CN107987574A - The paint preparation method that a kind of multi-functional and performance is stablized - Google Patents
The paint preparation method that a kind of multi-functional and performance is stablized Download PDFInfo
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- CN107987574A CN107987574A CN201711299158.3A CN201711299158A CN107987574A CN 107987574 A CN107987574 A CN 107987574A CN 201711299158 A CN201711299158 A CN 201711299158A CN 107987574 A CN107987574 A CN 107987574A
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- Prior art keywords
- paint
- performance
- stablized
- functional
- agent
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D4/00—Coating compositions, e.g. paints, varnishes or lacquers, based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; Coating compositions, based on monomers of macromolecular compounds of groups C09D183/00 - C09D183/16
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses the paint preparation method that a kind of multi-functional and performance is stablized, including following steps：Step S1：Using paint raw materials as major ingredient, initiator, 20% anti-wear agent, 14% fire retardant, 12% accelerating agent, 18% diluent that percentage by weight is 8% are added；Together it is put into mixer and is smashed and add water to obtain mixture A after stirring evenly.Step S2：It is 28% stabilizer that mixture A, which adds solution weight percentage, is maintained the temperature between 45 degrees Celsius to 50 degrees Celsius, continues stir about 12 minutes.Step S3：Resulting solution in step S2 is put into 2 3h of mixing in mixer, paint is made.The paint is according to said method prepared not only to make simply, toxic gas is not produced in manufacturing process, its dispersiveness, physics, mechanical performance, heat endurance and fire resistance are improved and improve with wear-resisting, fire prevention, and can waterproof, air-tightness be good, performance is stablized.
Description
Technical field
It is a kind of multi-functional and paint preparation side that performance is stablized specifically the present invention relates to Multifunctional paint field
Method.
Background technology
The general component of paint includes：Film forming matter, pigment, solvent, auxiliary agent.Oasis vegetation paint it is many basis into
Part uses plant material, belongs to pure natural substance.Paint is that one kind can firmly be covered in body surface, plays protection, decoration, mark
With the chemical mixture coating of other specific uses.More authoritative one book of coating process of Chinese coating circle is defined as：
" coating is a kind of material, and this material can be coated in object surface with different construction technologies, and formation adhesion is firm, has
Some strength, continuous solid film.The film common name film so formed, also known as paint film or coating." belong to organic chemical industry's high score
Sub- material, the film formed belong to high-molecular compound type.The classification for the chemical products passed through according to the modern times, coating belong to
Fine chemical product.Modern coating progressively becomes a kind of multi-functional engineering material, is one in chemical industry
Important industry.
Paint species now on the market is various, but with increase of the people to the functional requirement of paint, existing oil
Paint cannot meet this needs of people, and paint has no longer been only to realize protection, decoration functions just.Such as the patent No.
For 02115972, patent name is the patent application patent of " a kind of anticracking paint ", it is characterised in that is by paint freezing plastic, water
Mud mixes, its weight go out for：Paint 50%, freezing plastic 5%, cement 45%.Paint, which is applied on wall, will not fall off, and occurs without and splits
Line, it is pollution-free, particularly suitable for repairing metope.
However, the paint described in above-mentioned patent is also only protected substantially, the function of device, function is more single on the whole
One, it still cannot meet that the growing life requirement of existing people such as prevents fires, keeps the temperature etc. and keeping its stability
Aspect has been short of.
The content of the invention
For it is above-mentioned but under, it is an object of the invention to provide the paint preparation method that a kind of multi-functional and performance is stablized,
Not only preparation process is simple, but also the paint performance stabilization prepared also has the function of wear-resisting, fire prevention, waterproof.
The present invention is achieved through the following technical solutions：The paint preparation method that a kind of multi-functional and performance is stablized, including with
Under several steps：
Step S1：Using paint raw materials as major ingredient, the fire-retardant of initiator, 20% anti-wear agent, 14% that percentage by weight is 8% is added
Agent, 12% accelerating agent, 18% diluent；Together it is put into mixer and is smashed and add water to obtain mixture after stirring evenly
A。
Step S2：It is 28% stabilizer that mixture A, which adds solution weight percentage, maintains the temperature at 45 degrees Celsius to 50 and takes the photograph
Between family name's degree, continue stir about 12 minutes.
Step S3：Resulting solution in step S2 is put into mixing 2-3h in mixer, the mixture after mixing is passed through strong
Quick rotation chain rupture is carried out in drawing-in device press-in double screw extruder processed, 100-159 revs/min of rotary speed, is made institute
The paint stated.
In order to preferably realize the present invention, further, the fire retardant by following weight raw material prepare and
Into：Tricresyl phosphate -12-15 parts of diphenyl ester, amyl- 8-14 parts of the 1- enols propionic ester of 2- methyl -5- oxo rings, allyl isothiocyanate
2-3 parts, 4-8 parts of tri-2-ethylhexyl phosphate.Have that additive amount is few, the high and low cigarette of flame retarding efficiency, low using the fire retardant
The advantages that malicious, widely used, and work in-process does not produce toxic gas, its dispersiveness, physics, mechanical performance, heat endurance
And fire resistance is improved and improves.
In order to preferably realize the present invention, further, 50 degrees Celsius are maintained the temperature in the step S2.Through experiment
It was found that the speed highest and mixed effect that are mixed when maintaining the temperature under 50 degrees Celsius and being stirred are preferable.
In order to preferably realize the present invention, further, the anti-wear agent is alumina in Nano level or nano silicon dioxide.
Wearability, the resistance to scraping of product can be improved using the anti-wear agent, improves product self-cleaning property.With traditional low molecular weight auxiliary agent phase
Than the anti-wear agent of super high molecular weight will not reduce the mechanical property of product, not migrate, product surface non-greasy, smooth, Er Qiewu
Poison is non-dangerous article.
In order to preferably realize the present invention, further, the accelerating agent is in EP2220, EP3350 or EP-DS1300
It is any.Using three kinds of accelerating agents can prevent silver powder in aluminium paint come off and will not blackening, and the hard of paint film can be improved
Degree and resistance to scraping.Adhesive force promotes the auxiliary agent type resin that resin LTW is a kind of soft specific use, has extensive compatibility,
For improving internal layer adhesive force of the different base-materials to metal and inorganic matter and some plastics adhesive force coating.For some bases
Material, adhesive force promotion resin LTW can also improve pliability when room temperature and low temperature.
In order to preferably realize the present invention, further, the diluent is five acrylate of dipentaerythrite, crosses chlorine
One or more in ethene lacquer diluent or tetramethylol methane tetraacrylate.There is preferable dilution capacity using the diluent
With appropriate evaporation rate, and in the diluent it is ester-containing, ketone solvent ratio is higher, solubility property is good.
In order to preferably realize the present invention, further, the stabilizer is counted in parts by weight, by calcium stearate 40-50,
Zinc stearate 20-25, B diketone 30-60, nontoxic phosphite ester 40-70, antioxidant 10-15, hydrotalcite 5-8, OPE15-20,
EBS5-20 is formed.The stabilizer obtained by this formula has good dispersiveness, compatibility, a processing fluidity, wide adaptability,
Product surface finish is excellent；Good heat stability, initial stage, form and aspect were small, no precipitation phenomenon；Without heavy metal and other toxic components,
Without sulfation；Congo red testing time length, has excellent electrical insulating property, free from admixture, has efficient weatherability；The scope of application
Extensively, highly practical, dosage is few, has multifunctionality；In white article, whiteness is compared with its similar product more preferably.Not only have very
Good compatibility and the controlling to viscosity, and it is that a kind of excellent heat is steady that can provide good initial coloring and colour retention
Determine agent.
Compared with prior art, the present invention haing the following advantages and beneficial effect：
（1）The present invention by by calcium stearate 40-50, zinc stearate 20-25, B diketone 30-60, nontoxic phosphite ester 40-70,
The stabilizer of antioxidant 10-15, hydrotalcite 5-8, OPE15-20, EBS5-20 composition, ensure paint have well dispersiveness,
Compatibility, processing fluidity, wide adaptability, product surface finish are excellent；Good heat stability, initial stage, form and aspect were small, no to separate out now
As；Without heavy metal and other toxic components, no sulfation；Congo red testing time length, has excellent electrical insulating property, nothing
Impurity, has efficient weatherability.
（2）The present invention by alumina in Nano level or nano silicon dioxide be used as anti-wear agent can improve product wearability,
Resistance to scraping, improves product self-cleaning property.Compared with traditional low molecular weight auxiliary agent, the anti-wear agent of super high molecular weight will not reduce production
The mechanical property of product, does not migrate, product surface non-greasy, smooth, and nontoxic is non-dangerous article.
（3）The present invention is prepared by fire retardant by the raw material of following weight：2- methyl -5- oxo rings are amyl-
12-15 parts of 1- enol propionic esters, 1-2 parts of allyl isothiocyanate, 5-10 parts of tri-2-ethylhexyl phosphate, tricresyl phosphate-
Diphenyl ester 10-15.Have the advantages that additive amount is few, the high and low cigarette of flame retarding efficiency, low toxicity, widely used using the fire retardant, and
Work in-process does not produce toxic gas, its dispersiveness, physics, mechanical performance, heat endurance and fire resistance are improved and change
It is kind.
（4）The present invention is five acrylate of dipentaerythrite, Vinylidene Chloride lacquer diluent or Ji Wusi by diluent
One or more in alcohol tetraacrylate.There is preferable dilution capacity and appropriate evaporation rate using the diluent, and
And it is ester-containing in the diluent, ketone solvent ratio is higher, solubility property is good.
Embodiment
Embodiment 1：
The paint preparation method that a kind of multi-functional and performance of the present embodiment is stablized, including following steps：
Step S1：Using paint raw materials as major ingredient, the fire-retardant of initiator, 20% anti-wear agent, 14% that percentage by weight is 8% is added
Agent, 12% accelerating agent, 18% diluent；Together it is put into mixer and is smashed and add water to obtain mixture after stirring evenly
A。
Step S2：It is 28% stabilizer that mixture A, which adds solution weight percentage, maintains the temperature at 45 degrees Celsius to 50 and takes the photograph
Between family name's degree, continue stir about 12 minutes.
Step S3：Resulting solution in step S2 is put into mixing 2-3h in mixer, the mixture after mixing is passed through strong
Quick rotation chain rupture is carried out in drawing-in device press-in double screw extruder processed, 100-159 revs/min of rotary speed, is made institute
The paint stated.According to said method prepare the paint not only to make simply, toxic gas is not produced in manufacturing process, its dispersiveness, thing
Reason, mechanical performance, heat endurance and fire resistance are improved and improve with wear-resisting, fire prevention, and being capable of waterproof, air-tightness
Good, performance is stablized.
Embodiment 2：
The present embodiment does further optimization on the basis of embodiment 1, the fire retardant by following weight raw material system
It is standby to form：Amyl- 12-15 parts of the 1- enols propionic ester of 2- methyl -5- oxo rings, 1-2 parts of allyl isothiocyanate, tricresyl phosphate (2- second
Base hexyl) 5-10 parts of ester, tricresyl phosphate-diphenyl ester 10-15.Have that additive amount is few, flame retarding efficiency is high and low using the fire retardant
Cigarette, low toxicity, it is widely used the advantages that, and work in-process does not produce toxic gas, its dispersiveness, physics, mechanical performance, heat are steady
Qualitative and fire resistance is improved and improves.
The initiator is ammonium persulfate.
The other parts of the present embodiment are same as Example 1, and so it will not be repeated.
Embodiment 3：
The present embodiment does further optimization on the basis of embodiment 2, and the anti-wear agent is alumina in Nano level or nano-silica
SiClx.Wearability, the resistance to scraping of product can be improved using the anti-wear agent, improves product self-cleaning property.With traditional low molecular weight
Auxiliary agent is compared, and the anti-wear agent of super high molecular weight will not reduce the mechanical property of product, not migrate, product surface non-greasy, smooth,
And nontoxic is non-dangerous article.
The accelerating agent is EP2220, EP3350 or EP-DS1300.Silver powder in aluminium paint can be prevented using the accelerating agent
Come off and will not blackening, and the hardness and resistance to scraping of paint film can be improved.It is a kind of soft specific use that adhesive force, which promotes resin LTW,
Auxiliary agent type resin, there is extensive compatibility, metal and inorganic matter and some plastics are adhered to for improving different base-materials
The internal layer adhesive force of power coating.It is flexible when adhesive force promotes the resin LTW can also to improve room temperature and low temperature for some base materials
Property.
The diluent is five acrylate of dipentaerythrite, Vinylidene Chloride lacquer diluent or pentaerythrite tetrapropylene are sour
One or more in ester.There is preferable dilution capacity and appropriate evaporation rate, and the diluent using the diluent
In it is ester-containing, ketone solvent ratio is higher, solubility property is good.
The other parts of the present embodiment are same as Example 2, and so it will not be repeated.
Embodiment 4：
The present embodiment does further optimization on the basis of embodiment 3, and the stabilizer is counted in parts by weight, by calcium stearate
40-50, zinc stearate 20-25, B diketone 30-60, nontoxic phosphite ester 40-70, antioxidant 10-15, hydrotalcite 5-8, OPE15-
20, EBS5-20 compositions.The stabilizer obtained by this formula has good dispersiveness, compatibility, processing fluidity, adaptability
Extensively, product surface finish is excellent；Good heat stability, initial stage, form and aspect were small, no precipitation phenomenon；Without heavy metal and other it is poisonous into
Point, no sulfation；Congo red testing time length, has excellent electrical insulating property, free from admixture, has efficient weatherability；It is applicable in
Scope is wide, highly practical, and dosage is few, has multifunctionality；In white article, whiteness is compared with its similar product more preferably.Not only have
There are good compatibility and the controlling to viscosity, and it is a kind of excellent that can provide good initial coloring and colour retention
Heat stabilizer.
The other parts of the present embodiment are same as Example 3, and so it will not be repeated.
The above, is only presently preferred embodiments of the present invention, not does limitation in any form to the present invention, it is every according to
Any simply modification, the equivalent variations made according to the technical spirit of the present invention to above example, each fall within the protection of the present invention
Within the scope of.
Claims (7)
1. the paint preparation method that a kind of multi-functional and performance is stablized, it is characterised in that：Including following steps：
Step S1：Using paint raw materials as major ingredient, the fire-retardant of initiator, 20% anti-wear agent, 14% that percentage by weight is 8% is added
Agent, 12% accelerating agent, 18% diluent；Together it is put into mixer and is smashed and add water to obtain mixture after stirring evenly
A；
Step S2：It is 28% stabilizer that mixture A, which adds solution weight percentage, maintains the temperature at 45 degrees Celsius to 50 degrees Celsius
Between, continue stir about 12 minutes；
Step S3：Resulting solution in step S2 is put into mixing 4-6h in mixer, the mixture after mixing is fed by forcing
Expect to carry out quick rotation chain rupture in device press-in double screw extruder, 80-100 revs/min of rotary speed, is made the oil
Paint.
2. the paint preparation method that according to claim 1 a kind of multi-functional and performance is stablized, it is characterised in that：The step
50 degrees Celsius are maintained the temperature in rapid S2.
3. the paint preparation method that according to claim 1 a kind of multi-functional and performance is stablized, it is characterised in that：The resistance
Combustion agent is prepared by the raw material of following weight：Tricresyl phosphate -12-15 parts of diphenyl ester, 2- methyl -5- oxo rings are amyl-
8-14 parts of 1- enol propionic esters, 2-3 parts of allyl isothiocyanate, 4-8 parts of tri-2-ethylhexyl phosphate.
4. the paint preparation method that according to claim 1 a kind of multi-functional and performance is stablized, it is characterised in that：It is described resistance to
Grinding agent is alumina in Nano level or nano silicon dioxide.
5. the paint preparation method that according to claim 1 a kind of multi-functional and performance is stablized, it is characterised in that：The rush
It is any of EP2220, EP3350 or EP-DS1300 into agent.
6. the paint preparation method that according to claim 1 a kind of multi-functional and performance is stablized, it is characterised in that：It is described dilute
It is five acrylate of dipentaerythrite, Vinylidene Chloride lacquer diluent or one kind or more in tetramethylol methane tetraacrylate to release agent
Kind.
7. the paint preparation method that according to claim 1 a kind of multi-functional and performance is stablized, it is characterised in that：It is described steady
Determine agent to count in parts by weight, by calcium stearate 40-50, zinc stearate 20-25, B diketone 30-60, nontoxic phosphite ester 40-70,
Antioxidant 10-15, hydrotalcite 5-8, OPE15-20, EBS5-20 composition.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711299158.3A CN107987574A (en) | 2017-12-08 | 2017-12-08 | The paint preparation method that a kind of multi-functional and performance is stablized |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711299158.3A CN107987574A (en) | 2017-12-08 | 2017-12-08 | The paint preparation method that a kind of multi-functional and performance is stablized |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107987574A true CN107987574A (en) | 2018-05-04 |
Family
ID=62035919
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711299158.3A Pending CN107987574A (en) | 2017-12-08 | 2017-12-08 | The paint preparation method that a kind of multi-functional and performance is stablized |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107987574A (en) |
-
2017
- 2017-12-08 CN CN201711299158.3A patent/CN107987574A/en active Pending
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Application publication date: 20180504 |