CN108069700A - A kind of corrosion-resistant imitated wood floor board brick and preparation method thereof of corridor along the river - Google Patents

A kind of corrosion-resistant imitated wood floor board brick and preparation method thereof of corridor along the river Download PDF

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Publication number
CN108069700A
CN108069700A CN201711137341.3A CN201711137341A CN108069700A CN 108069700 A CN108069700 A CN 108069700A CN 201711137341 A CN201711137341 A CN 201711137341A CN 108069700 A CN108069700 A CN 108069700A
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river
corrosion
floor board
gangue
wood floor
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陈笑音
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Huzhou Nanxun Feng Qiang Wood Industry Co Ltd
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Huzhou Nanxun Feng Qiang Wood Industry Co Ltd
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Priority to CN201711137341.3A priority Critical patent/CN108069700A/en
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    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00—Clay-wares
    • C04B33/02—Preparing or treating the raw materials individually or as batches
    • C04B33/13—Compounding ingredients
    • C04B33/132—Waste materials; Refuse; Residues
    • C04B33/1324—Recycled material, e.g. tile dust, stone waste, spent refractory material
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00—Clay-wares
    • C04B33/02—Preparing or treating the raw materials individually or as batches
    • C04B33/13—Compounding ingredients
    • C04B33/131—Inorganic additives
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    • C04B33/00—Clay-wares
    • C04B33/02—Preparing or treating the raw materials individually or as batches
    • C04B33/13—Compounding ingredients
    • C04B33/132—Waste materials; Refuse; Residues
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00—Clay-wares
    • C04B33/02—Preparing or treating the raw materials individually or as batches
    • C04B33/13—Compounding ingredients
    • C04B33/132—Waste materials; Refuse; Residues
    • C04B33/1328—Waste materials; Refuse; Residues without additional clay
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00—Clay-wares
    • C04B33/02—Preparing or treating the raw materials individually or as batches
    • C04B33/13—Compounding ingredients
    • C04B33/16—Lean materials, e.g. grog, quartz
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81—Coating or impregnation
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    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427—Silicates other than clay, e.g. water glass
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427—Silicates other than clay, e.g. water glass
    • C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/42—Non metallic elements added as constituents or additives, e.g. sulfur, phosphor, selenium or tellurium
    • C04B2235/422—Carbon
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
    • C04B2235/9669—Resistance against chemicals, e.g. against molten glass or molten salts
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P40/00—Technologies relating to the processing of minerals
    • Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes

Abstract

The invention discloses a kind of corrosion-resistant imitated wood floor board brick of corridor along the river, main component is gangue, sodium silicate solution, bagasse, alumino-silicate cement, modified graphene oxide, imitation wood coating and river sand；The present invention is not only reused substantial amounts of gangue, reduces pollution, and at low cost, and the market competitiveness is strong；Main problem is that gangue is more open in preparation process, condensation effect is poor；The characteristics of present invention is in order to overcome gangue, bagasse, sodium silicate solution, magnesia and alumina modified graphene oxide are added in, adobe is pressed under high pressure, after coating imitation wood coating, it is sintered at a high temperature of 1,200 1300 DEG C, you can as qualified imitated wood floor board brick；Magnesia, alumina modified graphene form network-like spinel structure and are attached to around graphene at high temperature, and not only dispersion effect is good, and substantially increase the density of brick, and the corrosion resistance of acid rain is significantly improved.

Description

A kind of corrosion-resistant imitated wood floor board brick and preparation method thereof of corridor along the river
Technical field
The present invention relates to building material technical field more particularly to a kind of corrosion-resistant corridor along the river with imitated wood floor board brick and its Preparation method.
Background technology
Continuous with people's living environment improves and improves, requirement of the people to constructional ornamental material also increasingly compared with It is high.And timber floor is as one kind in construction material, due to its with corrosion resistance is strong, heat insulation effect is apparent and it is deep by people's Like；And the production field of traditional timber floor is to be made using wood or formed using sawdust face pressure system, it is seen then that The manufacturing process of the timber floor of both is to need to consume the substantial amounts of forest reserves, and then serious shadow will be caused to environment It rings, causes ecology by serious destruction.
With the continuous improvement of our urbanization in recent years, requirement of the people to quality of life is higher and higher；Various regions Landscape band along the river constantly is being built, the demand of imitated wood floor board brick is constantly being increased；And our some areas especially environment are dirty The problem of dye, causes acid rain phenomenon to happen occasionally, very serious to the erosion on floor, therefore it is necessary to study a kind of low cost, height The corrosion-resistant imitated wood floor board brick of corridor along the river of security.
The content of the invention
Technical problems based on background technology, the present invention propose a kind of corrosion-resistant imitated wood floor board brick of corridor along the river And preparation method thereof.
Technical scheme is as follows：
A kind of corrosion-resistant imitated wood floor board brick of corridor along the river, including following component：Gangue, sodium silicate solution, bagasse, Alumino-silicate cement, modified graphene oxide, imitation wood coating and river sand.
A kind of corrosion-resistant imitated wood floor board brick of corridor along the river includes the ingredient of following weight percent:
Gangue 50-60%
Magnesia 1-3%
Sodium silicate solution 8-12%
Bagasse 8-20%
Alumino-silicate cement 5-10%
Modified graphene oxide 0.05-0.1%
Imitation wood coating 1-5%
River sand surplus.
Preferably, the mass fraction of the sodium silicate solution is 3-8%.
Preferably, the magnesia and the grain size of river sand are 325 mesh.
Preferably, the modified graphene oxide is alumina modified graphene oxide.
A kind of corrosion-resistant preparation method of imitated wood floor board brick of corridor along the river, comprises the following steps：
A, gangue and alumino-silicate cement are crushed jointly, crosses 325 mesh sieves；
B, magnesia, river sand and modified graphene oxide are added in, under the conditions of 400rpm, is stirred together for 25-35min；
C, sodium silicate solution and bagasse are added in, adjusting mixing speed is 250-300rpm, stirs 40-60min；
D, adobe is depressed in 80-100KN pressure using friction press, after dry kiln drying, by what is dried After adobe single side paints imitation wood coating, 1200-1300 DEG C of sintering 2-3h；
E, after taking out floor tile, side is polished, and corner is corrected, you can.
The invention has the beneficial effects that：
Alumino-silicate cement is used in the present invention as frame；Magnesia, alumina modified graphene form network at high temperature The spinel structure of shape is simultaneously attached to around graphene, and not only dispersion effect is good, and substantially increases the density of brick, to acid rain Corrosion resistance significantly improve.
The present invention prepares imitated wood floor board brick using gangue as primary raw material, and substantial amounts of gangue is not only made to obtain weight It is multiple to utilize, reduce pollution, and also it is at low cost, the market competitiveness is strong；Main problem is that gangue ratio in preparation process Loosely, condensation effect is poor；The characteristics of present invention is in order to overcome gangue, add in bagasse, sodium silicate solution, magnesia and Alumina modified graphene oxide, is pressed into adobe under high pressure, after coating imitation wood coating, at a high temperature of 1200-1300 DEG C Sintering, you can as qualified imitated wood floor board brick.
Specific embodiment
Embodiment 1：
A kind of corrosion-resistant imitated wood floor board brick of corridor along the river includes the ingredient of following weight percent:
Gangue 55%
Magnesia 2%
Sodium silicate solution 10%
Bagasse 12%
Alumino-silicate cement 8%
Modified graphene oxide 0.08%
Imitation wood coating 3.5%
River sand surplus.
The mass fraction of the sodium silicate solution is 5%.
The magnesia and the grain size of river sand are 325 mesh.
The modified graphene oxide is alumina modified graphene oxide.
A kind of corrosion-resistant preparation method of imitated wood floor board brick of corridor along the river, comprises the following steps：
A, gangue and alumino-silicate cement are crushed jointly, crosses 325 mesh sieves；
B, magnesia, river sand and modified graphene oxide are added in, under the conditions of 400rpm, is stirred together for 30min；
C, sodium silicate solution and bagasse are added in, adjusting mixing speed is 280rpm, stirs 55min；
D, adobe is depressed in 85KN pressure using friction press, after dry kiln drying, adobe that will dry After single side paints imitation wood coating, 1280 DEG C of sintering 2.5h；
E, after taking out floor tile, side is polished, and corner is corrected, you can.
Embodiment 2：
A kind of corrosion-resistant imitated wood floor board brick of corridor along the river includes the ingredient of following weight percent:
Gangue 50%
Magnesia 1%
Sodium silicate solution 12%
Bagasse 8%
Alumino-silicate cement 10%
Modified graphene oxide 0.05%
Imitation wood coating 5%
River sand surplus.
The magnesia and the grain size of river sand are 325 mesh.
The mass fraction of the sodium silicate solution is 3%.
The modified graphene oxide is alumina modified graphene oxide.
A kind of corrosion-resistant preparation method of imitated wood floor board brick of corridor along the river, comprises the following steps：
A, gangue and alumino-silicate cement are crushed jointly, crosses 325 mesh sieves；
B, magnesia, river sand and modified graphene oxide are added in, under the conditions of 400rpm, is stirred together for 25min；
C, sodium silicate solution and bagasse are added in, adjusting mixing speed is 300rpm, stirs 40min；
D, adobe is depressed in 100KN pressure using friction press, after dry kiln drying, adobe that will dry After single side paints imitation wood coating, 1200 DEG C of sintering 3h；
E, after taking out floor tile, side is polished, and corner is corrected, you can.
Embodiment 3：
A kind of corrosion-resistant imitated wood floor board brick of corridor along the river includes the ingredient of following weight percent:
Gangue 60%
Magnesia 3%
Sodium silicate solution 8%
Bagasse 20%
Alumino-silicate cement 5%
Modified graphene oxide 0.1%
Imitation wood coating 1%
River sand surplus.
The mass fraction of the sodium silicate solution is 8%.
The magnesia and the grain size of river sand are 325 mesh.
The modified graphene oxide is alumina modified graphene oxide.
A kind of corrosion-resistant preparation method of imitated wood floor board brick of corridor along the river, comprises the following steps：
A, gangue and alumino-silicate cement are crushed jointly, crosses 325 mesh sieves；
B, magnesia, river sand and modified graphene oxide are added in, under the conditions of 400rpm, is stirred together for 35min；
C, sodium silicate solution and bagasse are added in, adjusting mixing speed is 250rpm, stirs 60min；
D, adobe is depressed in 80KN pressure using friction press, after dry kiln drying, adobe that will dry After single side paints imitation wood coating, 1300 DEG C of sintering 2h；
E, after taking out floor tile, side is polished, and corner is corrected, you can.
Comparative example 1
The magnesia of embodiment 1 is removed, remaining preparation method is constant.
Comparative example 2
The modified graphene oxide of embodiment 1 is removed, remaining preparation method is constant.
Every physical property of the imitated wood floor board brick of 1-3 of the embodiment of the present invention is tested, obtains following data：
Detection project Embodiment 1 Embodiment 2 Embodiment 3
Bulk density (g/m3) 3.52 3.55 3.48
Compressive resistance (Mpa) 14.8 14.5 14.3
Wearing coefficient (turns) 4270 4255 4250
The imitated wood floor board brick sample of embodiment 1-3 is put into the acid solution that pH is 4.0 and is impregnated for 24 hours, the quality of brick without It is decreased obviously, brick surface is without apparent pore.
The imitated wood floor board brick sample of comparative example 1-2 is put into the acid solution that pH is 4.0 and is impregnated for 24 hours, under the quality of brick 2-5% drops, and pore occurs in brick surface, and brick structure is substantially destroyed.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto, Any one skilled in the art in the technical scope disclosed by the present invention, technique according to the invention scheme and its Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (6)

1. a kind of corrosion-resistant imitated wood floor board brick of corridor along the river, which is characterized in that including following component：Gangue, sodium metasilicate are molten Liquid, bagasse, alumino-silicate cement, modified graphene oxide, imitation wood coating and river sand.
2. the corrosion-resistant imitated wood floor board brick of corridor along the river as described in claim 1, which is characterized in that including following weight percent The ingredient of ratio:
Gangue 60-75%
Sodium silicate solution 3-5%
Bagasse 1-3%
Alumino-silicate cement 0.5-1%
Modified graphene oxide 0.05-0.1%
Imitation wood coating 2-5%
River sand surplus.
3. the preparation method of the corrosion-resistant imitated wood floor board brick of corridor along the river as claimed in claim 2, which is characterized in that described The mass fraction of sodium silicate solution is 3-8%.
4. the corrosion-resistant imitated wood floor board brick of corridor along the river as claimed in claim 2, which is characterized in that the magnesia and river sand Grain size be 325 mesh.
5. the corrosion-resistant imitated wood floor board brick of corridor along the river as claimed in claim 2, which is characterized in that the modified oxidized stone Black alkene is alumina modified graphene oxide.
6. a kind of preparation method of the corrosion-resistant imitated wood floor board brick of corridor along the river, which is characterized in that comprise the following steps：
A, gangue and alumino-silicate cement are crushed jointly, crosses 325 mesh sieves；
B, magnesia, river sand and modified graphene oxide are added in, under the conditions of 400rpm, is stirred together for 25-35min；
C, sodium silicate solution and bagasse are added in, adjusting mixing speed is 250-300rpm, stirs 40-60min；
D, adobe is depressed in 80-100KN pressure using friction press, after dry kiln drying, adobe that will dry After single side paints imitation wood coating, 1200-1300 DEG C of sintering 2-3h；
E, after taking out floor tile, side is polished, and corner is corrected, you can.
CN201711137341.3A 2017-11-16 2017-11-16 A kind of corrosion-resistant imitated wood floor board brick and preparation method thereof of corridor along the river Pending CN108069700A (en)

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CN106630867A (en) * 2016-11-14 2017-05-10 长兴钦禾建材科技有限公司 Wood-like floor tile and preparation method thereof
CN106747503A (en) * 2016-12-09 2017-05-31 新昌县永佳耐火材料厂 A kind of anticorrosive refractory brick and preparation method thereof
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Application publication date: 20180525