CN108096870A - A kind of recycling device of DMAC - Google Patents

A kind of recycling device of DMAC Download PDF

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Publication number
CN108096870A
CN108096870A CN201810081539.2A CN201810081539A CN108096870A CN 108096870 A CN108096870 A CN 108096870A CN 201810081539 A CN201810081539 A CN 201810081539A CN 108096870 A CN108096870 A CN 108096870A
Authority
CN
China
Prior art keywords
hole
collecting box
sealing
plug
outside
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810081539.2A
Other languages
Chinese (zh)
Inventor
张立兴
刘萌萌
刘玉花
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tianjin Hengsheng Canada Technology Development Co Ltd
Original Assignee
Tianjin Hengsheng Canada Technology Development Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tianjin Hengsheng Canada Technology Development Co Ltd filed Critical Tianjin Hengsheng Canada Technology Development Co Ltd
Priority to CN201810081539.2A priority Critical patent/CN108096870A/en
Publication of CN108096870A publication Critical patent/CN108096870A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0003Condensation of vapours; Recovering volatile solvents by condensation by using heat-exchange surfaces for indirect contact between gases or vapours and the cooling medium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0033Other features
    • B01D5/0051Regulation processes; Control systems, e.g. valves
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0057Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
    • B01D5/006Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with evaporation or distillation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0078Condensation of vapours; Recovering volatile solvents by condensation characterised by auxiliary systems or arrangements
    • B01D5/009Collecting, removing and/or treatment of the condensate
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00Preparation of carboxylic acid amides
    • C07C231/22Separation; Purification; Stabilisation; Use of additives
    • C07C231/24Separation; Purification

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Automation & Control Theory (AREA)
  • Filling Or Discharging Of Gas Storage Vessels (AREA)

Abstract

The invention discloses a kind of recycling devices of DMAC, including installing plate, two stents are welded at the top of the installing plate, same collecting box is welded at the top of two stents, collecting box is arranged to hollow structure, first through hole is offered at the top of collecting box, fixing sleeve is equipped with conduit in first through hole, and one end of conduit is extended to outside collecting box, the one side of first through hole offers the second through hole, fixing sleeve is equipped with thermometer in second through hole, and is all extended at the top and bottom of thermometer outside the second through hole.The configuration of the present invention is simple, it is easy to operate, during ice water is used to condense dimethylacetamide amine gas, when ice water rises to a certain extent by the temperature in use of certain time, automatically audible-visual annunciator can be controlled to alarm, people is reminded timely to replace ice water, are effectively guaranteed the condensation effect of dimethylacetamide amine gas.

Description

A kind of recycling device of DMAC
Technical field
Patent of the present invention is related to wastewater collection technical field more particularly to a kind of recycling device of DMAC.
Background technology
With the development and progress of chemical industry, people are more and more deep in the exploration of chemical field, with variousization The synthesis of work material, the Industry Waste aqueous of various high concentrations generate therewith, and dimethyl acetamide (DMAC) is as important chemical industry Raw material is applied to the industries such as polyurethane, chemical fibre, therefore containing substantial amounts of in the waste water that generates during the production of these industries Dimethyl acetamide, these waste water for containing dimethyl acetamide, which can recycle, to be recycled.
At present, the recycling device of dimethyl acetamide is all by adding to the waste water containing dimethyl acetamide Heat, then by controlling temperature that dimethyl acetamide is made to be evaporated from waste water, then again using ice water to dimethylacetamide Amine gas are condensed to realize recycling for dimethyl acetamide, cold ice water is used to carry out dimethylacetamide amine gas In solidifying process, since the temperature of ice water can be raised slowly, timely ice water is replaced, but existing technology In, all it is that ice water is replaced by artificial estimation, the replacement for causing ice water not in time, causes dimethyl acetamide gas The condensation effect of body is bad, therefore patent of the present invention proposes solution on this question.
Patent of invention content
The purpose of patent of the present invention is and the cycling of a kind of DMAC proposed in order to solve shortcoming in the prior art Utilize device.
To achieve these goals, patent of the present invention employs following technical solution:
A kind of recycling device of DMAC including installing plate, is welded with two stents at the top of the installing plate, two Same collecting box is welded at the top of stent, collecting box is arranged to hollow structure, first through hole is offered at the top of collecting box, Fixing sleeve is equipped with conduit in first through hole, and one end of conduit is extended to outside collecting box, and the one side of first through hole offers second Through hole, fixing sleeve is equipped with thermometer in the second through hole, and is all extended at the top and bottom of thermometer outside the second through hole, collecting box One side be equipped with and be fixedly mounted on hutch at the top of installing plate, hutch is arranged to hollow structure, is opened up at the top of hutch There is third through-hole, one end that conduit is located at outside collecting box is run through third through-hole and extended in hutch, and the top of hutch is consolidated Fixed to be equipped with the cooling cylinder being set in outside conduit, the one side of conduit is equipped with the fourth hole being opened at the top of cooling cylinder, fourth hole Interior fixing sleeve is equipped with temperature sensor, and is all extended at the top and bottom of temperature sensor outside fourth hole, the hutch One side away from collecting box is equipped with power supply, control processor and the audible-visual annunciator being fixedly mounted on successively at the top of installing plate.
Preferably, the mounting blocks being fixedly mounted at the top of installing plate are equipped between two stents, the top of mounting blocks is fixed Heat block is installed, and the top of heat block and the bottom connection of collecting box touch, heat block is specially that the electricity of regulating power adds Heat block.
Preferably, the first charging hole is offered at the top of the collecting box, the first sealing-plug is arranged in the first charging hole, And first extends to outside the first charging hole at the top of sealing-plug, the one side of collecting box offers the first discharge hole, the first discharge hole The second sealing-plug is inside arranged with, and the one side of the second sealing-plug is extended to outside collecting box.
Preferably, the first sealing ring is arranged in the first through hole, conduit is set in the first sealing ring, the second through hole The second sealing-plug is inside arranged with, thermometer wrap is located in the second sealing ring, and the 3rd sealing ring, sheathed catheter are arranged in third through-hole It is located in the 3rd sealing ring, the 4th sealing ring is arranged in fourth hole, temperature sensor is set in the 4th sealing ring.
Preferably, one side of the hutch away from collecting box offers the second discharge hole, is arranged in the second discharge hole 3rd sealing-plug, and the one side of the 3rd sealing-plug is extended to outside hutch.
Preferably, one side of the conduit away from temperature sensor is equipped with the second charging hole being opened at the top of cooling cylinder, The 4th sealing-plug is arranged in second charging hole, and is extended at the top of the 4th sealing-plug outside the second charging hole, cooling cylinder it is remote One side from collecting box offers the 3rd discharge hole, and the 5th sealing-plug, and the one of the 5th sealing-plug are arranged in the 3rd discharge hole Side is extended to outside cooling cylinder.
Preferably, the output terminal of the power supply is electrically connected and is formed into a loop with control processor, control processor difference It is electrically connected and is formed into a loop with temperature sensor and audible-visual annunciator.
Compared with prior art, the advantageous effect of patent of the present invention is:
In patent of the present invention, pass through installing plate, stent, collecting box, first through hole, conduit, the second through hole, thermometer, storage Case, third through-hole, cooling cylinder, fourth hole, temperature sensor, power supply, control processor and audible-visual annunciator is hidden to be engaged, when During being condensed using ice water to dimethylacetamide amine gas, ice water rises to certain journey by the temperature in use of certain time When spending, automatically audible-visual annunciator can be controlled to alarm, people is reminded timely to replace ice water, are effectively guaranteed diformazan The condensation effect of yl acetamide gas, patent structure of the present invention is simple, easy to operate, when using ice water to dimethyl acetamide gas During body condenses, when ice water is risen to a certain extent by the temperature in use of certain time, acousto-optic can be automatically controlled Alarm is alarmed, and people is reminded timely to replace ice water, are effectively guaranteed the condensation effect of dimethylacetamide amine gas.
Description of the drawings
Fig. 1 is a kind of schematic cross-sectional view of the main view of the recycling device for DMAC that patent of the present invention proposes;
Fig. 2 is a kind of schematic cross-sectional view of the part A of the recycling device for DMAC that patent of the present invention proposes.
In figure:1 installing plate, 2 stents, 3 collecting boxs, 4 first through hole, 5 conduits, 6 second through holes, 7 thermometers, 8 hutch, 9 third through-holes, 10 cooling cylinders, 11 fourth holes, 12 temperature sensors, 13 power supplys, 14 control processors, 15 audible-visual annunciators.
Specific embodiment
Below in conjunction with the attached drawing in patent Example of the present invention, the technical solution in patent Example of the present invention is carried out It clearly and completely describes, it is clear that described embodiment is only patent part of the embodiment of the present invention rather than whole Embodiment.
With reference to Fig. 1-2, a kind of recycling device of DMAC, including installing plate 1, the top of installing plate 1 is welded with two Stent 2, the top of two stents 2 are welded with same collecting box 3, and collecting box 3 is arranged to hollow structure, the top of collecting box 3 First through hole 4 is offered, fixing sleeve is equipped with conduit 5 in first through hole 4, and one end of conduit 5 is extended to outside collecting box 3, and first The one side of through hole 4 offers the second through hole 6, and fixing sleeve is equipped with thermometer 7, and the top and bottom of thermometer 7 in the second through hole 6 It all extends to outside the second through hole 6, the one side of collecting box 3 is equipped with the hutch 8 for being fixedly mounted on 1 top of installing plate, and hutch 8 is set Hollow structure is set to, the top of hutch 8 offers third through-hole 9, and threeway is run through in one end that conduit 5 is located at outside collecting box 3 Hole 9 is simultaneously extended in hutch 8, and the top of hutch 8 is fixed with the cooling cylinder 10 being set in outside conduit 5, the one side of conduit 5 Equipped with the fourth hole 11 for being opened in 10 top of cooling cylinder, fixing sleeve is equipped with temperature sensor 12, and temperature in fourth hole 11 The top and bottom of sensor 12 are all extended to outside fourth hole 11, and one side of the hutch 10 away from collecting box 3 is equipped with solid successively It by installing plate 1, stent 2, is collected mounted in power supply 13, control processor 14 and the audible-visual annunciator 15 at 1 top of installing plate Dingan County Case 3, first through hole 4, conduit 5, the second through hole 6, thermometer 7, hutch 8, third through-hole 9, cooling cylinder 10, fourth hole 11, Temperature sensor 12, power supply 13 and control processor 14 and audible-visual annunciator 15 are engaged, when using ice water to dimethylacetamide During amine gas condense, when ice water is risen to a certain extent by the temperature in use of certain time, can automatically it control Audible-visual annunciator 16 is alarmed, and people is reminded timely to replace ice water, are effectively guaranteed the cold of dimethylacetamide amine gas Solidifying effect, patent structure of the present invention is simple, easy to operate, during ice water is used to condense dimethylacetamide amine gas, When ice water is risen to a certain extent by the temperature in use of certain time, audible-visual annunciator 16 can automatically be controlled to be reported It is alert, people is reminded timely to replace ice water, are effectively guaranteed the condensation effect of dimethylacetamide amine gas.
The mounting blocks for being fixedly mounted on 1 top of installing plate are equipped in patent of the present invention, between two stents 2, mounting blocks Top is installed with heat block, and the top of heat block and the bottom connection of collecting box 3 touch, and heat block is specially adjustable work( The electrical heating block of rate, the top of collecting box 3 offer the first charging hole, and the first sealing-plug, and are arranged in the first charging hole It is extended at the top of one sealing-plug outside the first charging hole, the one side of collecting box 3 offers the first discharge hole, the first discharge hole inner sleeve One side equipped with the second sealing-plug, and the second sealing-plug is extended to outside collecting box 3, and the first sealing ring is arranged in first through hole 4, Conduit 5 is set in the first sealing ring, and the second sealing-plug is arranged in the second through hole 6, and thermometer 7 is set in the second sealing ring It is interior, the 3rd sealing ring is arranged in third through-hole 9, conduit 5 is set in the 3rd sealing ring, and the 4th is arranged in fourth hole 11 Sealing ring, temperature sensor 12 are set in the 4th sealing ring, and one side of the hutch 8 away from collecting box 3 offers the second discharging Hole is arranged with the 3rd sealing-plug in the second discharge hole, and the one side of the 3rd sealing-plug is extended to outside hutch 8, and conduit 5 is away from temperature The one side of degree sensor 12 is equipped with the second charging hole for being opened in 10 top of cooling cylinder, and the 4th sealing is arranged in the second charging hole Plug, and extended at the top of the 4th sealing-plug outside the second charging hole, the one side of the separate collecting box 3 of cooling cylinder 10 offers the 3rd Discharge hole is arranged with the 5th sealing-plug in the 3rd discharge hole, and the one side of the 5th sealing-plug is extended to outside cooling cylinder 10, power supply 13 Output terminal be electrically connected and be formed into a loop with control processor 14, control processor 14 respectively with temperature sensor 12 and acousto-optic Alarm 15 is electrically connected and is formed into a loop, and passes through installing plate 1, stent 2, collecting box 3, first through hole 4, conduit 5, the second through hole 6th, thermometer 7, hutch 8, third through-hole 9, cooling cylinder 10, fourth hole 11, temperature sensor 12, power supply 13 and control process Device 14 and audible-visual annunciator 15 are engaged, and during ice water is used to condense dimethylacetamide amine gas, ice water passes through one When the temperature in use fixed time is risen to a certain extent, audible-visual annunciator 16 can automatically be controlled to alarm, remind people Ice water is timely replaced, is effectively guaranteed the condensation effect of dimethylacetamide amine gas, patent structure of the present invention is simple, operation Convenient, during ice water is used to condense dimethylacetamide amine gas, ice water rises by the temperature in use of certain time When to a certain extent, audible-visual annunciator 16 can automatically be controlled to alarm, people be reminded timely to replace ice water, effectively It ensure that the condensation effect of dimethylacetamide amine gas.
Operation principle:In use, working as needs to recycle the waste water containing dimethyl acetamide in collecting box 3 When, start heat block first, heat block heats the waste water containing dimethyl acetamide, by observing the reading on thermometer 7 Number adjusts the power of heat block, the waste water temperature containing dimethyl acetamide is made to be maintained in suitable scope, second containing dimethyl The waste water of amide gasifies by heating, dimethyl acetamide, and the gas of dimethyl acetamide is flowed by conduit 5 at this time Outside collecting box 3, then dimethylacetamide amine gas are condensed by the ice water in cooling cylinder 10, by the dimethyl of condensation Acetamide gas liquefaction is flowed under gravity in hutch 8, and the ice water in cooling cylinder 10 makes by certain time It can be risen with temperature afterwards, when the temperature of ice water rises to a certain extent, temperature sensor 12 is passed information at control Device 14 is managed, the control of control processor 14 starts audible-visual annunciator 15 and carries out sound-light alarm, people is reminded to replace ice water, are had Effect improves the promptness of ice water replacement.
The above is only the preferable specific embodiment of patent of the present invention, but the protection domain of patent of the present invention is not This is confined to, any one skilled in the art is in the technical scope of patent diselosesll of the present invention, according to the present invention Technical solution and its patent of invention design of patent are subject to equivalent substitution or change, should all cover the protection model in patent of the present invention Within enclosing.

Claims (7)

  1. A kind of 1. recycling device of DMAC, including installing plate (1), which is characterized in that the top welding of the installing plate (1) There are two stent (2), same collecting box (3) is welded at the top of two stents (2), collecting box (3) is arranged to hollow structure, First through hole (4) is offered at the top of collecting box (3), first through hole (4) interior fixing sleeve is equipped with conduit (5), and the one of conduit (5) End extends to collecting box (3) outside, and the one side of first through hole (4) offers the second through hole (6), fixes and is arranged in the second through hole (6) There is thermometer (7), and the second through hole (6) is all extended to outside at the top and bottom of thermometer (7), the one side of collecting box (3) is equipped with The hutch (8) being fixedly mounted at the top of installing plate (1), hutch (8) are arranged to hollow structure, and hutch is opened at the top of (8) Equipped with third through-hole (9), conduit (5) is located at the one end of collecting box (3) outside through third through-hole (9) and extends to hutch (8) It is interior, it is fixed at the top of hutch (8) and is set in the cooling cylinder (10) of conduit (5) outside, the one side of conduit (5), which is equipped with, to be opened in Fourth hole (11) at the top of cooling cylinder (10), fourth hole (11) interior fixing sleeve is equipped with temperature sensor (12), and temperature passes Fourth hole (11) is all extended at the top and bottom of sensor (12) outside, one side of the hutch (10) away from collecting box (3) Equipped with the power supply (13), control processor (14) and audible-visual annunciator (15) being fixedly mounted on successively at the top of installing plate (1).
  2. 2. the recycling device of a kind of DMAC according to claim 1, which is characterized in that set between two stents (2) There are the mounting blocks being fixedly mounted at the top of installing plate (1), heat block, and the top of heat block are installed at the top of mounting blocks It is touched with the bottom connection of collecting box (3), heat block is specially the electrical heating block of regulating power.
  3. A kind of 3. recycling device of DMAC according to claim 1, which is characterized in that the top of the collecting box (3) Portion offers the first charging hole, and the first sealing-plug is arranged in the first charging hole, and extends to first at the top of the first sealing-plug Outside charging hole, the one side of collecting box (3) offers the first discharge hole, and the second sealing-plug, and second are arranged in the first discharge hole The one side of sealing-plug extends to collecting box (3) outside.
  4. 4. the recycling device of a kind of DMAC according to claim 1, which is characterized in that in the first through hole (4) The first sealing ring is arranged with, conduit (5) is set in the first sealing ring, and the second sealing-plug, temperature are arranged in the second through hole (6) Meter (7) is set in the second sealing ring, is arranged with the 3rd sealing ring in third through-hole (9), conduit (5) is set in the 3rd sealing ring It is interior, the 4th sealing ring is arranged in fourth hole (11), temperature sensor (12) is set in the 4th sealing ring.
  5. 5. the recycling device of a kind of DMAC according to claim 1, which is characterized in that the hutch (8) is separate The one side of collecting box (3) offers the second discharge hole, and the 3rd sealing-plug, and the one of the 3rd sealing-plug are arranged in the second discharge hole Side extends to hutch (8) outside.
  6. 6. the recycling device of a kind of DMAC according to claim 1, which is characterized in that the conduit (5) is away from temperature The one side of degree sensor (12) is equipped with the second charging hole being opened at the top of cooling cylinder (10), and the 4th is arranged in the second charging hole Sealing-plug, and extended at the top of the 4th sealing-plug outside the second charging hole, the one side of the separate collecting box (3) of cooling cylinder (10) is opened Equipped with the 3rd discharge hole, the 5th sealing-plug is arranged in the 3rd discharge hole, and the one side of the 5th sealing-plug extends to cooling cylinder (10) outside.
  7. A kind of 7. recycling device of DMAC according to claim 1, which is characterized in that the output of the power supply (13) End with control processor (14) electric connection and be formed into a loop, control processor (14) respectively with temperature sensor (12) and acousto-optic Alarm (15).
CN201810081539.2A 2018-01-29 2018-01-29 A kind of recycling device of DMAC Pending CN108096870A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810081539.2A CN108096870A (en) 2018-01-29 2018-01-29 A kind of recycling device of DMAC

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810081539.2A CN108096870A (en) 2018-01-29 2018-01-29 A kind of recycling device of DMAC

Publications (1)

Publication Number Publication Date
CN108096870A true CN108096870A (en) 2018-06-01

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Application Number Title Priority Date Filing Date
CN201810081539.2A Pending CN108096870A (en) 2018-01-29 2018-01-29 A kind of recycling device of DMAC

Country Status (1)

Country Link
CN (1) CN108096870A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109847425A (en) * 2018-11-20 2019-06-07 江苏理文化工有限公司 A kind of methane chloride exhaust gas processing device

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3552189A (en) * 1968-07-26 1971-01-05 Commissariat Energie Atomique Apparatus for detecting scale formation
TW200424807A (en) * 2003-05-15 2004-11-16 Au Optronics Corp A system for recycling the stripper solution
CN202594810U (en) * 2012-05-07 2012-12-12 北京碧水源膜科技有限公司 Dimethylacetamide (DMAC) waste liquid recycling device
CN203591820U (en) * 2013-12-13 2014-05-14 淮南师范学院 Condensation pipe
CN203820658U (en) * 2014-05-21 2014-09-10 哈尔滨商业大学 Wine separating device
CN204910847U (en) * 2015-08-12 2015-12-30 江西国化实业有限公司 A recovery unit that is arranged in electrolysis waste material hydrogen fluoride
CN107537173A (en) * 2017-09-30 2018-01-05 江苏广盛源科技发展有限公司 A kind of alembic for separating dimethylacetamide amine aqueous solution
CN206902054U (en) * 2017-06-30 2018-01-19 云南城投碧水源膜科技有限责任公司 DMAC recovery systems

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3552189A (en) * 1968-07-26 1971-01-05 Commissariat Energie Atomique Apparatus for detecting scale formation
TW200424807A (en) * 2003-05-15 2004-11-16 Au Optronics Corp A system for recycling the stripper solution
CN202594810U (en) * 2012-05-07 2012-12-12 北京碧水源膜科技有限公司 Dimethylacetamide (DMAC) waste liquid recycling device
CN203591820U (en) * 2013-12-13 2014-05-14 淮南师范学院 Condensation pipe
CN203820658U (en) * 2014-05-21 2014-09-10 哈尔滨商业大学 Wine separating device
CN204910847U (en) * 2015-08-12 2015-12-30 江西国化实业有限公司 A recovery unit that is arranged in electrolysis waste material hydrogen fluoride
CN206902054U (en) * 2017-06-30 2018-01-19 云南城投碧水源膜科技有限责任公司 DMAC recovery systems
CN107537173A (en) * 2017-09-30 2018-01-05 江苏广盛源科技发展有限公司 A kind of alembic for separating dimethylacetamide amine aqueous solution

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109847425A (en) * 2018-11-20 2019-06-07 江苏理文化工有限公司 A kind of methane chloride exhaust gas processing device

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