CN107982293A - A kind of place of production of genunie medicinal materials Angelica sinensis is without sulphur processing method - Google Patents

A kind of place of production of genunie medicinal materials Angelica sinensis is without sulphur processing method Download PDF

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CN107982293A
CN107982293A CN201711177782.6A CN201711177782A CN107982293A CN 107982293 A CN107982293 A CN 107982293A CN 201711177782 A CN201711177782 A CN 201711177782A CN 107982293 A CN107982293 A CN 107982293A
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angelica sinensis
angelica
sinensis
vexed profit
temperature
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吴仲涛
阎玉珍
马中森
洪建雄
连宝军
边金鹏
车小娟
马政
付强
马成
张义贤
莫兆芳
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West Gansu Baohetang Pharmaceutical Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/23Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
    • A61K36/232Angelica
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10Preparation or pretreatment of starting material
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10Preparation or pretreatment of starting material
    • A61K2236/13Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10Preparation or pretreatment of starting material
    • A61K2236/15Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10Preparation or pretreatment of starting material
    • A61K2236/17Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting

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  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
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Abstract

The invention discloses a kind of place of production of genunie medicinal materials without sulphur processing method, belong to technical field of traditional Chinese medicines.The present invention by 1) clean bakee, 2) vexed profit section, 3) it is dry, 4) this four steps of packaging and storage realize that the place of production of Angelica sinensis is processed without sulphur.The processing method of the present invention can remove cleaning and bakee without removing clean impurity, evaporation section moisture, kill microorganism, prevent that the discoloration of Angelica sinensis product is spoiled, extend shelf life and the shelf-life of Angelica sinensis food, it is combined using temperature and humidity control and micro-wave vacuum, enhances the quality of Angelica sinensis and be effectively extracted the active ingredient of Angelica sinensis.Extract content 52.4%~54.7% in the present invention, moisture 9.9%~11.6%, 0.74~0.79%ml/g of volatile oil, forulic acid 0.079%~0.083%, SO23.1~3.4mg/kg of residual quantity.The content of each active ingredient is substantially better than the method for conventional machining Angelica sinensis, remarkable in economical benefits.

Description

A kind of place of production of genunie medicinal materials Angelica sinensis is without sulphur processing method
Technical field
The invention belongs to technical field of traditional Chinese medicines, it is related to the processing method of Angelica sinensis, and in particular to a kind of genunie medicinal materials Angelica sinensis The place of production is without sulphur processing method.
Background technology
Angelica sinensis, (scientific name:Angelica sinensis) alias it is dry return, the Qin which, western Angelica sinensis, Min Angelica sinensis, Radix Angelicae Sinensis, Angelica sinensis Body, culvert return tail, Angelica sinensis song, araliae cordatae, and perennial herb is 0.4-1 meters high.The month at florescence 6-7, the fruiting period 7-9 months.Chinese nineteen fifty-seven from Introduce a fine variety lovage in Europe.Main product the southeast of Gansu, more with Minxian County yield, quality is good, is secondly Yunnan, Sichuan, Shaanxi, Hubei etc. Save, be cultivation.Some domestic provinces and regions also introducing and planting.Its root can be used as medicine, and be one of most common Chinese medicine.With enriching blood and Blood, menstruction regulating and pain relieving, moisturize laxation, anticancer, anti-ageing the effect of preventing always, is immune.
Currently, the processing of Angelica sinensis is mainly using the methods of suning method, sulphur smoke-dried beancurd method, smoked a heatable brick bed method and micro-wave drying method pairs Angelica sinensis is processed.Wherein suning method is relatively slow, and sulphur smoke-dried beancurd method is easily destroyed the active ingredient of Angelica sinensis, enabling utilizes Angelica sinensis active ingredient it is less, can not meet demand of the people to Angelica sinensis high-quality, a heatable brick bed method and microwave drying are smoked in single use Method does not all reach the reserving degree of Angelica sinensis active ingredient.
Found through the literature search to the prior art, China Patent Publication No. CN103816193B, publication date in August, 2016 The patent application of 3 days discloses a kind of Angelica sinensis without sulphur processing method, and the invention is by cleaning, drying, shaping stacking, solar energy temperature Room is drying, sealing vanning, storage and etc. realize being processed without sulphur for Angelica sinensis.The invention realize Angelica sinensis without go mouldy, free from insect pests Phenomenon, but do not have a specific description for the quality of medicinal material of Angelica sinensis.
The content of the invention
It is an object of the invention to provide a kind of place of production of genunie medicinal materials Angelica sinensis without sulphur processing method, Angelica sinensis can be greatly improved The extraction of active ingredient, is ensured the raising of Angelica sinensis quality, prevents sulfur fumigation, be combined using temperature and humidity control with microwave drying Principle, lifts Angelica sinensis quality.
In order to achieve the above object, the present invention is achieved by the following scheme.
A kind of place of production of genunie medicinal materials Angelica sinensis includes the following steps without sulphur processing method:
1) cleaning bakees:Select fresh Angelica sinensis medicinal material to be placed in 45~65min of immersion, taking-up in preprepared solution A to dry in the air It is dry to seventy percent, then cleaned 2~3 times with high-pressure spray-type cleaning machine, to remove the impurity on Angelica sinensis surface;To at least Angelica sinensis medicinal material 60% be placed in the reaction vessel in heat-treating atmosphere, preheat 6~7min under conditions of being 40~50 DEG C in temperature, then will It is sent into step-by-step movement bakery and toasts, and dry-bulb temperature is risen to 36~38 DEG C by first stage, 2~3h, and wet-bulb temperature rises to 34 ~36 DEG C, until 25% Angelica sinensis its colour changed into yellow;Second stage, is heated up with the speed of 0.4 DEG C/h, dry-bulb temperature is risen to 38~39 DEG C, wet-bulb temperature rises to 36~37 DEG C, until 50% Angelica sinensis its colour changed into yellow;Phase III, dry-bulb temperature rise to 39 ~40 DEG C, wet-bulb temperature is constant, until 80% Angelica sinensis its colour changed into yellow;Fourth stage, keeps dry-bulb temperature and wet-bulb temperature not Become, after toasting 15~30min, the color of Angelica sinensis all turns yellow, and baking terminates;
2) vexed profit section:The Angelica sinensis medicinal material of cleaning baking step processing is taken to be placed in the matter of vexed profit in refined honey, Angelica sinensis and refined honey Amount is than being 11~12:1,1~3h of vexed profit, obtain vexed profit Radix Angelicae Sinensis Tabellae B;Vexed profit Radix Angelicae Sinensis Tabellae B is sent into block at a high speed in medicine cutter into Row section, is cut into the disk of 3~4mm, obtains Chinese angelica slicing C;It is leaching liquor that Chinese angelica slicing C, which is sent into containing volume ratio,:Yellow rice wine:Rice Vinegar is 9:1:2~4h of vexed profit in 2 container, obtains vexed profit Chinese angelica slicing;The leaching liquor soaks for hawthorn leaching liquor and inulin The volume ratio of the mixed liquor of extract, the hawthorn leaching liquor and inulin leaching liquor is 1:14~14:1;
3) it is dry:The Radix Angelicae Sinensis Tabellae of vexed profit slicing treatment is taken to be put into vacuum cold room, the initial temperature of refrigerating chamber is -4.5 DEG C~-3 DEG C, cool the temperature to -15 DEG C~-18 DEG C after refrigerating 3~4h;Radix Angelicae Sinensis Tabellae after freezing is warming up to 24 DEG C, is placed in roasting In room, 38 DEG C are warming up to 2.8 DEG C per hour of temperature, keeps the humidity in barn to be not less than 85%;Then Radix Angelicae Sinensis Tabellae is sent Enter and micro-wave vacuum is carried out in microwave vacuum dryer, microwave vacuum drying process is:3.4~3.8kPa of vacuum, microwave Power 54W, stops drying, drying time is 15~20min when Angelica sinensis medicinal material temperature is 42~44 DEG C in drying machine;Then will Temperature is down to 30~34 DEG C, and humidity is down to 22%~25%, and hold time 6h;
4) packaging and storage:Radix Angelicae Sinensis Tabellae through drying process is selected, foreign matter, rotten are picked out, then carried out Product packs, labelled, stamps lot number, vanning storage, ventilating and cooling place storage.
Further, the solution A in the cleaning baking step is pressed by haw thorn extract, inulin extract, distilled water According to mass ratio 11~15:11~15:70~90 proportional arrangement forms.
Compared with prior art, advantageous effects of the invention:
1) Angelica sinensis is toasted using segmented, helps largely to refine the active ingredient of Angelica sinensis, keep Angelica sinensis Color and luster is yellow or yellow-white, is cleaned after Angelica sinensis is soaked and then again, helps to remove the impurity in Angelica sinensis.
2) it is divided into the vexed profit of two parts to Angelica sinensis, vexed profit is to remove cleaning to bakee without clean impurity is removed for the first time, is evaporated Partial moisture, kills microorganism, while also allows for Chinese angelica slicing.Second vexed profit is then Angelica sinensis product electrochromic variable in order to prevent Taste, extends shelf life and the shelf-life of Angelica sinensis food.It is combined using temperature and humidity control and micro-wave vacuum, enhances Angelica sinensis Quality and the active ingredient for being effectively extracted Angelica sinensis.
3) extract content 52.4%~54.7% in the present invention, moisture 9.9%~11.6%, volatile oil 0.74~ 0.79%ml/g, forulic acid 0.079%~0.083%, SO23.1~3.4mg/kg of residual quantity.The content of each active ingredient is obvious Better than the method for conventional machining Angelica sinensis, remarkable in economical benefits.
Embodiment
Below by specific embodiment, technical scheme is further illustrated.It should be appreciated that this hair Bright embodiment is not limited to the following examples, and accommodation and/or change in any form made for the present invention all will Fall into protection scope of the present invention.
Embodiment 1
A kind of place of production of genunie medicinal materials Angelica sinensis includes the following steps without sulphur processing method:
1) cleaning bakees:Select fresh Angelica sinensis medicinal material to be placed in preprepared solution A and soak 45min, taking-up is dried in the air to seven Cheng Gan, is then cleaned 2 times with high-pressure spray-type cleaning machine, to remove the impurity on Angelica sinensis surface;By the 60% of at least Angelica sinensis medicinal material It is placed in the reaction vessel in heat-treating atmosphere, preheats 6min under conditions of being 40 DEG C in temperature, be then sent to step-by-step movement Toasted in bakery, the first stage, dry-bulb temperature is risen to 36 DEG C by 2h, and wet-bulb temperature rises to 34 DEG C, until 25% Angelica sinensis face Discoloration is yellow;Second stage, is heated up with the speed of 0.4 DEG C/h, and dry-bulb temperature is risen to 38 DEG C, and wet-bulb temperature rises to 36 DEG C, Until 50% Angelica sinensis its colour changed into yellow;Phase III, dry-bulb temperature rise to 39 DEG C, and wet-bulb temperature is constant, until 80% Angelica sinensis Its colour changed into yellow;Fourth stage, keeps dry-bulb temperature and wet-bulb temperature constant, and after toasting 15min, the color of Angelica sinensis all turns yellow, Baking terminates;Solution A in the cleaning baking step is by haw thorn extract, inulin extract, distilled water according to mass ratio 11:11:70 proportional arrangement forms.
2) vexed profit section:The Angelica sinensis medicinal material of cleaning baking step processing is taken to be placed in the matter of vexed profit in refined honey, Angelica sinensis and refined honey Amount is than being 11:1, vexed profit 1h, obtain vexed profit Radix Angelicae Sinensis Tabellae B;Vexed profit Radix Angelicae Sinensis Tabellae B is sent into block in medicine cutter at a high speed and is cut into slices, The disk of 3mm is cut into, obtains Chinese angelica slicing C;It is leaching liquor that Chinese angelica slicing C, which is sent into containing volume ratio,:Yellow rice wine:Rice vinegar is 9:1:2 Container in vexed profit 2h, obtain vexed profit Chinese angelica slicing;The leaching liquor is the mixed liquor of hawthorn leaching liquor and inulin leaching liquor, The volume ratio of the hawthorn leaching liquor and inulin leaching liquor is 1:14;
3) it is dry:The Radix Angelicae Sinensis Tabellae of vexed profit slicing treatment is taken to be put into vacuum cold room, the initial temperature of refrigerating chamber is -4.5 DEG C, cool the temperature to -15 DEG C after refrigerating 3h;Radix Angelicae Sinensis Tabellae after freezing is warming up to 24 DEG C, is placed in barn, with per hour 2.8 DEG C temperature be warming up to 38 DEG C, keep the humidity in barn to be not less than 85%;Then Radix Angelicae Sinensis Tabellae is sent into microwave vacuum dryer Middle carry out micro-wave vacuum, microwave vacuum drying process are:Vacuum 3.4kPa, microwave power 54W, when Angelica sinensis in drying machine Medicinal material temperature stops drying, drying time 15min when being 42 DEG C;30 DEG C are then cooled the temperature to, humidity is down to 22%, maintains Time 6h;
4) packaging and storage:Radix Angelicae Sinensis Tabellae through drying process is selected, foreign matter, rotten are picked out, then carried out Product packs, labelled, stamps lot number, vanning storage, ventilating and cooling place storage.
Embodiment 2
A kind of place of production of genunie medicinal materials Angelica sinensis includes the following steps without sulphur processing method:
1) cleaning bakees:Select fresh Angelica sinensis medicinal material to be placed in preprepared solution A and soak 55min, taking-up is dried in the air to seven Cheng Gan, is then cleaned 2 times with high-pressure spray-type cleaning machine, to remove the impurity on Angelica sinensis surface;By the 60% of at least Angelica sinensis medicinal material It is placed in the reaction vessel in heat-treating atmosphere, preheats 6min under conditions of being 45 DEG C in temperature, be then sent to step-by-step movement Toasted in bakery, the first stage, dry-bulb temperature is risen to 37 DEG C by 2h, and wet-bulb temperature rises to 35 DEG C, until 25% Angelica sinensis face Discoloration is yellow;Second stage, is heated up with the speed of 0.4 DEG C/h, and dry-bulb temperature is risen to 38 DEG C, and wet-bulb temperature rises to 36 DEG C, Until 50% Angelica sinensis its colour changed into yellow;Phase III, dry-bulb temperature rise to 39 DEG C, and wet-bulb temperature is constant, until 80% Angelica sinensis Its colour changed into yellow;Fourth stage, keeps dry-bulb temperature and wet-bulb temperature constant, and after toasting 26min, the color of Angelica sinensis all turns yellow, Baking terminates;Solution A in the cleaning baking step is by haw thorn extract, inulin extract, distilled water according to mass ratio 13:13:80 proportional arrangement forms.
2) vexed profit section:The Angelica sinensis medicinal material of cleaning baking step processing is taken to be placed in the matter of vexed profit in refined honey, Angelica sinensis and refined honey Amount is than being 12:1, vexed profit 2h, obtain vexed profit Radix Angelicae Sinensis Tabellae B;Vexed profit Radix Angelicae Sinensis Tabellae B is sent into block in medicine cutter at a high speed and is cut into slices, The disk of 3mm is cut into, obtains Chinese angelica slicing C;It is leaching liquor that Chinese angelica slicing C, which is sent into containing volume ratio,:Yellow rice wine:Rice vinegar is 9:1:2 Container in vexed profit 3h, obtain vexed profit Chinese angelica slicing;The leaching liquor is the mixed liquor of hawthorn leaching liquor and inulin leaching liquor, The volume ratio of the hawthorn leaching liquor and inulin leaching liquor is 11.5:1;
3) it is dry:The Radix Angelicae Sinensis Tabellae of vexed profit slicing treatment is taken to be put into vacuum cold room, the initial temperature of refrigerating chamber is -3.5 DEG C, cool the temperature to -16 DEG C after refrigerating 3~4h;Radix Angelicae Sinensis Tabellae after freezing is warming up to 24 DEG C, is placed in barn, with per hour 2.8 DEG C of temperature is warming up to 38 DEG C, keeps the humidity in barn to be not less than 85%;Then Radix Angelicae Sinensis Tabellae is sent into micro-wave vacuum Micro-wave vacuum is carried out in machine, microwave vacuum drying process is:Vacuum 3.6kPa, microwave power 54W, when working as in drying machine Return medicinal material temperature be 43 DEG C when stop drying, drying time 17min;32 DEG C are then cooled the temperature to, humidity is down to 23%, dimension Hold time 6h;
4) packaging and storage:Radix Angelicae Sinensis Tabellae through drying process is selected, foreign matter, rotten are picked out, then carried out Product packs, labelled, stamps lot number, vanning storage, ventilating and cooling place storage.
Embodiment 3
A kind of place of production of genunie medicinal materials Angelica sinensis includes the following steps without sulphur processing method:
1) cleaning bakees:Select fresh Angelica sinensis medicinal material to be placed in preprepared solution A and soak 65min, taking-up is dried in the air to seven Cheng Gan, is then cleaned 3 times with high-pressure spray-type cleaning machine, to remove the impurity on Angelica sinensis surface;By the 60% of at least Angelica sinensis medicinal material It is placed in the reaction vessel in heat-treating atmosphere, preheats 7min under conditions of being 50 DEG C in temperature, be then sent to step-by-step movement Toasted in bakery, the first stage, dry-bulb temperature is risen to 38 DEG C by 3h, and wet-bulb temperature rises to 36 DEG C, until 25% Angelica sinensis face Discoloration is yellow;Second stage, is heated up with the speed of 0.4 DEG C/h, and dry-bulb temperature is risen to 39 DEG C, and wet-bulb temperature rises to 37 DEG C, Until 50% Angelica sinensis its colour changed into yellow;Phase III, dry-bulb temperature rise to 40 DEG C, and wet-bulb temperature is constant, until 80% Angelica sinensis Its colour changed into yellow;Fourth stage, keeps dry-bulb temperature and wet-bulb temperature constant, and after toasting 30min, the color of Angelica sinensis all turns yellow, Baking terminates;Solution A in the cleaning baking step is by haw thorn extract, inulin extract, distilled water according to mass ratio 15:15:90 proportional arrangement forms.
2) vexed profit section:The Angelica sinensis medicinal material of cleaning baking step processing is taken to be placed in the matter of vexed profit in refined honey, Angelica sinensis and refined honey Amount is than being 12:1, vexed profit 3h, obtain vexed profit Radix Angelicae Sinensis Tabellae B;Vexed profit Radix Angelicae Sinensis Tabellae B is sent into block in medicine cutter at a high speed and is cut into slices, The disk of 4mm is cut into, obtains Chinese angelica slicing C;It is leaching liquor that Chinese angelica slicing C, which is sent into containing volume ratio,:Yellow rice wine:Rice vinegar is 9:1:2 Container in vexed profit 4h, obtain vexed profit Chinese angelica slicing;The leaching liquor is the mixed liquor of hawthorn leaching liquor and inulin leaching liquor, The volume ratio of the hawthorn leaching liquor and inulin leaching liquor is 14:1;
3) it is dry:The Radix Angelicae Sinensis Tabellae of vexed profit slicing treatment is taken to be put into vacuum cold room, the initial temperature of refrigerating chamber is -3 DEG C, - 18 DEG C are cooled the temperature to after 3~4h of refrigeration;Radix Angelicae Sinensis Tabellae after freezing is warming up to 24 DEG C, is placed in barn, with per hour 2.8 DEG C temperature be warming up to 38 DEG C, keep the humidity in barn to be not less than 85%;Then Radix Angelicae Sinensis Tabellae is sent into microwave vacuum dryer Middle carry out micro-wave vacuum, microwave vacuum drying process are:Vacuum 3.8kPa, microwave power 54W, when Angelica sinensis in drying machine Medicinal material temperature stops drying, drying time 20min when being 44 DEG C;34 DEG C are then cooled the temperature to, humidity is down to 25%, maintains Time 6h;
4) packaging and storage:Radix Angelicae Sinensis Tabellae through drying process is selected, foreign matter, rotten are picked out, then carried out Product packs, labelled, stamps lot number, vanning storage, ventilating and cooling place storage.
In order to further illustrate a kind of genunie medicinal materials Angelica sinensis place of production of the present invention without sulphur processing effect, above-described embodiment is being carried out When, while set and tried check experiment, it is specific as follows:
Control experiment example 1
Angelica sinensis and the vexed profit after refined honey processing are only carried out in step 2), other steps are the same as embodiment 1.
Control experiment example 2
Handled in step 3) using the method for sulfur fumigation, other steps are the same as embodiment 1.
For above-described embodiment and control experiment example, the genunie medicinal materials Angelica sinensis place of production of the invention is without sulphur processing effect such as following table It is shown:
As seen from the above table, using sulfur fumigation can havoc medicinal material greatly quality, method using the present invention handles Angelica sinensis Each active ingredient can maximumlly extract.Extract content 52.4%~54.7% in the present invention, moisture 9.9%~ 11.6%, 0.74~0.79%ml/g of volatile oil, forulic acid 0.079%~0.083%, SO23.1~3.4mg/kg of residual quantity.
The present invention can be summarized with others without prejudice to the concrete form of the spirit or essential characteristics of the present invention.No matter from which From the point of view of a bit, the embodiment above of the invention can only all be considered the description of the invention and cannot limit the present invention, right Claim indicates the scope of the present invention, therefore, any in the implication and scope suitable with claims of the present invention Change, be all considered as being included within Claims scope.

Claims (2)

1. a kind of place of production of genunie medicinal materials Angelica sinensis is without sulphur processing method, including cleaning bakees, vexed profit section, drying and packaging and storage Four steps, it is characterised in that:
The cleaning baking step:Select fresh Angelica sinensis medicinal material to be placed in 45~65min of immersion in preprepared solution A, take out Dry in the air to seventy percent dry, then cleaned 2~3 times with high-pressure spray-type cleaning machine, to remove the impurity on Angelica sinensis surface;To at least Angelica sinensis medicine The 60% of material is placed in the reaction vessel in heat-treating atmosphere, preheats 6~7min under conditions of being 40~50 DEG C in temperature, then It is sent in step-by-step movement bakery and toasts, dry-bulb temperature is risen to 36~38 DEG C by first stage, 2~3h, and wet-bulb temperature rises to 34~36 DEG C, until 25% Angelica sinensis its colour changed into yellow;Second stage, is heated up with the speed of 0.4 DEG C/h, by dry-bulb temperature liter To 38~39 DEG C, wet-bulb temperature rises to 36~37 DEG C, until 50% Angelica sinensis its colour changed into yellow;Phase III, dry-bulb temperature rise to 39~40 DEG C, wet-bulb temperature is constant, until 80% Angelica sinensis its colour changed into yellow;Fourth stage, keeps dry-bulb temperature and wet-bulb temperature Constant, after toasting 15~30min, the color of Angelica sinensis all turns yellow, and baking terminates;
The vexed profit slicing step:The Angelica sinensis medicinal material of cleaning baking step processing is taken to be placed in vexed profit in refined honey, Angelica sinensis and refined honey Mass ratio is 11~12:1,1~3h of vexed profit, obtain vexed profit Radix Angelicae Sinensis Tabellae B;Vexed profit Radix Angelicae Sinensis Tabellae B is sent into and is blocked in medicine cutter at a high speed Cut into slices, be cut into the disk of 3~4mm, obtain Chinese angelica slicing C;It is leaching liquor that Chinese angelica slicing C, which is sent into containing volume ratio,:Yellow rice wine: Rice vinegar is 9:1:2~4h of vexed profit in 2 container, obtains vexed profit Chinese angelica slicing;The leaching liquor is hawthorn leaching liquor and inulin The volume ratio of the mixed liquor of leaching liquor, the hawthorn leaching liquor and inulin leaching liquor is 1:14~14:1;
The drying steps:Take the Radix Angelicae Sinensis Tabellae of vexed profit slicing treatment to be put into vacuum cold room, the initial temperature of refrigerating chamber for- 4.5 DEG C~-3 DEG C, -15 DEG C~-18 DEG C are cooled the temperature to after refrigerating 3~4h;Radix Angelicae Sinensis Tabellae after freezing is warming up to 24 DEG C, is placed in In barn, 38 DEG C are warming up to 2.8 DEG C per hour of temperature, keeps the humidity in barn to be not less than 85%;Then by Radix Angelicae Sinensis Tabellae It is sent into microwave vacuum dryer and carries out micro-wave vacuum, microwave vacuum drying process is:Vacuum 3.4~3.8kPa, it is micro- Wave power 54W, stops drying, drying time is 15~20min when Angelica sinensis medicinal material temperature is 42~44 DEG C in drying machine;Then 30~34 DEG C are cooled the temperature to, humidity is down to 22%~25%, and hold time 6h.
2. a kind of place of production of genunie medicinal materials according to claim 1 is without sulphur processing method, it is characterised in that the cleaning Solution A in baking step is by haw thorn extract, inulin extract, distilled water according to mass ratio 11~15:11~15:70~90 Proportional arrangement form.
CN201711177782.6A 2017-11-23 2017-11-23 A kind of place of production of genunie medicinal materials Angelica sinensis is without sulphur processing method Pending CN107982293A (en)

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* Cited by examiner, † Cited by third party
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CN112587570A (en) * 2020-12-23 2021-04-02 河南省中医院(河南中医药大学第二附属医院) Pretreatment method of radix puerariae, radix scutellariae and rhizoma coptidis composition medicinal materials

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105616466A (en) * 2016-01-12 2016-06-01 昆明中农贸易有限公司 Preparation method of freeze-dried angelica
CN106945868A (en) * 2017-04-06 2017-07-14 成都众宜坊农业开发有限公司 The Habitat producing and packing method of a kind of Radix Angelicae Sinensis
CN107296819A (en) * 2017-06-20 2017-10-27 王逸帆 A kind of processing method for improving Chinese angelica volatile oil content

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105616466A (en) * 2016-01-12 2016-06-01 昆明中农贸易有限公司 Preparation method of freeze-dried angelica
CN106945868A (en) * 2017-04-06 2017-07-14 成都众宜坊农业开发有限公司 The Habitat producing and packing method of a kind of Radix Angelicae Sinensis
CN107296819A (en) * 2017-06-20 2017-10-27 王逸帆 A kind of processing method for improving Chinese angelica volatile oil content

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112587570A (en) * 2020-12-23 2021-04-02 河南省中医院(河南中医药大学第二附属医院) Pretreatment method of radix puerariae, radix scutellariae and rhizoma coptidis composition medicinal materials

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Application publication date: 20180504