CN108030863A - A kind of concocting method of hand ginseng and its hand ginseng powder, the granule pieces of gained - Google Patents
A kind of concocting method of hand ginseng and its hand ginseng powder, the granule pieces of gained Download PDFInfo
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- CN108030863A CN108030863A CN201711365583.8A CN201711365583A CN108030863A CN 108030863 A CN108030863 A CN 108030863A CN 201711365583 A CN201711365583 A CN 201711365583A CN 108030863 A CN108030863 A CN 108030863A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/898—Orchidaceae (Orchid family)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
- A61K9/16—Agglomerates; Granulates; Microbeadlets ; Microspheres; Pellets; Solid products obtained by spray drying, spray freeze drying, spray congealing,(multiple) emulsion solvent evaporation or extraction
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/12—Materials from mammals; Compositions comprising non-specified tissues or cells; Compositions comprising non-embryonic stem cells; Genetically modified cells
- A61K35/20—Milk; Whey; Colostrum
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Abstract
The present invention provides a kind of concocting method of hand ginseng and its hand ginseng powder, the granule pieces of gained.A kind of concocting method of hand ginseng, comprises the following steps：The milk of its weight 30% 200% is added in Xiang Shoucan, when infiltration 2 10 is small, is then taken out, it is dry at 60 80 DEG C.The concocting method of the present invention can be sufficiently reserved the active ingredient in hand ginseng, and improve the dissolution rate of ethanol soluble extractives, and the effect of tonifying Qi of the kidney of enhancing milk opponent's ginseng, improves the anti-aging of hand ginseng and oxidation resistant activity.
Description
Technical field
The present invention relates to the field of Chinese medicines, hand ginseng powder, the particle of concocting method and its gained more particularly, to a kind of hand ginseng
Medicine materical crude slice.
Background technology
Traditional Chinese medicine is the sharp keen weapon that the mankind struggle with disease, there is thousands of years of developing history, the category of Chinese medicine
It is various, there are more than 5000 to plant.Hand ginseng is mainly grown in the range of Qinghai-Tibet 2700~4000m of height above sea level in free of contamination bushes,
Other provinces and regions are also distributed.Modern medicine study shows that Gymnadenia conopsea contains ginsenoside, various saccharides, vitamin and mineral matter
Etc. multiple biological activities component, there is increase Brain circlulation, brain tonic enhancing memory, antiallergy, anti-oxidant, antifatigue, raising to be immunized
Power and other effects, has very high medical value, thus has the title of " not old grass ".Research finds that Gymnadenia conopsea is to senile dementia recently
The treatment and prevention significant effect of disease, further causes the extensive concern of domestic and international expert.
As traditional Tibetan medicine, hand ginseng is often taken together with milk, to have the function that to improve drug effect,《Ministry standard》Middle hand
The recommendation usage of ginseng is taken after mixing it with water with warm milk.With milk process hand join traditional handicraft be：First hand is joined in milk for a long time
Infiltration, then takes out drying.This concocting method does not have the synergistic effect given full play between milk and hand ginseng, can not be effective
Improve hand ginseng anti-aging and oxidation resistant activity.
In view of this, it is special to propose the present invention.
The content of the invention
The first object of the present invention is to provide a kind of concocting method of hand ginseng, and the concocting method can be sufficiently reserved
Active ingredient in hand ginseng, and the dissolution rate of ethanol soluble extractives is improved, the effect of tonifying Qi of the kidney of enhancing milk opponent's ginseng, from
And improve the anti-aging of hand ginseng and oxidation resistant activity.
The second object of the present invention is to provide a kind of hand ginseng powder, hand ginseng powder anti-aging and oxidation resistant active ratio
Existing product significantly improves.
The third object of the present invention is to provide a kind of granule of rhizome gymnadeniae medicine materical crude slice, the granule of rhizome gymnadeniae medicine materical crude slice not only anti-aging
Improved with oxidation resistant activity, and it is easy to use, both it can be used alone, can also compounding use.
In order to solve the above technical problems, the present invention provides following technical scheme：
A kind of concocting method of hand ginseng, comprises the following steps：
The milk of its weight 30%-200% is added in Xiang Shoucan, when infiltration 2-10 is small, is then taken out, at 60-80 DEG C
It is dry.
Difference of the invention with traditional concocting method is changing the condition of infiltration, and the baking after infiltration is existed
Carried out in former milk bath, so that milk is effectively cooperateed with hand ginseng, the effect of tonifying Qi of the kidney of enhancing hand ginseng.To sum up, the present invention is logical
Cross above Improving Measurements and avoid the effusion of active ingredient in hand ginseng, volatilization or rotten, improve its anti-aging and oxidation resistant work
Property, while improve the dissolution rate of ethanol soluble extractives, moreover it is possible to the toxic side effect of hand ginseng is more reduced, ensures drug safety
With it is effective.
Milk used in the present invention preferably uses fresh milk.
Above method can also be improved further, to reach more technique effects：
Preferably, the addition of the milk is the 30%-80% of hand ginseng.
Preferably, further included before the milk of its weight 30%-200% is added in the ginseng to hand：
Hand ginseng is processed into the thin slice that thickness is 1-2mm.
The specific surface area that hand joins on the one hand is improved by cutting into slices, increases its contact area with milk, on the other hand can be with
Reduce the difficulty of following process, moreover it is possible to improve product homogeneity.
The drying is that drying to water content is below 10wt%.
Water content influences the shelf-life of medicinal material, preferable by below 9.5wt% of water content with reference to cost consideration.
Preferably, the medicinal material obtained by above-mentioned concocting method can be used as crude drug to be used alone, or be compounded with other medicinal materials
Use, or continue to be processed into the medicinal material of other forms, such as continue to be ground into hand ginseng powder.
Preferably, the method for crushing is that ultramicro grinding to granularity is 33~180 μm.
After ultramicro grinding, dissolubility, dispersiveness, adsorptivity, the chemical reactivity etc. of hand ginseng are improved, in water
Dissolution rate and dissolution rate higher, but particle diameter is meticulous has little effect, but cost is substantially improved, and considers, preferable particle diameter
For 33~180 μm.
Preferably, the method for the ultramicro grinding is：
When crushing 1 is small at 10-20 DEG C or so, TYM-30 micronizers can be selected in pulverizer.
Preferably, before being infiltrated with milk, the impurity examined in qualified hand ginseng is removed, cleans, dries, more than
Pretreatment, lifts product quality.
Powder is joined using hand made from above method
Following quality index can at least be reached：
The content of Gastrodin be more than 0.15wt% in hand ginseng powder, the content of p-Hydroxybenzylalcohol be 0.11wt% with
On.
Preferably, the weight percentage of ethanol soluble extractives is more than 10.65% in the hand ginseng powder.
Equally, hand ginseng powder can be used alone made from process above, and also can be formulated compound with other Chinese medicines shares.As
For Instant Drinks medicament in use, being preferably made following medicament：
That is hand ginseng powder is formed through being granulated.
Preferably, the method for the granulation is：
Join the mixed liquor that alcohol-water is added in powder to hand, stir evenly, softwood is made, pelletized by granulator, then sieve
Whole grain；The volume ratio of ethanol is 60-80% in the mixed liquor of the alcohol-water.
Adding the mixed liquor of 60-80% alcohol-waters can make granulation uniform and be made it have with reference to the characteristic that hand is joined suitable
When mobility, so as to be agglomerated into the particle for being easy to dissolution in alcohol-water, moreover it is possible to further enhance hand ginseng and tonify Qi of the kidney work
With can also effectively prevent the isolation of active ingredient.
After granule pieces are made using above-mentioned any means, packed with infusion packet, can directly rush convert into suspension, immersion or
Decoction liquor is taken, and instructions of taking is convenient and absorptivity is high.Infusion packet standard pack used, uniform specification, encapsulation is tight, is not easy
The moisture absorption, avoids Chinese medicine storage or quality problems such as go rancid, change colour, damaging by worms, going mouldy that improper storage is brought.
To sum up, compared with prior art, invention achieves following technique effect：
(1) effect that hand ginseng is tonified Qi of the kidney, and anti-aging and oxidation resistant activity are improved；
(2) content of active ingredient in hand ginseng powder is improved；
(3) dissolution rate of hand ginseng powder ethanol soluble extractives is improved；
(4) quality control processed is realized；
(5) any excipients are free of in hand ginseng Ultramicro-powder or granular medicine, not only can effectively keep the Chinese medicine in itself
Possessed all natural characteristic, and its preparation process is very simple, easily forms industrialized production.
Embodiment
Technical scheme is clearly and completely described below in conjunction with embodiment, but ability
Field technique personnel will be understood that following described embodiment is part of the embodiment of the present invention, instead of all the embodiments,
The present invention is merely to illustrate, and is not construed as limiting the scope of the invention.Based on the embodiments of the present invention, the common skill in this area
Art personnel all other embodiments obtained without making creative work, belong to the model that the present invention protects
Enclose.The person that is not specified actual conditions in embodiment, the condition suggested according to normal condition or manufacturer carry out.Agents useful for same or instrument
Production firm person is not specified, is the conventional products that can be obtained by commercially available purchase.
The following embodiments of the present invention are based primarily upon the technique for being processed hand with milk and being joined：
Add the milk of its weight 30%-200% in Xiang Shoucan, when infiltration 2-10 is small, then decocted at 60-80 DEG C to
Juice is boiled dry.
Preferably, the addition of the milk is the 30%-80% of hand ginseng.
Preferably, further included before the milk of its weight 30%-200% is added in the ginseng to hand：
Hand ginseng is processed into the thin slice that thickness is 1-2mm.
Preferably, the decoction is that decoction to water content is below 10wt%.
A kind of hand joins powder, after hand is considered and handled reason using concocting method presented above, crushes and obtains；
Preferably, the method for crushing is that ultramicro grinding to granularity is 33~180 μm.
Preferably, the content of Gastrodin is more than 0.15wt% in the hand ginseng powder, and the content of p-Hydroxybenzylalcohol is
More than 0.11wt%.
Preferably, the weight percentage of ethanol soluble extractives is more than 10.65% in the hand ginseng powder.
A kind of granule of rhizome gymnadeniae medicine materical crude slice, hand ginseng powder by mentioned earlier are formed through being granulated.
Preferably, the method for the granulation is：
Join the mixed liquor that alcohol-water is added in powder to hand, stir evenly, softwood is made, pelletized by granulator, then sieve
Whole grain；The volume ratio of ethanol is 60-80% in the mixed liquor of the alcohol-water.
Preferably, the volume ratio of ethanol is 60%-80% in the mixed liquor of the alcohol-water.
Difference lies in the parameter of every step process difference for each embodiment of the present invention.
Embodiment 1
Process hand ginseng
The first step：Cleaning
Qualified hand will be examined to join Chinese medicine, remove impurity, clean, dry.
Second step：Section
Ginseng of washing one's hands is taken, hand ginseng medicinal material is cut into the thin slice of 1-2mm.
3rd step：Milk infiltrates
The milk of its weight 30% is added in Xiang Shoucan, when infiltration 2-10 is small.
3rd step：It is dry
Sufficient hand ginseng will be infiltrated to take out, the dry 8h at 60 DEG C.
4th step：Ultramicro grinding
Dried hand is joined into ultramicro grinding 10min, fineness scope is 180 μm or so.
Embodiment 2-6
Essentially consist in that to process milk amount used different from the difference of embodiment 1, respectively 60wt%, 80%, 100%,
150%th, 200%, corresponding drying time is respectively 8h, 8h, 8h, 8h, 17h, 17h.
Embodiment 7-10
It is different to essentially consist in the time of ultramicro grinding from the difference of embodiment 1, crush respectively 20min, 30min, 40min,
60min。
Embodiment 11
Granule of rhizome gymnadeniae potus
Process hand ginseng
The first step：Cleaning
Qualified hand will be examined to join Chinese medicine, remove impurity, clean, dry.
Second step：Section
Ginseng of washing one's hands is taken, hand ginseng medicinal material is cut into the thin slice of 1-2mm.
3rd step：Milk infiltrates
The milk of its weight 30% is added in Xiang Shoucan, when infiltration 2-10 is small.
3rd step：It is dry
Sufficient hand ginseng will be infiltrated to take out, the dry 8h at 60 DEG C.
4th step：Ultramicro grinding
Dried hand is joined into ultramicro grinding 10min, fineness scope is 180 μm or so.
5th step：Bonding
Join to hand and water (15mL is added per 50g), stirring granulation, dry at 60 DEG C, sieving are added in Ultramicro-powder.
Embodiment 12-14
It is different that the adhesive of granulation addition is essentially consisted in from the difference of embodiment 11, water is replaced with to 40% alcohol-water respectively
(20mL is added per 50g), 60% alcohol-water (27mL is added per 50g), 80% alcohol-water (35mL is added per 50g).
Embodiment 15-16
Difference lies in addition to immersion, also decocted, the addition of milk is respectively 150% in milk with embodiment 1
With 200%, in ginseng of going smoothly piece the content of Gastrodin and p-Hydroxybenzylalcohol be respectively 0.11% and 0.06% (embodiment 15),
0.08% and 0.05% (embodiment 16).
The technique of embodiment 15 is：
Process hand ginseng
The first step：Cleaning
Qualified hand will be examined to join Chinese medicine, remove impurity, clean, dry.
Second step：Section
Ginseng of washing one's hands is taken, hand ginseng medicinal material is cut into the thin slice of 1-2mm.
3rd step：Milk infiltrates
The milk of its weight 150% is added in Xiang Shoucan, when infiltration 2 is small, then decocts 2h.
3rd step：It is dry
Hand after decoction is joined and is taken out, the dry 8h at 60 DEG C, goes smoothly and join Gastrodin and p-Hydroxybenzylalcohol in piece
Content is respectively 0.11% and 0.06%.
4th step：Ultramicro grinding
Dried hand is joined into ultramicro grinding 10min, fineness scope is 180 μm or so.
Embodiment 16
From embodiment 15 difference lies in the addition of milk is different, 200%, Gastrodin and to hydroxyl in ginseng of going smoothly piece
The content of phenmethylol is respectively 0.08%, 0.05%.
Detect the moisture of dried hand ginseng piece in embodiment 1 to 6, alcohol extract content, gastrodin content and right
Salicylic alcohol content, the results are shown in Table 1.
Table 1
Embodiment 1,7-10 finally go smoothly ginseng powder particle diameter it is as shown in table 2, go smoothly and join Gastrodin and to hydroxyl in powder
The content of phenmethylol is as shown in table 3.
Table 2
Table 3
The quality of the potus of the gained of embodiment 11 to 14 is as shown in table 4.
Table 4
Contrast above example and understand that product provided by the present invention and method there are following characteristics：
1st, grinding time is longer, and particle diameter is about small, but alcohol extract in hand ginseng and Gastrodin and p-Hydroxybenzylalcohol
Content can reduce, and preferable grinding time is 10min；
When the 2nd, being processed with milk, it is not that milk dosage is the higher the better, is preferably added to 80% milk；
When the 3rd, making adhesive with the mixed liquor of alcohol-water, preferred alcohol volume ratio is 60% mixed liquor.
Finally it should be noted that：The above embodiments are only used to illustrate the technical solution of the present invention., rather than its limitations；To the greatest extent
Pipe is described in detail the present invention with reference to foregoing embodiments, it will be understood by those of ordinary skill in the art that：Its according to
Can so modify to the technical solution described in foregoing embodiments, either to which part or all technical characteristic into
Row equivalent substitution；And these modifications or replacement, the essence of appropriate technical solution is departed from various embodiments of the present invention technology
The scope of scheme.
Claims (10)
1. a kind of concocting method of hand ginseng, it is characterised in that comprise the following steps：
The milk of its weight 30%-200% is added in Xiang Shoucan, when infiltration 2-10 is small, is then taken out, it is dry at 60-80 DEG C.
2. the concocting method of hand ginseng according to claim 1, it is characterised in that the addition of the milk is joined for the hand
30%-80%.
3. the concocting method of hand ginseng according to claim 1, it is characterised in that add its weight in the ginseng to hand
Further included before the milk of 30%-200%：
Hand ginseng is processed into the thin slice that thickness is 1-2mm.
4. the concocting method of hand ginseng according to claim 1, it is characterised in that the drying is that drying to water content is
Below 10wt%.
5. a kind of hand joins powder, it is characterised in that after hand is considered and handled reason using the concocting method described in claim 1-4, crushes
And obtain；
Preferably, the method for crushing is that ultramicro grinding to granularity is 33~180 μm.
6. hand according to claim 5 joins powder, it is characterised in that the content of Gastrodin is 0.15wt% in the hand ginseng powder
More than, the content of p-Hydroxybenzylalcohol is more than 0.11wt%.
7. hand according to claim 5 joins powder, it is characterised in that the weight percent of ethanol soluble extractives in the hand ginseng powder
Content is more than 10.65%.
8. a kind of granule of rhizome gymnadeniae medicine materical crude slice, it is characterised in that powder is joined by claim 5-7 any one of them hand and is formed through being granulated.
9. granule of rhizome gymnadeniae medicine materical crude slice according to claim 8, it is characterised in that the method for the granulation is：
Join the mixed liquor that alcohol-water is added in powder to hand, stir evenly, softwood is made, pelletized by granulator, then sieve is whole
Grain；The volume ratio of ethanol is 0-80% in the mixed liquor of the alcohol-water.
10. granule of rhizome gymnadeniae medicine materical crude slice according to claim 9, it is characterised in that ethanol in the mixed liquor of the alcohol-water
Volume ratio is 60%-80%.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109276651A (en) * | 2018-10-23 | 2019-01-29 | 江西景德中药股份有限公司 | Gymnadenia conopsea medicine materical crude slice and its concocting method |
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| CN104147373A (en) * | 2014-08-25 | 2014-11-19 | 济南康众医药科技开发有限公司 | Preparation method of high-activity gymnadenia conopsea |
| CN106692687A (en) * | 2017-02-06 | 2017-05-24 | 奥乌力吉 | Quality improvement process for Mongolian medicine gymnadenia conopsea tuber |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104147373A (en) * | 2014-08-25 | 2014-11-19 | 济南康众医药科技开发有限公司 | Preparation method of high-activity gymnadenia conopsea |
| CN106692687A (en) * | 2017-02-06 | 2017-05-24 | 奥乌力吉 | Quality improvement process for Mongolian medicine gymnadenia conopsea tuber |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109276651A (en) * | 2018-10-23 | 2019-01-29 | 江西景德中药股份有限公司 | Gymnadenia conopsea medicine materical crude slice and its concocting method |
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