CN108047944A - A kind of antirust agent and preparation method thereof - Google Patents
A kind of antirust agent and preparation method thereof Download PDFInfo
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- CN108047944A CN108047944A CN201711183545.0A CN201711183545A CN108047944A CN 108047944 A CN108047944 A CN 108047944A CN 201711183545 A CN201711183545 A CN 201711183545A CN 108047944 A CN108047944 A CN 108047944A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D191/00—Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D4/00—Coating compositions, e.g. paints, varnishes or lacquers, based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; Coating compositions, based on monomers of macromolecular compounds of groups C09D183/00 - C09D183/16
- C09D4/06—Organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond in combination with a macromolecular compound other than an unsaturated polymer of groups C09D159/00 - C09D187/00
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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Abstract
The present invention provides a kind of antirust agent and preparation method thereof.Preparation method is as follows：Step 1:By sulfurized lard, hydrogenation Oleum Verniciae fordii, oil-soluble silicon wax, dinonyl naphthalene sulfonate barium, dodecenylsuccinic acid, 3 (3,5 di-t-butyl, 4 hydroxy phenyl) Isooctyl acrylate monomer and oxidized petrolatum barium soap mixing, stir 10 20min under 200 250r/min of rotating speed under ultrasound condition；Step 2:Polyacrylamide, guar gum and water are mixed, are heated to 60 70 DEG C, stirs 10 20min；Step 3:Above-mentioned mixed liquor is mixed, adds remaining ingredient, is cooled to room temperature, vibration mixes to obtain the final product.The antirust agent of the present invention, has extraordinary salt tolerant fog effect and moisture-proof thermal effect, and rust-proof effect is very good.
Description
Technical field
The present invention relates to the chemical synthesis agent fields used in metal working technical area, and in particular to a kind of antirust agent and
Its preparation method.
Background technology
Metal material occurs caused by chemistry, electrochemistry and physical reactions to go bad and destroy to be known as metal with ambient enviroment
Corrosion, wherein corrosion is most common metal erosion form, and surface oxidisation can make performance and the business of metal product and mechanical equipment
Product value is greatly damaged or even can cause major accident.Investigation result is shown：Countries in the world every year because metal erosion and
The economic loss brought accounts for the 2%~4% of its gross national product, considerably beyond every annual because of fire, floods, disaster caused by a windstorm, earthquake
Etc. loss caused by disasters, caused by indirect loss it is then more surprising and be difficult to estimate.Therefore people exist for a long time
It is constantly explored on the road of anti-corruption antirust, is one of currently used method wherein antirust agent is selected to protect metal product.
The content of the invention
Technical problems to be solved：It is an object of the invention to provide a kind of antirust agent, have extraordinary salt tolerant fog effect with
And moisture-proof thermal effect, rust-proof effect are very good.
Technical solution：A kind of antirust agent, includes in parts by weight：30-50 parts of sulfurized lard, hydrogenation 20-30 parts of Oleum Verniciae fordii,
5-10 parts of oil-soluble silicon wax, 2-5 parts of dinonyl naphthalene sulfonate barium, 2-4 parts of dodecenylsuccinic acid, 4-8 parts of Laurate alcohol ester phenylacetate,
3-6 parts of castor oil polyoxyethylene ether, 3-6 parts of methyl glycol fatty acid ester, 5-10 parts of polyacrylamide, 2-5 parts of guar gum, oxidation stone
1-2 parts of grease barium soap, 1-3 parts of dibutyl hydroxy toluene, 3- (3,5- di-tert-butyl-hydroxy phenyls) Isooctyl acrylate monomer 1-3
Part, 0.5-1 parts of dialkyl diphenylamine, 1-3 parts of modified soy bean lipoid, 2-5 parts of molecule distillating monoglyceride, 15-25 parts of water.
It is further preferred that a kind of antirust agent, includes in parts by weight：40 parts of sulfurized lard, hydrogenation Oleum Verniciae fordii
25 parts, 7.5 parts of oil-soluble silicon wax, 3.5 parts of dinonyl naphthalene sulfonate barium, 3 parts of dodecenylsuccinic acid, 6 parts of Laurate alcohol ester phenylacetate,
4.5 parts of castor oil polyoxyethylene ether, 4.5 parts of methyl glycol fatty acid ester, 7 parts of polyacrylamide, 3.5 parts of guar gum, petroleum oxidate
1.5 parts of fat barium soap, 2 parts of dibutyl hydroxy toluene, 2 parts of 3- (3,5- di-tert-butyl-hydroxy phenyls) Isooctyl acrylate monomer, dioxane
0.8 part of base diphenylamines, 2 parts of modified soy bean lipoid, 3.5 parts of molecule distillating monoglyceride, 20 parts of water.
The preparation method of above-mentioned antirust agent comprises the following steps：
Step 1:By sulfurized lard, hydrogenation Oleum Verniciae fordii, oil-soluble silicon wax, dinonyl naphthalene sulfonate barium, dodecenylsuccinic acid, 3-
(3,5- di-tert-butyl-hydroxy phenyl) Isooctyl acrylate monomer and oxidized petrolatum barium soap mixing, the rotating speed under ultrasound condition
10-20min is stirred under 200-250r/min；
Step 2:Polyacrylamide, guar gum and water are mixed, are heated to 60-70 DEG C, stirs 10-20min；
Step 3:Above-mentioned mixed liquor is mixed, adds remaining ingredient, is cooled to room temperature, vibration mixes to obtain the final product.
It is further preferred that rotating speed is 230r/min in step 1.
It is further preferred that heating temperature is 65 DEG C in step 2, mixing time 15min.
Advantageous effect：The present invention antirust agent have extraordinary salt tolerant fog effect and moisture-proof thermal effect, cold-reduced sheet and
Galvanized sheet passes through SH/T0533 anti-corrosive grease rust prevention test test pieces after salt spray test, lamination experiment and damp heat test
All reach 1 grade after the grading of corrosion assessment method, rust-proof effect is very good, and sample stands intact substantially.
Specific embodiment
Embodiment 1
A kind of antirust agent, includes in parts by weight：30 parts of sulfurized lard, 20 parts of Oleum Verniciae fordii of hydrogenation, 5 parts of oil-soluble silicon wax, two nonyls
2 parts of base naphthalene sulfonate barium, 2 parts of dodecenylsuccinic acid, 4 parts of Laurate alcohol ester phenylacetate, 3 parts of castor oil polyoxyethylene ether, propylene glycol
3 parts of aliphatic ester, 5 parts of polyacrylamide, 2 parts of guar gum, 1 part of oxidized petrolatum barium soap, 1 part of dibutyl hydroxy toluene, 3- (3,
5- di-tert-butyl-hydroxy phenyls) 1 part of Isooctyl acrylate monomer, 0.5 part of dialkyl diphenylamine, 1 part of modified soy bean lipoid, molecule
Distill 2 parts of monoglyceride, 15 parts of water.
The preparation method of above-mentioned antirust agent is：
Step 1:By sulfurized lard, hydrogenation Oleum Verniciae fordii, oil-soluble silicon wax, dinonyl naphthalene sulfonate barium, dodecenylsuccinic acid, 3-
(3,5- di-tert-butyl-hydroxy phenyl) Isooctyl acrylate monomer and oxidized petrolatum barium soap mixing, the rotating speed under ultrasound condition
10min is stirred under 200r/min；
Step 2:Polyacrylamide, guar gum and water are mixed, are heated to 60 DEG C, stirs 10min；
Step 3:Above-mentioned mixed liquor is mixed, adds remaining ingredient, is cooled to room temperature, vibration mixes to obtain the final product.
Embodiment 2
A kind of antirust agent, includes in parts by weight：35 parts of sulfurized lard, 25 parts of Oleum Verniciae fordii of hydrogenation, 6 parts of oil-soluble silicon wax, two nonyls
3 parts of base naphthalene sulfonate barium, 3 parts of dodecenylsuccinic acid, 5 parts of Laurate alcohol ester phenylacetate, 4 parts of castor oil polyoxyethylene ether, propylene glycol
4 parts of aliphatic ester, 6 parts of polyacrylamide, 3 parts of guar gum, 1.5 parts of oxidized petrolatum barium soap, 1.5 parts of dibutyl hydroxy toluene,
1.5 parts of 3- (3,5- di-tert-butyl-hydroxy phenyls) Isooctyl acrylate monomer, 0.6 part of dialkyl diphenylamine, modified soy bean lipoid
1.5 parts, 3 parts of molecule distillating monoglyceride, 20 parts of water.
The preparation method of above-mentioned antirust agent is：
Step 1:By sulfurized lard, hydrogenation Oleum Verniciae fordii, oil-soluble silicon wax, dinonyl naphthalene sulfonate barium, dodecenylsuccinic acid, 3-
(3,5- di-tert-butyl-hydroxy phenyl) Isooctyl acrylate monomer and oxidized petrolatum barium soap mixing, the rotating speed under ultrasound condition
10-20min is stirred under 220r/min；
Step 2:Polyacrylamide, guar gum and water are mixed, are heated to 65 DEG C, stirs 15min；
Step 3:Above-mentioned mixed liquor is mixed, adds remaining ingredient, is cooled to room temperature, vibration mixes to obtain the final product.
Embodiment 3
A kind of antirust agent, includes in parts by weight：40 parts of sulfurized lard, 25 parts of Oleum Verniciae fordii of hydrogenation, 7.5 parts of oil-soluble silicon wax, two
3.5 parts of nonyl naphthalene barium sulfonate, 3 parts of dodecenylsuccinic acid, 6 parts of Laurate alcohol ester phenylacetate, 4.5 parts of castor oil polyoxyethylene ether,
4.5 parts of methyl glycol fatty acid ester, 7 parts of polyacrylamide, 3.5 parts of guar gum, 1.5 parts of oxidized petrolatum barium soap, dibutyl hydroxy
2 parts of toluene, 2 parts of 3- (3,5- di-tert-butyl-hydroxy phenyls) Isooctyl acrylate monomer, 0.8 part of dialkyl diphenylamine, modified soybean
Phosphatidase 2 part, 3.5 parts of molecule distillating monoglyceride, 20 parts of water.
The preparation method of above-mentioned antirust agent is：
Step 1:By sulfurized lard, hydrogenation Oleum Verniciae fordii, oil-soluble silicon wax, dinonyl naphthalene sulfonate barium, dodecenylsuccinic acid, 3-
(3,5- di-tert-butyl-hydroxy phenyl) Isooctyl acrylate monomer and oxidized petrolatum barium soap mixing, the rotating speed under ultrasound condition
15min is stirred under 230r/min；
Step 2:Polyacrylamide, guar gum and water are mixed, are heated to 65 DEG C, stirs 15min；
Step 3:Above-mentioned mixed liquor is mixed, adds remaining ingredient, is cooled to room temperature, vibration mixes to obtain the final product.
Embodiment 4
A kind of antirust agent, includes in parts by weight：45 parts of sulfurized lard, 25 parts of Oleum Verniciae fordii of hydrogenation, 9 parts of oil-soluble silicon wax, two nonyls
4 parts of base naphthalene sulfonate barium, 3.5 parts of dodecenylsuccinic acid, 7 parts of Laurate alcohol ester phenylacetate, 5 parts of castor oil polyoxyethylene ether, the third two
5 parts of alcohol fatty acid ester, 9 parts of polyacrylamide, 4 parts of guar gum, 1.5 parts of oxidized petrolatum barium soap, dibutyl hydroxy toluene 2.5
Part, 2.5 parts of 3- (3,5- di-tert-butyl-hydroxy phenyls) Isooctyl acrylate monomer, 0.9 part of dialkyl diphenylamine, modified soybean phosphorus
2.5 parts of fat, 4 parts of molecule distillating monoglyceride, 20 parts of water.
The preparation method of above-mentioned antirust agent is：
Step 1:By sulfurized lard, hydrogenation Oleum Verniciae fordii, oil-soluble silicon wax, dinonyl naphthalene sulfonate barium, dodecenylsuccinic acid, 3-
(3,5- di-tert-butyl-hydroxy phenyl) Isooctyl acrylate monomer and oxidized petrolatum barium soap mixing, the rotating speed under ultrasound condition
15min is stirred under 240r/min；
Step 2:Polyacrylamide, guar gum and water are mixed, are heated to 65 DEG C, stirs 15min；
Step 3:Above-mentioned mixed liquor is mixed, adds remaining ingredient, is cooled to room temperature, vibration mixes to obtain the final product.
Embodiment 5
A kind of antirust agent, includes in parts by weight：50 parts of sulfurized lard, 30 parts of Oleum Verniciae fordii of hydrogenation, 10 parts of oil-soluble silicon wax, two nonyls
5 parts of base naphthalene sulfonate barium, 4 parts of dodecenylsuccinic acid, 8 parts of Laurate alcohol ester phenylacetate, 6 parts of castor oil polyoxyethylene ether, propylene glycol
6 parts of aliphatic ester, 10 parts of polyacrylamide, 5 parts of guar gum, 2 parts of oxidized petrolatum barium soap, 3 parts of dibutyl hydroxy toluene, 3-
3 parts of (3,5- di-tert-butyl-hydroxy phenyls) Isooctyl acrylate monomer, 1 part of dialkyl diphenylamine, 3 parts of modified soy bean lipoid, molecule
Distill 5 parts of monoglyceride, 25 parts of water.
The preparation method of above-mentioned antirust agent is：
Step 1:By sulfurized lard, hydrogenation Oleum Verniciae fordii, oil-soluble silicon wax, dinonyl naphthalene sulfonate barium, dodecenylsuccinic acid, 3-
(3,5- di-tert-butyl-hydroxy phenyl) Isooctyl acrylate monomer and oxidized petrolatum barium soap mixing, the rotating speed under ultrasound condition
20min is stirred under 250r/min；
Step 2:Polyacrylamide, guar gum and water are mixed, are heated to 70 DEG C, stirs 20min；
Step 3:Above-mentioned mixed liquor is mixed, adds remaining ingredient, is cooled to room temperature, vibration mixes to obtain the final product.
Comparative example 1
Difference lies in replace hydrogenation Oleum Verniciae fordii with sulfurized lard with embodiment 1 for the present embodiment.Specifically：
A kind of antirust agent, includes in parts by weight：50 parts of sulfurized lard, 5 parts of oil-soluble silicon wax, 2 parts of dinonyl naphthalene sulfonate barium, ten
2 parts of dialkylene succinic acid, 4 parts of Laurate alcohol ester phenylacetate, 3 parts of castor oil polyoxyethylene ether, 3 parts of methyl glycol fatty acid ester, poly- third
5 parts of acrylamide, 2 parts of guar gum, 1 part of oxidized petrolatum barium soap, 1 part of dibutyl hydroxy toluene, 3- (3,5- di-t-butyl -4- hydroxyls
Base phenyl) 1 part of Isooctyl acrylate monomer, 0.5 part of dialkyl diphenylamine, 1 part of modified soy bean lipoid, 2 parts of molecule distillating monoglyceride, water
15 parts.
The preparation method of above-mentioned antirust agent is：
Step 1:By sulfurized lard, oil-soluble silicon wax, dinonyl naphthalene sulfonate barium, dodecenylsuccinic acid, 3- (bis- tertiary fourths of 3,5-
Base -4- hydroxy phenyls) Isooctyl acrylate monomer and oxidized petrolatum barium soap mixing, stirred under ultrasound condition under rotating speed 200r/min
10min；
Step 2:Polyacrylamide, guar gum and water are mixed, are heated to 60 DEG C, stirs 10min；
Step 3:Above-mentioned mixed liquor is mixed, adds remaining ingredient, is cooled to room temperature, vibration mixes to obtain the final product.
Comparative example 2
Difference lies in do not contain polyacrylamide and guar gum with embodiment 1 for the present embodiment.Specifically：
A kind of antirust agent, includes in parts by weight：30 parts of sulfurized lard, 20 parts of Oleum Verniciae fordii of hydrogenation, 5 parts of oil-soluble silicon wax, two nonyls
2 parts of base naphthalene sulfonate barium, 2 parts of dodecenylsuccinic acid, 4 parts of Laurate alcohol ester phenylacetate, 3 parts of castor oil polyoxyethylene ether, propylene glycol
3 parts of aliphatic ester, 1 part of oxidized petrolatum barium soap, 1 part of dibutyl hydroxy toluene, 3- (3,5- di-tert-butyl-hydroxy phenyls) third
1 part of the different monooctyl ester of olefin(e) acid, 0.5 part of dialkyl diphenylamine, 1 part of modified soy bean lipoid, 2 parts of molecule distillating monoglyceride, 15 parts of water.
The preparation method of above-mentioned antirust agent is：
Step 1:By sulfurized lard, hydrogenation Oleum Verniciae fordii, oil-soluble silicon wax, dinonyl naphthalene sulfonate barium, dodecenylsuccinic acid, 3-
(3,5- di-tert-butyl-hydroxy phenyl) Isooctyl acrylate monomer and oxidized petrolatum barium soap mixing, the rotating speed under ultrasound condition
10min is stirred under 200r/min；
Step 2:It adds in remaining ingredient, is cooled to room temperature, vibration mixes to obtain the final product.
Comparative example 3
Difference lies in do not contain oil-soluble silicon wax with embodiment 1 for the present embodiment.Specifically：
A kind of antirust agent, includes in parts by weight：30 parts of sulfurized lard, hydrogenation 20 parts of Oleum Verniciae fordii, 2 parts of dinonyl naphthalene sulfonate barium,
It is 2 parts of dodecenylsuccinic acid, 4 parts of Laurate alcohol ester phenylacetate, 3 parts of castor oil polyoxyethylene ether, 3 parts of methyl glycol fatty acid ester, poly-
5 parts of acrylamide, 2 parts of guar gum, 1 part of oxidized petrolatum barium soap, 1 part of dibutyl hydroxy toluene, 3- (3,5- di-t-butyls -4-
Hydroxy phenyl) 1 part of Isooctyl acrylate monomer, 0.5 part of dialkyl diphenylamine, 1 part of modified soy bean lipoid, 2 parts of molecule distillating monoglyceride,
15 parts of water.
The preparation method of above-mentioned antirust agent is：
Step 1:By sulfurized lard, hydrogenation Oleum Verniciae fordii, dinonyl naphthalene sulfonate barium, dodecenylsuccinic acid, 3- (bis- tertiary fourths of 3,5-
Base -4- hydroxy phenyls) Isooctyl acrylate monomer and oxidized petrolatum barium soap mixing, stirred under ultrasound condition under rotating speed 200r/min
10min；
Step 2:Polyacrylamide, guar gum and water are mixed, are heated to 60 DEG C, stirs 10min；
Step 3:Above-mentioned mixed liquor is mixed, adds remaining ingredient, is cooled to room temperature, vibration mixes to obtain the final product.
Performance evaluation：
Test material：Steel plate uses cold-reduced sheet, is polished into minute surface；Zine plate uses zinc-plated raw sheet, spare after oil removing.
Salt spray test：8 h of constant temperature, naturally cold after reference 0081 standards of SH/T, i.e. test piece are heated to 35 DEG C in salt fog cabinet
But to room temperature, 16 h of standing are a test period (d), test 2 d.
Lamination is tested：8 h of constant temperature after reference 0367 standards of SH, i.e. test piece are heated to 49 ± 1 DEG C in damp and hot slot is natural
It is cooled to room temperature, 16 h of standing are a test period (d), test 20 d.
Damp heat test：By 80 standards of GB/T 2361-, i.e. test piece is heated to 49 ± 1 DEG C in damp and hot examination case, and test piece frame turns
Speed is 0.33 ± 0.01 r/min, and continuous to run 8 h, out of service, 16 h of standing are a test period (d), test 15 d.
Test piece is graded by SH/T0533 anti-corrosive grease rust prevention test test piece corrosion assessment methods.
Table 1
From upper table 1, the antirust agent of the application has extraordinary salt tolerant fog effect and moisture-proof thermal effect, cold-reduced sheet and plating
Zine plate becomes rusty after salt spray test, lamination experiment and damp heat test by SH/T0533 anti-corrosive grease rust prevention tests test piece
All reach 1 grade after erosion assessment method grading, rust-proof effect is very good, and sample stands intact substantially.
Claims (5)
1. a kind of antirust agent, it is characterised in that：Include in parts by weight：30-50 parts of sulfurized lard, hydrogenation 20-30 parts of Oleum Verniciae fordii,
5-10 parts of oil-soluble silicon wax, 2-5 parts of dinonyl naphthalene sulfonate barium, 2-4 parts of dodecenylsuccinic acid, 4-8 parts of Laurate alcohol ester phenylacetate,
3-6 parts of castor oil polyoxyethylene ether, 3-6 parts of methyl glycol fatty acid ester, 5-10 parts of polyacrylamide, 2-5 parts of guar gum, oxidation stone
1-2 parts of grease barium soap, 1-3 parts of dibutyl hydroxy toluene, 3- (3,5- di-tert-butyl-hydroxy phenyls) Isooctyl acrylate monomer 1-3
Part, 0.5-1 parts of dialkyl diphenylamine, 1-3 parts of modified soy bean lipoid, 2-5 parts of molecule distillating monoglyceride, 15-25 parts of water.
2. a kind of antirust agent according to claim 1, it is characterised in that：Include in parts by weight：40 parts of sulfurized lard, hydrogen
Change 25 parts of Oleum Verniciae fordii, 7.5 parts of oil-soluble silicon wax, 3.5 parts of dinonyl naphthalene sulfonate barium, 3 parts of dodecenylsuccinic acid, phenylacetic acid bay
6 parts of alcohol ester, 4.5 parts of castor oil polyoxyethylene ether, 4.5 parts of methyl glycol fatty acid ester, 7 parts of polyacrylamide, 3.5 parts of guar gum,
1.5 parts of oxidized petrolatum barium soap, 2 parts of dibutyl hydroxy toluene, 3- (3,5- di-tert-butyl-hydroxy phenyls) Isooctyl acrylate monomer
2 parts, 0.8 part of dialkyl diphenylamine, 2 parts of modified soy bean lipoid, 3.5 parts of molecule distillating monoglyceride, 20 parts of water.
3. the preparation method of claim 1 to 2 any one of them antirust agent, it is characterised in that：Comprise the following steps：
Step 1:By sulfurized lard, hydrogenation Oleum Verniciae fordii, oil-soluble silicon wax, dinonyl naphthalene sulfonate barium, dodecenylsuccinic acid, 3-
(3,5- di-tert-butyl-hydroxy phenyl) Isooctyl acrylate monomer and oxidized petrolatum barium soap mixing, the rotating speed under ultrasound condition
10-20min is stirred under 200-250r/min；
Step 2:Polyacrylamide, guar gum and water are mixed, are heated to 60-70 DEG C, stirs 10-20min；
Step 3:Above-mentioned mixed liquor is mixed, adds remaining ingredient, is cooled to room temperature, vibration mixes to obtain the final product.
4. the preparation method of antirust agent according to claim 1, it is characterised in that：Rotating speed is 230r/ in the step 1
min。
5. the preparation method of antirust agent according to claim 1, it is characterised in that：Heating temperature is 65 in the step 2
DEG C, mixing time 15min.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711183545.0A CN108047944A (en) | 2017-11-23 | 2017-11-23 | A kind of antirust agent and preparation method thereof |
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| CN201711183545.0A CN108047944A (en) | 2017-11-23 | 2017-11-23 | A kind of antirust agent and preparation method thereof |
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| CN106281621A (en) * | 2016-08-17 | 2017-01-04 | 吴江华威特种油有限公司 | A kind of anticorrosive oil composition and preparation method thereof |
| CN106634324A (en) * | 2016-09-27 | 2017-05-10 | 李昌柱 | High-efficient water-based antirust paint and preparation method thereof |
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2017
- 2017-11-23 CN CN201711183545.0A patent/CN108047944A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103087808A (en) * | 2012-10-12 | 2013-05-08 | 布兰诺工业包装材料(上海)有限公司 | Fast-drying hard film rust preventive oil and preparation method thereof |
| CN104250580A (en) * | 2013-06-26 | 2014-12-31 | 中国石油化工股份有限公司 | Antirust oil composition and application thereof |
| CN104498168A (en) * | 2014-12-31 | 2015-04-08 | 芜湖华金冲压加工件厂 | Water-based lubricant for metal stamping |
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| CN106634324A (en) * | 2016-09-27 | 2017-05-10 | 李昌柱 | High-efficient water-based antirust paint and preparation method thereof |
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