CN107973288A - 一种氮掺杂碳纳米角的制备方法 - Google Patents
一种氮掺杂碳纳米角的制备方法 Download PDFInfo
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- CN107973288A CN107973288A CN201711373983.3A CN201711373983A CN107973288A CN 107973288 A CN107973288 A CN 107973288A CN 201711373983 A CN201711373983 A CN 201711373983A CN 107973288 A CN107973288 A CN 107973288A
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- carbon nanohorn
- doping
- doping carbon
- electric arc
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 128
- 229910052799 carbon Inorganic materials 0.000 title claims abstract description 95
- 239000002116 nanohorn Substances 0.000 title claims abstract description 78
- 238000002360 preparation method Methods 0.000 title description 6
- 238000010891 electric arc Methods 0.000 claims abstract description 48
- 229910002804 graphite Inorganic materials 0.000 claims abstract description 28
- 239000010439 graphite Substances 0.000 claims abstract description 28
- 238000000034 method Methods 0.000 claims abstract description 25
- 238000006243 chemical reaction Methods 0.000 claims abstract description 14
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 44
- 229910052757 nitrogen Inorganic materials 0.000 claims description 22
- 239000007789 gas Substances 0.000 claims description 11
- 238000002156 mixing Methods 0.000 claims description 2
- 238000004833 X-ray photoelectron spectroscopy Methods 0.000 abstract description 12
- 239000002086 nanomaterial Substances 0.000 abstract description 9
- 239000002245 particle Substances 0.000 abstract description 5
- 230000005540 biological transmission Effects 0.000 abstract description 3
- 230000008569 process Effects 0.000 abstract description 3
- 230000008901 benefit Effects 0.000 abstract description 2
- 239000003575 carbonaceous material Substances 0.000 description 8
- 125000004433 nitrogen atom Chemical group N* 0.000 description 7
- 239000000126 substance Substances 0.000 description 6
- 239000002041 carbon nanotube Substances 0.000 description 5
- 229910021393 carbon nanotube Inorganic materials 0.000 description 5
- 241000132500 Dahlia <angiosperm> Species 0.000 description 4
- 235000012040 Dahlia pinnata Nutrition 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000003054 catalyst Substances 0.000 description 3
- 238000004627 transmission electron microscopy Methods 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 238000001069 Raman spectroscopy Methods 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 238000004220 aggregation Methods 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- 125000004429 atom Chemical group 0.000 description 2
- DLGYNVMUCSTYDQ-UHFFFAOYSA-N azane;pyridine Chemical compound N.C1=CC=NC=C1 DLGYNVMUCSTYDQ-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 150000001721 carbon Chemical group 0.000 description 2
- 125000000524 functional group Chemical group 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 229910021645 metal ion Inorganic materials 0.000 description 2
- 239000012779 reinforcing material Substances 0.000 description 2
- 238000002336 sorption--desorption measurement Methods 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- -1 therefore Chemical group 0.000 description 2
- XMWRBQBLMFGWIX-UHFFFAOYSA-N C60 fullerene Chemical compound C12=C3C(C4=C56)=C7C8=C5C5=C9C%10=C6C6=C4C1=C1C4=C6C6=C%10C%10=C9C9=C%11C5=C8C5=C8C7=C3C3=C7C2=C1C1=C2C4=C6C4=C%10C6=C9C9=C%11C5=C5C8=C3C3=C7C1=C1C2=C4C6=C2C9=C5C3=C12 XMWRBQBLMFGWIX-UHFFFAOYSA-N 0.000 description 1
- 239000002879 Lewis base Substances 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- WDTXDIAHMFGTJS-UHFFFAOYSA-N [N].O=N Chemical compound [N].O=N WDTXDIAHMFGTJS-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000002019 doping agent Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 229910003472 fullerene Inorganic materials 0.000 description 1
- 229910021389 graphene Inorganic materials 0.000 description 1
- 238000005087 graphitization Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 150000007527 lewis bases Chemical class 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 230000000802 nitrating effect Effects 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 150000003233 pyrroles Chemical class 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 239000002109 single walled nanotube Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/01—Crystal-structural characteristics depicted by a TEM-image
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
- C01P2002/82—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by IR- or Raman-data
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
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- Carbon And Carbon Compounds (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
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CN201711373983.3A CN107973288B (zh) | 2017-12-19 | 2017-12-19 | 一种氮掺杂碳纳米角的制备方法 |
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CN201711373983.3A CN107973288B (zh) | 2017-12-19 | 2017-12-19 | 一种氮掺杂碳纳米角的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN107973288A true CN107973288A (zh) | 2018-05-01 |
CN107973288B CN107973288B (zh) | 2021-03-02 |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109019564A (zh) * | 2018-09-30 | 2018-12-18 | 王浩兰 | 一种碳纳米材料的后处理方法 |
CN109095455A (zh) * | 2018-09-30 | 2018-12-28 | 王浩兰 | 一种碳纳米材料的制备方法 |
CN109970047A (zh) * | 2019-03-27 | 2019-07-05 | 昆明理工大学 | 一种由碳纳米角制备石墨烯量子点的方法 |
CN110459778A (zh) * | 2019-07-23 | 2019-11-15 | 中国科学院福建物质结构研究所 | 一种新型纳米碳催化剂材料及其制备方法和应用 |
CN112591737A (zh) * | 2020-12-16 | 2021-04-02 | 昆明理工大学 | 一种回收废旧锂离子电池负极石墨制备碳纳米角的方法 |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101759179A (zh) * | 2010-01-22 | 2010-06-30 | 北京大学 | 一种碳纳米角的制备方法 |
CN104118870B (zh) * | 2014-07-09 | 2017-05-31 | 北京大学 | 一种氮掺杂石墨烯的制备方法及氮掺杂石墨烯 |
CN104609390A (zh) * | 2015-01-20 | 2015-05-13 | 北京清大际光科技发展有限公司 | 一种电弧法制备碳纳米角的方法 |
-
2017
- 2017-12-19 CN CN201711373983.3A patent/CN107973288B/zh active Active
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109019564A (zh) * | 2018-09-30 | 2018-12-18 | 王浩兰 | 一种碳纳米材料的后处理方法 |
CN109095455A (zh) * | 2018-09-30 | 2018-12-28 | 王浩兰 | 一种碳纳米材料的制备方法 |
CN109970047A (zh) * | 2019-03-27 | 2019-07-05 | 昆明理工大学 | 一种由碳纳米角制备石墨烯量子点的方法 |
CN110459778A (zh) * | 2019-07-23 | 2019-11-15 | 中国科学院福建物质结构研究所 | 一种新型纳米碳催化剂材料及其制备方法和应用 |
CN112591737A (zh) * | 2020-12-16 | 2021-04-02 | 昆明理工大学 | 一种回收废旧锂离子电池负极石墨制备碳纳米角的方法 |
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Effective date of registration: 20211105 Address after: 200135 room 2207a, No. 28, Maji Road, China (Shanghai) pilot Free Trade Zone, 2001 Century Avenue, Pudong New Area, Shanghai Patentee after: Shanghai Chuchun Industrial Co.,Ltd. Address before: 650093 No. 253, Xuefu Road, Wuhua District, Yunnan, Kunming Patentee before: Kunming University of Science and Technology |
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Effective date of registration: 20220908 Address after: Plant No. 1, Pilot Base Park, north side of Huancheng Road, west side of Taishan Road, Pizhou Economic Development Zone, Xuzhou City, Jiangsu Province, 221300 Patentee after: Jiangsu Fengchi carbon based New Materials Research Institute Co.,Ltd. Address before: 200135 room 2207a, No. 28, Maji Road, China (Shanghai) pilot Free Trade Zone, 2001 Century Avenue, Pudong New Area, Shanghai Patentee before: Shanghai Chuchun Industrial Co.,Ltd. |