pending legal-status Critical Current

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Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N11/00Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume, or surface-area of porous materials
    • G01N2015/0023Investigating dispersion of liquids
    • G01N2015/003Investigating dispersion of liquids in liquids, e.g. emulsion

Abstract

A kind of method for judging lithium ion battery glue dispersion effect, comprises the following steps:(1)Prepare positive and negative anodes glue;(2)A certain amount of glue is taken to beat slowly and into wide-mouth bottle and is sealed room temperature preservation, stand 24~48 it is small when, test and gelatin viscosity and recorded when 4 is small;(3)With infrared lamp light through wide-mouth bottle glue, go out from the vertical direction of incident light in wide-mouth bottle glue whether one existing bright " access ";(4)Glue is divided into 10~20 parts to other containers and tests solid content, makes solid content distribution map.Present invention has the advantages that by the way that glue, the solid content of different position, Tyndall phenomenon and viscosity three broad aspects that change with time determine the dispersion effect of positive and negative electrode glue and provide a kind of method of simple possible in stirring container, and this method is simple, device simple is simultaneously effective, it is easy to operate, quickly glue dispersion effect can be judged.

Description

A kind of method for judging lithium ion battery glue dispersion effect
Technical field
The invention mainly relates to technical field of lithium ion, disperse more particularly, to a kind of judgement lithium ion battery glue The method of effect.
Background technology
Lithium ion battery has operating voltage high, and higher than energy, capacity is big, and self discharge is small, good cycle, service life It is long, it is light-weight the advantages that, have become the light-weighted critical energy component of electric vehicle, be the representative of modern high performance battery, It is the major impetus source of the ideal source of the portable electric appts such as mobile phone, laptop, cordless power tool etc. One of.For lithium ion battery production, the preparation of glue is crucial first of battery production before anode and cathode slurry is prepared Process directly affects electrode and battery quality and performance, such as battery capacity, the uniformity of internal resistance, the quality of cycle performance etc.. In order to ensure the quality of lithium ion battery, it is of great significance to good and bad judge of its positive and negative anodes glue quality.
The content of the invention
The present invention be directed to above-mentioned backgrounds to propose a kind of method for judging lithium ion battery glue dispersion effect, and purpose exists Judge lithium ion battery plus-negative plate glue dispersion effect quality method in providing, the quality for improving lithium ion battery is consistent with battery Property.
The technical solution adopted by the present invention is:
A kind of method for judging lithium ion battery glue dispersion effect, specifically includes following steps:
(1)According to itself company's system formulation proportion requirement, positive and negative anodes glue is prepared using a mixing bowl;
(2)From a mixing bowl just prepared glue, take a certain amount of glue beat slowly into wide-mouth bottle and be sealed room temperature guarantor It deposits, when standing 24~48 is small(The common preservation usage time of battery industry glue), gelatin viscosity is tested when 4 is small and is carried out Whether record, see the viscosity within the production time in the range of technique mark;
(3)With infrared lamp light through wide-mouth bottle glue, go out from the vertical direction of incident light in wide-mouth bottle glue whether One existing bright " access ", have " access " glue is then colloid, represents to be uniformly dispersed, does not have the glue of " access " then For solution, scattered unevenness is represented;
(4)The glue of a mixing bowl is divided into 10~20 parts to other containers and tests solid content, makes solid content distribution map, Solid content is scattered more uniform closer to representing.Since when glue is uniformly dispersed, the glue in a mixing bowl different position, i.e. average mark It should be consistent to the glue solid content of other containers into several pieces.
The beneficial effects of the present invention are:By the way that glue, the solid content of different position, dindar are existing in stirring container As and viscosity three broad aspects that change with time determine the dispersion effect of positive and negative electrode glue and provide a kind of side of simple possible Method, and detection method is simple, device simple is simultaneously effective, easy to operate, and quickly glue dispersion effect can be sentenced It is fixed, excessive glue is avoided to prepare waste and glue Quality Detection waste of time of mixing time etc..
Description of the drawings
Fig. 1 is trend chart when gelatin viscosity 48 is small.
Fig. 2 is " access " schematic diagram that infrared ray tests glue.
Fig. 3 is that the glue of a mixing bowl is divided into the solid content schematic diagram tested after 20 parts of parts.
Specific embodiment
Below in conjunction with the embodiment of the present invention and attached drawing, the technical solution in the embodiment of the present invention is carried out clear, complete Ground describes, it is clear that described embodiment is only part of the embodiment of the present invention, instead of all the embodiments.Based on this hair Embodiment in bright, ordinary skill and technologist obtained without making creative work it is all its His embodiment, belongs to the scope of protection of the invention.
Embodiment 1
(1)According to itself company's system formulation proportion requirement, positive and negative anodes glue is prepared using a mixing bowl;
(2)From a mixing bowl just prepared glue, take a certain amount of glue beat slowly into wide-mouth bottle and be sealed room temperature guarantor It deposits, gelatin viscosity is tested when 4 is small when standing 24 is small and is recorded, viscosity is qualified to be uniformly dispersed for judgement;
(3)With infrared lamp light through wide-mouth bottle glue, go out from the vertical direction of incident light in wide-mouth bottle glue whether One existing bright " access ", have " access " glue is then colloid, represents to be uniformly dispersed;
(4)The glue of a mixing bowl is divided into 10 parts to other containers and tests solid content, makes solid content distribution map, admittedly contain Amount can determine that in technological standards to be uniformly dispersed.
Embodiment 2
(1)According to itself company's system formulation proportion requirement, positive and negative anodes glue is prepared using a mixing bowl;
(2)From a mixing bowl just prepared glue, take a certain amount of glue beat slowly into wide-mouth bottle and be sealed room temperature guarantor It deposits, gelatin viscosity is tested when 4 is small when standing 36 is small and is recorded, viscosity is qualified to be uniformly dispersed for judgement;
(3)With infrared lamp light through wide-mouth bottle glue, go out from the vertical direction of incident light in wide-mouth bottle glue whether One existing bright " access ", have " access " glue is then colloid, represents to be uniformly dispersed;
(4)The glue of a mixing bowl is divided into 15 parts to other containers and tests solid content, makes solid content distribution map, admittedly contain Amount can determine that in technological standards to be uniformly dispersed.
Embodiment 3
(1)According to itself company's system formulation proportion requirement, positive and negative anodes glue is prepared using a mixing bowl;
(2)From a mixing bowl just prepared glue, take a certain amount of glue beat slowly into wide-mouth bottle and be sealed room temperature guarantor It deposits, gelatin viscosity is tested when 4 is small when standing 48 is small and is recorded, viscosity is qualified to be uniformly dispersed for judgement;
(3)With infrared lamp light through wide-mouth bottle glue, go out from the vertical direction of incident light in wide-mouth bottle glue whether One existing bright " access ", have " access " glue is then colloid, represents to be uniformly dispersed;
(4)The glue of a mixing bowl is divided into 20 parts to other containers and tests solid content, makes solid content distribution map, admittedly contain Amount can determine that in technological standards to be uniformly dispersed.
More than content is only to design example and explanation of the invention, affiliated those skilled in the art Various modifications or additions are done to described specific embodiment or are substituted in a similar way, without departing from invention Design or surmount scope defined in the claims, be within the scope of protection of the invention.

Claims (1)

  1. A kind of 1. method for judging lithium ion battery glue dispersion effect, which is characterized in that this method specifically includes following steps:
    (1)According to itself company's system formulation proportion requirement, positive and negative anodes glue is prepared using a mixing bowl;
    (2)From a mixing bowl just prepared glue, take a certain amount of glue beat slowly into wide-mouth bottle and be sealed room temperature guarantor Deposit, stand 24~48 it is small when, test and gelatin viscosity and recorded when 4 is small, see viscosity within the production time whether In the range of technique mark;
    (3)With infrared lamp light through wide-mouth bottle glue, go out from the vertical direction of incident light in wide-mouth bottle glue whether One existing bright " access ", have " access " glue is then colloid, represents to be uniformly dispersed, does not have the glue of " access " then For solution, scattered unevenness is represented;
    (4)The glue of a mixing bowl is divided into 10~20 parts to other containers and tests solid content, makes solid content distribution map, Solid content is scattered more uniform closer to representing.
CN201611054825.7A 2016-11-25 2016-11-25 A kind of method for judging lithium ion battery glue dispersion effect Pending CN108106967A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611054825.7A CN108106967A (en) 2016-11-25 2016-11-25 A kind of method for judging lithium ion battery glue dispersion effect

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611054825.7A CN108106967A (en) 2016-11-25 2016-11-25 A kind of method for judging lithium ion battery glue dispersion effect

Publications (1)

Publication Number Publication Date
CN108106967A true CN108106967A (en) 2018-06-01

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CN201611054825.7A Pending CN108106967A (en) 2016-11-25 2016-11-25 A kind of method for judging lithium ion battery glue dispersion effect

Country Status (1)

Country Link
CN (1) CN108106967A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109211714A (en) * 2018-10-31 2019-01-15 桑顿新能源科技有限公司 A kind of evaluation method of pulp of lithium ion battery stability
CN113358603A (en) * 2021-06-04 2021-09-07 中国核动力研究设计院 Solution uniformity evaluation device and method

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20010046461A (en) * 1999-11-12 2001-06-15 조충환 The gel electrolyte for a sealed lead storage battery
CN101551369A (en) * 2008-03-31 2009-10-07 深圳市比克电池有限公司 Method for testing sizing agent consistency and coating roller
CN102354756A (en) * 2011-11-03 2012-02-15 湖南丰源业翔晶科新能源股份有限公司 Burdening technology for slurry used by nanometer ferrous phosphate lithium ion battery
CN104577071A (en) * 2015-01-28 2015-04-29 山东齐星新能源科技有限责任公司 Dry-powder pulping method of lithium-ion battery
CN105449205A (en) * 2015-12-17 2016-03-30 山东精工电子科技有限公司 Preparation method for waterborne lithium iron phosphate slurry
CN106124363A (en) * 2016-07-14 2016-11-16 曙鹏科技(深圳)有限公司 A kind of evaluating method of lithium ion battery plus-negative plate Stability of Slurry

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20010046461A (en) * 1999-11-12 2001-06-15 조충환 The gel electrolyte for a sealed lead storage battery
CN101551369A (en) * 2008-03-31 2009-10-07 深圳市比克电池有限公司 Method for testing sizing agent consistency and coating roller
CN102354756A (en) * 2011-11-03 2012-02-15 湖南丰源业翔晶科新能源股份有限公司 Burdening technology for slurry used by nanometer ferrous phosphate lithium ion battery
CN104577071A (en) * 2015-01-28 2015-04-29 山东齐星新能源科技有限责任公司 Dry-powder pulping method of lithium-ion battery
CN105449205A (en) * 2015-12-17 2016-03-30 山东精工电子科技有限公司 Preparation method for waterborne lithium iron phosphate slurry
CN106124363A (en) * 2016-07-14 2016-11-16 曙鹏科技(深圳)有限公司 A kind of evaluating method of lithium ion battery plus-negative plate Stability of Slurry

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109211714A (en) * 2018-10-31 2019-01-15 桑顿新能源科技有限公司 A kind of evaluation method of pulp of lithium ion battery stability
CN113358603A (en) * 2021-06-04 2021-09-07 中国核动力研究设计院 Solution uniformity evaluation device and method

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Address after: 518105 4th Floor, Building A2, Liyuan Bay Industrial Park, 168 Honghu Road, Yanchuan, Songgang, Baoan District, Shenzhen City, Guangdong Province

Applicant after: Shenzhen Greende Energy Group Co., Ltd.

Applicant after: Huizhou College

Address before: 518105 4th Floor, Building A2, Liyuan Bay Industrial Park, 168 Honghu Road, Yanchuan, Songgang, Baoan District, Shenzhen City, Guangdong Province

Applicant before: Shenzhen Green's moral limited energy company

Applicant before: Huizhou College

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Application publication date: 20180601

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