CN107987792A - A kind of high osmosis construction structure glue and preparation method thereof - Google Patents
A kind of high osmosis construction structure glue and preparation method thereof Download PDFInfo
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- CN107987792A CN107987792A CN201711240897.5A CN201711240897A CN107987792A CN 107987792 A CN107987792 A CN 107987792A CN 201711240897 A CN201711240897 A CN 201711240897A CN 107987792 A CN107987792 A CN 107987792A
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- China
- Prior art keywords
- component
- raw material
- aerosil
- structure glue
- construction structure
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J201/00—Adhesives based on unspecified macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
- C08K3/36—Silica
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/16—Nitrogen-containing compounds
- C08K5/17—Amines; Quaternary ammonium compounds
- C08K5/18—Amines; Quaternary ammonium compounds with aromatically bound amino groups
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
A kind of high osmosis construction structure glue, including the raw material of following mass parts are prepared：Component A:Unsaturated-resin 95 105, silica flour 95 105, calcium activated 8 12, aerosil 46, dimethylaniline 0.4 0.6；B component:Benzoyl peroxide 10 20, dibutyl ester 8 12, aerosil 0.5 1.5, precipitated calcium carbonate 8 12；The component A and the proportioning of B component are A:B=20:1 (mass parts) beneficial effects of the present invention are：Inventive formulation is reasonable, processing technology is scientific and normal, construction structure glue adhesive property after preparation is superior, and intensity and wilfulness are superior to similar product, and the use of calcium activated is employed in raw material, infiltrative enhancing is fully ensured that, dibutyl ester in raw material uses, and instead of in similar product and is used as curing agent using water, it is ensured that the strong diffusivity of product after overall preparation, operation is relatively convenient, substantially improves the brittleness of waterborne curing agent solidfied material.
Description
Technical field
The present invention relates to construction structure glue processing technique field, and in particular to a kind of high osmosis construction structure glue and its
Preparation method.
Background technology
Building structure adhesive is widely used in construction and installation, finishing, sealing, structural adhesive because of its excellent properties
Deng in field, building trade in the pillar industry first developed as China, China's architecture adhesion agent no matter in kind also
It is all rapidly to be developed in yield, the developing direction of modern architecture will be that design standard, mechanization of building operation, component are pre-
Inhibition and generation and the lightweight of building materials, high-strength and multifunction.And the extensive use of building structure adhesive, by accelerate this four change into
Journey, and improving speed of application, beautifying constructure, improving construction quality, saving man-hour and energy environment protection, reduction pollution etc.
All various aspects are all significant, therefore adhesive for building becomes one of important chemical building material.
Anchoring adhesive its actual product is exquisite meets the eye on every side, but in current technical field, there are substantial amounts of different components,
But not a kind of comparatively preferable product, since structure glue acts on interior of building in itself, built in implantation
After building thing inside, it is necessary to ensure its actual mobile performance of structure glue, ensure its actual effective performance, so as to obtain phase
To the adhesive property of more large area, but in actual mobility, in the market is led again without the presence of such a product
The unilateral performance for causing structure glue to use in itself, cannot get good use.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of processing technology scientific and normal, and formula is taken rationally, system
Product is big in the street at the station of structure glue reality after standby, uses efficiently and effectively high osmosis construction structure glue and preparation method thereof.
The technical problems to be solved by the invention are realized using following technical scheme：
A kind of high osmosis construction structure glue, it is characterised in that the raw material including following mass parts is prepared：
Component A
Unsaturated-resin 95-105, silica flour 95-105, calcium activated 8-12, aerosil 4-6, dimethylaniline
0.4-0.6；
B component
Benzoyl peroxide 10-20, dibutyl ester 8-12, aerosil 0.5-1.5, precipitated calcium carbonate 8-12；
The component A and the proportioning of B component are A:B=20:1 (mass parts).
Preferred mass part of above-mentioned each raw material is：
Component A
Unsaturated-resin 100, silica flour 100, calcium activated 10, aerosil 5, dimethylaniline 0.5；
B component
Benzoyl peroxide 15, dibutyl ester 10, aerosil 1, precipitated calcium carbonate 10；
The component A and the proportioning of B component are A:B=20:1 (mass parts).
Unsaturated-resin in the raw material is 191# unsaturated-resins；The particle mesh number of the silica flour is 325
Mesh；
The method for preparing above-mentioned high osmosis construction structure glue, it is characterised in that comprise the following steps：
1) it is the unsaturated-resin heating stirring in component A raw material is uniform, it is spare；
2) after merging the silica flour in component A raw material, calcium activated and aerosil, it is spare to obtain pulvis；
3) compounded after the material in above-mentioned steps 1 and step 2 is merged uniformly, then by the dimethyl in raw material
Aniline is added thereto, and after being again stirring for uniformly, obtains component A initial material；
4) benzoyl peroxide in B component raw material, dibutyl ester, aerosil and precipitated calcium carbonate are stirred equal
After even, B component initial material is obtained,
5) by the B component initial material installation 20 in the component A initial material in above-mentioned steps 3 and step 4:1 mass ratio is answered
After stirring evenly, you can obtain this product.
Beneficial effects of the present invention are：Inventive formulation is reasonable, and processing technology is scientific and normal, the building structure after preparation
Glue sticking superior performance, intensity and wilfulness are superior to similar product, and the use of calcium activated is employed in raw material, is fully ensured that
Infiltrative enhancing, the dibutyl ester in raw material use, instead of in similar product and be used as curing agent using water, it is ensured that integrally
The strong diffusivity of product after preparation, operation is relatively convenient, substantially improves the brittleness of waterborne curing agent solidfied material.
Embodiment
In order to make the technical means, the creative features, the aims and the efficiencies achieved by the present invention easy to understand, below
In conjunction with specific embodiments, the present invention is further explained.
Embodiment 1
A kind of high osmosis construction structure glue, including the raw material of following mass parts are prepared：
Component A
Unsaturated-resin 95, silica flour 95, calcium activated 8, aerosil 4, dimethylaniline 0.4；
B component
Benzoyl peroxide 10, dibutyl ester 8, aerosil 0.5, precipitated calcium carbonate 8；
The component A and the proportioning of B component are A:B=20:1 (mass parts).
The method for preparing above-mentioned high osmosis construction structure glue, comprises the following steps：
1) it is the unsaturated-resin heating stirring in component A raw material is uniform, it is spare；
2) after merging the silica flour in component A raw material, calcium activated and aerosil, it is spare to obtain pulvis；
3) compounded after the material in above-mentioned steps 1 and step 2 is merged uniformly, then by the dimethyl in raw material
Aniline is added thereto, and after being again stirring for uniformly, obtains component A initial material；
4) benzoyl peroxide in B component raw material, dibutyl ester, aerosil and precipitated calcium carbonate are stirred equal
After even, B component initial material is obtained,
5) by the B component initial material installation 20 in the component A initial material in above-mentioned steps 3 and step 4:1 mass ratio is answered
After stirring evenly, you can obtain this product.
Embodiment 2
A kind of high osmosis construction structure glue, including the raw material of following mass parts are prepared：
Component A
Unsaturated-resin 105, silica flour 105, calcium activated 12, aerosil 6, dimethylaniline 0.6；
B component
Benzoyl peroxide 20, dibutyl ester 12, aerosil 1.5, precipitated calcium carbonate 12；
The component A and the proportioning of B component are A:B=20:1 (mass parts).
The method for preparing above-mentioned high osmosis construction structure glue, comprises the following steps：
1) it is the unsaturated-resin heating stirring in component A raw material is uniform, it is spare；
2) after merging the silica flour in component A raw material, calcium activated and aerosil, it is spare to obtain pulvis；
3) compounded after the material in above-mentioned steps 1 and step 2 is merged uniformly, then by the dimethyl in raw material
Aniline is added thereto, and after being again stirring for uniformly, obtains component A initial material；
4) benzoyl peroxide in B component raw material, dibutyl ester, aerosil and precipitated calcium carbonate are stirred equal
After even, B component initial material is obtained,
5) by the B component initial material installation 20 in the component A initial material in above-mentioned steps 3 and step 4:1 mass ratio is answered
After stirring evenly, you can obtain this product.
Embodiment 3
A kind of high osmosis construction structure glue, including the raw material of following parts by weight are prepared：
Component A
191# unsaturated-resins 100kg, silica flour 100kg, calcium activated 10kg, aerosil 5kg, dimethyl benzene
Amine 0.5kg；
B component
Benzoyl peroxide 15kg, dibutyl ester 10kg, aerosil 1kg, precipitated calcium carbonate 10kg；
The component A and the proportioning of B component are A:B=20:1 (mass parts).
The method for preparing above-mentioned high osmosis construction structure glue, it is characterised in that comprise the following steps：
1) it is the unsaturated-resin heating stirring in component A raw material is uniform, it is spare；
2) after merging the silica flour in component A raw material, calcium activated and aerosil, it is spare to obtain pulvis；
3) compounded after the material in above-mentioned steps 1 and step 2 is merged uniformly, then by the dimethyl in raw material
Aniline is added thereto, and after being again stirring for uniformly, obtains component A initial material；
4) benzoyl peroxide in B component raw material, dibutyl ester, aerosil and precipitated calcium carbonate are stirred equal
After even, B component initial material is obtained,
5) by the B component initial material installation 20 in the component A initial material in above-mentioned steps 3 and step 4:1 mass ratio is answered
After stirring evenly, you can obtain this product.
It is the construction structure glue performance parameter data prepared in the application below；
| Penetration depth (mm) | Compression strength (MPa) | The fixed line time (s) | |
| Embodiment 1 | 25 | 88 | 352 |
| Embodiment 2 | 24 | 89 | 385 |
| Embodiment 3 | 26 | 91 | 402 |
| The prior art | 13 | 71 | 1523 |
It can be seen from the above that in the application, the construction structure glue of preparation, its actual fixed line time and compression strength are higher by
Existing product index, and the actual penetration depth of glue is also higher by 11-13mm in the prior art in the application, so as to
To determine the permeability of the glue reality in the application, high intensity during bonding ensure that.
The basic principles, main features and the advantages of the invention have been shown and described above.The skill of the industry
Art personnel it should be appreciated that the present invention is not limited to the above embodiments, the above embodiments and description only describe
The principle of the present invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, this
A little changes and improvements all fall within the protetion scope of the claimed invention.The claimed scope of the invention is by appended claim
Book and its equivalent thereof.
Claims (5)
1. a kind of high osmosis construction structure glue, it is characterised in that the raw material including following mass parts is prepared：
Component A
Unsaturated-resin 95-105, silica flour 95-105, calcium activated 8-12, aerosil 4-6, dimethylaniline 0.4-
0.6；
B component
Benzoyl peroxide 10-20, dibutyl ester 8-12, aerosil 0.5-1.5, precipitated calcium carbonate 8-12；
The component A and the proportioning of B component are A:B=20:1 (mass parts).
2. high osmosis construction structure glue according to claim 1, it is characterised in that preferred mass part of each raw material is：
Component A
Unsaturated-resin 100, silica flour 100, calcium activated 10, aerosil 5, dimethylaniline 0.5；
B component
Benzoyl peroxide 15, dibutyl ester 10, aerosil 1, precipitated calcium carbonate 10；
The component A and the proportioning of B component are A:B=20:1 (mass parts).
3. high osmosis construction structure glue according to claim 1, it is characterised in that：Unsaturated-resin in the raw material
For 191# unsaturated-resins；The particle mesh number of the silica flour is 325 mesh.
A kind of 4. high osmosis construction structure glue according to claim 1, it is characterised in that：The diluent is poly- third
Hexanediol diglycidyl ether.
5. the method for application 1 or 2 middle and high infiltration permeability construction structure glue of the claims, it is characterised in that comprise the following steps：
1) it is the unsaturated-resin heating stirring in component A raw material is uniform, it is spare；
2) after merging the silica flour in component A raw material, calcium activated and aerosil, it is spare to obtain pulvis；
3) compound uniformly after the material in above-mentioned steps 1 and step 2 is merged, then add the dimethylaniline in raw material
Enter wherein, after being again stirring for uniformly, obtain component A initial material；
4) after the benzoyl peroxide in B component raw material, dibutyl ester, aerosil and precipitated calcium carbonate being stirred evenly,
B component initial material is obtained,
5) by the B component initial material installation 20 in the component A initial material in above-mentioned steps 3 and step 4:1 mass ratio carries out compounding and stirs
After mixing uniformly, you can obtain this product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711240897.5A CN107987792A (en) | 2017-11-30 | 2017-11-30 | A kind of high osmosis construction structure glue and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711240897.5A CN107987792A (en) | 2017-11-30 | 2017-11-30 | A kind of high osmosis construction structure glue and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107987792A true CN107987792A (en) | 2018-05-04 |
Family
ID=62034741
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711240897.5A Pending CN107987792A (en) | 2017-11-30 | 2017-11-30 | A kind of high osmosis construction structure glue and preparation method thereof |
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| CN (1) | CN107987792A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102816534A (en) * | 2012-08-14 | 2012-12-12 | 北京海斯迪克新材料有限公司 | Structure adhesive for metal adhesion, and preparation method thereof |
| CN103571422A (en) * | 2012-07-27 | 2014-02-12 | 武汉市石代高新建材有限公司 | Novel marble adhesive |
-
2017
- 2017-11-30 CN CN201711240897.5A patent/CN107987792A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103571422A (en) * | 2012-07-27 | 2014-02-12 | 武汉市石代高新建材有限公司 | Novel marble adhesive |
| CN102816534A (en) * | 2012-08-14 | 2012-12-12 | 北京海斯迪克新材料有限公司 | Structure adhesive for metal adhesion, and preparation method thereof |
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Application publication date: 20180504 |