CN107942042A - The anti-aging test device and moulding process of a kind of chemicals pail pack - Google Patents

The anti-aging test device and moulding process of a kind of chemicals pail pack Download PDF

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Publication number
CN107942042A
CN107942042A CN201711194812.4A CN201711194812A CN107942042A CN 107942042 A CN107942042 A CN 107942042A CN 201711194812 A CN201711194812 A CN 201711194812A CN 107942042 A CN107942042 A CN 107942042A
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China
Prior art keywords
pail pack
turntable
tested
chemicals
aging test
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CN201711194812.4A
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Chinese (zh)
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CN107942042B (en
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浦陈龙
朱永刚
殷福华
朱龙
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Jiangyin Jianghua Microelectronic Material Co Ltd
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Jiangyin Jianghua Microelectronic Material Co Ltd
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/44Resins; Plastics; Rubber; Leather
    • G01N33/442Resins; Plastics
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01MTESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
    • G01M13/00Testing of machine parts

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  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Testing Resistance To Weather, Investigating Materials By Mechanical Methods (AREA)

Abstract

The invention discloses a kind of anti-aging test device of chemicals pail pack, including cabinet or building with sealing inner cavity and hermatic door, the bottom surface of sealing inner cavity is rotatably provided with turntable, and turntable is used to carry pail pack to be tested, and turntable is connected with rotary drive mechanism;The side of turntable is provided with the ultraviolet lamp of adjustable wavelength, seals in inner cavity and is additionally provided with explosion-proof heating element and wind turbine;Exhaust outlet is provided with cabinet or building, exhaust outlet is connected with relief valve and exhaust pipe, feed inlet of the exhaust pipe for connecting exhaust outlet, relief valve and pail pack to be tested, and the bottom of cabinet or building is provided with leakage fluid dram.The anti-aging test device of the chemicals pail pack by setting heating member, ultraviolet lamp and turntable at the same time in the inner cavity of sealing, and pressure in bottle is stablized by relief valve, the experiment to pail pack is set to help to investigate the influence of nitric acid, ultraviolet light and heating condition to pail pack mechanical property etc. closer to use condition.

Description

The anti-aging test device and moulding process of a kind of chemicals pail pack
Technical field
The present invention relates to quartz crucible mold technical field, and in particular to a kind of anti-aging test dress of chemicals pail pack Put and moulding process.
Background technology
Chemicals discharging packaging is mainly packed using plastic barrel, real due to the use of custom and the difference of content, pail pack The use process on border is inconsistent.By taking nitric acid as an example, normal use habit is to use up nitric acid completely, but actually uses process In, it may occur that phenomena such as remaining sales volume nitric acid and being exposed to the sun, the nitric acid after heating can decomposite oxides of nitrogen gas, and strong oxygen The property changed nitric acid can also accelerate the aging of clinker pail pack in the case where being exposed to the sun.Gas rise can pass through bottle in the bottle of preceding problem Lid pressure release, but later problem can cause pail pack Material Strength and flexibility decrease, and brittleness increase, there are serious safety is hidden Suffer from.In addition, pail pack also inevitably runs into the above problem during chemical transport.Therefore, it is necessary to chemicals Pail pack carries out the sampling Detection of stringent incoming test and recycling bin, during subsequent use that safety is hidden to ensure Trouble minimizes.
It is for the anticorrosion test process of plastic barrel in the prior art:Directly bucket is placed in chemicals, then corrosion Property chemicals temperature be maintained at 75 degrees Celsius and submerge 48 it is small when after, staving should not have it is any rupture, blistering or deformation.Plastic barrel Ageing-resistant test include Outdoor exposure test method and artificial ageing test method, wherein artificial ageing test method includes heat Burn-in test, the exposure degradation under wet heat condition, hyperbaric oxygen and pressure-air heat ageing and artificial weathering's burn-in test.
The anti-aging test equipment that complex factors are directed to specific to chemicals pail pack is had no in the prior art.
The content of the invention
It is an object of the present invention to overcome defect existing in the prior art, there is provided a kind of chemicals pail pack it is resistance to Ageing test apparatus, few using crackle of the crucible base of the above-mentioned mould preparation demoulding in dehydration is stood, scrappage is low.
To realize above-mentioned technique effect, the technical scheme is that:A kind of anti-aging test dress of chemicals pail pack Put, it is characterised in that including cabinet or building with sealing inner cavity and hermatic door, the bottom surface for sealing inner cavity is rotatably set There is turntable, turntable is used to carry pail pack to be tested, and turntable is connected with rotary drive mechanism;The side of turntable is provided with can The ultraviolet lamp of adjusting wavelength, seals in inner cavity and is additionally provided with explosion-proof heating element and wind turbine;It is provided with cabinet or building Exhaust outlet, exhaust outlet are connected with relief valve and exhaust pipe, and exhaust pipe is used to connect exhaust outlet, relief valve and pail pack to be tested The bottom of feed inlet, cabinet or building is provided with leakage fluid dram.
Driven by rotary disc includes the pail pack to be tested rotation of nitric acid, to ensure each part in pail pack side by uniform irradiation. Under conditions of heating and ultraviolet lighting, nitric acid accelerated decomposition, caused oxides of nitrogen gas can increase the pressure in pail pack, Said structure can timely pressure release, ensure ultraviolet light process lasting progress.
Need to connect the pressure gauge just achievable real time monitoring for pressure in bucket on pail pack to be tested.In order to avoid hair Raw movement interference, exhaust pipe are connected by swivel joint with the connector of pail pack feed inlet to be tested.Swivel joint can be straight The pail pack only for top surface with a feed inlet of line style or L-shaped, can connect exhaust pipe and pressure by crossover sub Meter connection.
When relief valve or pressure gauge break down, it is quick-fried that defective packages bucket occurs that injection nitric acid, most serious can occur Split, in order to avoid nitric acid splashes, preferable technical solution is that turntable top surface is provided with transparent plastic cylinder, transparent plastic cylinder Height be not less than the height of pail pack to be tested, the air outlet of wind turbine is open upper and lower corresponding with transparent plastic cylinder, transparent Liquid outlet is provided between plastic cylinder bottom and turntable.Based on practical structures, liquid outlet is arranged on the bottom of transparent plastic cylinder End, controls the discharging of liquid, further, liquid valve is provided with liquid outlet for convenience.
Further, the air inlet of wind turbine, which is connected with, is air-dried filter, is coagulated to avoid the water vapour in sealing cavity Knot influences ultraviolet light direct projection on transparent plastic cylinder, so that Aging simulation is inaccurate.
For the safety of guarantee test, preferable technical solution is, heating element is steam pipe coil, the both ends of steam pipe coil It is connected with the feeding machanism outside cabinet or building.
Common, turntable is metal material, to avoid turntable from reacting with nitric acid, while ensures nitric acid not corrosion electrical motor Etc. equipment, preferable technical solution is that head cover is detachably provided with turntable, and the surface of transparent plastic cylinder and head cover, which is fixed, to be connected Connect, the driving mechanism periphery of turntable is provided with blast ring, and the periphery of blast ring is provided with cricoid overflow launder, the bottom of overflow launder Communicated with leakage fluid dram;The outer rim of head cover is arranged in overflow launder.Generation nitric acid overflows, and nitric acid is flowed out via liquid outlet, and via The outer rim of head cover is imported in overflow launder, eventually flows to the leakage fluid dram of the bottom of cabinet or building.Overflow launder groove width is smaller, will not Trolley translation is hindered, the pail pack for filling nitric acid is transported easy to trolley.
For the ease of pail pack position, preferable technical solution be provided with head cover it is matched with pail pack bottom Concave part.
Discharge is read in order to further facilitate the fast of leak fluid, preferable technical solution is to be provided with around concave part Diversion trench, diversion trench one end are communicated with concave part, and the other end of diversion trench extends to the capping edge of head cover.
Since volume plastic barrel of the prior art is different, the position of charging hole is differed, using flexible exhaust The torsion of exhaust pipe easily occurs for tube capacity, the easy gas leakage of exhaust pipe, in order to facilitate being telescopically connected for exhaust pipe, preferable technical solution For exhaust pipe is composed for hard pipeline section and flexible pipeline section, and flexible pipeline section is connected with exhaust outlet, and stretch pipeline section and and telescoping tube Hard pipeline section one end of section connection is set in guide cylinder, and the top of guide cylinder is fixedly connected with cabinet or building inner surface, The center overlapping of axles of exhaust outlet, exhaust pipe and turntable, the inlet end of exhaust pipe are provided with linear swivel joint, linear rotation Connector is used to be connected with the exhaust crossover sub of pail pack feed inlet to be tested.
The second object of the present invention is to provide a kind of anti-aging test method of chemicals pail pack, it is characterised in that Comprise the following steps:
S1:By the pail pack to be tested equipped with predetermined 70% nitric acid of Packing Unit molar concentration as on turntable, in pail pack to be tested Feed inlet on connect pressure gauge and exhaust pipe, the end of exhaust pipe and be located at the ullage of pail pack to be tested;
S2:Open ultraviolet lamp, heating element, start rotary disc driving mechanism, treat test bag barrelling carry out the scheduled time, temperature and The burin-in process of ultraviolet wavelength, when pressure is more than an atmospheric pressure, opening relief valve pressure release in pail pack to be tested;
S3:After the completion of burin-in process, pail pack to be tested is taken out, discharge nitric acid in bucket, cool down 10~30min, after cleaning-drying It is tested for the property.
Specifically, predetermined temperature is specifically chosen in 20-80 DEG C, ultraviolet wavelength is specifically chosen between 100-300nm.
Preferable technical solution is that performance test includes stress cracking experiment, drop test and pile test.
The advantages of the present invention are:
The anti-aging test device of the chemicals pail pack by setting heating member, ultraviolet lamp and turning at the same time in the inner cavity of sealing Disk, and pressure in bottle is stablized by relief valve, pail pack single factor experiment method of the prior art is different from, is made to pail pack Experiment closer to use condition, help to investigate the influence of nitric acid, ultraviolet light and heating condition to pail pack mechanical property etc..
Brief description of the drawings
Fig. 1 is the structure diagram of the anti-aging test device embodiment 1 of chemicals pail pack of the present invention;
Fig. 2 is the structure diagram of embodiment 2.
In figure:1st, cabinet;2nd, turntable;3rd, rotary drive mechanism;4th, ultraviolet lamp;5th, heating element;6th, wind turbine;7th, it is vented Mouthful;8th, relief valve;9th, exhaust pipe;91st, hard pipeline section;92nd, stretch pipeline section;10th, leakage fluid dram;11st, transparent plastic cylinder;12nd, go out Liquid mouth;13rd, head cover;14th, blast ring;15th, overflow launder;16th, concave part;17th, diversion trench;18th, guide cylinder;19th, linear rotates Connector.
Embodiment
With reference to the accompanying drawings and examples, the embodiment of the present invention is further described.Following embodiments are only For clearly illustrating technical scheme, and it is not intended to limit the protection scope of the present invention and limits the scope of the invention.
Embodiment 1
As shown in Figure 1, the anti-aging test device of 1 chemicals pail pack of embodiment, including with the cabinet 1 for sealing inner cavity or build Thing is built, the bottom surface for sealing inner cavity is rotatably provided with turntable 2, and turntable 2 is used to carry pail pack to be tested, and turntable 2 drives with rotation Motivation structure 3 is connected;The side of turntable 2 is provided with the ultraviolet lamp 4 of adjustable wavelength, is additionally provided with sealing inner cavity explosion-proof Heating element 5 and wind turbine 6;Exhaust outlet 7 is provided with cabinet 1 or building, exhaust outlet 7 is connected with relief valve 8 and exhaust pipe 9, Exhaust pipe 9 is used for the feed inlet for connecting exhaust outlet 7, relief valve 8 and pail pack to be tested, the bottom setting of cabinet 1 or building There is leakage fluid dram 10.
Rotary drive mechanism includes motor, gear reducer and gear drive in embodiment 1.
Turntable top surface is provided with transparent plastic cylinder 11, and the height of transparent plastic cylinder 11 is not less than pail pack to be tested Highly, the air outlet of wind turbine 6 and the opening of transparent plastic cylinder 11 are corresponding up and down, and 11 bottom of transparent plastic cylinder is provided with out liquid Mouth 12.
Heating element 5 is steam pipe coil, and the both ends of steam pipe coil are connected with the feeding machanism outside cabinet or building.
1 transfer panel surface of embodiment coats one layer of corrosion prevention film.
Embodiment 2
As shown in Fig. 2, embodiment 2 and embodiment 1 difference lies in:Head cover 13, transparent plastic cylinder are detachably provided with turntable 2 Body 11 is fixedly connected with the surface of head cover 13, and the driving mechanism periphery of turntable 2 is provided with blast ring 14, and the periphery of blast ring 14 is set Cricoid overflow launder 15 is equipped with, the bottom of overflow launder 15 is communicated with leakage fluid dram 10;The outer rim of head cover 13 is arranged in overflow launder 15.
Concave part 16 matched with pail pack bottom is provided with head cover 13.
Diversion trench 17 is provided with around concave part 16,17 one end of diversion trench is communicated with concave part 16, diversion trench 17 it is another One end extends to the capping edge of head cover 13, i.e. liquid outlet is arranged on the head cover of turntable.
Exhaust pipe 9 is composed for hard pipeline section 91 and flexible pipeline section 92, and flexible pipeline section 92 is connected with exhaust outlet 7, is stretched Pipeline section 92 and 91 one end of hard pipeline section being connected with flexible pipeline section 92 are set in guide cylinder 18, the top of guide cylinder 18 and cabinet Or building inner surface is fixedly connected, the center overlapping of axles of exhaust outlet 7, exhaust pipe 9 and turntable 2, the inlet end of exhaust pipe 9 is set There is linear swivel joint 19, linear swivel joint 19 is used to connect with the exhaust crossover sub of pail pack feed inlet to be tested Connect.
The anti-aging test method of chemicals pail pack comprises the following steps:
S1:By the pail pack to be tested equipped with predetermined 70% nitric acid of Packing Unit molar concentration as on turntable, in pail pack to be tested Feed inlet on connect pressure gauge and exhaust pipe, the end of exhaust pipe and be located at the ullage of pail pack to be tested;
S2:Open ultraviolet lamp, heating element, start rotary disc driving mechanism, treat test bag barrelling carry out the scheduled time, temperature and The burin-in process of ultraviolet wavelength, when pressure is more than an atmospheric pressure, opening relief valve pressure release in pail pack to be tested;
S3:After the completion of burin-in process, pail pack to be tested is taken out, discharge nitric acid in bucket, cool down 10~30min, after cleaning-drying It is tested for the property.
Performance test includes stress cracking experiment, drop test and pile test.
In use, being filled with nitric acid into container to be tested first, then container to be tested is transferred on turntable with fork truck, Exhaust pipe is communicated with the feed inlet of container, installation pressure gauge etc., then operating personnel withdraw from closing inner chamber, begin to warm up, is purple Outer illumination and turntable, it is furthermore preferred that first removing the water vapour in closing inner chamber(Utilize the air of cabinet either internally or externally Device for drying and filtering).
Further, it is necessary to control system is equipped with, to ensure that pressure reaches predetermined in temperature and container to be tested Value is that the control system and air bleeding valve of corresponding heating element can be with fast reactions.
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art For member, without departing from the technical principles of the invention, some improvements and modifications can also be made, these improvements and modifications Also it should be regarded as protection scope of the present invention.

Claims (9)

1. a kind of anti-aging test device of chemicals pail pack, it is characterised in that including with sealing inner cavity and hermatic door Cabinet or building, the bottom surface for sealing inner cavity are rotatably provided with turntable, and turntable is used to carry pail pack to be tested, turntable and rotation Turn driving mechanism mating connection;The side of turntable is provided with the ultraviolet lamp of adjustable wavelength, is additionally provided with sealing inner cavity explosion-proof Heating element and wind turbine;Exhaust outlet is provided with cabinet or building, exhaust outlet is connected with relief valve and exhaust pipe, exhaust pipe For connecting the feed inlet of exhaust outlet, relief valve and pail pack to be tested, the bottom of cabinet or building is provided with leakage fluid dram.
2. the anti-aging test device of chemicals pail pack according to claim 1, it is characterised in that turntable top surface is set Have a transparent plastic cylinder, the height of transparent plastic cylinder is not less than the height of pail pack to be tested, the air outlet of wind turbine with it is transparent The opening of plastic cylinder is corresponding up and down, and liquid outlet is provided between transparent plastic cylinder bottom and turntable.
3. the anti-aging test device of chemicals pail pack according to claim 1, it is characterised in that heating element is steaming Vapour coil pipe, the both ends of steam pipe coil are connected with the feeding machanism outside cabinet or building.
4. the anti-aging test device of chemicals pail pack according to claim 2, it is characterised in that detachable on turntable Head cover is provided with, transparent plastic cylinder is fixedly connected with the surface of head cover, and the driving mechanism periphery of turntable is provided with blast ring, is prevented The periphery of quick-fried ring is provided with cricoid overflow launder, and the bottom of overflow launder is communicated with leakage fluid dram;The outer rim of head cover is arranged on overflow launder In.
5. the anti-aging test device of chemicals pail pack according to claim 4, it is characterised in that be provided with head cover With the matched concave part in pail pack bottom.
6. the anti-aging test device of chemicals pail pack according to claim 5, it is characterised in that around concave part Diversion trench is provided with, diversion trench one end is communicated with concave part, and the other end of diversion trench extends to the capping edge of head cover.
7. the anti-aging test device of chemicals pail pack according to claim 1, it is characterised in that exhaust pipe is hard Pipeline section and flexible pipeline section are composed, and flexible pipeline section is connected with exhaust outlet, flexible pipeline section and the stereoplasm tube being connected with flexible pipeline section Duan Yiduan is set in guide cylinder, and the top of guide cylinder is fixedly connected with cabinet or building inner surface, exhaust outlet, exhaust pipe and The center overlapping of axles of turntable, the inlet end of exhaust pipe are provided with linear swivel joint, linear swivel joint be used for it is to be measured Try the exhaust crossover sub connection of pail pack feed inlet.
A kind of 8. anti-aging test method of chemicals pail pack, it is characterised in that comprise the following steps:
S1:By the pail pack to be tested equipped with predetermined 70% nitric acid of Packing Unit molar concentration as on turntable, in pail pack to be tested Feed inlet on connect pressure gauge and exhaust pipe, the end of exhaust pipe and be located at the ullage of pail pack to be tested;
S2:Open ultraviolet lamp, heating element, start rotary disc driving mechanism, treat test bag barrelling carry out the scheduled time, temperature and The burin-in process of ultraviolet wavelength, when pressure is more than an atmospheric pressure, opening relief valve pressure release in pail pack to be tested;
S3:After the completion of burin-in process, pail pack to be tested is taken out, discharge nitric acid in bucket, cool down 10~30min, after cleaning-drying It is tested for the property.
9. the anti-aging test method of chemicals pail pack according to claim 7, it is characterised in that performance test includes Stress cracking experiment, drop test and pile test.
CN201711194812.4A 2017-11-24 2017-11-24 Aging resistance test device and method for chemical packaging barrel Active CN107942042B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111610142A (en) * 2020-06-02 2020-09-01 浙江工业大学 Corrosion device for metal corrosion fatigue test
CN114354164A (en) * 2021-12-30 2022-04-15 宁波市产品食品质量检验研究院(宁波市纤维检验所) Garbage bin performance detection device

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Publication number Priority date Publication date Assignee Title
JP2004132857A (en) * 2002-10-11 2004-04-30 Yokohama Rubber Co Ltd:The Heat aging test device
CN102346158A (en) * 2011-09-19 2012-02-08 深圳市建筑科学研究院有限公司 Damp heat aging test device
CN105043964A (en) * 2015-07-16 2015-11-11 哈尔滨工业大学 Test apparatus for ultraviolet aging acceleration of asphalt-based materials
CN205483952U (en) * 2016-01-01 2016-08-17 长安大学 Light and heat coupling aging test box
CN205808891U (en) * 2016-07-07 2016-12-14 东莞市顶好新材料科技有限公司 One is applied to high performance material ultraviolet atmospheric exposure test device
CN206146932U (en) * 2016-09-28 2017-05-03 山西省交通科学研究院 Pitch ageing tests device of controllable temperature light water wind
CN206504992U (en) * 2017-02-21 2017-09-19 科谱研发技术中心(青岛)有限公司 Plastics heat aging test chamber

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004132857A (en) * 2002-10-11 2004-04-30 Yokohama Rubber Co Ltd:The Heat aging test device
CN102346158A (en) * 2011-09-19 2012-02-08 深圳市建筑科学研究院有限公司 Damp heat aging test device
CN105043964A (en) * 2015-07-16 2015-11-11 哈尔滨工业大学 Test apparatus for ultraviolet aging acceleration of asphalt-based materials
CN205483952U (en) * 2016-01-01 2016-08-17 长安大学 Light and heat coupling aging test box
CN205808891U (en) * 2016-07-07 2016-12-14 东莞市顶好新材料科技有限公司 One is applied to high performance material ultraviolet atmospheric exposure test device
CN206146932U (en) * 2016-09-28 2017-05-03 山西省交通科学研究院 Pitch ageing tests device of controllable temperature light water wind
CN206504992U (en) * 2017-02-21 2017-09-19 科谱研发技术中心(青岛)有限公司 Plastics heat aging test chamber

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111610142A (en) * 2020-06-02 2020-09-01 浙江工业大学 Corrosion device for metal corrosion fatigue test
CN111610142B (en) * 2020-06-02 2024-06-11 浙江工业大学 Corrosion device for metal corrosion fatigue test
CN114354164A (en) * 2021-12-30 2022-04-15 宁波市产品食品质量检验研究院(宁波市纤维检验所) Garbage bin performance detection device
CN114354164B (en) * 2021-12-30 2023-12-12 宁波市产品食品质量检验研究院(宁波市纤维检验所) Garbage bin performance detection device

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