CN108017452A - A kind of biogas slurry bio-feritlizer and preparation method thereof - Google Patents

A kind of biogas slurry bio-feritlizer and preparation method thereof Download PDF

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Publication number
CN108017452A
CN108017452A CN201810060489.XA CN201810060489A CN108017452A CN 108017452 A CN108017452 A CN 108017452A CN 201810060489 A CN201810060489 A CN 201810060489A CN 108017452 A CN108017452 A CN 108017452A
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parts
biogas slurry
feritlizer
bio
biogas
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CN201810060489.XA
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Inventor
张晴雯
李贵春
郑莉
张爱平
刘杏认
杨正礼
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Institute of Environment and Sustainable Development in Agriculturem of CAAS
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Institute of Environment and Sustainable Development in Agriculturem of CAAS
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Priority to CN201810060489.XA priority Critical patent/CN108017452A/en
Priority to CN202310806653.8A priority patent/CN116836024A/en
Publication of CN108017452A publication Critical patent/CN108017452A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05DINORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D9/00Other inorganic fertilisers
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • C05F17/20Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation using specific microorganisms or substances, e.g. enzymes, for activating or stimulating the treatment
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/40Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting fertiliser dosage or release rate; for affecting solubility
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/60Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/10Solid or semi-solid fertilisers, e.g. powders
    • C05G5/12Granules or flakes

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Tropical Medicine & Parasitology (AREA)
  • Plant Pathology (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Molecular Biology (AREA)
  • Soil Sciences (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses a kind of biogas slurry bio-feritlizer and preparation method thereof, belongs to agricultural organic waste application technology as the second resource field.The biogas slurry bio-feritlizer is prepared by the raw material of following parts by weight:50 80 parts of biogas slurry, 30 55 parts of biogas residue, 0.1 2 parts of microbial bacterial agent, 0.5 2 parts of zeolite powder, 10 30 parts of swine excrement, 10 20 parts of Folium Meliae, 10 20 parts of camphortree leaf, 0.5 2 parts of wheat bran, 0.2 1 parts of vinasse, 10 20 parts of crop material, 15 parts of shaping assistant.The biogas slurry bio-feritlizer of the present invention make use of largely discarded biogas slurry, biogas residue, wheat bran, vinasse and crop material, improves salvage value, reduces environmental pollution.This method for preparing fertilizer is simple, and can effectively improve fertile soil power, has antibacterial insecticidal effect, and fertility persistent high efficiency is harmless to human body and environment.

Description

A kind of biogas slurry bio-feritlizer and preparation method thereof
Technical field
The present invention relates to agricultural organic waste application technology as the second resource field, and in particular to a kind of biogas slurry bio-feritlizer and Its preparation method.
Background technology
China is large agricultural country, and planting industry is the basis of agricultural, and it is that the primary of agricultural development is appointed to ensure grain effective supply Business.China has supported in the world 1/5 population with the world 1/3 chemical fertilizer, and a large amount of inputs of fertilizer solve staple food supply and ask Topic, but with intensive agriculture fast development, environmental problem is increasingly prominent caused by chemical fertilizer is lost in and pesticide is abused Go out, farmland fertility declines, and diseases and pests of agronomic crop is difficult to effectively suppress.Make article with what chemical fertilizer and pesticide producing went out Matter is greatly affected.On the other hand, as China's livestock and poultry cultivation large-scale development, biogas engineering Large scale construction and popularization make With the Utilizing question of biogas slurry and biogas residue also increasingly becomes intractable.Therefore, the intensivization development of planting industry aquaculture is badly in need of getting through breeding Link, makes full use of the organic wastes such as biogas slurry to prepare biomass fertilizers, and recycling safe is used for farmland.
Existing biogas slurry bio-feritlizer preparation process is complicated, and protection effect is poor, it is impossible to meets agricultural demand.
Therefore design that a kind of preparation process is simple, the biogas slurry bio-fertilizer with increasing soil fertility and with protection effect Material and preparation method thereof has great practical value.
The content of the invention
The present invention provides a kind of biogas slurry bio-feritlizer, can solve the above problem of the prior art.
The present invention provides a kind of biogas slurry bio-feritlizer, it is prepared by the raw material of following parts by weight:50-80 parts of biogas slurry, 30-55 parts of biogas residue, 0.1-2 parts of microbial bacterial agent, 0.5-2 parts of zeolite powder, 10-30 parts of swine excrement, 10-20 parts of Folium Meliae, camphor tree 10-20 parts of leaf, 0.5-2 parts of wheat bran, 0.2-1 parts of vinasse, 10-20 parts of crop material, 1-5 parts of shaping assistant.
It is preferred that the biogas slurry bio-feritlizer is prepared by the raw material of following parts by weight:60 parts of biogas slurry, 45 parts of biogas residue, 1 part of microbial bacterial agent, 1 part of zeolite powder, 24 parts of swine excrement, 15 parts of Folium Meliae, 15 parts of camphortree leaf, 1 part of wheat bran, 0.5 part of vinasse, work 18 parts of thing stalk, 3 parts of shaping assistant.
It is preferred that the biogas slurry bio-feritlizer is prepared by the raw material of following parts by weight:55 parts of biogas slurry, 40 parts of biogas residue, 0.8 part of microbial bacterial agent, 1.2 parts of zeolite powder, 20 parts of swine excrement, 12 parts of Folium Meliae, 15 parts of camphortree leaf, 1.5 parts of wheat bran, vinasse 1 Part, 15 parts of crop material, 2 parts of shaping assistant.
It is preferred that the biogas slurry bio-feritlizer is prepared by the raw material of following parts by weight:65 parts of biogas slurry, 50 parts of biogas residue, 1.2 parts of microbial bacterial agent, 0.8 part of zeolite powder, 16 parts of swine excrement, 12 parts of Folium Meliae, 18 parts of camphortree leaf, 1.8 parts of wheat bran, vinasse 0.5 part, 13 parts of crop material, 4 parts of shaping assistant.
It is preferred that the microbial bacterial agent is combined including bacillus subtilis or black-koji mould or both.
It is preferred that the shaping assistant includes one in bentonite, sodium carboxymethylcellulose, cornstarch or wheaten starch Kind or several combinations.
Present invention also offers the preparation method of the biogas slurry bio-feritlizer, comprise the following steps:
A, biogas slurry is carried out first that filtrate is obtained by filtration, flocculant is added into filtrate, organic sulfur TMT-15 is added, fills Divide stirring, then precipitation removes sediment, the biogas slurry after being handled;
B, crush:Folium Meliae, camphortree leaf and crop material are crushed;
C, Folium Meliae, camphortree leaf, wheat bran, vinasse, crop material and swine excrement after will be broken be added to the natural pond after processing In liquid, microbial bacterial agent is then added, is fermented to obtain fermenting mixture at 15-40 DEG C;
D, biogas residue, zeolite powder and shaping assistant will be added in the fermenting mixture after step c, and stirred evenly;
E, carry out granulating and forming using comminutor, after drying to obtain the final product.
It is preferred that in step a, the addition of flocculant is the 0.5-5% of filtrate quality, the addition of organic sulfur TMT-15 For the 0.5-1.5 ‰ of filtrate quality.
It is preferred that the fermentation temperature in step c is 18-35 DEG C.
Compared with prior art, the beneficial effects of the invention are as follows:The biogas slurry bio-feritlizer of the present invention make use of substantial amounts of useless Biogas slurry, biogas residue, wheat bran, vinasse and crop material are abandoned, improves salvage value, reduces environmental pollution.China tree therein Leaf and camphortree leaf, which combine, possesses good pesticide-germicide effect, and wheat bran and vinasse etc. are not only that microorganism provides good nutrients Matter, also has the effect for promoting fertilizer efficiency to play concurrently.The preparation method of this fertilizer not remove only largely harmful heavy metal, Er Qiehuan Border is friendly, will not produce secondary pollution.This method for preparing fertilizer is simple, and can effectively improve fertile soil power, has anti- Bacterium insecticidal effect, fertility persistent high efficiency are harmless to human body and environment.
Embodiment
The embodiment of the present invention is described in detail below, it is to be understood that protection scope of the present invention is not Limited by embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are not making creativeness All other embodiments obtained on the premise of work, belong to the scope of protection of the invention.
Embodiment 1:
A kind of biogas slurry bio-feritlizer provided by the invention, is prepared by the raw material of following parts by weight:60 parts of biogas slurry, biogas residue 45 parts, 1 part of microbial bacterial agent, 1 part of zeolite powder, 24 parts of swine excrement, 15 parts of Folium Meliae, 15 parts of camphortree leaf, 1 part of wheat bran, vinasse 0.5 Part, 18 parts of crop material, cornstarch or 3 parts of wheaten starch.
Embodiment 2:
A kind of biogas slurry bio-feritlizer provided by the invention, is prepared by the raw material of following parts by weight:55 parts of biogas slurry, biogas residue 40 parts, 0.8 part of microbial bacterial agent, 1.2 parts of zeolite powder, 20 parts of swine excrement, 12 parts of Folium Meliae, 15 parts of camphortree leaf, 1.5 parts of wheat bran, 1 part of vinasse, 15 parts of crop material, 1 part of bentonite, 1 part of sodium carboxymethylcellulose.
Embodiment 3:
A kind of biogas slurry bio-feritlizer provided by the invention, is prepared by the raw material of following parts by weight:65 parts of biogas slurry, biogas residue 50 parts, 1.2 parts of microbial bacterial agent, 0.8 part of zeolite powder, 16 parts of swine excrement, 12 parts of Folium Meliae, 18 parts of camphortree leaf, 1.8 parts of wheat bran, 0.5 part of vinasse, 13 parts of crop material, 4 parts of bentonite.
Embodiment 4:
Microbial bacterial agent therein is mixed for bacillus subtilis and black-koji mould with arbitrary proportion.
Embodiment 5:
The preparation method of the biogas slurry bio-feritlizer of the present invention, comprises the following steps:
A, biogas slurry is carried out first that filtrate is obtained by filtration, 3% flocculant of filtrate quality is added into filtrate, is added 1.2 ‰ organic sulfur TMT-15, is sufficiently stirred, and then precipitation removes sediment, the biogas slurry after being handled;
B, crush:Folium Meliae, camphortree leaf and crop material are crushed;
C, Folium Meliae, camphortree leaf, wheat bran, vinasse, crop material and swine excrement after will be broken be added to the natural pond after processing In liquid, bacillus subtilis and black-koji mould are then added, is fermented to obtain fermenting mixture at 18 DEG C;
D, biogas residue, zeolite powder and shaping assistant will be added in the fermenting mixture after step c, and stirred evenly;
E, carry out granulating and forming using comminutor, after drying to obtain the final product.
Embodiment 6:
The preparation method of the biogas slurry bio-feritlizer of the present invention, comprises the following steps:
A, biogas slurry is carried out first that filtrate is obtained by filtration, 1% flocculant of filtrate quality is added into filtrate, adds filtrate The organic sulfur TMT-15 of quality 0.8 ‰, is sufficiently stirred, and then precipitation removes sediment, the biogas slurry after being handled;
B, crush:Folium Meliae, camphortree leaf and crop material are crushed;
C, Folium Meliae, camphortree leaf, wheat bran, vinasse, crop material and swine excrement after will be broken be added to the natural pond after processing In liquid, bacillus subtilis and black-koji mould are then added, is fermented to obtain fermenting mixture at 25 DEG C;
D, biogas residue, zeolite powder and shaping assistant will be added in the fermenting mixture after step c, and stirred evenly;
E, carry out granulating and forming using comminutor, after drying to obtain the final product.
Embodiment 7:
The preparation method of the biogas slurry bio-feritlizer of the present invention, comprises the following steps:
A, biogas slurry is carried out first that filtrate is obtained by filtration, the flocculant of filtrate quality 2% is added into filtrate, adds filter The organic sulfur TMT-15 of liquid quality 1.0 ‰, is sufficiently stirred, and then precipitation removes sediment, the biogas slurry after being handled;
B, crush:Folium Meliae, camphortree leaf and crop material are crushed;
C, Folium Meliae, camphortree leaf, wheat bran, vinasse, crop material and swine excrement after will be broken be added to the natural pond after processing In liquid, bacillus subtilis and black-koji mould are then added, is fermented to obtain fermenting mixture at 35 DEG C;
D, biogas residue, zeolite powder and shaping assistant will be added in the fermenting mixture after step b, and stirred evenly;
E, carry out granulating and forming using comminutor, after drying to obtain the final product.
Wherein, shaping assistant includes one kind or several in bentonite, sodium carboxymethylcellulose, cornstarch or wheaten starch The combination of kind.
Wherein, the addition of flocculant is generally the 0.5-5% of filtrate quality, and the addition of organic sulfur TMT-15 is 0.5- 1.5 ‰, in practical operation specific addition be subject to reach needed for metal removal rate.
The fertilizer of sample 1,2,3 prepared by the preparation method that the embodiment of the present invention 1,2,3 distinguishes embodiment 5,6,7 is supported foster Composition detection analysis in table 1:
1 sample of table, 1,2,3 Fertilizer nutrient component content
The present invention sample 1 fertilizer with the dose of 9t/ha be used for Chinese cabbage plant, as a result Chinese cabbage yield increase by 55% with On, and pest and disease damage is largely reduced.
The fertilizer of the sample 2 of the present invention is used for corn planting with the dose of 7t/ha, as a result corn yield increase by 15% More than.
The all technical and heavy metal limit technical indicator of the fertilizer of the present invention meet NY-884-201《Biology has Machine fertilizer》Standard.
The biogas slurry bio-feritlizer of the present invention make use of largely discarded biogas slurry, biogas residue, wheat bran, vinasse and crop material, Salvage value is improved, reduces environmental pollution.This method for preparing fertilizer is simple, and can effectively improve fertile soil Power, has antibacterial insecticidal effect, and fertility persistent high efficiency is harmless to human body and environment.Undeclared part involved in the present invention The same as the prior art or use prior art is carried out.
Disclosed above is only several specific embodiments of the present invention, and still, the embodiment of the present invention is not limited to this, is appointed What what those skilled in the art can think change should all fall into protection scope of the present invention.

Claims (10)

1. a kind of biogas slurry bio-feritlizer, it is characterised in that be prepared by the raw material of following parts by weight:50-80 parts of biogas slurry, biogas residue 30-55 parts, 0.1-2 parts of microbial bacterial agent, 0.5-2 parts of zeolite powder, 10-30 parts of swine excrement, 10-20 parts of Folium Meliae, camphortree leaf 10- 20 parts, 0.5-2 parts of wheat bran, 0.2-1 parts of vinasse, 10-20 parts of crop material, 1-5 parts of shaping assistant.
2. biogas slurry bio-feritlizer as claimed in claim 1, it is characterised in that the biogas slurry bio-feritlizer is by following parts by weight Raw material is prepared:60 parts of biogas slurry, 45 parts of biogas residue, 1 part of microbial bacterial agent, 1 part of zeolite powder, 24 parts of swine excrement, 15 parts of Folium Meliae, 15 parts of camphortree leaf, 1 part of wheat bran, 0.5 part of vinasse, 18 parts of crop material, 3 parts of shaping assistant.
3. biogas slurry bio-feritlizer as claimed in claim 1, it is characterised in that the biogas slurry bio-feritlizer is by following parts by weight Raw material is prepared:55 parts of biogas slurry, 40 parts of biogas residue, 0.8 part of microbial bacterial agent, 1.2 parts of zeolite powder, 20 parts of swine excrement, Folium Meliae 12 parts, 15 parts of camphortree leaf, 1.5 parts of wheat bran, 1 part of vinasse, 15 parts of crop material, 2 parts of shaping assistant.
4. biogas slurry bio-feritlizer as claimed in claim 1, it is characterised in that the biogas slurry bio-feritlizer is by following parts by weight Raw material is prepared:65 parts of biogas slurry, 50 parts of biogas residue, 1.2 parts of microbial bacterial agent, 0.8 part of zeolite powder, 16 parts of swine excrement, Folium Meliae 12 parts, 18 parts of camphortree leaf, 1.8 parts of wheat bran, 0.5 part of vinasse, 13 parts of crop material, 4 parts of shaping assistant.
5. the biogas slurry bio-feritlizer as described in claim 1-4 is any, it is characterised in that the microbial bacterial agent includes withered grass bud Spore bacillus or black-koji mould or both combine.
6. the biogas slurry bio-feritlizer as described in claim 1-4 is any, it is characterised in that the shaping assistant include bentonite, One or more of combinations in sodium carboxymethylcellulose, cornstarch or wheaten starch.
7. the biogas slurry bio-feritlizer as described in claim 1-4 is any, it is characterised in that the biogas slurry bio-feritlizer, which further includes, to be removed Smelly dose.
8. the preparation method of the biogas slurry bio-feritlizer as described in claim 1-4 is any, it is characterised in that comprise the following steps:
A, biogas slurry is carried out first that filtrate is obtained by filtration, flocculant is added into filtrate, organic sulfur TMT-15 is added, fully stirs Mix, then precipitation removes sediment, the biogas slurry after being handled;
B, crush:Folium Meliae, camphortree leaf and crop material are crushed;
C, Folium Meliae, camphortree leaf, wheat bran, vinasse, crop material and swine excrement after will be broken be added in the biogas slurry after processing, Then microbial bacterial agent is added, is fermented to obtain fermenting mixture at 15-40 DEG C;
D, biogas residue, zeolite powder and shaping assistant will be added in the fermenting mixture after step c, and stirred evenly;
E, carry out granulating and forming using comminutor, after drying to obtain the final product.
9. the preparation method of biogas slurry bio-feritlizer as claimed in claim 8, it is characterised in that in step a, the addition of flocculant The 0.5-5% for filtrate quality is measured, the addition of organic sulfur TMT-15 is the 0.5-1.5 ‰ of filtrate quality.
10. the preparation method of biogas slurry bio-feritlizer as claimed in claim 8, it is characterised in that the fermentation temperature in step c is 18-35℃。
CN201810060489.XA 2018-01-22 2018-01-22 A kind of biogas slurry bio-feritlizer and preparation method thereof Pending CN108017452A (en)

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Publication number Priority date Publication date Assignee Title
CN110679431A (en) * 2019-11-05 2020-01-14 河北省农林科学院石家庄果树研究所 Peach seed emergence substrate and seedling raising method
CN110773563A (en) * 2019-11-27 2020-02-11 广西壮族自治区农业科学院 Method for repairing cadmium-zinc polluted soil by using grass dragon
CN111233582A (en) * 2020-03-18 2020-06-05 漳州御品茶业有限公司 Organic fertilizer for organic tea and preparation method thereof

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CN104671860A (en) * 2015-02-25 2015-06-03 新疆恒丰现代农业科技股份有限公司 Bioorganic fertilizer using agricultural waste as raw materials and preparation method of bioorganic fertilizer

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CN104447087A (en) * 2014-11-19 2015-03-25 柳州市源晨农副产品有限公司 Organic fertilizer with sterilizing and insecticidal functions
CN104671860A (en) * 2015-02-25 2015-06-03 新疆恒丰现代农业科技股份有限公司 Bioorganic fertilizer using agricultural waste as raw materials and preparation method of bioorganic fertilizer

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110679431A (en) * 2019-11-05 2020-01-14 河北省农林科学院石家庄果树研究所 Peach seed emergence substrate and seedling raising method
CN110773563A (en) * 2019-11-27 2020-02-11 广西壮族自治区农业科学院 Method for repairing cadmium-zinc polluted soil by using grass dragon
CN110773563B (en) * 2019-11-27 2021-08-27 广西壮族自治区农业科学院 Method for repairing cadmium-zinc polluted soil by using grass dragon
CN111233582A (en) * 2020-03-18 2020-06-05 漳州御品茶业有限公司 Organic fertilizer for organic tea and preparation method thereof

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Application publication date: 20180511