CN108015072A - A kind of automatic flushing device of glass sample bottle - Google Patents
A kind of automatic flushing device of glass sample bottle Download PDFInfo
- Publication number
- CN108015072A CN108015072A CN201610994462.9A CN201610994462A CN108015072A CN 108015072 A CN108015072 A CN 108015072A CN 201610994462 A CN201610994462 A CN 201610994462A CN 108015072 A CN108015072 A CN 108015072A
- Authority
- CN
- China
- Prior art keywords
- bottom plate
- sample bottle
- cloche
- bottle
- solvent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/20—Cleaning containers, e.g. tanks by using apparatus into or on to which containers, e.g. bottles, jars, cans are brought
- B08B9/28—Cleaning containers, e.g. tanks by using apparatus into or on to which containers, e.g. bottles, jars, cans are brought the apparatus cleaning by splash, spray, or jet application, with or without soaking
- B08B9/30—Cleaning containers, e.g. tanks by using apparatus into or on to which containers, e.g. bottles, jars, cans are brought the apparatus cleaning by splash, spray, or jet application, with or without soaking and having conveyors
- B08B9/32—Rotating conveyors
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/20—Cleaning containers, e.g. tanks by using apparatus into or on to which containers, e.g. bottles, jars, cans are brought
- B08B9/28—Cleaning containers, e.g. tanks by using apparatus into or on to which containers, e.g. bottles, jars, cans are brought the apparatus cleaning by splash, spray, or jet application, with or without soaking
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Automatic Analysis And Handling Materials Therefor (AREA)
Abstract
The invention belongs to laboratory equipment cleaning technique field, and in particular to a kind of device that can be realized sample injection bottle and clean automatically；The purpose of the present invention, in view of the shortcomings of the prior art, offer is a kind of to be directed to pollutant different in sample bottle, using the interaction cleaning of variety classes solvent, the automatic flushing device of efficiently portable glass sample bottle；The technical scheme is that：A kind of automatic flushing device of glass sample bottle, including solvent bottle, plunger pump, pipeline, leg, solvent shower nozzle, sample bottle, sample bottle wheel disc, sealing axis, gear motor, bottom plate, cloche, nozzle base and sealing-plug；The disk of through hole is equipped with centered on the bottom plate, cloche is buckled on bottom plate, sealing-plug is equipped between the lower edge and bottom plate of cloche, gear motor is equipped with below bottom plate, the gear motor is equipped with sealing axis, sealing axis gos deep into cloche through bottom plate central through hole, and the sealing axis upper end is equipped with sample wheel disc on cloche interior sealing axis.
Description
Technical field
The invention belongs to laboratory equipment cleaning technique field, and in particular to a kind of automatic cleaning dress of glass sample bottle
Put.
Background technology
Need to use substantial amounts of glass sample injection bottle in Analysis of Organic Substances test, as the requirement of analysis test is higher and higher,
It is also higher and higher to the cleanliness factor of sample bottle.The sample bottle either newly purchased or the sample bottle after are required to carry out clear
Wash.The cleaning of a large amount of sample bottles needs to expend experimenter's great effort, while consumes a large amount of organic solvents, does not have to environment
It is good.At present, substantially there are two kinds to the cleaning way of sample bottle：A kind of is to be soaked in closed container with a large amount of organic solvents,
Achieve the purpose that cleaning by repeatedly replacing fresh solvent, this mode can reach the cleaning purpose of sample bottle, but need
The organic solvent amount of consumption is especially big, and the processing to organic liquid waste causes pressure；The second way is used in closed container
Organic solvent is fumigated, and is condensed and is cleaned in sample bottle by the steam of organic solvent, and this mode realizes organic
The recycling of solvent, but cleaning efficiency is relatively low, takes longer.Regarding to the issue above and shortcoming, the present invention provides one kind
Efficiently, environmentally friendly sample bottle cleaning equipment.
The content of the invention
The purpose of the present invention, in view of the shortcomings of the prior art, providing a kind of for pollutant different in sample bottle, use
The interaction cleaning of variety classes solvent, the automatic flushing device of efficiently portable glass sample bottle.
The technical scheme is that：
A kind of automatic flushing device of glass sample bottle, including solvent bottle, plunger pump, pipeline, leg, solvent shower nozzle, sample
Product bottle, sample bottle wheel disc, sealing axis, gear motor, bottom plate, cloche, nozzle base and gasket；Set centered on the bottom plate
There is the disk of through hole, cloche is buckled on bottom plate, and gasket is equipped between the lower edge and bottom plate of cloche, is equipped with and subtracts below bottom plate
Speed motor, the gear motor are equipped with sealing axis, and sealing axis gos deep into cloche through bottom plate central through hole, the sealing axis
Upper end is equipped with sample wheel disc on cloche interior sealing axis, and the cloche internal backplane is equipped with nozzle base, two solvents
Nozzle is arranged on nozzle base and is connected by pipeline through bottom plate with two plunger pumps outside cloche, and two plunger pumps lead to
Pipeline is crossed respectively with two solvent bottles to be connected.
The plate upper surface is provided with diversion trench and solvent recovery hole, and wherein solvent recovery hole by pipeline and is arranged on bottom plate
The solvent recovery bottle of lower end is connected.
The sample wheel plate edge is equipped with two circle fixed installation holess, and a sample bottle is equipped with each fixed installation holes.
The plunger pump is for stainless steel or PEEK materials, it can be achieved that the adjusting of 0.2~10ml/min flow velocitys, maximum working pressure
4000psi；
The rotating speed of the gear motor is adjustable in 0~30r/min；
Equipped with gasket it is software polytetrafluoro material between the lower edge and bottom plate of the cloche.
The beneficial effects of the invention are as follows：
It is few that 1. the present invention possesses solvent dosage；Pollutant different in sample bottle can be directed to, using variety classes solvent
Interaction cleaning, can also select suitable solvent according to actual conditions；
2. using high-pressure wash mode, the sample bottle containing solid residue is particularly suitable for, without hairbrush cleaning process；
3. equipment volume is small, easy to be applicable in the quantitative recovery, it can be achieved that organic solvent in laboratory；
4. cleaning efficiency is high, corresponding scavenging period can be set according to sample bottle clean level, and the degree of automation is high, sample
Bottle sets corresponding cleaning process, it can be achieved that Program Purge, realizes that cleaning waste liquid recycles automatically using gravity after installation is complete.
Brief description of the drawings
Fig. 1 is a kind of automatic flushing device structure chart of glass sample bottle；
Fig. 2 is sample wheel disc schematic diagram；
Fig. 3 is floor diagram；
Embodiment
The present invention is further introduced with embodiment below in conjunction with the accompanying drawings：
A kind of automatic flushing device of glass sample bottle, including solvent bottle 1, plunger pump 2, pipeline 3, leg 4, solvent shower nozzle
5th, sample bottle 6, sample bottle wheel disc 7, sealing axis 8, gear motor 9, bottom plate 11, cloche 12, nozzle base 13 and gasket 16；
The disk of through hole is equipped with centered on the bottom plate 11, cloche 12 is buckled on bottom plate 11, the lower edge and bottom plate 11 of cloche 12 it
Between be equipped with gasket 16, the lower section of bottom plate 11 is equipped with gear motor 9, and the gear motor 9 is equipped with sealing axis 8, seals axis 8 and passes through
11 central through hole of bottom plate gos deep into cloche 12, and the sealing axis upper end is equipped with sample wheel disc on 12 interior sealing axis 8 of cloche
7,12 internal backplane 11 of cloche, which is equipped with 13, two solvent shower nozzles 5 of nozzle base and is arranged on nozzle base 13, passes through pipe
Road 3 is connected through bottom plate 11 with two plunger pumps 2 outside cloche 12, and two plunger pumps 2 are molten with two respectively by pipeline 3
Agent bottle 1 is connected,
11 upper surface of bottom plate is provided with diversion trench 15 and solvent recovery hole 14, wherein solvent recovery hole by pipeline 3 with
Solvent recovery bottle 10 arranged on 11 lower end of bottom plate is connected.
7 edge of sample wheel disc is equipped with two circle fixed installation holess, and a sample bottle 6 is equipped with each fixed installation holes.
The plunger pump 2 for stainless steel or PEEK materials, it can be achieved that 0.2~10ml/min flow velocitys are adjusted, press by highest work
Power 4000psi；
The rotating speed of the gear motor 9 is adjustable in 0~30r/min；
Equipped with gasket 16 it is software polytetrafluoro material between the lower edge and bottom plate 11 of the cloche 12.
The present invention operates in accordance with the following steps：
Rapid one, device is linked in sequence, suitable reagent is added in reagent bottle A, B；
Step 2: opening power supply, plunger flow rate pump and scavenging period are set；
Step 3: the sample bottle selection for different size is adapted to sample bottle wheel disc, by sample bottle back-off in fixing groove；
Step 4: cloche is buckled, it is ensured that sealing；
Step 5: connect waste collection bottle；
Step 6: opening governor motor, rotating speed is set, ensures that sample bottle comes into full contact with solvent；
Step 7: starting plunger pump, start to clean.
Step 8: cleaning finishes, sample bottle is taken out.
Embodiment 1
Step 1: device is linked in sequence, chromatographic pure dichloromethane is added in reagent bottle I, is added in reagent bottle II
Chromatographically pure n-hexane；
Step 2: opening power supply, the plunger pump of PEEK materials is selected, following Program Purge event is set：From 0~6min,
A pumps are run, it is 2.5ml/min to set dichloromethane flow velocity；From 6~12min, operation B pumps, it is 2.5ml/ to set n-hexane flow velocity
Min, total run time 12min；
Step 3: selecting 60, the wheel disc of 1.5ml sample bottles, sample bottle is buckled in fixing groove respectively；Using double sprays
Mouth is cleaned.
Step 4: cloche is buckled, it is ensured that sealing；
Step 5: connect waste collection bottle；
Step 6: opening governor motor, setting rotating speed is 1r min-1；
Step 7: starting plunger pump, start to clean；
Step 8: cleaning finishes, sample bottle is taken out.
Embodiment 2
Step 1: device is linked in sequence, Chromatographic Pure Methanol is added in reagent bottle I, chromatography is added in reagent bottle II
Pure hexane；
Step 2: opening power supply, select the plug of stainless steel to pump, following Program Purge event is set：From 0~10min,
B pumps are run, it is 5ml/min to set n-hexane flow velocity；From 10~15min, operation A pumps, setting methanol flow rate is 2.5ml/min,
Total run time is 15min；
Step 3: selecting 120, the wheel disc of 1.5ml sample bottles, sample bottle is buckled in fixing groove respectively；Using three
Nozzle is cleaned.
Step 4: cloche is buckled, it is ensured that sealing；
Step 5: connect waste collection bottle；
Step 6: opening governor motor, setting rotating speed is 10r min-1；
Step 7: starting plunger pump, start to clean；
Step 8: cleaning finishes, sample bottle is taken out.
Embodiment 3
Step 1: device is linked in sequence, Chromatographic Pure Methanol is added in reagent bottle I, chromatography is added in reagent bottle II
Absolute dichloromethane；
Step 2: opening power supply, select the plug of stainless steel to pump, following Program Purge event is set：From 0~10min,
B pumps are run, it is 5ml/min to set dichloromethane flow velocity；From 10~15min, A flow rate pumps 2.5ml/min, B flow rate pump is set
2.5ml/min；From 15~20min, operation A pumps, setting methanol flow rate is 5ml/min；Total run time is 20min；
Step 3: 30, the wheel disc of 5ml sample bottles are selected, by sample bottle back-off in fixing groove；Carried out using single injector
Cleaning.
Step 4: cloche is buckled, it is ensured that sealing；
Step 5: connect waste collection bottle；
Step 6: opening governor motor, setting rotating speed is 5r min-1；
Step 7: starting plunger pump, start to clean；
Step 8: cleaning finishes, sample bottle is taken out.
Claims (6)
- A kind of 1. automatic flushing device of glass sample bottle, it is characterised in that：Including solvent bottle (1), plunger pump (2), pipeline (3), leg (4), solvent shower nozzle (5), sample bottle (6), sample bottle wheel disc (7), sealing axis (8), gear motor (9), bottom plate (11), cloche (12), nozzle base (13) and sealing-plug (16)；The disk of through hole, glass are equipped with centered on the bottom plate (11) Glass cover (12) is buckled on bottom plate (11), and sealing-plug (16), bottom plate (11) are equipped between the lower edge and bottom plate (11) of cloche (12) Lower section is equipped with gear motor (9), and the gear motor (9) is equipped with sealing axis (8), and sealing axis (8) passes through bottom plate (11) center Through hole gos deep into cloche (12), and the sealing axis upper end is equipped with sample wheel disc (7) on cloche (12) interior sealing axis (8), Cloche (12) internal backplane (11) is equipped with nozzle base (13), two solvent shower nozzles (5) are arranged on nozzle base (13) Upper to be connected by pipeline (3) through two plunger pumps (2) of the bottom plate (11) with cloche (12) outside, two plunger pumps (2) are logical Pipeline (3) is crossed respectively with two solvent bottles (1) to be connected.
- A kind of 2. automatic flushing device of glass sample bottle as claimed in claim 1, it is characterised in that：On the bottom plate (11) Surface is provided with diversion trench (15) and solvent recovery hole (14), and wherein solvent recovery hole is by pipeline (3) and under bottom plate (11) The solvent recovery bottle (10) at end is connected.
- A kind of 3. automatic flushing device of glass sample bottle as claimed in claim 1, it is characterised in that：The sample wheel disc (7) edge is equipped with two circle fixed installation holess, is equipped with a sample bottle (6) in each fixed installation holes, sample bottle is buckled in installation Kong Zhong.
- A kind of 4. automatic flushing device of glass sample bottle as claimed in claim 1, it is characterised in that：The plunger pump (2) For stainless steel or PEEK materials, it can be achieved that 0.2~10ml/min flow velocitys are adjusted, maximum working pressure 4000psi.
- A kind of 5. automatic flushing device of glass sample bottle as claimed in claim 1, it is characterised in that：The gear motor (9) rotating speed is adjustable in 0~30r/min.
- A kind of 6. automatic flushing device of glass sample bottle as claimed in claim 1, it is characterised in that：The cloche (12) Lower edge and bottom plate (11) between equipped with gasket (16) be software polytetrafluoro material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610994462.9A CN108015072A (en) | 2016-11-01 | 2016-11-01 | A kind of automatic flushing device of glass sample bottle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610994462.9A CN108015072A (en) | 2016-11-01 | 2016-11-01 | A kind of automatic flushing device of glass sample bottle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108015072A true CN108015072A (en) | 2018-05-11 |
Family
ID=62083803
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610994462.9A Pending CN108015072A (en) | 2016-11-01 | 2016-11-01 | A kind of automatic flushing device of glass sample bottle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108015072A (en) |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH11198993A (en) * | 1998-01-08 | 1999-07-27 | Toyo Seikan Kaisha Ltd | Mechanism for sterilizing and cleaning container |
| CN201644438U (en) * | 2010-04-23 | 2010-11-24 | 北京同泰联科技发展有限公司 | Sample bottle automatic cleaning machine |
| CN203330069U (en) * | 2013-05-11 | 2013-12-11 | 燕京啤酒(玉林)有限公司 | Spraying pipe cleaning device of bottle cleaning machine |
| CN103706146A (en) * | 2013-12-10 | 2014-04-09 | 核工业北京地质研究院 | Column extraction system and extraction method for organic materials in solid particles |
| CN205128549U (en) * | 2015-10-08 | 2016-04-06 | 永仁绿原农业开发有限公司 | External synchronization belt cleaning device in bottle |
| CN205463493U (en) * | 2016-03-24 | 2016-08-17 | 浙江泰康药业集团有限公司 | Bottle cleaning machine |
| CN206747206U (en) * | 2017-05-24 | 2017-12-15 | 安徽博蜂生物科技有限公司 | A kind of rotary bottle washing machine |
-
2016
- 2016-11-01 CN CN201610994462.9A patent/CN108015072A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH11198993A (en) * | 1998-01-08 | 1999-07-27 | Toyo Seikan Kaisha Ltd | Mechanism for sterilizing and cleaning container |
| CN201644438U (en) * | 2010-04-23 | 2010-11-24 | 北京同泰联科技发展有限公司 | Sample bottle automatic cleaning machine |
| CN203330069U (en) * | 2013-05-11 | 2013-12-11 | 燕京啤酒(玉林)有限公司 | Spraying pipe cleaning device of bottle cleaning machine |
| CN103706146A (en) * | 2013-12-10 | 2014-04-09 | 核工业北京地质研究院 | Column extraction system and extraction method for organic materials in solid particles |
| CN205128549U (en) * | 2015-10-08 | 2016-04-06 | 永仁绿原农业开发有限公司 | External synchronization belt cleaning device in bottle |
| CN205463493U (en) * | 2016-03-24 | 2016-08-17 | 浙江泰康药业集团有限公司 | Bottle cleaning machine |
| CN206747206U (en) * | 2017-05-24 | 2017-12-15 | 安徽博蜂生物科技有限公司 | A kind of rotary bottle washing machine |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN204769670U (en) | Washing device of immunodetection analytical instrument | |
| CN108435788B (en) | Pollute restoration of soil and administer device | |
| CN106890836A (en) | A kind of cleaning equipment of mobile phone camera eyeglass | |
| CN210305039U (en) | Contaminated soil restoration test device | |
| CN105664583B (en) | A kind of pharmaceutical extracting solution filtration device | |
| CN108015072A (en) | A kind of automatic flushing device of glass sample bottle | |
| CN104550152B (en) | A kind of nuclear-magnetism can washing apparatus | |
| CN206631631U (en) | A kind of experimental bench for being easy to Recycling of waste liquid | |
| CN216460842U (en) | Different position soil prosthetic devices in brown land | |
| CN115572966A (en) | Metal casting surface passivation method | |
| CN205587398U (en) | Dual spray rinsing of test tube and device that spin -dries | |
| CN207175630U (en) | A kind of environment-friendly type collecting medical waste liquid processing unit | |
| CN204892469U (en) | Wash integrated equipment of chromatographic column | |
| CN211282199U (en) | Manual mercury drop collecting device | |
| CN201524686U (en) | Adsorption column cleaning machine | |
| CN209567836U (en) | A kind of organic pollutant extraction equipment | |
| CN205263041U (en) | Opposition high performance liquid chromatography post washs and regenerating unit | |
| CN201436088U (en) | An oil absorption buoy applied to an industrial washer | |
| CN205324303U (en) | Automatic dual washing of liquid and device that spin -dries annotated of test tube | |
| CN205324304U (en) | Automatic liquid washing and device that spin -dries annotated of test tube | |
| CN205587399U (en) | Dual jetter of test tube | |
| CN205587387U (en) | Automatic dual belt cleaning device of liquid that annotates of test tube | |
| CN217033777U (en) | Gas chromatography-mass spectrometer capable of automatically sampling in essence research and development | |
| CN219745827U (en) | Soil remediation device | |
| CN205380124U (en) | Dual washing of test tube and device that spin -dries with water level monitoring |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180511 |
|
| RJ01 | Rejection of invention patent application after publication |