CN107970874A - A kind of magnetic agitation Hydrothermal Synthesiss device - Google Patents
A kind of magnetic agitation Hydrothermal Synthesiss device Download PDFInfo
- Publication number
- CN107970874A CN107970874A CN201711456716.2A CN201711456716A CN107970874A CN 107970874 A CN107970874 A CN 107970874A CN 201711456716 A CN201711456716 A CN 201711456716A CN 107970874 A CN107970874 A CN 107970874A
- Authority
- CN
- China
- Prior art keywords
- lid
- autoclave body
- hydrothermal synthesiss
- magnetic agitation
- reaction kettle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000001027 hydrothermal synthesis Methods 0.000 title claims abstract description 43
- 238000013019 agitation Methods 0.000 title claims abstract description 19
- 238000006243 chemical reaction Methods 0.000 claims abstract description 49
- 238000003760 magnetic stirring Methods 0.000 claims abstract description 16
- 238000003756 stirring Methods 0.000 abstract description 17
- 230000009471 action Effects 0.000 abstract description 3
- 238000011160 research Methods 0.000 description 6
- 239000000463 material Substances 0.000 description 5
- 239000000843 powder Substances 0.000 description 5
- 230000015572 biosynthetic process Effects 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 238000003786 synthesis reaction Methods 0.000 description 4
- 238000010586 diagram Methods 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 230000004044 response Effects 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 229910001385 heavy metal Inorganic materials 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000002203 pretreatment Methods 0.000 description 2
- 239000011573 trace mineral Substances 0.000 description 2
- 235000013619 trace mineral Nutrition 0.000 description 2
- 229910002971 CaTiO3 Inorganic materials 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 229910002370 SrTiO3 Inorganic materials 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000000862 absorption spectrum Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 229910002113 barium titanate Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 229910052793 cadmium Inorganic materials 0.000 description 1
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 238000012512 characterization method Methods 0.000 description 1
- 238000009614 chemical analysis method Methods 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 230000002860 competitive effect Effects 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000009854 hydrometallurgy Methods 0.000 description 1
- 238000004933 hydrothermal crystal growth Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000010423 industrial mineral Substances 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 238000001819 mass spectrum Methods 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 229910052761 rare earth metal Inorganic materials 0.000 description 1
- 150000002910 rare earth metals Chemical class 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The present invention provides a kind of magnetic agitation Hydrothermal Synthesiss device, belongs to Hydrothermal Synthesiss device field, including magnetic stirring apparatus, heater and reaction kettle, temperature sensor, pressure sensor, controller；The magnetic stirring apparatus has work top, and the reaction kettle is positioned on the work top；The reaction kettle has autoclave body and lid, and the lid is placed on above autoclave body；The heater is loop configuration, and the heaters set is arranged on the outside of the autoclave body.Stirring magneton is put into reaction kettle with magnetic stirring apparatus, by magnetic stirring apparatus, stirring magneton can be driven to be rotated in reaction kettle, stirring action is played to mixed liquor by it.By this Hydrothermal Synthesiss device, it can be sufficiently mixed mixed liquor in reaction kettle, obtain the mixed liquor being more uniformly distributed.
Description
Technical field
The present invention relates to Hydrothermal Synthesiss device field, in particular to a kind of magnetic agitation Hydrothermal Synthesiss device.
Background technology
The initial main purpose of hydro-thermal method is synthetic water Thermal origin mineral, explores their formation conditions in nature, is water
The industrial mineral of thermal synthesis and crystal are laid a good foundation.Nineteen sixties, hydrothermal synthesis method are used to complex functionality pottery
The various knot product powder such as BaTiO of ceramic material3, CaTiO3, SrTiO3Deng.The eighties Japan presses with hydro-thermal method synthesis PZT
It is successful in terms of electric body knot product powder.In recent years, with hydro-thermal method synthetic inorganic material, grinding for various ultra-fine knot product powder is prepared
Study carefully and apply, the concern of many people is also result in China, is permitted in terms of hydro-thermal research where Chinese Academy of Sciences's emtallurgy research
More research work.Chemistry Dept. of Jilin Univ. establishes research department, the hydro-thermal of inorganic microporous product body material is closed from imported from America equipment
Into having obtained encouraging progress.Xibei College of Light Industry's inorganic non-metallic material and engineering department, make Hydrothermal Synthesiss equipment by oneself, establish
Corresponding research institution, achieved in terms of the synthesis of the knot product powder of PZT pyroelectrics, piezoelectrics crystalline powder and BaTiO3 compared with
Big progress.These illustrate that hydrothermal synthesis method has become a kind of tool of current manufacture high-performance high reliability ceramic material
Competitive method.This method also has in numerous areas such as the manufacture of water product, hydrometallurgy, environmental protection, lique factions of coal
Wide prospect.
Hydrothermal synthesis reaction kettle is the common small sized reactor of chemical laboratory, and the medium available for same composition is in different bars
Response situation under part is tested or tested for the medium response situation under the same conditions of different component.This production
Product make heating constant-temperature equipment using electric drying oven with forced convection, and agitating shaft in babinet is driven and installed in stirring by motor reducer
The microreactor mixed on axis rotates, and achievees the purpose that stirring reaction.
Hydrothermal synthesis reaction kettle is a kind of closed container that can decompose indissoluble material.Available for atomic absorption spectrum and wait from
Molten sample pretreatment in the analyses such as son transmitting；It can also be used for the synthetic reaction of low dose；Also using strong acid in tank body or highly basic
And high temperature high pressure enclosed environment achievees the purpose that rapid-digestion indissoluble material.Gas phase, liquid phase, plasma spectrum mass spectrum,
Sample pre-treatments are done in the chemical analysis method such as Atomic absorption and atomic fluorescence.Cleared up when being measure trace element and trace element
The competent assistant of sample.
Hydrothermal synthesis reaction kettle can be applied in the determining heavy metals such as lead, copper, cadmium, zinc, calcium, manganese, iron, mercury, be alternatively arranged as
A kind of high-purity reaction vessel of high-temperature-resistant high-pressure-resistant anti-corrosion, and organic synthesis, Hydrothermal Synthesiss, crystal growth or Specimen eliminating extraction
Take etc..Residual heavy metal, agriculture, food, mud, rare earth, aquatic products, organic matter etc. are cleared up in sample pre-treatments.Therefore, in stone
The research and life of the departments such as oiling work, biomedicine, material science, geologic chemistry, environmental science, Food Science, commodity inspection
It is widely used in production.
In the prior art, traditional hydrothermal synthesis reaction kettle structure design is more unreasonable, it is impossible to effectively to reaction
Mixed liquor is stirred in kettle.
The content of the invention
The present invention provides a kind of magnetic agitation Hydrothermal Synthesiss device, it is intended to solves existing for Hydrothermal Synthesiss device in the prior art
The above problem.
What the embodiment of the present invention was realized in：
A kind of magnetic agitation Hydrothermal Synthesiss device, including magnetic stirring apparatus, heater and reaction kettle；The magnetic agitation utensil
There is work top, the reaction kettle is positioned on the work top；The reaction kettle has autoclave body and lid, the cover cap
Above autoclave body；The heater is loop configuration, and the heaters set is arranged on the outside of the autoclave body.
Further, in the preferred embodiment of the invention, the autoclave body has columned inner cavity, and the lid bottom connects
Agitating shaft is connected to, the agitating shaft stretches into the autoclave body, and the agitating shaft deviates the axis of the inner cavity.
Further, in the preferred embodiment of the invention, the top of the autoclave body has a connected unit, the connected unit it is straight
Footpath is more than the diameter of autoclave body, and the heater is arranged at the lower section of connected unit.
Further, in the preferred embodiment of the invention, circumferentially arranged more screw rods, the screw rod in the connected unit
Axis parallel to autoclave body axis；Multiple connecting holes are provided with the lid, the screw rod passes through the connecting hole.
Further, in the preferred embodiment of the invention, the lid is disc structure, and the sidepiece of lid is symmetrically arranged with
Two holding rods, the holding rod are set along the radial direction of lid.
Further, in the preferred embodiment of the invention, the bottom of the lid is provided with blind hole, the lid from bottom to top
The sidepiece of body is provided with pressure reducing valve, and the pressure reducing valve connects the blind hole.
Further, in the preferred embodiment of the invention, pressure gauge is provided with the top of the lid, the pressure gauge connects
Lead to the blind hole.
Further, in the preferred embodiment of the invention, the pressure gauge has one, and the pressure reducing valve is provided with two,
The blind hole is provided with three；The pressure gauge connects one of blind hole, and two pressure reducing valves connect another two blind hole.
Further, in the preferred embodiment of the invention, the bottom of the autoclave body is provided with mounting base, the mounting base bag
Base and footstock are included, through hole is both provided with the middle part of the base and footstock；The top of the base has the connecting seat of annular,
The footstock bottom has mounting hole, and the connecting seat penetrates the mounting hole, enables footstock with respect to base rotation；It is described to add
Hot device is positioned on the footstock.
Further, in the preferred embodiment of the invention, the connecting seat and mounting hole are connected by bearing, the installation
The top in hole has boss, and the internal diameter of boss is adapted with the outside diameter of autoclave body.
The beneficial effects of the invention are as follows：The Hydrothermal Synthesiss device that the present invention is obtained by above-mentioned design, it is with magnetic agitation
Device, stirring magneton is lost in reaction kettle, by magnetic stirring apparatus, stirring magneton can be driven to be rotated in reaction kettle, to mixed
Close liquid and play stirring action.It by this Hydrothermal Synthesiss device, can be sufficiently mixed mixed liquor in reaction kettle, obtain more equal
Even mixed liquor.
Brief description of the drawings
, below will be to required use in embodiment in order to illustrate more clearly of the technical solution of embodiment of the present invention
Attached drawing be briefly described, it will be appreciated that the following drawings illustrate only certain embodiments of the present invention, therefore be not to be seen as
It is the restriction to scope, for those of ordinary skill in the art, without creative efforts, can be with root
Other relevant attached drawings are obtained according to these attached drawings.
Fig. 1 is the structure diagram for the Hydrothermal Synthesiss device that embodiment of the present invention provides；
Fig. 2 is the structure diagram of reaction kettle in the Hydrothermal Synthesiss device that embodiment of the present invention provides；
Fig. 3 is the elevational schematic view of reaction kettle lid in the Hydrothermal Synthesiss device that embodiment of the present invention provides；
Fig. 4 is the structure diagram of mounting base in the Hydrothermal Synthesiss device that embodiment of the present invention provides.
Icon：Magnetic stirring apparatus 110, heater 120, reaction kettle 130, autoclave body 131, lid 132, agitating shaft 133, connection
Platform 134, screw rod 135, holding rod 136, nut 137, blind hole 138, pressure reducing valve 139, pressure gauge 140, mounting base 150, base 151,
Footstock 152, connecting seat 153, boss 154.
Embodiment
To make the purpose, technical scheme and advantage of embodiment of the present invention clearer, implement below in conjunction with the present invention
Attached drawing in mode, is clearly and completely described the technical solution in embodiment of the present invention, it is clear that described reality
The mode of applying is a part of embodiment of the present invention, rather than whole embodiments.Based on the embodiment in the present invention, ability
The every other embodiment that domain those of ordinary skill is obtained without creative efforts, belongs to the present invention
The scope of protection.Therefore, below the detailed description of the embodiments of the present invention to providing in the accompanying drawings be not intended to limit will
The scope of the present invention of protection is sought, but is merely representative of the selected embodiment of the present invention.
In the description of the present invention, it is to be understood that the term of indicating position or position relationship is based on shown in attached drawing
Orientation or position relationship, be for only for ease of the description present invention and simplify description, rather than instruction or imply signified element
There must be specific orientation, with specific azimuth configuration and operation, therefore be not considered as limiting the invention.
In the present invention, unless otherwise clearly defined and limited, term " installation ", " connected ", " connection ", " fixation " etc.
Term should be interpreted broadly, for example, it may be fixedly connected or be detachably connected, or integrally；Can be that machinery connects
Connect or be electrically connected；It can be directly connected, can also be indirectly connected by intermediary, can be in two elements
The connection in portion or the interaction relationship of two elements.For the ordinary skill in the art, can be according to specific feelings
Condition understands the concrete meaning of above-mentioned term in the present invention.
In the present invention, unless otherwise clearly defined and limited, fisrt feature can be with or below second feature
Directly contacted including the first and second features, can also include the first and second features not be direct contact but by them it
Between other characterisation contact.Moreover, fisrt feature is on second feature, top and above to include fisrt feature special second
Directly over sign and oblique upper, or be merely representative of fisrt feature level height and be higher than second feature.Fisrt feature second feature it
Under, lower section and fisrt feature included below are immediately below second feature and obliquely downward, or be merely representative of fisrt feature level height
Less than second feature.
Embodiment.
Present embodiments provide a kind of magnetic agitation Hydrothermal Synthesiss device.It loses stirring magneton with magnetic stirring apparatus 110
Enter in reaction kettle 130, by magnetic stirring apparatus 110, stirring magneton can be driven to be rotated in reaction kettle 130, mixed liquor is risen
To stirring action.By this Hydrothermal Synthesiss device, it can be sufficiently mixed mixed liquor in reaction kettle 130, be more uniformly distributed
Mixed liquor.
Referring to Fig. 1, this Hydrothermal Synthesiss device includes magnetic stirring apparatus 110, heater 120 and reaction kettle 130；Magnetic force stirs
Mixing device 110 has work top, and reaction kettle 130 is positioned on work top；Reaction kettle 130 has autoclave body 131 and lid 132,
Lid 132 is placed on the top of autoclave body 131；Heater 120 is loop configuration, and heater 120 is sheathed on the outside of autoclave body 131.
Autoclave body 131 has columned inner cavity, and 132 bottom of lid is connected with agitating shaft 133, and agitating shaft 133 stretches into autoclave body
131, and agitating shaft 133 deviates the axis of inner cavity.
As shown in Fig. 2, the top of autoclave body 131 has connected unit 134, the diameter of connected unit 134 is more than the straight of autoclave body 131
Footpath, heater 120 are arranged at the lower section of connected unit 134.Circumferentially arranged more screw rods 135 in connected unit 134, screw rod 135
Axis of the axis parallel to autoclave body 131；Multiple connecting holes are provided with lid 132, screw rod 135 passes through connecting hole, and in screw rod
135 end coupling nut 137, is fixed lid 132 and autoclave body 131 by nut 137.
As shown in figure 3, lid 132 is disc structure, the sidepiece of lid 132 is symmetrically arranged with two holding rods 136, holding rod
136 are set along the radial direction of lid 132.The bottom of lid 132 is provided with blind hole 138 from bottom to top, and the sidepiece of lid 132 is provided with
Pressure reducing valve 139, pressure reducing valve 139 connect blind hole 138.The top of lid 132 is provided with pressure gauge 140, and pressure gauge 140 connects blind hole
138.Pressure gauge 140 has one, and pressure reducing valve 139 is provided with two, and blind hole 138 is provided with three；Pressure gauge 140 connects wherein one
A blind hole 138, two pressure reducing valves 139 also connect a blind hole 138 respectively.
Magnetic stirring apparatus 110 is the Laboratory Instruments for liquid mixing, is mainly used for stirring or heating stirring is low at the same time
The liquid or solidliquid mixture of viscosity.Its basic principle is to utilize the magnetic field principle that identical charges repel each other, there is a natural attraction between the sexes, uses magnetic
Field, which promotes, places magnetic stirrer progress circumferential running in a reservoir, so as to achieve the purpose that agitated liquid.
Work top is a part for magnetic stirring apparatus 110, and reaction kettle 130 is placed on work top, at work,
Stirring magneton is lost in reaction kettle 130, by magnetic stirring apparatus 110 stirring magneton can be driven to be rotated in reaction kettle 130,
Play the role of mixed liquor in stirred autoclave 130.
Reaction kettle 130 is arranged to, with lid 132 and autoclave body 131, mixed liquor is added in reaction kettle 130.
Heater 120 is arranged to loop configuration, and is set in the outside of autoclave body 131 so that heater 120 can be from reaction kettle
130 sidepiece heats reaction kettle 130, is heated mixed liquor in reaction kettle 130, plays the role of accelerating reaction, reaches
To the suitable temperature of experiment.
Agitating shaft 133 is set in 132 bottom of lid, agitating shaft 133 is stretched into autoclave body 131, when mixed liquor is being stirred magnetic
During subband turn is moved, due to the presence of agitating shaft 133, make to produce relative rotation between agitating shaft 133 and mixed liquor, make
The agitating shaft 133 for obtaining strip plays the role of futher stirring to mixed liquor, and further mixed liquor is mixed, and obtains more
Good mixed effect.
The top of autoclave body 131 sets connected unit 134, autoclave body 131 is easily connected with lid 132, simultaneously because even
Connecing platform 134 has larger size, and heater 120 can be kept out from top, heater 120 is kept out below connected unit 134,
Heater 120 is set stably to be connected on autoclave body 131.
By screw rod 135, nut 137, stably autoclave body 131 and lid 132 can be connected, in autoclave body 131 and lid
Sealing ring is set between 132, makes that there is therebetween better seal effect.
Holding rod 136 is set in 132 sidepiece of lid so that lid 132 can be gripped easily；Conveniently remove and install.
Pressure reducing valve 139 is set in 132 sidepiece of lid, the pressure in reaction kettle 130 can be reduced by pressure reducing valve 139, is risen
To safety guarantee.
132 bottom of lid sets blind hole 138, pressure reducing valve 139 is set connection blind hole 138 so that 132 overall dimensions of lid
What can be set is thicker, while lid 132 has higher intensity, and gases at high pressure can be leaked.
Pressure gauge 140 is set at the top of lid 132, pressure gauge 140 can reflect the pressure in reaction kettle 130, convenient
Observation.
Pressure gauge 140 connects magnetic stirring apparatus 110, reponse system can be set, by pressure feedback to magnetic stirring apparatus
110。
Pressure gauge 140 and two pressure reducing valves 139 are respectively communicated with different blind holes 138 so that pressure reducing valve 139 can be from difference
Position in reaction kettle 130 to depressurizing.In reaction kettle 130 evenly.
The Hydrothermal Synthesiss device set in this way, can be such that mixed liquor in reaction kettle 130 is mixed well, so as to
More easily tested.
In the present embodiment, the bottom of autoclave body 131 is provided with mounting base 150, and mounting base 150 includes base 151 and footstock
152, the middle part of base 151 and footstock 152 is both provided with through hole；The top of base 151 has the connecting seat 153 of annular, footstock
152 bottoms have mounting hole, and connecting seat 153 penetrates mounting hole, footstock 152 is rotated relative to base 151；Heater 120
It is positioned on footstock 152.Connecting seat 153 and mounting hole are connected by bearing, and the top of mounting hole has boss 154, boss 154
Internal diameter be adapted with the outside diameter of autoclave body 131.
By setting mounting base 150, can rotate 120 relative response kettle 130 of heater, to 130 side wall of reaction kettle into
The heating that row is more uniformly distributed, makes the mixed liquor mixing everywhere of reaction kettle 130 evenly, heating is evenly.
Mounting base 150 is set in outside autoclave body 131, and is located at 130 bottom position of reaction kettle, is limited heater 120
It is formed between mounting base 150 and connected unit 134.
As shown in figure 4, base 151 keeps not turning, footstock 152 can be rotated relative to base 151.Base 151 and footstock 152
Through hole is respectively provided with, autoclave body 131 is passed through；The top of base 151 sets connecting seat 153, and bottom can be realized by connecting seat 153
The connection of seat 151 and footstock 152, and footstock 152 is smoothly rotated.
Footstock 152 has boss 154, and 154 internal diameter of boss is adapted to 131 outside diameter of autoclave body, makes mounting base 150 and autoclave body 131
After connection, therebetween with less gap, heater 120 is set to obtain greater area of support；Heater 120 is placed
In mounting base 150, rotating footstock 152 can drive heater 120 to rotate；Rotating heater 120 makes footstock 152 with respect to base
151 rotate, and heater 120 is easily rotated.In addition, Hydrothermal Synthesiss device further include temperature sensor, pressure sensor,
The control units such as controller, to complete the control work of Hydrothermal Synthesiss device.
The foregoing is merely the preferred embodiment of the present invention, is not intended to limit the invention, for this area
For technical staff, the invention may be variously modified and varied.Within the spirit and principles of the invention, that is made is any
Modification, equivalent substitution, improvement etc., should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of magnetic agitation Hydrothermal Synthesiss device, it is characterised in that including magnetic stirring apparatus, heater and reaction kettle；The magnetic
Power blender has work top, and the reaction kettle is positioned on the work top；The reaction kettle has autoclave body and lid,
The lid is placed on above autoclave body；The heater is loop configuration, and the heaters set is arranged on the outside of the autoclave body.
2. magnetic agitation Hydrothermal Synthesiss device according to claim 1, it is characterised in that the autoclave body has in columned
Chamber, the lid bottom are connected with agitating shaft, and the agitating shaft stretches into the autoclave body, and the agitating shaft deviates the inner cavity
Axis.
3. magnetic agitation Hydrothermal Synthesiss device according to claim 1, it is characterised in that the top of the autoclave body has connection
Platform, the diameter of the connected unit are more than the diameter of autoclave body, and the heater is arranged at the lower section of connected unit.
4. magnetic agitation Hydrothermal Synthesiss device according to claim 3, it is characterised in that circumferentially arranged in the connected unit
More screw rods, the axis of the axis of the screw rod parallel to autoclave body；Multiple connecting holes are provided with the lid, the screw rod is worn
Cross the connecting hole.
5. magnetic agitation Hydrothermal Synthesiss device according to claim 4, it is characterised in that the lid is disc structure, lid
The sidepiece of body is symmetrically arranged with two holding rods, and the holding rod is set along the radial direction of lid.
6. magnetic agitation Hydrothermal Synthesiss device according to claim 1, it is characterised in that the bottom of the lid is from bottom to top
Blind hole is provided with, the sidepiece of the lid is provided with pressure reducing valve, and the pressure reducing valve connects the blind hole.
7. magnetic agitation Hydrothermal Synthesiss device according to claim 6, it is characterised in that pressure is provided with the top of the lid
Power table, the pressure gauge connect the blind hole.
8. magnetic agitation Hydrothermal Synthesiss device according to claim 7, it is characterised in that the pressure gauge has one, described
Pressure reducing valve is provided with two, and the blind hole is provided with three；The pressure gauge connects one of blind hole, two pressure reducing valve connections
Another two blind hole.
9. magnetic agitation Hydrothermal Synthesiss device according to claim 1, it is characterised in that the bottom of the autoclave body is provided with peace
Seat is filled, the mounting base includes base and footstock, through hole is both provided with the middle part of the base and footstock；The top of the base
Connecting seat with annular, the footstock bottom have mounting hole, and the connecting seat penetrates the mounting hole, enables footstock phase
To base rotation；The heater is positioned on the footstock.
10. magnetic agitation Hydrothermal Synthesiss device according to claim 9, it is characterised in that the connecting seat and mounting hole lead to
Bearing connection is crossed, the top of the mounting hole has boss, and the internal diameter of boss is adapted with the outside diameter of autoclave body.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711456716.2A CN107970874A (en) | 2017-12-27 | 2017-12-27 | A kind of magnetic agitation Hydrothermal Synthesiss device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711456716.2A CN107970874A (en) | 2017-12-27 | 2017-12-27 | A kind of magnetic agitation Hydrothermal Synthesiss device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107970874A true CN107970874A (en) | 2018-05-01 |
Family
ID=62008081
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711456716.2A Pending CN107970874A (en) | 2017-12-27 | 2017-12-27 | A kind of magnetic agitation Hydrothermal Synthesiss device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107970874A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109126677A (en) * | 2018-10-24 | 2019-01-04 | 中国科学院高能物理研究所 | Reaction in-situ device |
| CN110586012A (en) * | 2019-09-18 | 2019-12-20 | 中国科学院上海硅酸盐研究所 | Aerospace aerogel preparation device |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202387459U (en) * | 2011-12-28 | 2012-08-22 | 陈磊 | High-temperature high-pressure photochemical reactor with gas-liquid sampling function |
| CN205413081U (en) * | 2015-12-02 | 2016-08-03 | 重庆市长寿区世才科技有限公司 | General electric jacket of spherical beaker of many sizes |
| WO2016192405A1 (en) * | 2015-05-29 | 2016-12-08 | 浙江科技学院 | Hydrothermal reaction kettle |
| CN205893333U (en) * | 2016-07-08 | 2017-01-18 | 广州信粤密封胶有限公司 | High -efficient thermal response stove |
| CN207805615U (en) * | 2017-12-27 | 2018-09-04 | 盐城工学院 | A kind of magnetic agitation hydrothermal synthesis device |
-
2017
- 2017-12-27 CN CN201711456716.2A patent/CN107970874A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202387459U (en) * | 2011-12-28 | 2012-08-22 | 陈磊 | High-temperature high-pressure photochemical reactor with gas-liquid sampling function |
| WO2016192405A1 (en) * | 2015-05-29 | 2016-12-08 | 浙江科技学院 | Hydrothermal reaction kettle |
| CN205413081U (en) * | 2015-12-02 | 2016-08-03 | 重庆市长寿区世才科技有限公司 | General electric jacket of spherical beaker of many sizes |
| CN205893333U (en) * | 2016-07-08 | 2017-01-18 | 广州信粤密封胶有限公司 | High -efficient thermal response stove |
| CN207805615U (en) * | 2017-12-27 | 2018-09-04 | 盐城工学院 | A kind of magnetic agitation hydrothermal synthesis device |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109126677A (en) * | 2018-10-24 | 2019-01-04 | 中国科学院高能物理研究所 | Reaction in-situ device |
| CN110586012A (en) * | 2019-09-18 | 2019-12-20 | 中国科学院上海硅酸盐研究所 | Aerospace aerogel preparation device |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107970874A (en) | A kind of magnetic agitation Hydrothermal Synthesiss device | |
| Hasani et al. | Equilibrium and kinetic studies of azo dye (Basic Red 18) adsorption onto montmorillonite: Numerical simulation and laboratory experiments | |
| CN110343259B (en) | Green fluorescent sandwich type zinc coordination polymer and preparation method and application thereof | |
| CN207805615U (en) | A kind of magnetic agitation hydrothermal synthesis device | |
| CN204395891U (en) | A kind of agitator device with heating function | |
| Bocanegra et al. | Gasification study of winery waste using a hydrothermal diamond anvil cell | |
| Fegade et al. | Effective adsorption of Fuchsine dye on FeZnOAC: kinetic, isotherm, double-layer modelling and reusability study | |
| CN105536626A (en) | Programmable control type double-temperature-control and double-speed-control stirring device | |
| JP2020532413A (en) | Methods, devices, and systems for processing and filtering carbonaceous compositions | |
| CN205666968U (en) | Heating device for biochemistry | |
| CN110357122A (en) | The method of oil shale waste modified synthesis X-type zeolite | |
| CN205462043U (en) | But programming control's fast agitating unit of two accuses of two accuse temperature | |
| CN206064415U (en) | A kind of laboratory highly effective reaction kettle | |
| CN107474818A (en) | A kind of high temperature resistant micro emulsion acid system and preparation method thereof | |
| CN207805631U (en) | A kind of stirring type water heat seal is grown up to be a useful person and reaction system | |
| CN208554265U (en) | A kind of automatic shaking table equipment on the rocks | |
| CN207805614U (en) | A kind of multifunctional magnetic-force stirring hydrothermal synthesis device and reaction system | |
| CN107930566A (en) | A kind of multifunctional magnetic-force stirring Hydrothermal Synthesiss device and reaction system | |
| CN205659688U (en) | Parallel experimental facilities | |
| CN108295710A (en) | Agitator tank for chemical industry auto-control | |
| CN208591824U (en) | A kind of senior chemistry test tube stirring reaction experiment device | |
| CN213078301U (en) | Multifunctional water bath constant temperature oscillator | |
| Poós et al. | Thermal dewatering of waste sludge in an agitated drum dryer | |
| CN105689018A (en) | Parallel experiment equipment and parallel experiment method | |
| CN209631069U (en) | A kind of petroleum refining uniform stirrer |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |