CN108057409A - A kind of reaction kettle - Google Patents

A kind of reaction kettle Download PDF

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Publication number
CN108057409A
CN108057409A CN201711453512.3A CN201711453512A CN108057409A CN 108057409 A CN108057409 A CN 108057409A CN 201711453512 A CN201711453512 A CN 201711453512A CN 108057409 A CN108057409 A CN 108057409A
Authority
CN
China
Prior art keywords
stirrer paddle
baffle
autoclave body
reaction kettle
agitating shaft
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711453512.3A
Other languages
Chinese (zh)
Inventor
曹亚萍
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Wuxi Its Macro Packaging Material Factory
Original Assignee
Wuxi Its Macro Packaging Material Factory
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Wuxi Its Macro Packaging Material Factory filed Critical Wuxi Its Macro Packaging Material Factory
Priority to CN201711453512.3A priority Critical patent/CN108057409A/en
Publication of CN108057409A publication Critical patent/CN108057409A/en
Pending legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/11Stirrers characterised by the configuration of the stirrers
    • B01F27/19Stirrers with two or more mixing elements mounted in sequence on the same axis
    • B01F27/192Stirrers with two or more mixing elements mounted in sequence on the same axis with dissimilar elements
    • B01F27/1921Stirrers with two or more mixing elements mounted in sequence on the same axis with dissimilar elements comprising helical elements and paddles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/50Mixing receptacles
    • B01F35/53Mixing receptacles characterised by the configuration of the interior, e.g. baffles for facilitating the mixing of components
    • B01F35/531Mixing receptacles characterised by the configuration of the interior, e.g. baffles for facilitating the mixing of components with baffles, plates or bars on the wall or the bottom
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/006Baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • B01J19/20Stationary reactors having moving elements inside in the form of helices, e.g. screw reactors

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The present invention provides a kind of reaction kettles, can solve the setting of existing agitating shaft and stirring blade, can not realize the technical issues of stirring and mixed effect are poor comprehensively.The reaction kettle, it is characterised in that:Stirrer paddle includes being fixed on the first stirrer paddle, the second stirrer paddle and the 3rd stirrer paddle on agitating shaft from top to bottom, and the first stirrer paddle is less than the radius of spin of the second stirrer paddle for the radius of spin that helical-ribbon type blade, the second stirrer paddle and the 3rd stirrer paddle are turbine type blade and the 3rd stirrer paddle;Corresponding first stirrer paddle, the second stirrer paddle and the 3rd stirrer paddle are separately installed with first baffle, second baffle and third baffle on the madial wall of autoclave body, first baffle, second baffle and third baffle are successively decreased successively along the width of agitating shaft radial direction, and second baffle and third baffle are uniformly provided with deflector hole respectively.

Description

A kind of reaction kettle
Technical field
The present invention relates to chemical reaction devices, and in particular to a kind of reaction kettle.
Background technology
Reaction kettle is a kind of reaction vessel, by the structure design and parameter configuration to container, realizes adding for technological requirement The mixture function of hot, evaporation, cooling and low high speed.The setting of the agitating shaft and stirring blade of traditional reaction kettle, can not realize Stirring comprehensively, and mixed effect is poor, influences product quality, so as to reduce production efficiency.
The content of the invention
In view of the above-mentioned problems, the present invention provides a kind of reaction kettle, setting for existing agitating shaft and stirring blade can be solved It puts, can not realize the technical issues of stirring and mixed effect are poor comprehensively.
Its technical solution is a kind of such, reaction kettle, including autoclave body, motor, agitating shaft and stirrer paddle, the kettle Upper end, the lower end of body are accordingly equipped with upper cover, low head, and the motor is fixed on the upper cover, the one end of the mixing shaft Connect the shaft of the motor, the other end stretches into the autoclave body and rotational support is in the axis body bearing of autoclave body bottom, feature It is:The stirrer paddle include being fixed on from top to bottom the first stirrer paddle on the agitating shaft, the second stirrer paddle and 3rd stirrer paddle, the first stirrer paddle are turbine type paddle for helical-ribbon type blade, the second stirrer paddle and the 3rd stirrer paddle The radius of spin of leaf and the 3rd stirrer paddle is less than the radius of spin of the second stirrer paddle;It is corresponding on the madial wall of the autoclave body First stirrer paddle, the second stirrer paddle and the 3rd stirrer paddle are separately installed with first baffle, second baffle and third baffle, The first baffle, second baffle and third baffle are successively decreased successively along the width of agitating shaft radial direction, the second baffle and the 3rd Baffle is uniformly provided with deflector hole respectively.
Further, first stirrer paddle is arranged in pairs, between the first paired stirrer paddle by with agitating shaft Affixed they sup-port.
Further, the first baffle, second baffle and third baffle pass through the inside of baffle bearing and autoclave body respectively Wall is fixedly connected and gap setting.
Further, be arranged with inner sleeve and housing outside the autoclave body and low head successively, the inner sleeve and the autoclave body it Between cavity in spiral deflector is installed, the inner side end and end face outside of the deflector respectively with the autoclave body Lateral wall, the madial wall of the inner sleeve are tightly connected to form spiral flow-guiding channel, and upper end, the lower end of the inner sleeve are corresponding Equipped with being taken over what the flow-guiding channel connected, thermal insulation material is filled in the cavity between the housing and the autoclave body.
Further, the axis body bearing includes support plate, pressing plate, copper sheathing and support feet, and the support plate is circumferentially fixed There is support feet, the support feet is fixed on the autoclave body bottom, and the support plate and and support plate are fixed in the copper sheathing setting Perforation face, one end of the copper sheathing and support plate adjoining is equipped with the male half coupling of radial direction, and the pressing plate is sheathed on the copper sheathing Outside and equipped with concave mouth corresponding with the male half coupling, the pressing plate is fixedly connected with the support plate.
Further, the upper end head is equipped with manhole and the first end having with manhole cooperation that is connected through the hinge Lid, the manhole periphery are equipped with link block, are connected with connecting rod by shaft on the link block, are covered from bottom to top on the connecting rod Equipped with spring, briquetting, the connecting rod top is threaded with the knob for being pressed the briquetting, and the briquetting is equipped with strip, described First end is covered with the card slot with strip cooperation.
Further, the first end is covered equipped with thief hole, and the second end cap is threaded on thief hole.
The present invention reaction kettle, by be fixed on agitating shaft from top to bottom be distributed helical-ribbon type the first stirrer paddle, The second stirrer paddle and the 3rd stirrer paddle of turbine type, corresponding first stirrer paddle, the second agitating paddle on the madial wall of autoclave body Leaf and the 3rd stirrer paddle are separately installed with first baffle, second baffle and third baffle, can realize comprehensive stirring;And the 3rd The radius of spin of stirrer paddle is less than the radius of spin of the second stirrer paddle, and first baffle, second baffle and third baffle edge are stirred The width for mixing axis radial direction successively decreases successively, and second baffle and third baffle are uniformly provided with deflector hole respectively, can take into account liquid On the premise of viscosity influences blade life, it is ensured that be sufficiently mixed.
Description of the drawings
Fig. 1 is the structural diagram of the present invention.
Fig. 2 is the structure diagram after the partial enlargement in Fig. 1 at A.
Fig. 3 is the structure diagram after the partial enlargement in Fig. 1 at B.
Fig. 4 is the structure diagram after the partial enlargement in Fig. 1 at C.
Fig. 5 is the structure diagram after the partial enlargement at manhole position in Fig. 1.
Specific embodiment
As shown in Fig. 1 ~ Fig. 5, a kind of reaction kettle, including autoclave body 1, motor 14, agitating shaft 15 and stirrer paddle, autoclave body 1 Upper end, lower end upper cover 7, low head 8 are accordingly installed, motor 14 is fixed on upper cover 7, agitating shaft by motor support base 13 The shaft of 15 one end connection motor, the other end stretches into autoclave body 1 and rotational support is in the axis body bearing of 1 bottom of autoclave body, agitating paddle Leaf includes the first stirrer paddle 16, the second stirrer paddle 18 and the 3rd stirrer paddle that are fixed on from top to bottom on agitating shaft 15 19, the first stirrer paddle 16 for helical-ribbon type blade, the second stirrer paddle 18 and the 3rd stirrer paddle 19 be turbine type blade simultaneously And the 3rd the radius of spin of stirrer paddle 19 be less than the radius of spin of the second stirrer paddle 18, the first stirrer paddle 16 sets in pairs It puts, is supported between the first paired stirrer paddle 16 by the supporting rod 17 affixed with agitating shaft 15;It is right on the madial wall of autoclave body 1 The first stirrer paddle 16, the second stirrer paddle 18 and the 3rd stirrer paddle 19 is answered to be separately installed with first baffle 36, second baffle 37 and third baffle 38, first baffle 36, second baffle 37 and third baffle 38 successively decrease successively along the width of 15 radial direction of agitating shaft, Second baffle 37 and third baffle 38 are uniformly provided with deflector hole, first baffle 36, second baffle 37 and third baffle 38 respectively It is fixedly connected with simultaneously gap setting with the madial wall of autoclave body 1 by baffle bearing respectively.
Inner sleeve 2 and housing 3 are arranged with successively outside autoclave body 1 and low head 8, installation in the cavity 5 between inner sleeve 2 and autoclave body 1 Have a spiral deflector 4, the inner side end and end face outside of deflector 4 respectively with the lateral wall of autoclave body 1, the inside of inner sleeve 2 Wall is tightly connected to form spiral flow-guiding channel, and the upper end of inner sleeve 2 is equipped with the take over 9 connected with flow-guiding channel, tube bank 11, Tube bank 11 is equipped with plug 12, and the lower end of inner sleeve 2 is equipped with the take over 10 connected with flow-guiding channel, the chamber between housing 3 and autoclave body 1 Thermal insulation material 6 is filled in body 5.
Axis body bearing includes support plate 22, pressing plate 25, copper sheathing 24 and support feet 23, and support plate 22 is circumferentially fixed support feet 23, support feet 23 is fixed on 1 bottom of autoclave body, the setting of copper sheathing 24 be fixed on support plate 22 and with the perforation face of support plate 22, copper Set 24 is equipped with the male half couplings of radial direction with one end that support plate 22 abuts, and it is outer and be equipped with and male half coupling pair that pressing plate 25 is sheathed on copper sheathing 24 The concave mouth answered, pressing plate are fixedly connected with support plate 22, and 25 be chuck, are sheathed on outside copper sheathing and are fixedly connected with pressing plate 25.
Upper end head is equipped with manhole 21 and is connected with the first end cap 26 coordinated with manhole 21, manhole 21 by hinge 27 Periphery is equipped with link block 30, is connected with connecting rod 31 by shaft on link block 30, is arranged with spring, pressure on connecting rod 31 from bottom to top Block 32,31 top of connecting rod are threaded with the knob 33 of press fitting briquetting 32, and briquetting 32 is equipped with strip, and the outer 34 of the first end cap is set There is the card slot with strip cooperation, sealing ring 35 is embedded on the lower face of the first end cap;First end cap 26 is equipped with thief hole 28, The second end cap 29 is threaded on thief hole 28.
20 be support feet 23 in Fig. 1, is used to support entire reaction kettle.

Claims (7)

1. a kind of reaction kettle, including autoclave body, motor, agitating shaft and stirrer paddle, upper end, the lower end of the autoclave body are accordingly installed There are upper cover, a low head, the motor is fixed on the upper cover, and the one end of the mixing shaft connects the shaft, another of the motor One end is stretched into the autoclave body and rotational support is in the axis body bearing of autoclave body bottom, it is characterised in that:The stirrer paddle includes The first stirrer paddle, the second stirrer paddle and the 3rd stirrer paddle being fixed on from top to bottom on the agitating shaft, the first stirring Blade is the spiral shell that helical-ribbon type blade, the second stirrer paddle and the 3rd stirrer paddle are turbine type blade and the 3rd stirrer paddle Revolve the radius of spin that radius is less than the second stirrer paddle;Corresponding first stirrer paddle, the second stirring on the madial wall of the autoclave body Blade and the 3rd stirrer paddle are separately installed with first baffle, second baffle and third baffle, the first baffle, second baffle Successively decrease successively along the width of agitating shaft radial direction with third baffle, the second baffle and third baffle are uniformly provided with water conservancy diversion respectively Hole.
2. a kind of reaction kettle according to claim 1, it is characterised in that:First stirrer paddle is arranged in pairs, in pairs The first stirrer paddle between pass through the they sup-port affixed with agitating shaft.
3. a kind of reaction kettle according to claim 1, it is characterised in that:The first baffle, second baffle and third gear Plate is fixedly connected respectively by baffle bearing with the madial wall of autoclave body and gap setting.
4. a kind of reaction kettle according to claim 1, it is characterised in that:In being arranged with successively outside the autoclave body and low head Set and housing are equipped with spiral deflector, the inside of the deflector in the cavity between the inner sleeve and the autoclave body End face and end face outside are tightly connected to form spiral lead respectively with the madial wall of the lateral wall of the autoclave body, the inner sleeve Circulation road, upper end, the lower end of the inner sleeve are correspondingly provided with to be taken over what the flow-guiding channel connected, the housing and the autoclave body Between cavity in be filled with thermal insulation material.
5. a kind of reaction kettle according to claim 1, it is characterised in that:The axis body bearing includes support plate, pressing plate, copper Set and support feet, the support plate is circumferentially fixed support feet, and the support feet is fixed on the autoclave body bottom, and the copper sheathing erects It is vertical be fixed on the support plate and with the perforation face of support plate, the copper sheathing is with one end that support plate abuts equipped with the convex of radial direction Seam allowance, the pressing plate are sheathed on outside the copper sheathing and equipped with concave mouth corresponding with the male half coupling, the pressing plate and the branch Fagging is fixedly connected.
6. a kind of reaction kettle according to claim 1, it is characterised in that:The upper end head is equipped with manhole and passes through hinge Chain link has the first end cap with manhole cooperation, and the manhole periphery is equipped with link block, passes through shaft on the link block Connecting rod is connected with, is arranged with spring, briquetting on the connecting rod from bottom to top, the connecting rod top is threaded with the press fitting pressure The knob of block, the briquetting are equipped with strip, and the first end is covered with the card slot with strip cooperation.
7. a kind of reaction kettle according to claim 6, it is characterised in that:The first end is covered equipped with thief hole, sampling The second end cap is threaded on hole.
CN201711453512.3A 2017-12-28 2017-12-28 A kind of reaction kettle Pending CN108057409A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711453512.3A CN108057409A (en) 2017-12-28 2017-12-28 A kind of reaction kettle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711453512.3A CN108057409A (en) 2017-12-28 2017-12-28 A kind of reaction kettle

Publications (1)

Publication Number Publication Date
CN108057409A true CN108057409A (en) 2018-05-22

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108905946A (en) * 2018-09-05 2018-11-30 上海世卿防滑防护科技有限公司 A kind of novel gas-liquid reaction kettle and its stirring mixing method
CN109777678A (en) * 2019-02-28 2019-05-21 南通中集安瑞科食品装备有限公司 Agitating device and container with the agitating device

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH08252444A (en) * 1996-03-22 1996-10-01 Sumitomo Heavy Ind Ltd Stirrer
CN202113867U (en) * 2011-06-14 2012-01-18 安徽亚兰德新能源材料有限公司 Special reactor for producing dynamic spherical nickel hydroxide
CN102921366A (en) * 2011-08-11 2013-02-13 许洪军 Helical ribbon type reaction kettle with double stirrers arranged at top and bottom
CN203525634U (en) * 2013-11-01 2014-04-09 长沙中联重科环卫机械有限公司 Agitation device and agitation system
CN203916555U (en) * 2014-06-24 2014-11-05 湖州华仑助剂科技有限公司 The two stirring type water cement grinding aids stirred tanks of a kind of mechanical gas
CN204485713U (en) * 2015-03-18 2015-07-22 长岭炼化岳阳工程设计有限公司 A kind of catalyst cake stirred tank
CN205386443U (en) * 2016-02-23 2016-07-20 绍兴县邦德助剂有限公司 But reation kettle stirring rake of independent assortment
CN206652498U (en) * 2017-04-21 2017-11-21 青海快驴电动汽车科技有限公司 A kind of reactor for being used to prepare micron order threadiness nickel oxalate
CN207823020U (en) * 2017-12-28 2018-09-07 无锡其宏包装材料厂 A kind of reaction kettle

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH08252444A (en) * 1996-03-22 1996-10-01 Sumitomo Heavy Ind Ltd Stirrer
CN202113867U (en) * 2011-06-14 2012-01-18 安徽亚兰德新能源材料有限公司 Special reactor for producing dynamic spherical nickel hydroxide
CN102921366A (en) * 2011-08-11 2013-02-13 许洪军 Helical ribbon type reaction kettle with double stirrers arranged at top and bottom
CN203525634U (en) * 2013-11-01 2014-04-09 长沙中联重科环卫机械有限公司 Agitation device and agitation system
CN203916555U (en) * 2014-06-24 2014-11-05 湖州华仑助剂科技有限公司 The two stirring type water cement grinding aids stirred tanks of a kind of mechanical gas
CN204485713U (en) * 2015-03-18 2015-07-22 长岭炼化岳阳工程设计有限公司 A kind of catalyst cake stirred tank
CN205386443U (en) * 2016-02-23 2016-07-20 绍兴县邦德助剂有限公司 But reation kettle stirring rake of independent assortment
CN206652498U (en) * 2017-04-21 2017-11-21 青海快驴电动汽车科技有限公司 A kind of reactor for being used to prepare micron order threadiness nickel oxalate
CN207823020U (en) * 2017-12-28 2018-09-07 无锡其宏包装材料厂 A kind of reaction kettle

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108905946A (en) * 2018-09-05 2018-11-30 上海世卿防滑防护科技有限公司 A kind of novel gas-liquid reaction kettle and its stirring mixing method
CN108905946B (en) * 2018-09-05 2024-01-23 上海世卿防滑防护科技有限公司 Novel gas-liquid reaction kettle and stirring and mixing method thereof
CN109777678A (en) * 2019-02-28 2019-05-21 南通中集安瑞科食品装备有限公司 Agitating device and container with the agitating device

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