CN107987793A - A kind of combined high temperature sealing material machining manufacture using graphite as matrix - Google Patents

A kind of combined high temperature sealing material machining manufacture using graphite as matrix Download PDF

Info

Publication number
CN107987793A
CN107987793A CN201610947633.2A CN201610947633A CN107987793A CN 107987793 A CN107987793 A CN 107987793A CN 201610947633 A CN201610947633 A CN 201610947633A CN 107987793 A CN107987793 A CN 107987793A
Authority
CN
China
Prior art keywords
graphite
alloy wire
bar
fibrous material
sealing material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610947633.2A
Other languages
Chinese (zh)
Inventor
罗文莉
高广启
张雷
岳振玉
孟庆鹏
王峰
金鑫
郝丽伟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Petroleum and Chemical Corp
Sinopec Research Institute of Petroleum Engineering Shengli Co
Original Assignee
China Petroleum and Chemical Corp
Sinopec Research Institute of Petroleum Engineering Shengli Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Petroleum and Chemical Corp, Sinopec Research Institute of Petroleum Engineering Shengli Co filed Critical China Petroleum and Chemical Corp
Priority to CN201610947633.2A priority Critical patent/CN107987793A/en
Publication of CN107987793A publication Critical patent/CN107987793A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K3/00Materials not provided for elsewhere
    • C09K3/10Materials in mouldable or extrudable form for sealing or packing joints or covers
    • C09K3/1025Materials in mouldable or extrudable form for sealing or packing joints or covers characterised by non-chemical features of one or more of its constituents
    • C09K3/1028Fibres
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K3/00Materials not provided for elsewhere
    • C09K3/10Materials in mouldable or extrudable form for sealing or packing joints or covers
    • C09K3/1003Pure inorganic mixtures
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K3/00Materials not provided for elsewhere
    • C09K3/10Materials in mouldable or extrudable form for sealing or packing joints or covers
    • C09K2003/1034Materials or components characterised by specific properties

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Sealing Devices (AREA)

Abstract

The invention discloses a kind of combined high temperature sealing material machining manufacture using graphite as matrix, comprise the following steps:Graphite bar, fibrous material, B alloy wire are got out first;B alloy wire is added in graphite bar and fibrous material;The graphite bar of B alloy wire or graphite bar, the fibrous material of the single B alloy wire of parcel are wound, according to 18:1 proportioning, is knitted to form soft graphite sill;The soft graphite sill of formation is filled in professional columnar mould, compacting forms molding cylindrical type, circular platform type flexible seals coat the sheet copper of 1.2mm 1.8mm thickness at shaping circular platform type flexible seals both ends, and remaining molding cylindrical type flexible seals use the netted cladding of flexible steel wire.The present invention greatly improves the resistance to elevated temperatures of sealing material, meets heavy oil wells steam injection and production requirement.

Description

A kind of combined high temperature sealing material machining manufacture using graphite as matrix
Technical field
It is specifically a kind of using graphite as the compound of matrix the present invention relates to the machining manufacture of high-temperature sealing material High-temperature sealing material machining manufacture.
Background technology
When exploiting deep-layer heavy crude, steam injecting temperature improves, and production temperature will also raise, generally 350 DEG C -400 DEG C, therefore The heat resistance of downhole tool is required to improve.Downhole tool sealing material is generally using nitrile rubber, hydrogenated butyronitrile rubber at present Glue, fluorubber etc., although this kind of rubber meets seal request, its heat resistance is poor, usually exists with good elasticity Between 100 DEG C -240 DEG C.Conventional rubber materials heat resistance cannot meet the requirement of thick oil thermal extraction exploitation via steam injection.This Outside, it is graphite to commonly use industrial heat-resisting material, it is mainly used for high-temperature pipe elbow junction, is resistant to more than 600 DEG C high temperature, but The static seal of 2mm can only be no more than as seal clearance.Since its is frangible, elasticity it is small the characteristics of, though with good high temperature resistant Performance, can not be used for the big annular space deformation of thick oil thermal extraction downhole tool.Therefore it is badly in need of invention one kind with graphite high temperature resistant material Matter is the combined high temperature sealing material processing method of matrix, can process the high temperature sealing material of suitable thickened oil recovery.
In the prior art, graphite paper is high-carbon scale graphite is chemically treated that high-temperature expansion rolling forms.It is manufacture The basic material of various graphite seals.Be widely used in the industries such as electric power, oil, chemical industry, instrument, machinery, diamond machine, Pipe, pump, the dynamic sealing of valve and static seal, are the preferable novel seal materials for substituting the conventional seals such as rubber, fluoroplastics, asbestos Material.
In the prior art, the material similar with graphite paper also has graphite rope, graphite line etc..
Fibrous material includes inorfil, and inorfil includes asbestos, glass fibre.It is commonly used to make the asbestos being electrically insulated It is chrysotile, main chemical compositions are the positive britesorb (3MgO2SiO22H2O) containing the crystallization water.When temperature is up to 450 At~700 DEG C, chrysotile will lose water of constitution and become powder.Asbestos fibre in electrician has long fibre (by adding by hand Work forms) and staple fiber (by machine select and obtain) divide, their common feature is that have very high heat resistance, but dielectric properties compared with Difference, is typically used as heat safe low voltage motor, electrical apparatus insulation, sealing and gasket material.
The content of the invention
It is an object of the invention to provide a kind of combined high temperature sealing material machining manufacture using graphite as matrix, make The resistance to elevated temperatures of sealing material greatly improves, and meets heavy oil wells steam injection and production requirement.
In order to achieve the above objectives, present invention employs following technical solution, a kind of combined high temperature using graphite as matrix Sealing material machining manufacture, comprises the following steps:
Graphite bar, fibrous material, B alloy wire are got out first;
B alloy wire is added in graphite bar and fibrous material, addition manner there are two kinds, and one is wrapped in for 3-5 root B alloy wires Graphite bar surface and fibrous material surface;Secondly B alloy wire 3-5 roots are wrapped in inside graphite bar and inside fibrous material;
The graphite bar of B alloy wire or graphite bar, the fibrous material of the single B alloy wire of parcel are wound, according to parts by weight 18:1 Proportioning, is knitted to form soft graphite sill, i.e. graphite line on braiding machine.
B alloy wire winds the step of graphite bar and is, B alloy wire and graphite bar by braiding packing machine through 8 ingots, 18 ingots, 24 ingots into Row cross cap compiles the graphite-based material to form rope form, i.e. graphite rope;The graphite rope of formation is filled in columnar mould, in pressure For under 60 tons, room temperature is suppressed to form molding cylindrical type, circular platform type flexible seals by 4-5 hour, its density is 1.4- 1.5, hardness HB80-90.
The sheet copper of 1.2mm-1.8mm thickness is coated at shaping circular platform type flexible seals both ends, it is remaining molding Cylindrical type flexible seals use the netted cladding of flexible steel wire.
The sheet copper is handled by high tempering heat treatment process.Compared to the prior art, the present invention have with Lower beneficial effect:
1st, the processing method greatly improves the resistance to elevated temperatures of sealing material, meets heavy oil wells steam injection and production requirement.
2nd, graphite-based with the addition of reinforcement steel wire, make the increase of its sealing intensity.
3rd, the sheet copper of cladding is due to certain ductility, can extruded anisotropic graphite be deformed, can set In casing wall.
4th, the netted cladding of flexible steel wire avoids being squeezed the separation of powdered graphite, it is ensured that leakproofness.
Embodiment
Embodiment 1:
Ready-made graphite bar, fibrous material, B alloy wire are directly bought in market;
A kind of combined high temperature sealing material machining manufacture using graphite as matrix, comprises the following steps:
Add B alloy wire in graphite bar and fibrous material, addition manner for 3 B alloy wires be wrapped in graphite bar surface and Fibrous material surface;
Graphite bar, the fibrous material of B alloy wire are wound, according to parts by weight 18:1 proportioning, is knitted to form soft on braiding machine Property graphite-based material, i.e. graphite line.
B alloy wire winds the step of graphite bar and is, B alloy wire and graphite bar by braiding packing machine through 8 ingots, 18 ingots, 24 ingots into Row cross cap compiles the graphite-based material to form rope form, i.e. graphite rope;The graphite rope of formation is filled in columnar mould, in pressure For under 60 tons, room temperature is suppressed to form molding cylindrical type, circular platform type flexible seals by 4 hours, its density is 1.4- 1.5, hardness HB80-90.
The sheet copper of 1.2mm thickness, remaining molding cylindrical type are coated at shaping circular platform type flexible seals both ends Flexible seals use the netted cladding of flexible steel wire.
Embodiment 2:
Ready-made graphite bar, fibrous material, B alloy wire are directly bought in market;
A kind of combined high temperature sealing material machining manufacture using graphite as matrix, comprises the following steps:
B alloy wire is added in graphite bar and fibrous material, addition manner is wrapped in inside graphite bar for 5 B alloy wires Inside fibrous material;
Graphite bar, the fibrous material of single B alloy wire are wrapped up, according to parts by weight 18:1 proportioning, weaves shape on braiding machine Into soft graphite sill, i.e. graphite line.
B alloy wire winds the step of graphite bar and is, B alloy wire and graphite bar by braiding packing machine through 8 ingots, 18 ingots, 24 ingots into Row cross cap compiles the graphite-based material to form rope form, i.e. graphite rope;The graphite rope of formation is filled in columnar mould, in pressure For under 60 tons, room temperature is suppressed to form molding cylindrical type, circular platform type flexible seals by 5 hours, its density is 1.4- 1.5, hardness HB80-90.
The sheet copper of 1.8mm thickness, remaining molding cylindrical type are coated at shaping circular platform type flexible seals both ends Flexible seals use the netted cladding of flexible steel wire.
Embodiment 3:
Ready-made graphite bar, fibrous material, B alloy wire are directly bought in market;
A kind of combined high temperature sealing material machining manufacture using graphite as matrix, comprises the following steps:
B alloy wire is added in graphite bar and fibrous material, addition manner there are two kinds, and one is wrapped in stone for 4 B alloy wires Ink-stick surface and fibrous material surface;Secondly B alloy wire 4 is wrapped in inside graphite bar and inside fibrous material;
The graphite bar of B alloy wire or graphite bar, the fibrous material of the single B alloy wire of parcel are wound, according to parts by weight 18:1 Proportioning, is knitted to form soft graphite sill, i.e. graphite line on braiding machine.
B alloy wire winds the step of graphite bar and is, B alloy wire and graphite bar by braiding packing machine through 8 ingots, 18 ingots, 24 ingots into Row cross cap compiles the graphite-based material to form rope form, i.e. graphite rope;The graphite rope of formation is filled in columnar mould, in pressure For under 60 tons, room temperature is suppressed to form molding cylindrical type, circular platform type flexible seals by 4.5 hours, its density is 1.4- 1.5, hardness HB80-90.
The sheet copper of 1.5mm thickness, remaining molding cylindrical type are coated at shaping circular platform type flexible seals both ends Flexible seals use the netted cladding of flexible steel wire.
The foregoing is merely presently preferred embodiments of the present invention, is not used to limit the scope of the claims of the present invention, other are with this The equivalence changes of the patent spirit of invention, should all belong to the scope of the claims of the present invention.

Claims (4)

1. a kind of combined high temperature sealing material machining manufacture using graphite as matrix, comprises the following steps:
Graphite bar, fibrous material, B alloy wire are got out first;
B alloy wire is added in graphite bar and fibrous material, addition manner there are two kinds, and one is wrapped in graphite for 3-5 root B alloy wires Bar surface and fibrous material surface;Secondly B alloy wire 3-5 roots are wrapped in inside graphite bar and inside fibrous material;
The graphite bar of B alloy wire or graphite bar, the fibrous material of the single B alloy wire of parcel are wound, according to parts by weight 18:1 proportioning, Soft graphite sill, i.e. graphite line are knitted to form on braiding machine.
2. a kind of combined high temperature sealing material machining manufacture using graphite as matrix according to claim 1, it is special The step of sign is, B alloy wire winding graphite bar is that B alloy wire and graphite bar are carried out by braiding packing machine through 8 ingots, 18 ingots, 24 ingots Cross cap compiles the graphite-based material to form rope form, i.e. graphite rope;The graphite rope of formation is filled in columnar mould, is in pressure Under 60 tons, room temperature is suppressed to form molding cylindrical type, circular platform type flexible seals by 4-5 hour, its density is 1.4- 1.5, hardness HB80-90.
3. a kind of combined high temperature sealing material machining manufacture using graphite as matrix according to claim 2, it is special Sign is, the sheet copper of 1.2mm-1.8mm thickness, remaining molding circle are coated at shaping circular platform type flexible seals both ends Column type flexible seals use the netted cladding of flexible steel wire.
4. a kind of combined high temperature sealing material machining manufacture using graphite as matrix according to claim 3, it is special Sign is that the sheet copper is handled by high tempering heat treatment process.
CN201610947633.2A 2016-10-26 2016-10-26 A kind of combined high temperature sealing material machining manufacture using graphite as matrix Pending CN107987793A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610947633.2A CN107987793A (en) 2016-10-26 2016-10-26 A kind of combined high temperature sealing material machining manufacture using graphite as matrix

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610947633.2A CN107987793A (en) 2016-10-26 2016-10-26 A kind of combined high temperature sealing material machining manufacture using graphite as matrix

Publications (1)

Publication Number Publication Date
CN107987793A true CN107987793A (en) 2018-05-04

Family

ID=62028788

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610947633.2A Pending CN107987793A (en) 2016-10-26 2016-10-26 A kind of combined high temperature sealing material machining manufacture using graphite as matrix

Country Status (1)

Country Link
CN (1) CN107987793A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110375068A (en) * 2019-07-25 2019-10-25 宁波信幸隆密封制品有限公司 A kind of band-like carbon seal ring and its processing technology and process equipment
CN110439999A (en) * 2019-08-15 2019-11-12 广州安卓机械科技有限公司 A kind of graphite packing line Wiring technology

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1106443A (en) * 1994-11-22 1995-08-09 萧山市密封件厂 Method for prodn. of flexible graphite weaving filler
CN1676977A (en) * 2004-03-31 2005-10-05 日本皮拉工业株式会社 Braiding yarn made of expanded graphite, and gland packing
CN2777290Y (en) * 2005-03-22 2006-05-03 浙江国泰密封材料股份有限公司 High temp. resistant high-pressure resistant packer
CN202971888U (en) * 2012-11-23 2013-06-05 杭州麦克密封材料有限公司 High-temperature resistant sealing packing
CN203202394U (en) * 2012-12-07 2013-09-18 浙江国泰密封材料股份有限公司 Reinforced-type high-temperature and high-pressure resistant soft graphite sealing ring
CN203272776U (en) * 2013-05-06 2013-11-06 青岛强龙电力石化配件有限公司 Nickel base graphite packing for high temperature and high pressure
CN203717905U (en) * 2013-07-23 2014-07-16 简诺(上海)密封制品有限公司 Notch-free reinforced woven sealing gasket ring

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1106443A (en) * 1994-11-22 1995-08-09 萧山市密封件厂 Method for prodn. of flexible graphite weaving filler
CN1676977A (en) * 2004-03-31 2005-10-05 日本皮拉工业株式会社 Braiding yarn made of expanded graphite, and gland packing
CN2777290Y (en) * 2005-03-22 2006-05-03 浙江国泰密封材料股份有限公司 High temp. resistant high-pressure resistant packer
CN202971888U (en) * 2012-11-23 2013-06-05 杭州麦克密封材料有限公司 High-temperature resistant sealing packing
CN203202394U (en) * 2012-12-07 2013-09-18 浙江国泰密封材料股份有限公司 Reinforced-type high-temperature and high-pressure resistant soft graphite sealing ring
CN203272776U (en) * 2013-05-06 2013-11-06 青岛强龙电力石化配件有限公司 Nickel base graphite packing for high temperature and high pressure
CN203717905U (en) * 2013-07-23 2014-07-16 简诺(上海)密封制品有限公司 Notch-free reinforced woven sealing gasket ring

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110375068A (en) * 2019-07-25 2019-10-25 宁波信幸隆密封制品有限公司 A kind of band-like carbon seal ring and its processing technology and process equipment
CN110439999A (en) * 2019-08-15 2019-11-12 广州安卓机械科技有限公司 A kind of graphite packing line Wiring technology

Similar Documents

Publication Publication Date Title
CN107987793A (en) A kind of combined high temperature sealing material machining manufacture using graphite as matrix
CN103850653B (en) The manufacture method of insulation oil sleeve pipe
CN102719773B (en) Method for manufacturing zirconium plate corrugated pipe
CN203757290U (en) Oil extracting pipe with nanometer aerogel felt
CN204792101U (en) Stand wear and tear exploration cable is used to oil well
CN104715825A (en) High-temperature resistant fireproof cable
CN1645524A (en) Preparation and products of high temperature resistant and corrosionproof electric cables with polyfluorinated ethylene isolation
CN204294716U (en) The expanding compound tube end sizing of hydraulic pressure of dual-metal clad steel pipe and sealing device
CN208804337U (en) PPR composite thermal-insulating pipe
CN201137699Y (en) Low ignition loss graphite weaving buchan
CN104033606A (en) Pipeline-trepanning sealing plug
CN2544086Y (en) Thermal-insulation oil production pipe for thick oil
CN103850654B (en) The manufacture method of the heat insulation tubing and casing of prestressing force
CN2919766Y (en) Carboform electrothermal bushing
CN204573468U (en) A kind of high-temperature resistant tube wire terminal protective equipment
CN207113609U (en) A kind of more enamel-covered wires pass through the sealing structure of hyperbar electric furnace cover
CN202580336U (en) Thermoplastic large-caliber polytetrafluoroethylene thin-walled pipe
CN106090485B (en) A kind of insulating joint of the mechanical connecting band flexible glue layer of disassembly
CN2618025Y (en) Environmental protective steel copper composite pipe
CN205879388U (en) Multistage temperature thermocouple
CN204901201U (en) Fluorine plastic seal device for fluid
CN202150276U (en) PEEK guide line for nuclear energy generator
CN206976055U (en) Enhanced electric cable of submersible pump
CN2644839Y (en) Annular tube compensator
CN103292067A (en) Steel frame reinforced type petroleum pipe

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20180504