CN108047005A - A kind of energy-saving dimethyl ether production system - Google Patents

A kind of energy-saving dimethyl ether production system Download PDF

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Publication number
CN108047005A
CN108047005A CN201711435438.2A CN201711435438A CN108047005A CN 108047005 A CN108047005 A CN 108047005A CN 201711435438 A CN201711435438 A CN 201711435438A CN 108047005 A CN108047005 A CN 108047005A
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CN
China
Prior art keywords
babinet
dimethyl ether
effect
fixedly connected
energy
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711435438.2A
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Chinese (zh)
Inventor
凡殿才
吴珍汉
刘克朝
王超
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anhui Haoyuan Chemical Industry (Group) Co Ltd
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Anhui Haoyuan Chemical Industry (Group) Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anhui Haoyuan Chemical Industry (Group) Co Ltd filed Critical Anhui Haoyuan Chemical Industry (Group) Co Ltd
Priority to CN201711435438.2A priority Critical patent/CN108047005A/en
Publication of CN108047005A publication Critical patent/CN108047005A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01Preparation of ethers
    • C07C41/09Preparation of ethers by dehydration of compounds containing hydroxy groups
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F24HEATING; RANGES; VENTILATING
    • F24HFLUID HEATERS, e.g. WATER OR AIR HEATERS, HAVING HEAT-GENERATING MEANS, e.g. HEAT PUMPS, IN GENERAL
    • F24H3/00Air heaters
    • F24H3/02Air heaters with forced circulation
    • F24H3/04Air heaters with forced circulation the air being in direct contact with the heating medium, e.g. electric heating element
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Combustion & Propulsion (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

The invention discloses a kind of energy-saving dimethyl ether production systems, including the first babinet, filler pipe is communicated at the top of first babinet, the second babinet is provided on the right side of first babinet, the 3rd babinet is provided on the right side of second babinet, the 4th babinet is provided on the right side of the 3rd babinet.The present invention is by setting the first babinet, achieve the effect that place synthesis gas, pass through heat block, achieve the effect that heat synthesis gas, pass through the second babinet, achieve the effect that produce dimethyl ether, pass through the 3rd babinet, achieve the effect that cool down dimethyl ether, pass through motor, achieve the effect that drive rotation axis rotation, pass through rotation axis, achieve the effect that drive fixed plate rotation, the assimilation effect of dimethyl ether and soft water can be increased, pass through the 4th babinet, achieve the effect that manufacture dimethyl ether with high purity, the production system is not required big energy to be catalyzed when generating dimethyl ether, energy dissipation will not be made, it is convenient for people to use.

Description

A kind of energy-saving dimethyl ether production system
Technical field
The present invention relates to dimethyl ether production equipment technologies, are specially a kind of energy-saving dimethyl ether production system.
Background technology
Dimethyl ether is used mainly as the spray carrier of aerosol industry at present, and the purposes of dimethyl ether is continuous in recent years obtains With exploitation, it such as can be used as aerosol propellant, mix refrigerant can also be used as vapour, diesel engine alternative fuel and directly It substitutes oil liquefied gas and makees domestic fuel, in addition, dimethyl ether is also used as clean fuel and for producing the dilute hydrocarbon of low-carbon, dive It is huge in market, dimethyl ether needs to be chemically reacted using process units in production, and existing process units exists When generating dimethyl ether big energy is needed to be catalyzed, it is easy to energy dissipation is caused, so as to add the consumption of cost.
The content of the invention
Technical problems based on background technology, the present invention propose one kind, have dimethyl ether need not in production The characteristics of big energy is catalyzed, does not easily cause energy dissipation, solve dimethyl ether needs big energy to be urged when generating The problem of changing, be easy to causeing energy dissipation.
The present invention provides following technical solution:A kind of energy-saving dimethyl ether production system, including the first babinet, described first Filler pipe is communicated at the top of babinet, the second babinet is provided on the right side of first babinet, is set on the right side of second babinet The 3rd babinet is equipped with, the 4th babinet is provided on the right side of the 3rd babinet, collecting box is provided at the top of the 4th babinet, Discharge nozzle is communicated at the top of the collecting box;
It is fixedly connected with heat block on the left of first cabinets cavity, the bottom on the right side of first cabinets cavity is fixed Temperature sensor is connected with, second babinet is internally provided with metal-zeolitic dual-function catalyst, the 3rd babinet Top is fixedly connected with motor, and the shaft of the motor is fixedly connected with rotation axis, and the bottom of the rotation axis extends to the 3rd The inside of babinet has been fixedly connected with connecting rod at the top and bottom of the rotation axis both sides, and the connecting rod is away from rotation axis One end be fixedly connected with fixed plate.
Preferably, the bottom on the right side of first babinet is connected by the first connecting tube with the second babinet, second case Top on the right side of body is connected by the second connecting tube with the 3rd babinet, and the surface of second connecting tube is provided with heat exchanger, institute It states the top on the right side of the 3rd babinet to connect with the 4th babinet by the 3rd connecting tube, the 4th casing top passes on left Four connecting tubes are connected with collecting box.
Preferably, the surface of the fixed plate offers through hole, and the quantity of the through hole is several, and in equidistant point Cloth.
Preferably, the bottom of the rotation axis is fixedly connected with connecting plate, and the both sides of the connecting plate bottom are fixed to be connected Sliding block is connected to, the bottom of the 3rd cabinets cavity offers sliding slot, and the sliding block is slidably connected with sliding slot.
Preferably, be fixedly connected with wind turbine on the right side of the collecting box bottom, the air inlet of the wind turbine by pipeline with Collecting box connects, and the air outlet of the wind turbine is connected by pipeline with the 4th babinet.
Compared with prior art, beneficial effects of the present invention are as follows:
1st, the present invention achievees the effect that place synthesis gas, by heat block, reach to synthesis gas by setting the first babinet The effect of heating by the second babinet, achievees the effect that produce dimethyl ether, by the 3rd babinet, reaches and dimethyl ether is cooled down Effect, by motor, achieve the effect that drive rotation axis rotation, by rotation axis, achieve the effect that drive fixed plate rotation, The assimilation effect of dimethyl ether and soft water can be increased, by the 4th babinet, achieve the effect that manufacture dimethyl ether with high purity, the production system System is not required big energy to be catalyzed when generating dimethyl ether, will not make energy dissipation, convenient for people to use.
2nd, the present invention achievees the effect that, to temperature detection in the first babinet, to avoid the occurrence of temperature mistake by temperature sensor High situation by metal-zeolitic dual-function catalyst, achievees the effect that avoiding the occurrence of can not give birth to auxiliary dimethyl ether production The situation of dimethyl ether is produced, by heat exchanger, achievees the effect that heat dimethyl ether, by connecting rod, reaches and fixed plate is supported Effect, avoid the occurrence of the situation to drop, by through hole, the effect of stirring can be increased, by connecting plate, reach auxiliary fixing plate The effect of stirring can increase the effect of stirring, by sliding block and sliding slot, achieve the effect that auxiliary connection board rotates, avoid the occurrence of The situation that connecting plate drops by wind turbine, can be cycled the dimethyl ether in collecting box, it is ensured that the uniformity of dimethyl ether.
Description of the drawings
Fig. 1 is a kind of schematic diagram proposed by the present invention;
Fig. 2 is the sectional view of the 3rd babinet of the invention.
In figure:1 first babinet, 2 filler pipes, 3 second babinets, 4 the 3rd babinets, 5 the 4th babinets, 6 collecting boxs, 7 discharge nozzles, 8 heat blocks, 9 temperature sensors, 10 metals-zeolitic dual-function catalyst, 11 motors, 12 rotation axis, 13 connecting rods, 14 are fixed Plate, 15 first connecting tubes, 16 second connecting tubes, 17 heat exchangers, 18 the 3rd connecting tubes, 19 the 4th connecting tubes, 20 through holes, 21 connections Plate, 22 sliding blocks, 23 sliding slots, 24 wind turbines.
Specific embodiment
Below in conjunction with the attached drawing in the embodiment of the present invention, the technical solution in the embodiment of the present invention is carried out clear, complete Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, those of ordinary skill in the art are obtained every other without making creative work Embodiment belongs to the scope of protection of the invention.
- 2 are please referred to Fig.1, a kind of energy-saving dimethyl ether production system, including the first babinet 1, the inside of the first babinet 1 is set Composite catalyst Cu-ZnA1/HZSM-5 is equipped with, the bottom on 1 right side of the first babinet is connected by the first connecting tube 15 and the second babinet 3 Logical, the top on 3 right side of the second babinet is connected by the second connecting tube 16 with the 3rd babinet 4, and the surface of the second connecting tube 16 is set There is heat exchanger 17, by heat exchanger 17, achieve the effect that heat dimethyl ether, the top on 4 right side of the 3rd babinet connects by the 3rd Take over 18 connects with the 4th babinet 5, and the 4th connecting tube 19 that passes on left at 5 top of the 4th babinet is connected with collecting box 6, the first case The top of body 1 is communicated with filler pipe 2, and the right side of the first babinet 1 is provided with the second babinet 3, and the right side of the second babinet 3 is provided with Three babinets 4, the right side of the 3rd babinet 4 are provided with the 4th babinet 5, and the top of the 4th babinet 5 is provided with collecting box 6,6 bottom of collecting box Wind turbine 24 is fixedly connected on the right side of portion, by wind turbine 24, can be cycled the dimethyl ether in collecting box 6, it is ensured that diformazan The uniformity of ether, the air inlet of wind turbine 24 are connected by pipeline with collecting box 6, and the air outlet of wind turbine 24 passes through pipeline and the 4th case Body 5 connects, and the top of collecting box 6 is communicated with discharge nozzle 7;
Heat block 8 is fixedly connected on the left of first babinet, 1 inner cavity, temperature can be heated to 250 to 280 DEG C by heat block 8, Pressure inside first babinet 1 is 2.0 to 5.0MPA, and air speed is 500 to 2000/h, and the bottom on the right side of 1 inner cavity of the first babinet is consolidated Surely temperature sensor 9 is connected with, by temperature sensor 9, achievees the effect that, to temperature detection in the first babinet 1, to avoid the occurrence of The excessively high situation of temperature, the second babinet 3 are internally provided with metal-zeolitic dual-function catalyst 10, and metal-zeolite is difunctional to urge III types of model SD219- of agent 10 by metal-zeolitic dual-function catalyst 10, reach the effect to auxiliary dimethyl ether production Fruit, avoids the occurrence of the situation that can not produce dimethyl ether, and the top of the 3rd babinet 4 is fixedly connected with motor 11, the shaft of motor 11 Rotation axis 12 is fixedly connected with, the bottom of rotation axis 12 is fixedly connected with connecting plate 21, by connecting plate 21, reaches auxiliary and fixes The effect that plate 14 stirs, can increase the effect of stirring, the both sides of 21 bottom of connecting plate have been fixedly connected with sliding block 22, the 3rd babinet The bottom of 4 inner cavities offers sliding slot 23, and sliding block 22 is slidably connected with sliding slot 23, by sliding block 22 and sliding slot 23, reaches auxiliary and connects The effect that fishplate bar 21 rotates, avoids the occurrence of the situation that connecting plate 21 drops, the bottom of rotation axis 12 extends to the interior of the 3rd babinet 4 Portion, rotation axis have been fixedly connected with connecting rod 13 at the top and bottom of 12 both sides, by connecting rod 13, reach to fixed plate 14 The effect of support avoids the occurrence of the situation to drop, and the one end of connecting rod 13 away from rotation axis 12 is fixedly connected with fixed plate 14, fixed The surface of plate 14 offers through hole 20, by through hole 20, can increase the effect of stirring, the quantity of through hole 20 is several, and is in It is equally spaced, by setting the first babinet 1, achievees the effect that place synthesis gas, by heat block 8, reach and synthesis gas is heated Effect, by the second babinet 3, achieve the effect that produce dimethyl ether, by the 3rd babinet 4, reach to dimethyl ether cooling Effect by motor 11, achievees the effect that rotation axis 12 is driven to rotate, by rotation axis 12, reaches and fixed plate 14 is driven to rotate Effect, the assimilation effect of dimethyl ether and soft water can be increased, by the 4th babinet 5, achieve the effect that manufacture dimethyl ether with high purity, The production system is not required big energy to be catalyzed when generating dimethyl ether, will not make energy dissipation, convenient for people to use.
In use, by setting the first babinet 1, achieve the effect that place synthesis gas, by heat block 8, reach to synthesis The effect of gas heating by the second babinet 3, achievees the effect that produce dimethyl ether, by the 3rd babinet 4, reach to dimethyl ether The effect of cooling by motor 11, achievees the effect that rotation axis 12 is driven to rotate, by rotation axis 12, reaches drive fixed plate The effect of 14 rotations, can increase the assimilation effect of dimethyl ether and soft water, by the 4th babinet 5, reach manufacture dimethyl ether with high purity Effect, which is not required big energy to be catalyzed, will not make energy dissipation, be convenient for people to when generating dimethyl ether Use.
In summary:The energy-saving dimethyl ether production system passes through the first babinet 1, the second babinet 3, the 3rd babinet 4, The cooperation of four babinets 5, collecting box 6, heat block 8, metal-zeolitic dual-function catalyst 10, motor 11 and fixed plate 14 solves two The problem of methyl ether needs big energy to be catalyzed, be easy to cause energy dissipation when generating.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto, Any one skilled in the art in the technical scope disclosed by the present invention, technique according to the invention scheme and its Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (5)

1. a kind of energy-saving dimethyl ether production system, including the first babinet (1), it is characterised in that:The top of first babinet (1) Portion is communicated with filler pipe (2), and the second babinet (3), the right side of second babinet (3) are provided on the right side of first babinet (1) Side is provided with the 3rd babinet (4), and the 4th babinet (5) is provided on the right side of the 3rd babinet (4), the 4th babinet (5) Top is provided with collecting box (6), and discharge nozzle (7) is communicated at the top of the collecting box (6);
It is fixedly connected with heat block (8) on the left of first babinet (1) inner cavity, the bottom on the right side of the first babinet (1) inner cavity Portion is fixedly connected with temperature sensor (9), and second babinet (3) is internally provided with metal-zeolitic dual-function catalyst (10), motor (11) is fixedly connected at the top of the 3rd babinet (4), the shaft of the motor (11) is fixedly connected with rotation Axis (12), the bottom of the rotation axis (12) extend to the inside of the 3rd babinet (4), the top of rotation axis (12) both sides and Bottom has been fixedly connected with connecting rod (13), and the one end of the connecting rod (13) away from rotation axis (12) is fixedly connected with fixed plate (14)。
2. a kind of energy-saving dimethyl ether production system according to claim 1, it is characterised in that:First babinet (1) The bottom on right side is connected by the first connecting tube (15) with the second babinet (3), and the top on the right side of second babinet (3) passes through Two connecting tubes (16) are connected with the 3rd babinet (4), and the surface of second connecting tube (16) is provided with heat exchanger (17), and described Top on the right side of three babinets (4) is connected by the 3rd connecting tube (18) with the 4th babinet (5), at the top of the 4th babinet (5) The 4th connecting tube (19) is passed on left to connect with collecting box (6).
3. a kind of energy-saving dimethyl ether production system according to claim 1, it is characterised in that:The fixed plate (14) Surface offers through hole (20), and the quantity of the through hole (20) is several, and is in be equally spaced.
4. a kind of energy-saving dimethyl ether production system according to claim 1, it is characterised in that:The rotation axis (12) Bottom is fixedly connected with connecting plate (21), and the both sides of connecting plate (21) bottom have been fixedly connected with sliding block (22), and described The bottom of three babinets (4) inner cavity offers sliding slot (23), and the sliding block (22) is slidably connected with sliding slot (23).
5. a kind of energy-saving dimethyl ether production system according to claim 1, it is characterised in that:Collecting box (6) bottom Wind turbine (24) is fixedly connected on the right side of portion, the air inlet of the wind turbine (24) is connected by pipeline with collecting box (6), the wind The air outlet of machine (24) is connected by pipeline with the 4th babinet (5).
CN201711435438.2A 2017-12-26 2017-12-26 A kind of energy-saving dimethyl ether production system Pending CN108047005A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711435438.2A CN108047005A (en) 2017-12-26 2017-12-26 A kind of energy-saving dimethyl ether production system

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711435438.2A CN108047005A (en) 2017-12-26 2017-12-26 A kind of energy-saving dimethyl ether production system

Publications (1)

Publication Number Publication Date
CN108047005A true CN108047005A (en) 2018-05-18

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CN201711435438.2A Pending CN108047005A (en) 2017-12-26 2017-12-26 A kind of energy-saving dimethyl ether production system

Country Status (1)

Country Link
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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2389710Y (en) * 1999-09-28 2000-08-02 周至譓 Solvent recovery device
AU2002302124B2 (en) * 2001-11-07 2004-01-22 Air Products And Chemicals, Inc. Separation process for one-step production of dimethyl ether from synthesis gas
US20060287405A1 (en) * 2005-06-17 2006-12-21 Korea Gas Corporation Process for the preparation of dimethylether from hydrocarbons
CN101033427A (en) * 2007-04-04 2007-09-12 苏宏文 Dimethyl ether prepared from marsh gas and preparing method for the same
CN101687747A (en) * 2007-07-12 2010-03-31 赫多特普索化工设备公司 Process for the preparation of dimethyl ether
CN203916433U (en) * 2014-04-18 2014-11-05 罗先武 A kind of gas cleaning plant
CN206613418U (en) * 2017-03-09 2017-11-07 南京源港精细化工有限公司 One kind mixes oar

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2389710Y (en) * 1999-09-28 2000-08-02 周至譓 Solvent recovery device
AU2002302124B2 (en) * 2001-11-07 2004-01-22 Air Products And Chemicals, Inc. Separation process for one-step production of dimethyl ether from synthesis gas
US20060287405A1 (en) * 2005-06-17 2006-12-21 Korea Gas Corporation Process for the preparation of dimethylether from hydrocarbons
CN101033427A (en) * 2007-04-04 2007-09-12 苏宏文 Dimethyl ether prepared from marsh gas and preparing method for the same
CN101687747A (en) * 2007-07-12 2010-03-31 赫多特普索化工设备公司 Process for the preparation of dimethyl ether
CN203916433U (en) * 2014-04-18 2014-11-05 罗先武 A kind of gas cleaning plant
CN206613418U (en) * 2017-03-09 2017-11-07 南京源港精细化工有限公司 One kind mixes oar

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Application publication date: 20180518