CN108030720A

CN108030720A - A kind of low energy consumption cosmetic composition emulsion stabilizer

Info

Publication number: CN108030720A
Application number: CN201711323016.6A
Authority: CN
Inventors: 沈华忠; 李易珊
Original assignee: Jane (guangzhou) Cosmetics Co Ltd
Current assignee: Jane (guangzhou) Cosmetics Co Ltd
Priority date: 2017-12-12
Filing date: 2017-12-12
Publication date: 2018-05-15

Abstract

The present invention provides a kind of low energy consumption cosmetic composition emulsion stabilizer, is made of following raw material：Stearic acid, olive oil, lanolin, citric acid, potassium sorbate, polyoxyethylene methyl glucoside stearate, polyethylene glycol, Jojoba, phosphatide and acrylic acid, compared with prior art, the present invention have following beneficial effect：The various cosmetic compositions that physicochemical property stabilization can be formed in cosmetic composition can be added in the emulsified oil water mixture of room temperature state.

Description

A kind of low energy consumption cosmetic composition emulsion stabilizer

Technical field

The present invention is a kind of low energy consumption cosmetic composition emulsion stabilizer, belongs to cosmetic technical field.

Background technology

With the development of medicine and cosmetic science, pursuit of the people to the securities of cosmetics and mildness is increasingly Height, environmentally protective to be praised highly by many responsible enterprises as large natural environment is destroyed, production technology is to low energy consumption, low dirt Dye, low consumption target stride forward, and the low consumption of the energy becomes following trend.

Therefore, it is necessary to a kind of cosmetic emulsifier combination for being capable of providing the low consumption energy and easily prepare；Also need Want a kind of cosmetic emulsifier combination for being capable of providing gentle safety；With greater need for a kind of makeup with excellent stability Product emulsifier combination.

The content of the invention

It is in view of the deficienciess of the prior art, steady with emulsification it is an object of the present invention to provide a kind of low energy consumption cosmetic composition Determine agent, to solve the problems mentioned in the above background technology.

To achieve these goals, the present invention is to realize by the following technical solutions：A kind of low energy consumption cosmetics group Compound emulsion stabilizer, is made of following raw material：Stearic acid, olive oil, lanolin, citric acid, potassium sorbate, polyoxyethylene Methyl glucoside stearate, polyethylene glycol, Jojoba, phosphatide and acrylic acid.

Further, the olive oil in raw material is a kind of Extra Virgin, olive oleic acid in the olive oil in raw material Degree is less than 0.8%.

Further, using potato dry powder, the starch dregs of rice and amyloid agricultural and sideline product as raw material, with culture medium, under normal pressure Boiling, is cooled to inoculation temperature, accesses koji, loads koji plate fermentation, then using calcium carbonate neutralization and the technique of sulfuric acid solution Zymotic fluid is extracted, obtains the citric acid in raw material.

Further, acetylene in tetrahydrofuran will be dissolved in, in the presence of the catalyst that nickelous bromide and copper bromide form, with one Carbonoxide and water reaction, are made acrylic acid, are solvent with tetrahydrofuran in the reaction, it is possible to reduce the danger of HIGH PRESSURE TREATMENT acetylene Danger；Catalyst does not have to the carbonyl nickel used in original Lei Peifa at the same time, need to use nickel salt, by propylene and air and vapor by necessarily rubbing You are than mixing, and in the presence of the composite catalysts such as molybdenum-bismuth, methacrylaldehyde is made in 310-470 DEG C of reaction temperature, atmospheric pressure oxidation, yield Mixed up to 90%, then by methacrylaldehyde with air and vapor by certain mol proportion, in the presence of the composite catalysts such as molybdenum-vanadium, reaction The acrylic acid in raw material is made in 300-470 DEG C of temperature, atmospheric pressure oxidation.

Further, add alchlor with the wool washing sewage of wool, obtain lanolated mud slurry, suck moisture, obtain rotten Mud, takes mud 600kg, adds benzene 480kg, stirring while adding, 56 DEG C of insulation 1h of heating, stop stirring, precipitate 1h, benzene liquid after clarification Lanolin 6%-40% is dissolved, is moved into destilling tower, heating distillation, up to 34%, is cooled to less than 40 DEG C releasings, obtains sheep to containing lanolin Hair fat crude product, takes lanolin crude product 2100kg to put into reaction pot, is heated to 50 DEG C, then 50% (g/g) sulfuric acid solution of heat is added In lanolin crude product, 45min is stirred, precipitates half an hour, benzene lipid layer adds light ethanol, adds water, 60 DEG C of heating and thermal insulation, it is small to stir half When, half an hour is precipitated, acid treatment benzene fat is obtained, takes acid treatment benzene fat to add ethanol 180kg, be gradually added 300g/L sodium hydroxide solutions About 70kg, adjusts pH9, adds water 180kg, keeps the temperature 60 DEG C, is continuously agitated from being added ethanol, is further continued for stirring to adding water to finish 10min, stands, and precipitates 1h, and benzene lipid layer adds light ethanol, stirs, and precipitates 1h, must neutralize benzene fat, takes and neutralizes benzene fat, adds 3.8% peroxide Change hydrogen 24kg, stirring, keeps the temperature 60 DEG C, precipitates 35min, keeps pH8-9, adds light ethanol, precipitates 2h, obtains commercial benzene fat, to refined Benzene fat is distilled, and 110 DEG C of liquid temperature is evaporated in vacuo untill not distilling, and is cooled to 60 DEG C, is added ethanol, is stirred, and precipitates 1h, separation Go out lower floor's lanolin, add ethanol, heating stirring 10min, discards ethanol, and ethanol to the greatest extent is steamed in decompression, and the filtering of spun silk cloth, obtains in raw material Lanolin.

Beneficial effects of the present invention：A kind of low energy consumption cosmetic composition emulsion stabilizer of the present invention, can be in room The emulsified oil water mixture of temperature state, is added to the various cosmetic combinations that physicochemical property stabilization can be formed in cosmetic composition Thing.

Embodiment

To make the technical means, the creative features, the aims and the efficiencies achieved by the present invention easy to understand, with reference to Embodiment, the present invention is further explained.

The present invention provides a kind of technical solution：A kind of low energy consumption cosmetic composition emulsion stabilizer, by following raw material Form：Stearic acid, olive oil, lanolin, citric acid, potassium sorbate, polyoxyethylene methyl glucoside stearate, poly- second two Alcohol, Jojoba, phosphatide and acrylic acid.

Olive oil in raw material is a kind of Extra Virgin, and olive oil acidity is less than in the olive oil in raw material 0.8%。

Using potato dry powder, the starch dregs of rice and amyloid agricultural and sideline product as raw material, with culture medium, under normal pressure boiling, cooling To inoculation temperature, koji is accessed, loads koji plate fermentation, is then neutralized using calcium carbonate and the technique of sulfuric acid solution extracts fermentation Liquid, obtains the citric acid in raw material.

Acetylene in tetrahydrofuran will be dissolved in, in the presence of the catalyst that nickelous bromide and copper bromide form, with carbon monoxide and Water reacts, and acrylic acid is made, is solvent with tetrahydrofuran in the reaction, it is possible to reduce the danger of HIGH PRESSURE TREATMENT acetylene；Urge at the same time Agent does not have to the carbonyl nickel used in original Lei Peifa, only need to use nickel salt, propylene is mixed with air and vapor by certain mol proportion, In the presence of the composite catalysts such as molybdenum-bismuth, methacrylaldehyde is made in 310-470 DEG C of reaction temperature, atmospheric pressure oxidation, and yield is up to 90%, then incites somebody to action Methacrylaldehyde is mixed with air and vapor by certain mol proportion, in the presence of the composite catalysts such as molybdenum-vanadium, reaction temperature 300- 470 DEG C, the acrylic acid in raw material is made in atmospheric pressure oxidation.

Add alchlor with the wool washing sewage of wool, obtain lanolated mud slurry, suck moisture, obtain mud, take mud 600kg, adds benzene 480kg, stirring while adding, 56 DEG C of insulation 1h of heating, stop stirring, precipitate 1h, benzene liquid dissolving wool after clarification Fat 6%-40%, moves into destilling tower, and heating distillation, up to 34%, is cooled to less than 40 DEG C releasings, it is thick to obtain lanolin to containing lanolin Product, take lanolin crude product 2100kg to put into reaction pot, are heated to 50 DEG C, then 50% (g/g) sulfuric acid solution of heat is added lanolin In crude product, 45min is stirred, precipitates half an hour, benzene lipid layer adds light ethanol, adds water, and 60 DEG C of heating and thermal insulation, is stirred half an hour, precipitation Half an hour, obtains acid treatment benzene fat, takes acid treatment benzene fat to add ethanol 180kg, is gradually added 300g/L sodium hydroxide solutions about 70kg, PH9 is adjusted, adds water 180kg, keeps the temperature 60 DEG C, is continuously agitated from being added ethanol, is further continued for stirring 10min, stands to adding water to finish, 1h is precipitated, benzene lipid layer adds light ethanol, stirs, and precipitates 1h, must neutralize benzene fat, takes and neutralizes benzene fat, adds 3.8% hydrogen peroxide 24kg, stir Mix, keep the temperature 60 DEG C, precipitate 35min, keep pH8-9, add light ethanol, precipitate 2h, obtain commercial benzene fat, commercial benzene fat is steamed Evaporate, 110 DEG C of liquid temperature is evaporated in vacuo untill not distilling, and is cooled to 60 DEG C, is added ethanol, is stirred, and is precipitated 1h, is isolated lower floor's wool Fat, adds ethanol, and heating stirring 10min, discards ethanol, and ethanol to the greatest extent is steamed in decompression, and the filtering of spun silk cloth, obtains the lanolin in raw material.

As one embodiment of the present of invention：A kind of low energy consumption cosmetic composition emulsion stabilizer of the present invention, can In the emulsified oil water mixture of room temperature state, to be added to the various makeups that physicochemical property stabilization can be formed in cosmetic composition Product composition.

The basic principles, main features and the advantages of the invention have been shown and described above, for this area skill For art personnel, it is clear that the invention is not restricted to the details of above-mentioned one exemplary embodiment, and without departing substantially from the present invention spirit or In the case of essential characteristic, the present invention can be realized in other specific forms.Therefore, in all respects, should all incite somebody to action Embodiment regards exemplary as, and is non-limiting, the scope of the present invention by appended claims rather than on state Bright restriction, it is intended that including all changes fallen in the implication and scope of the equivalency of claim in the present invention It is interior.

Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each embodiment is only wrapped Containing an independent technical solution, this narrating mode of specification is only that those skilled in the art should for clarity Using specification as an entirety, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art It is appreciated that other embodiment.

Claims

A kind of 1. low energy consumption cosmetic composition emulsion stabilizer, it is characterised in that：It is made of following raw material：Stearic acid, olive Olive oil, lanolin, citric acid, potassium sorbate, polyoxyethylene methyl glucoside stearate, polyethylene glycol, Jojoba, phosphatide And acrylic acid.
A kind of 2. low energy consumption cosmetic composition emulsion stabilizer according to claim 1, it is characterised in that：In raw material Olive oil be a kind of Extra Virgin, olive oil acidity is less than 0.8% in the olive oil in raw material.
A kind of 3. low energy consumption cosmetic composition emulsion stabilizer according to claim 1, it is characterised in that：Done with potato Powder, the starch dregs of rice and amyloid agricultural and sideline product are raw material, and with culture medium, boiling under normal pressure, is cooled to inoculation temperature, access Koji, loads koji plate fermentation, is then neutralized using calcium carbonate and the technique of sulfuric acid solution extracts zymotic fluid, obtain the lemon in raw material Lemon acid.
A kind of 4. low energy consumption cosmetic composition emulsion stabilizer according to claim 1, it is characterised in that：It will be dissolved in Acetylene in tetrahydrofuran, in the presence of the catalyst that nickelous bromide and copper bromide form, reacts with carbon monoxide and water, propylene is made Acid, is solvent with tetrahydrofuran in the reaction, it is possible to reduce the danger of HIGH PRESSURE TREATMENT acetylene；Catalyst does not have to former thunder pendant at the same time Carbonyl nickel used in method, only need to use nickel salt, propylene is mixed with air and vapor by certain mol proportion, compound in molybdenum-bismuth etc. In the presence of catalyst, methacrylaldehyde is made in 310-470 DEG C of reaction temperature, atmospheric pressure oxidation, and yield is up to 90%, then by methacrylaldehyde and air And vapor is mixed by certain mol proportion, in the presence of the composite catalysts such as molybdenum-vanadium, 300-470 DEG C of reaction temperature, atmospheric pressure oxidation The acrylic acid in raw material is made.
A kind of 5. low energy consumption cosmetic composition emulsion stabilizer according to claim 1, it is characterised in that：Use wool Wool washing sewage add alchlor, obtain lanolated mud slurry, suck moisture, obtain mud, take mud 600kg, add benzene 480kg, it is stirring while adding, 56 DEG C of insulation 1h are heated, stops stirring, precipitates 1h, benzene liquid dissolves lanolin 6%-40% after clarification, moves Enter in destilling tower, heating distillation, up to 34%, is cooled to less than 40 DEG C releasings, obtains lanolin crude product, take lanolin thick to containing lanolin Product 2100kg puts into reaction pot, is heated to 50 DEG C, then 50% (g/g) sulfuric acid solution of heat is added in lanolin crude product, stirring 45min, precipitates half an hour, and benzene lipid layer adds light ethanol, adds water, and 60 DEG C of heating and thermal insulation, stirs half an hour, precipitates half an hour, obtains sour Benzene fat is handled, takes acid treatment benzene fat to add ethanol 180kg, is gradually added 300g/L sodium hydroxide solutions about 70kg, pH9 is adjusted, adds water 180kg, keeps the temperature 60 DEG C, is continuously agitated from being added ethanol to adding water to finish, and is further continued for stirring 10min, stands, precipitates 1h, benzene Lipid layer adds light ethanol, and stirring, precipitates 1h, must neutralize benzene fat, takes and neutralizes benzene fat, adds 3.8% hydrogen peroxide 24kg, stirs, insulation 60 DEG C, 35min is precipitated, keeps pH8-9, adds light ethanol, 2h is precipitated, obtains commercial benzene fat, commercial benzene fat is distilled, liquid temperature 110 DEG C be evaporated in vacuo untill not distilling, be cooled to 60 DEG C, add ethanol, stir, precipitate 1h, isolate lower floor's lanolin, add ethanol, Heating stirring 10min, discards ethanol, and ethanol to the greatest extent is steamed in decompression, and the filtering of spun silk cloth, obtains the lanolin in raw material.