CN108070413A - A kind of polarization fuel oil additive and preparation method thereof - Google Patents
A kind of polarization fuel oil additive and preparation method thereof Download PDFInfo
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- CN108070413A CN108070413A CN201710742040.7A CN201710742040A CN108070413A CN 108070413 A CN108070413 A CN 108070413A CN 201710742040 A CN201710742040 A CN 201710742040A CN 108070413 A CN108070413 A CN 108070413A
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/18—Organic compounds containing oxygen
- C10L1/1802—Organic compounds containing oxygen natural products, e.g. waxes, extracts, fatty oils
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/18—Organic compounds containing oxygen
- C10L1/182—Organic compounds containing oxygen containing hydroxy groups; Salts thereof
- C10L1/1822—Organic compounds containing oxygen containing hydroxy groups; Salts thereof hydroxy group directly attached to (cyclo)aliphatic carbon atoms
- C10L1/1824—Organic compounds containing oxygen containing hydroxy groups; Salts thereof hydroxy group directly attached to (cyclo)aliphatic carbon atoms mono-hydroxy
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/18—Organic compounds containing oxygen
- C10L1/19—Esters ester radical containing compounds; ester ethers; carbonic acid esters
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/18—Organic compounds containing oxygen
- C10L1/19—Esters ester radical containing compounds; ester ethers; carbonic acid esters
- C10L1/1905—Esters ester radical containing compounds; ester ethers; carbonic acid esters of di- or polycarboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/10—Liquid carbonaceous fuels containing additives
- C10L1/14—Organic compounds
- C10L1/22—Organic compounds containing nitrogen
- C10L1/222—Organic compounds containing nitrogen containing at least one carbon-to-nitrogen single bond
- C10L1/223—Organic compounds containing nitrogen containing at least one carbon-to-nitrogen single bond having at least one amino group bound to an aromatic carbon atom
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- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Liquid Carbonaceous Fuels (AREA)
- Solid Fuels And Fuel-Associated Substances (AREA)
Abstract
The present invention relates to fuel oil technical field of modification, it is proposed that a kind of polarization fuel oil additive, the polarization fuel oil additive are made of the raw material of following mass fraction:Methanol:29 32 parts;Methyl ricinolcic acid:51 54 parts;Camphor:25 parts;Cyclohexylamine:13 parts;Single oleic acid formicester:69 parts;Glycerine:36 parts, while propose a kind of polarization fuel oil additive production method, S1:Dissolution of raw material, S2:Stand peaceful, S3:Add camphor, S4:Eliminate emulsification, S5:Tinning uses; it can completely be reacted with the aliphatic acid in fuel oil by methyl ricinolcic acid and single oleic acid formicester in the present invention; fuel is made fully to burn in engine; carbon distribution generation is not had; fuel oil is helped to promote power in combustion; can be with the efficiency of combustion of the promotion fuel of high degree by using a kind of fuel oil that polarizes in the present invention, while the cylinder body for not damaging engine of fuel oil in combustion can be protected, there is good anti-wear effect.
Description
Technical field
The present invention relates to fuel oil technical field of modification, are concretely related to a kind of polarization fuel oil additive and its making
Method.
Background technology
It polarizes (polarization), self-explanatory characters' object produces a polarization under certain condition, makes its property compared with original
The phenomenon that state is deviateed.Such as molecular polarization (dipole moment increase), photon polarization (polarization), electrode polarization.Characterization is uniform
The electric field intensity (or magnetic vector) of plane wave is directed toward the property of variation in space, is sweared by the electric field of sine wave on a set point
The track of E ends is measured to illustrate.Optically it is referred to as to polarize.By the characteristics of electric field intensity track it can be divided into linear polarization,
Three kinds of circular polarisation and elliptic polarization.
Polarization technique is a kind of technology for the polarizability for having and each substance being induced to generate strength in simple terms.This skill
Art can make polarization structural arrangement in fuel molecule, change the burning behavior of fuel molecule, reduce the entropy of combustion process
Variation, while traditional sliding friction can be changed over rolling friction by polarization agent, and intermetallic frictional force is greatly reduced, and be promoted
Fuel combustion efficiency achievees the effect that energy-saving and emission-reduction.
Fuel oil (heavy oil) produced thermal energy after burning can be converted further into mechanical or electrical energy, be commonly used to for example
Boiler or engine.Since environmental protection consciousness improves in the world a few days ago, caused by the burning of various countries' strict supervision petrochemical material
Therefore how exhaust gas, reduces fuel oil combustion and discharges oxysulfide (SOx), nitrogen oxides (NOx) and oxycarbide (COx)
The concentration and total amount of pollutants are waited, for a key subjects of current environment protection.
Since crackate component accounting is quite big in conventional fuel oil, usually it is present with burning in combustion and does not fill
Point situation, it is serious to cause to occur carbon deposit, and large quantity of exhaust gas is generated after burning, environment will be caused great harm, because being
It reduces cost, environmental protection, improve efficiency, optimize technique, it is often necessary to add in additive, common addition in product oil
Agent has anti-knock agent, antioxidant, matal deactivator, antistatic agent, wear-resistant antirust agent, flow improving agent etc., phosphate or phosphate
Derivative is the main component of fuel additive, can not only play wear-resistant anti-rust action, but also can play anti-oxidant, anti-ageing be turned into
With.
In recent years, people do extensive work for the research of fuel oil additive.But most additive exists really
Some properties of fuel oil are improved to a certain extent, but their performances are single, and can be it is possible that complete containing unreacted
Aliphatic acid, it is insufficient that the complete aliphatic acid of unreacted can cause fuel to burn in engine, and carbon distribution generation, over-emitting black exhaust has peculiar smell
Deng, and common fuel oil additive can only improve a certain performance of fuel oil, for fuel oil other performances not
It improves.
The content of the invention
Therefore the present invention proposes a kind of polarization fuel oil additive and preparation method thereof, can be with the comprehensive of improvement fuel oil
Can, the aliphatic acid not reacted completely in fuel oil is eliminated, so as to improve the efficiency of combustion of fuel oil, prevents from damaging during fuel oil combustion
Evil engine cylinder body.
The technical proposal of the invention is realized in this way:A kind of polarization fuel oil additive, the polarization fuel oil addition
Agent is made of the raw material of following mass fraction:Methanol:29-32 parts;Methyl ricinolcic acid:51-54 parts;Camphor:2-5 parts;Hexamethylene
Amine:1-3 parts;Single oleic acid formicester:6-9 parts;Glycerine:3-6 parts.
Prepare a kind of weight proportion of the raw material for the fuel oil additive preferred weight ratio that polarizes of the present invention:Methanol:30-31
Part;Methyl ricinolcic acid:52-53 parts;Camphor:3-4 parts;Cyclohexylamine:1-2 parts;Single oleic acid formicester:7-8 parts;Glycerine:4-5 parts.
Prepare a kind of weight proportion of the raw material for the fuel oil additive preferred weight ratio that polarizes of the present invention:Methanol:30 parts;Castor
Numb methyl oleate:52 parts;Camphor:3 parts;Cyclohexylamine:1 part;Single oleic acid formicester:7 parts;Glycerine:4 parts.
Prepare a kind of weight proportion of the raw material for the fuel oil additive preferred weight ratio that polarizes of the present invention:Methanol:31 parts;Castor
Numb methyl oleate:53 parts;Camphor:4 parts;Cyclohexylamine:2 parts;Single oleic acid formicester:8 parts;Glycerine:5 parts.
A kind of polarization fuel oil additive production method, the production method are as follows:
S1:Dissolution of raw material, methanol, ricinoleic acid formicester and the single oleic acid formicester for taking out certain mass number are slowly added to mix
Blender is closed to carry out being sufficiently mixed dissolving;
S2:Standing sedimentation will pass through the dissolved raw materials of step S1 and stand 8~15min, and make raw material in mixing agitator
It restores calm, the electrostatic that removal process S1 stirrings generate is processed convenient for subsequent process;
S3:Add camphor, take out camphor and camphor clayed into power shape, into the raw material after step S2 standings plus
Enter the camphor powder of corrresponding quality number, raw material generates emulsion.
S4:Eliminate emulsification, raw material into step S3 adds in glycerine and cyclohexylamine, and addition while is stirred, and emulsifies
Phenomenon disappears to form finished product polarization fuel oil additive.
S5:Tinning uses, and will pass through step S4 treated finished products polarization fuel oil additive and be packed into finished pot input makes
With.
A kind of effect of each component raw material for the fuel oil additive that polarizes and property are described below in the present invention:
Methanol:Methanol is structure saturated monohydroxy alcohol the simplest, and molecular weight 32.04, boiling point is 64.7 DEG C.Methanol vapor
Oil is a kind of novel environment friendly fuel, is automobile fuel substitute, it is the important component of new energy.Crude oil be the whole world most
Main primary energy, the essence of current energy shortage is crude oil shortage.Vehicle fuel is the most important application field of crude oil, is accounted for
More than the 70% of global crude oil total flow.Methanol gasoline is a kind of " with coal for replacing oil " path, can be as the substitute of gasoline
So as to fulfill the partial alternative to crude oil, additive methanol content of the present invention is combustion adjuvant, and the power of engine is basic
Constant, the thermal efficiency increases, and smoke intensity is also declined.
Methyl ricinolcic acid:It is not soluble in water, alcohols is slightly soluble in, for the preparation of special organic chemicals, as fuel
The ingredient of oil additive can play wear-resistant combustion-supporting effect.
Camphor:Camphor has effects that orifice opening, qi stagnation removing, wards off that foul, desinsection is antipruritic, swelling and pain relieving, cures mainly mange scabies
Itch, injuries from falls as well, the symptoms such as toothache.Main component is camphane class compound for pure gum camphor, is contributed in the present invention
Raw material forms emulsion.
Cyclohexylamine:Colourless liquid.There is fish raw meat amine smell.Relative density 0.8647 (25/25 DEG C).134.5 DEG C of boiling point.Solidification
- 17.7 DEG C of point.Refractive index 1.4565 (25 DEG C).It can be miscible with water and common organic solvents.Can volatilize with vapor, and with water shape
Into azeotropic mixture.It is inflammable, toxic.For synthetic sweetening agent, corrosion inhibitor, vulcanization accelerator, emulsifier, antistatic agent,
Emulsion condensation agent, oil product additive, corrosion inhibitor, fungicide, agrochemical.It can be by cyclohexanol ammonolysis or by aniline in height
It is hydrogenated with and is made under mild high pressure.
Single oleic acid formicester:Olein (1-oleoylglycerol) is oleic acid (octadecenic acid) and glycerine (glycerine)
The product of polymerization, belongs to unsaturated glyceride.It can hydrolyze, can also occur with hydrogen addition with nitric acid under the conditions of acid-base property
Nitration reaction.Surfactant, food stabilizer, plastic, rubber auxiliary agent are commonly used for, is reacted with the aliphatic acid in fuel oil,
The aliphatic acid not reacted completely in fuel oil is eliminated, wear-resistant combustion-supporting work can be preferably played with the cooperation of ricinoleic acid formicester
With.
Glycerine:Colourless, odorless, sweet, appearance is in clear and bright viscous liquid state, is a kind of organic matter, tide can be absorbed from air
Gas can also absorb hydrogen sulfide, hydrogen cyanide and sulfur dioxide.It is insoluble in benzene, chloroform, carbon tetrachloride, carbon disulfide, petroleum ether and oil
Class eliminates the emulsion in additive.
By above disclosure, beneficial effects of the present invention are:Added in the present invention methanol, ricinoleic acid formicester and
Single oleic acid formicester can completely react with the aliphatic acid in fuel oil, fuel is made fully to burn in engine, does not have carbon distribution
Generation helps fuel oil to promote power in combustion, can very big journey by using a kind of polarization fuel oil in the present invention
The efficiency of combustion of the promotion fuel of degree, while the cylinder body for not damaging engine of fuel oil in combustion can be protected, have
There is good anti-wear effect.
Specific embodiment
Technical solution is clearly and completely described below in conjunction with specific embodiment, it is clear that described implementation
Example is only part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common
Technical staff's all other embodiments obtained without creative efforts belong to the model that the present invention protects
It encloses.
A kind of polarization fuel oil additive, the polarization fuel oil additive are made of the raw material of following mass fraction:First
Alcohol:29-32 parts;Methyl ricinolcic acid:51-54 parts;Camphor:2-5 parts;Cyclohexylamine:1-3 parts;Single oleic acid formicester:6-9 parts;It is sweet
Oil:3-6 parts.
A kind of polarization fuel oil additive production method, the production method are as follows:
S1:Dissolution of raw material, methanol, ricinoleic acid formicester and the single oleic acid formicester for taking out certain mass number are slowly added to mix
Blender is closed to carry out being sufficiently mixed dissolving;
S2:Standing sedimentation will pass through the dissolved raw materials of step S1 and stand 8~15min, and make raw material in mixing agitator
It restores calm, the electrostatic that removal process S1 stirrings generate is processed convenient for subsequent process;
S3:Add camphor, take out camphor and camphor clayed into power shape, into the raw material after step S2 standings plus
Enter the camphor powder of corrresponding quality number, raw material generates emulsion.
S4:Eliminate emulsification, raw material into step S3 adds in glycerine and cyclohexylamine, and addition while is stirred, and emulsifies
Phenomenon disappears to form finished product polarization fuel oil additive.
S5:Tinning uses, and will pass through step S4 treated finished products polarization fuel oil additive and be packed into finished pot input makes
With.
Polarize fuel oil additive component list
The polarization fuel oil additive of embodiment 1 to 9 different component of embodiment is prepared according to above-mentioned production method,
Then the different polarization fuel oil additive of these component contents is separately added into the fuel oil of nine parts of same 5000L, so
The phenomenon that starting engine observation combustion process afterwards, while the efficiency of combustion situation of fuel oil is measured, while increase by one group of comparison
Experiment, the fuel oil for taking out portion 5000L add in common fuel oil additive as a comparison case, and specific combustion case is as follows
Table:
Fuel oil combustion situation table
Embodiment | Combustion heat value (kilocalorie) | Whether carbon distribution is had | Cylinder body state | Whether pollutant is generated |
Embodiment 1 | 10987 | Nothing | Moderate is worn | Pollutant load is low |
Embodiment 2 | 10520 | Nothing | Moderate is worn | Pollutant load is low |
Embodiment 3 | 11500 | Nothing | Without abrasion | Pollution-free substance |
Embodiment 4 | 11000 | Nothing | Mild wear | Pollutant load is low |
Embodiment 5 | 10893 | Nothing | Mild wear | Pollutant load is low |
Embodiment 6 | 11325 | Nothing | Mild wear | Pollution-free substance |
Embodiment 7 | 11157 | Nothing | Mild wear | Pollutant load is low |
Embodiment 8 | 11086 | Nothing | Mild wear | Pollutant load is low |
Embodiment 9 | 10782 | There is a small amount of carbon deposit | Moderate is worn | Pollutant load hinge is low |
Comparative example | 10000 | There are a large amount of carbon deposits | Severe is worn | There is partial contamination substance |
As seen from the above table, comparative example is fuel oil additive, after adding in conventional fuel oil additive post fuel oil firing
The calorific value of generation is 10000 kilocalories, and the heat sent in combustion is not high, while cylinder interior abrasion is more, does not utilize
The long-time service of engine cylinder body.
In the present invention embodiment 3 be most preferred embodiment, methanol:30L;Methyl ricinolcic acid:52L;Camphor:3g;Cyclohexylamine:
1L;Single oleic acid formicester:7L;Glycerine:4L, and the calorific value after the fuel oil additive post fuel oil firing added in embodiment 3 is
11500 kilocalories fully burn, carbon distribution will not be formed in cylinder, entire combustion process is very clean, and engine cylinder body is not made
Into any damage, so as to the combustibility of comprehensive promotion fuel oil, play based on wear-resistant, combustion-supporting, peace and quiet answers
Close effect.Protect fuel oil in combustion do not damage cylinder body.
The content of methyl ricinolcic acid and single oleic acid formicester is higher in embodiment 9, causes to generate one in combustion
A little carbon distributions, do not burn fully, and the wear scar diameter of fuel oil is larger, and moderate abrasion is generated to the cylinder body of engine.
Finally illustrate, the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, although with reference to compared with
The present invention is described in detail in good embodiment, it will be understood by those of ordinary skill in the art that, it can be to the skill of the present invention
Art scheme is modified or replaced equivalently, and without departing from the objective and scope of technical solution of the present invention, should all be covered at this
Among the right of invention.
Claims (5)
1. a kind of polarization fuel oil additive, it is characterised in that:The original of the fuel oil additive by following mass fraction that polarize
Material composition:Methanol:29-32 parts;Methyl ricinolcic acid:51-54 parts;Camphor:2-5 parts;Cyclohexylamine:1-3 parts;Single oleic acid formicester:
6-9 parts;Glycerine:3-6 parts.
2. a kind of polarization fuel oil additive according to claim 1, it is characterised in that:The polarization fuel oil additive
It is made of the raw material of following mass fraction:Methanol:30-31 parts;Methyl ricinolcic acid:52-53 parts;Camphor:3-4 parts;Cyclohexylamine:
1-2 parts;Single oleic acid formicester:7-8 parts;Glycerine:4-5 parts.
3. a kind of polarization fuel oil additive according to claim 1, it is characterised in that:The polarization fuel oil additive
It is made of the raw material of following mass fraction:Methanol:30 parts;Methyl ricinolcic acid:52 parts;Camphor:3 parts;Cyclohexylamine:1 part;Single oil
Sour formicester:7 parts;Glycerine:4 parts.
4. a kind of polarization fuel oil additive according to claim 1, it is characterised in that:The polarization fuel oil additive
It is made of the raw material of following mass fraction:Methanol:31 parts;Methyl ricinolcic acid:53 parts;Camphor:4 parts;Cyclohexylamine:2 parts;Single oil
Sour formicester:8 parts;Glycerine:5 parts.
5. a kind of polarization fuel oil additive production method, it is characterised in that:The production method is as follows:
S1:Dissolution of raw material, methanol, ricinoleic acid formicester and the single oleic acid formicester of taking-up certain mass number are slowly added to mixing and stir
Device is mixed to carry out being sufficiently mixed dissolving;
S2:Standing sedimentation will pass through the dissolved raw materials of step S1 and stand 8~15min, raw material is made to recover in mixing agitator
Calmness, the electrostatic that removal process S1 stirrings generate, is processed convenient for subsequent process;
S3:Camphor is added, take out camphor and camphor is clayed into power shape, phase is added in into the raw material after step S2 standings
The camphor powder of mass fraction is answered, raw material generates emulsion.
S4:Eliminate emulsification, raw material into step S3 adds in glycerine and cyclohexylamine, and addition while is stirred, emulsion
Disappearance forms finished product polarization fuel oil additive.
S5:Tinning uses, and will pass through step S4 treated finished products polarization fuel oil additive and be packed into finished pot and come into operation.
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Cited By (1)
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CN112175681A (en) * | 2020-09-15 | 2021-01-05 | 深圳市诚进能源有限公司 | Novel energy-saving liquid fuel |
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Application publication date: 20180525 |