CN108070298A - A kind of high gloss prepared Chinese ink and preparation method - Google Patents
A kind of high gloss prepared Chinese ink and preparation method Download PDFInfo
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- CN108070298A CN108070298A CN201810010598.0A CN201810010598A CN108070298A CN 108070298 A CN108070298 A CN 108070298A CN 201810010598 A CN201810010598 A CN 201810010598A CN 108070298 A CN108070298 A CN 108070298A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/16—Writing inks
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- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The present invention relates to prepared Chinese ink technical field more particularly to a kind of high gloss prepared Chinese ink and preparation methods；Raw material including following weight parts：4.5 10.7 parts of 12 18 parts of toner, 24 30 parts of gelatine, 180 220 parts of deionized water and auxiliary agent, auxiliary agent include 23 parts of carbonate, 14 parts of dispersant, 0.2 1 parts of wetting agent, 0.8 1.5 parts of antifoaming agent, 0.5 1.2 parts of preservative；The invention also discloses its preparation methods；By the effect of gelatine, in addition finer polishing, makes the prepared Chinese ink fluent writing of preparation, ink blok is uniform, blackness is high, glossiness is high, and prepared Chinese ink stability is good, can preserve for a long time.
Description
Technical field
The present invention relates to prepared Chinese ink technical field more particularly to a kind of high gloss prepared Chinese ink and preparation methods.
Background technology
Chinese seem there is a kind of preference for black, and the calligraphy and painting art of bimillennium is handed down by ink.Ancient times
Production method to modern ink also continues to develop, and prepared Chinese ink has become the necessity of painting and calligraphy fan creation.At present, commercially available prepared Chinese ink
Generally existing shortcomings：Writing blackness, brightness are not high enough, it is difficult to meet artist and high-quality artistic work creation is wanted
It asks, and prepared Chinese ink stability is poor, is also easy to produce precipitation, it is difficult to which long-term to preserve, freezeout easily occurs in when low temperature.
The content of the invention
It is an object of the invention to overcome above-mentioned the deficiencies in the prior art, a kind of high gloss prepared Chinese ink is provided.
The technical solution adopted by the present invention to solve the technical problems is：
Construct a kind of high gloss prepared Chinese ink, the raw material including following weight parts：12-18 parts of toner, 24-30 parts of gelatine,
4.5-10.7 parts of 180-220 parts of deionized water and auxiliary agent.
High gloss prepared Chinese ink of the present invention, wherein, the auxiliary agent includes 2-3 parts of carbonate, 1-4 parts of dispersant, profit
0.2-1 parts of humectant, 0.8-1.5 parts of antifoaming agent, 0.5-1.2 parts of preservative.
High gloss prepared Chinese ink of the present invention, wherein, the carbonate is sodium carbonate.
High gloss prepared Chinese ink of the present invention, wherein, the toner is carbon black.
High gloss prepared Chinese ink of the present invention, wherein, the carbon black DBP oil factors (cm3/100g) are 140 ± 10, than
Surface area (m2/g) is 65 ± 8, and tinting strength, tinting power (%) is 125 ± 10.
A kind of preparation method of high gloss prepared Chinese ink is constructed, including taking 100-130 parts of gelatine water, adds in 1-3 parts of auxiliary agent,
60-90 parts of deionized water, stirring, obtains the first mixed liquor；12-18 parts of toner is taken, adds in 1.2-5 parts of auxiliary agent, deionized water
30-50 parts, 1-2h is ground by rotating speed 1000-2000r/min, obtains the second mixed liquor；By first mixed liquor and described
Second mixed liquor in mass ratio 1:0.8-1.2 is mixed, and adds in auxiliary agent, and stirring obtains the 3rd mixed liquor.
The preparation method of high gloss prepared Chinese ink of the present invention, wherein, in first mixed liquor, auxiliary agent is carbonic acid
Sodium；In second mixed liquor, auxiliary agent is dispersant and wetting agent；In 3rd mixed liquor, auxiliary agent is preservative and antifoaming agent.
The preparation method of high gloss prepared Chinese ink of the present invention, wherein, described dispersant 1-4 parts, wetting agent 0.2-1
Part, 0.5-1.2 parts of preservative, 0.8-1.5 parts of antifoaming agent.
The preparation method of high gloss prepared Chinese ink of the present invention, wherein, grain size is less than 5 μm in second mixed liquor.
The preparation method of high gloss prepared Chinese ink of the present invention, wherein, the toner is carbon black.
The beneficial effects of the present invention are：High gloss prepared Chinese ink of the present invention, by the collocation of each raw material, in addition finer
Polishing, makes the prepared Chinese ink fluent writing of preparation, ink blok is uniform, blackness is high, glossiness is high, and prepared Chinese ink stability is good, can preserve for a long time.
Specific embodiment
In order to make the purpose, technical scheme and advantage of the embodiment of the present invention clearer, implement below in conjunction with the present invention
Technical solution in example carries out clear, complete description, it is clear that and described embodiment is the section Example of the present invention, and
It is not all of embodiment.Based on the embodiment of the present invention, those of ordinary skill in the art are not before making the creative labor
All other embodiments obtained are put, belong to protection scope of the present invention.
Term " first ", " second ", " the 3rd " etc. are only used for distinguishing description, and it is not intended that indicating or implying relatively heavy
The property wanted.
Referenced herein " embodiment " is it is meant that a particular feature, structure, or characteristic described can wrap in conjunction with the embodiments
Containing at least one embodiment of the present invention.Each position in the description occur the phrase might not each mean it is identical
Embodiment, nor the independent or alternative embodiment with other embodiments mutual exclusion.Those skilled in the art explicitly and
Implicitly understand, embodiment described herein can be combined with other embodiments.
A kind of preparation method of high gloss prepared Chinese ink provided in an embodiment of the present invention is specifically described below.
A kind of high gloss prepared Chinese ink, the raw material including following weight parts：12-18 parts of toner, 24-30 parts of gelatine, go from
Sub- water 180-220 parts and 4.5-10.7 parts of auxiliary agent；Toner is carbon black, and preferred carbon black DBP oil factors (cm3/100g) are
140 ± 10, specific surface area (m2/g) is 65 ± 8, and tinting strength, tinting power (%) is 125 ± 10；Auxiliary agent includes 2-3 parts of carbonate, dispersant
1-4 parts, 0.2-1 parts of wetting agent, 0.8-1.5 parts of antifoaming agent, 0.5-1.2 parts of preservative.
The selection of each raw material and proportioning increase by scientific design, so as to cooperate between various raw materials and can play collaboration
The effect of effect, using this proportioning, the active ingredient interaction of various raw materials and supplement can make the prepared Chinese ink of preparation write stream
Freely, ink blok is uniform, blackness is high, glossiness is high, and prepared Chinese ink stability is good, can preserve for a long time.
It should be noted that preferred carbonate is sodium carbonate, wetting agent is water-soluble nonionic surfactant, is disappeared
Infusion is mineral oil defoaming agent, preservative is potassium cinnamate, isothiazolinone, calcium propionate, one kind in Kathon CG preservative or
Several compositions.
The preparation method of this kind of high gloss prepared Chinese ink includes：100-130 parts of gelatine water are taken, 1-3 parts of carbonate is added in, goes
60-90 parts of ionized water, stirring, obtains the first mixed liquor；Take 12-18 parts of toner, 1-4 parts of bonus point powder, wetting agent 0.2-1
Part, 30-50 parts of deionized water grinds 1-2h by rotating speed 1000-2000r/min, obtains the second mixed liquor；By described first
Mixed liquor and second mixed liquor in mass ratio 1:0.8-1.2 is mixed, and adds in 0.5-1.2 parts of preservative, antifoaming agent 0.8-
1.5 parts, stirring obtains the 3rd mixed liquor.
Preferably, 24-30 parts of gelatine is taken, adds 80-100 parts of water, when immersion 24 is small, 80 degrees Celsius is heated to, adds in carbonic acid
1-3 parts of sodium, stirs evenly, it is made fully to dissolve, be cooled to room temperature, and adds in 60-90 parts of deionized water, stirs evenly, and obtains the
One mixed liquor；12-18 parts of carbon black is taken, 1-4 parts of bonus point powder, 0.2-1 parts of wetting agent, 30-50 parts of deionized water, sand mill is at a high speed
1-2h, rotating speed 1000-2000r/min are ground, obtains the second mixed liquor that grain size is less than 5 μm；First mixed liquor and second are mixed
Close liquid in mass ratio 1:1 mixing, adds in 0.5-1.2 parts of preservative, and 0.8-1.5 parts of antifoaming agent stirs evenly, and obtains the 3rd mixing
Liquid.
Embodiment 1：
A kind of preparation method of high gloss prepared Chinese ink, comprises the following steps：
26 parts of gelatine is taken, adds 80 parts of water, when immersion 24 is small, is heated to 80 degrees Celsius, adds in 1.5 parts of sodium carbonate, stirring is equal
It is even, it is made fully to dissolve, is cooled to room temperature, 70 parts of deionized water is added in, stirs evenly, obtain the first mixed liquor.
It is 145 to select DBP oil factors (cm3/100g), and specific surface area (m2/g) is 63, and tinting strength, tinting power (%) is 128 color
Plain 15 parts of carbon black adds 2.2 parts of acrylic polymer dispersant, 0.5 part of water-soluble nonionic surfactant, deionization
40 parts of water, sand mill high speed grinding 2h, rotating speed 1500r/min obtain the second mixed liquor that grain size is less than 5 μm.
By the first mixed liquor and the second mixed liquor in mass ratio 1:1 mixing adds in 0.6 part of calcium propionate, mineral oils defoaming
0.9 part of agent, stirs evenly, and obtains the 3rd mixed liquor.
By the effect of gelatine, in addition finer polishing, make the prepared Chinese ink fluent writing of preparation, ink blok is uniform, blackness is high,
Glossiness is high, and prepared Chinese ink stability is good, can preserve for a long time.
Embodiment 2：
A kind of preparation method of high gloss prepared Chinese ink, comprises the following steps：
27 parts of gelatine is taken, adds 100 parts of water, when immersion 24 is small, is heated to 80 degrees Celsius, adds in 2 parts of sodium carbonate, stirring is equal
It is even, it is made fully to dissolve, is cooled to room temperature, 75 parts of deionized water is added in, stirs evenly, obtain the first mixed liquor.
It is 145 to select DBP oil factors (cm3/100g), and specific surface area (m2/g) is 63, and tinting strength, tinting power (%) is 128 color
Plain 16 parts of carbon black adds 2.6 parts of acrylic polymer dispersant, 0.6 part of water-soluble nonionic surfactant, deionization
45 parts of water, sand mill high speed grinding 1.5h, rotating speed 1800r/min obtain the second mixed liquor that grain size is less than 5 μm.
By the first mixed liquor and the second mixed liquor in mass ratio 1:1 mixing, adds in 0.7 part of potassium cinnamate, mineral oils disappears
1 part of infusion, stirs evenly, and obtains the 3rd mixed liquor.
Embodiment 3：
A kind of preparation method of high gloss prepared Chinese ink, comprises the following steps：
24 parts of gelatine is taken, adds 85 parts of water, when immersion 24 is small, is heated to 80 degrees Celsius, adds in 1.8 parts of sodium carbonate, stirring is equal
It is even, it is made fully to dissolve, is cooled to room temperature, 80 parts of deionized water is added in, stirs evenly, obtain the first mixed liquor.
It is 145 to select DBP oil factors (cm3/100g), and specific surface area (m2/g) is 63, and tinting strength, tinting power (%) is 128 color
Plain 17 parts of carbon black adds 3 parts of acrylic polymer dispersant, 0.8 part of water-soluble nonionic surfactant, deionized water
50 parts, sand mill high speed grinding 1h, rotating speed 2000r/min, obtain the second mixed liquor that grain size is less than 5 μm.
By the first mixed liquor and the second mixed liquor in mass ratio 1:1 mixing, adds in 0.8 part of isothiazolinone, mineral oils
1 part of antifoaming agent, stirs evenly, and obtains the 3rd mixed liquor.
Embodiment 4：
A kind of preparation method of high gloss prepared Chinese ink, comprises the following steps：
30 parts of gelatine is taken, adds 90 parts of water, when immersion 24 is small, is heated to 80 degrees Celsius, adds in 2.3 parts of sodium carbonate, stirring is equal
It is even, it is made fully to dissolve, is cooled to room temperature, 85 parts of deionized water is added in, stirs evenly, obtain the first mixed liquor.
It is 145 to select DBP oil factors (cm3/100g), and specific surface area (m2/g) is 63, and tinting strength, tinting power (%) is 128 color
Plain 18 parts of carbon black adds 2.8 parts of acrylic polymer dispersant, 0.9 part of water-soluble nonionic surfactant, deionization
45 parts of water, sand mill high speed grinding 2h, rotating speed 1800r/min obtain the second mixed liquor that grain size is less than 5 μm.
By the first mixed liquor and the second mixed liquor in mass ratio 1:1 mixing, adds in 1 part of Kathon CG preservative, mineral oils disappears
1.2 parts of infusion, stirs evenly, and obtains the 3rd mixed liquor.
Comparative example 1：
33 parts of gelatine is taken, adds 110 parts of water, when immersion 24 is small, is heated to 80 degrees Celsius, adds in 3.6 parts of sodium carbonate, stirring is equal
It is even, it is made fully to dissolve, is cooled to room temperature, 95 parts of deionized water is added in, stirs evenly, obtain the first mixed liquor.
It is 155 to select DBP oil factors (cm3/100g), and specific surface area (m2/g) is 63, and tinting strength, tinting power (%) is 128 pigment
18 parts of carbon black adds 3.2 parts of acrylic polymer dispersant, 1.1 parts of water-soluble nonionic surfactant, deionized water
53 parts, sand mill high speed grinding 2h, rotating speed 2100r/min obtain the second mixed liquor.
By the first mixed liquor and the second mixed liquor in mass ratio 1:1.2 mixing, add in 1.3 parts of Kathon CG preservative, mineral oil
1.6 parts of class antifoaming agent, stirs evenly, and obtains the 3rd mixed liquor.
Comparative example 2：
21 parts of gelatine is taken, adds 78 parts of water, when immersion 24 is small, is heated to 80 degrees Celsius, adds in 1.5 parts of sodium carbonate, stirring is equal
It is even, it is made fully to dissolve, is cooled to room temperature, 85 parts of deionized water is added in, stirs evenly, obtain the first mixed liquor.
It is 128 to select DBP oil factors (cm3/100g), and specific surface area (m2/g) is 62, and tinting strength, tinting power (%) is 128 color
Plain 17 parts of carbon black adds 2.8 parts of acrylic polymer dispersant, 0.8 part of water-soluble nonionic surfactant, deionization
41 parts of water, sand mill high speed grinding 2h, rotating speed 1500r/min obtain the second mixed liquor.
By the first mixed liquor and the second mixed liquor in mass ratio 1:0.78 mixing, adds in 0.8 part of Kathon CG preservative, mineral oil
0.8 part of class antifoaming agent, stirs evenly, and obtains the 3rd mixed liquor.
By prepared Chinese ink and commercially available prepared Chinese ink (the Chongqing China of high gloss prepared Chinese ink, comparative example 1-2 made from 1-5 of the embodiment of the present invention
Occasion prepared Chinese ink, one obtain pavilion prepared Chinese ink) performance control experiment is carried out, as a result such as following table：
Remarks："+" representative energy degree value in table, "+", and to represent respective performances more excellent；Conversely, the fewer representative of "+"
Respective performances are poorer.
From table data, the blackness of the prepared Chinese ink of embodiment 1-4, glossiness, ink blok uniformity, stability, frost resistance are equal
Very well, should the result shows that, due to effective collocation in prepared Chinese ink provided by the invention, blackness, glossiness, the ink blok for making prepared Chinese ink are uniform
Property, stability, frost resistance are obtained for raising.
The prepared Chinese ink effect of embodiment 1-4 is matched somebody with somebody higher than each raw material for the prepared Chinese ink that comparison prepared Chinese ink 1 and 2, comparison prepared Chinese ink 1 and 2 provide
Than not in scope provided in an embodiment of the present invention, should the result shows that, using each raw material of prepared Chinese ink provided in an embodiment of the present invention
Proportioning can effectively improve the blackness of prepared Chinese ink, glossiness, ink blok uniformity, stability, frost resistance.
In conclusion by a kind of high gloss prepared Chinese ink provided in an embodiment of the present invention, blackness, glossiness, the ink of this prepared Chinese ink
Stain uniformity, stability, frost resistance have obtained effective raising；By a kind of high gloss prepared Chinese ink provided in an embodiment of the present invention
Preparation method, by the collocation of each raw material, in addition finer polishing, make the prepared Chinese ink fluent writing of preparation, ink blok is uniform, black
Degree is high, glossiness is high, and prepared Chinese ink stability is good, can preserve for a long time.
It should be appreciated that for those of ordinary skills, can be improved or converted according to the above description,
And all these modifications and variations should all belong to the protection domain of appended claims of the present invention.
Claims (10)
1. a kind of high gloss prepared Chinese ink, it is characterised in that：Raw material including following weight parts：12-18 parts of toner, gelatine 24-
30 parts, 4.5-10.7 parts of 180-220 parts of deionized water and auxiliary agent.
2. high gloss prepared Chinese ink according to claim 1, which is characterized in that the auxiliary agent includes 2-3 parts of carbonate, disperses
1-4 parts of agent, 0.2-1 parts of wetting agent, 0.8-1.5 parts of antifoaming agent, 0.5-1.2 parts of preservative.
3. high gloss prepared Chinese ink according to claim 2, which is characterized in that the carbonate is sodium carbonate.
4. high gloss prepared Chinese ink according to claim 1, which is characterized in that the toner is carbon black.
5. high gloss prepared Chinese ink according to claim 4, which is characterized in that the carbon black DBP oil factors (cm3/100g)
For 140 ± 10, specific surface area (m2/g) is 65 ± 8, and tinting strength, tinting power (%) is 125 ± 10.
6. a kind of preparation method of high gloss prepared Chinese ink as described in any of claims 1, which is characterized in that including following
Step：
100-130 parts of gelatine water are taken, add in 1-3 parts of auxiliary agent, 60-90 parts of deionized water, stirring obtains the first mixed liquor；
12-18 parts of toner is taken, adds in 1.2-5 parts of auxiliary agent, 30-50 parts of deionized water is ground by rotating speed 1000-2000r/min
1-2h is ground, obtains the second mixed liquor；
By first mixed liquor and second mixed liquor in mass ratio 1:0.8-1.2 is mixed, and adds in auxiliary agent, and stirring obtains
3rd mixed liquor.
7. high gloss prepared Chinese ink according to claim 6, which is characterized in that in first mixed liquor, auxiliary agent is carbonic acid
Sodium；In second mixed liquor, auxiliary agent is dispersant and wetting agent；In 3rd mixed liquor, auxiliary agent is preservative and antifoaming agent.
8. high gloss prepared Chinese ink according to claim 7, which is characterized in that 1-3 parts of sodium carbonate, described dispersant 1-4 parts,
0.2-1 parts of wetting agent, 0.5-1.2 parts of preservative, 0.8-1.5 parts of antifoaming agent.
9. high gloss prepared Chinese ink according to claim 6, which is characterized in that grain size is less than 5 μm in second mixed liquor.
10. high gloss prepared Chinese ink according to claim 6, which is characterized in that the toner is carbon black.
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| CN201810010598.0A CN108070298A (en) | 2018-01-05 | 2018-01-05 | A kind of high gloss prepared Chinese ink and preparation method |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810010598.0A CN108070298A (en) | 2018-01-05 | 2018-01-05 | A kind of high gloss prepared Chinese ink and preparation method |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110951095A (en) * | 2019-11-20 | 2020-04-03 | 华协书画院有限公司 | Multifunctional melanin pure natural plastic color master batch |
| CN111320893A (en) * | 2020-04-24 | 2020-06-23 | 河北青竹画材科技有限公司 | Antibacterial ink and preparation method thereof |
| CN116554729A (en) * | 2023-05-10 | 2023-08-08 | 孚玉山房(北京)文化有限公司 | Color ink easy to clean and preparation method thereof |
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| CN102492332A (en) * | 2011-12-05 | 2012-06-13 | 天津市鸵鸟墨水有限公司 | Novel ink and production method thereof |
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2018
- 2018-01-05 CN CN201810010598.0A patent/CN108070298A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102492332A (en) * | 2011-12-05 | 2012-06-13 | 天津市鸵鸟墨水有限公司 | Novel ink and production method thereof |
Non-Patent Citations (1)
| Title |
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| 《化工百科全书》编辑委员会等: "《化工百科全书（第15卷）》", 31 December 1997, 化学工业出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110951095A (en) * | 2019-11-20 | 2020-04-03 | 华协书画院有限公司 | Multifunctional melanin pure natural plastic color master batch |
| CN111320893A (en) * | 2020-04-24 | 2020-06-23 | 河北青竹画材科技有限公司 | Antibacterial ink and preparation method thereof |
| CN116554729A (en) * | 2023-05-10 | 2023-08-08 | 孚玉山房(北京)文化有限公司 | Color ink easy to clean and preparation method thereof |
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