CN107910142A - A kind of stainless steel based insulation component and its manufacture method - Google Patents
A kind of stainless steel based insulation component and its manufacture method Download PDFInfo
- Publication number
- CN107910142A CN107910142A CN201711311391.9A CN201711311391A CN107910142A CN 107910142 A CN107910142 A CN 107910142A CN 201711311391 A CN201711311391 A CN 201711311391A CN 107910142 A CN107910142 A CN 107910142A
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- Prior art keywords
- stainless steel
- based insulation
- insulation component
- insulating layer
- steel based
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B17/00—Insulators or insulating bodies characterised by their form
- H01B17/56—Insulating bodies
- H01B17/62—Insulating-layers or insulating-films on metal bodies
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B19/00—Apparatus or processes specially adapted for manufacturing insulators or insulating bodies
Abstract
The present invention relates to technical field of electronic materials, there is provided a kind of stainless steel based insulation component and its manufacture method.A kind of manufacture method of stainless steel based insulation component, including offer dielectric paste and stainless steel substrate, the dielectric paste include glass dust and ceramic powder；Green compact are made through casting technique in the dielectric paste, the surface that the green compact are covered in the stainless steel substrate obtains component to be sintered；Required stainless steel based insulation component will be obtained after the component sinter molding to be sintered, which includes stainless steel substrate and the insulating layer for being covered in stainless steel substrate surface.The manufacture method of the stainless steel based insulation component, forms insulating layer using casting technique, can disposably complete, production efficiency is high.The present invention also provides a kind of stainless steel based insulation component, have the advantages that service life is long.
Description
Technical field
The present invention relates to technical field of electronic materials, more particularly to a kind of stainless steel based insulation component and its manufacture method.
Background technology
Heating element is to realize the class component that electric energy is converted to thermal energy, and various heating equipments will use heating element
To generate heat.With electric heating products becoming increasingly popular in numerous areas such as household electrical appliances, industrial electrical equipment, electronic equipment, automobile industries, electric heating
The application of element becomes more and more extensive, so people are also higher and higher to the performance requirement of heating element each side.Wherein, it is thick
Film circuit type heating element has the advantages of firing rate is fast, energy-efficient, has obtained more and more favors.At present, thick film
Circuit type heating element is to use silk-screen printing technique, and printed medium slurry forms insulating layer on substrate.But this mode,
Need repeatedly to be printed, there are the problem of low production efficiency.
The content of the invention
It is an object of the invention to provide a kind of stainless steel based insulation component and its manufacture method, formed using casting technique
Insulating layer, can disposably complete, and production efficiency is high.
In order to solve the above technical problems, invention uses technical solution as described below.A kind of stainless steel based insulation component
Manufacture method, including offer dielectric paste and stainless steel substrate, the dielectric paste include glass dust and ceramic powder；It will be given an account of
Green compact are made through casting technique in chylema material, and the surface that the green compact are covered in the stainless steel substrate obtains component to be sintered；
Required stainless steel based insulation component will be obtained after the component sinter molding to be sintered, which includes
Stainless steel substrate and the insulating layer for being covered in stainless steel substrate surface.
Preferably, the difference of the glass dust and the thermal coefficient of expansion of the stainless steel substrate is less than 6 × 10-6/℃。
Preferably, the ceramic powder includes the one or more in aluminium oxide, magnesia, zirconium oxide, silica.
Preferably, the thickness of the green compact is 50-500 μm.
Preferably, the sintering uses once sintered, and sintering temperature is 600-1000 DEG C.
A kind of stainless steel based insulation component, including stainless steel substrate and the insulating layer for being covered in stainless steel substrate surface, institute
It is that the green sintering formed by casting technique is made to state insulating layer.
Preferably, the insulating layer side grade is less than 5 °.
Preferably, the smooth densification of the surface of insulating layer, its coverage rate are 85-100%.
Preferably, the thickness of insulating layer is 28-268 μm.
Preferably, the breakdown voltage of the insulating layer is 1800-4000V.
The beneficial effects of the present invention are：
The present invention provides a kind of manufacture method of stainless steel based insulation component, and insulating layer is formed using casting technique, can be with
Disposable to complete, production efficiency is high.And relative to the existing manufacture method using silk-screen printing technique, due to without repeatedly printing
Brush, the insulating layer good integrity formed, obtained stainless steel based insulation component service life length.
Present invention also offers a kind of stainless steel based insulation component, since insulating layer is made of by casting technique, institute's shape
Into insulating layer good integrity, the stainless steel based insulation component service life length.
Brief description of the drawings
Fig. 1 is the flow diagram of the manufacture method of stainless steel based insulation component provided by the present invention.
Fig. 2 is the structure diagram of stainless steel based insulation component provided by the present invention.
Embodiment
To make those of ordinary skill in the art that the purpose, technical scheme and advantage of invention be more clearly understood, below
Invention is further elaborated in conjunction with the accompanying drawings and embodiments.
Embodiment one
Also referring to Fig. 1, Fig. 2, a kind of manufacture method of stainless steel based insulation component, including：
Step S1：There is provided dielectric paste and stainless steel substrate 2, the dielectric paste includes glass dust and ceramic powder；
Step S2：Green compact are made through casting technique in the dielectric paste, the green compact are covered in the stainless base steel
The surface of material 2 obtains component to be sintered；
Step S2：Required stainless steel based insulation component will be obtained after the component sinter molding to be sintered, this is stainless
Base steel insulating element includes stainless steel substrate 2 and the insulating layer 1 for being covered in 2 surface of stainless steel substrate.
The manufacture method of stainless steel based insulation component provided by the present invention, insulating layer is formed using casting technique, can be with
Disposable to complete, production efficiency is high.And relative to the existing manufacture method using silk-screen printing technique, due to without repeatedly printing
Brush, the insulating layer good integrity formed, obtained stainless steel based insulation component service life length.Also, due to using curtain coating
Technique, is not in reticulate pattern, and 1 side grade of insulating layer does not have slope even less than 5 ° in the smooth densification in 1 surface of insulating layer
Degree.Further, since using green compact are first made, then the mode on 2 surface of stainless steel substrate is covered in, can be according to stainless steel substrate 2
The green compact to match with 2 size of stainless steel substrate are made, so as to fulfill comprehensive covering, its coverage rate can reach 85-100%,
And it can be very good to realize 100% coverage rate.In some specific embodiments, the green compact are covered in described stainless
The surface of steel substrate 2 is：Using 2 surface of wet with solvent green compact and stainless steel substrate, then both are bonded.
In the mill by controlling the thickness of green compact, so as to control the thickness of insulating layer 1,1 thickness of insulating layer it is controllable
Property is good.It is appreciated that when green compact thickness is larger, insulating layer 1 is thicker, influences heat transfer and the heat radiation energy of stainless steel based insulation component
Power；When green compact thickness is smaller, the thickness of insulating layer 1 is also smaller, and breakdown voltage is relatively low, influences security performance.It is preferable at some
In embodiment, the thickness of the green compact is 50-500 μm, and 1 thickness of insulating layer of obtained stainless steel based insulation component is 28-
268 μm, it both can guarantee that heat transfer and the heat dissipation effect of stainless steel based insulation component, and also can guarantee that insulating layer 1 had higher breakdown
Voltage.The breakdown voltage of the insulating layer 1 can reach 1800-4000V.
Preferably, the sintering uses once sintered, and sintering temperature is 600-1000 DEG C.Due to being formed using casting technique
Insulating layer 1, using once sintered, the high cost of production efficiency is low；By determining sintering temperature, it can ensure insulating layer well
1 molding effect.Due to using stainless steel substrate 2, it is preferred that sintering temperature is 700-900 DEG C, optimal is sintering temperature
For 850 DEG C.
Preferably, the difference of the glass dust and the thermal coefficient of expansion of the stainless steel substrate 2 is less than 6 × 10-6/ DEG C, energy
Avoid during sintering not being bonded well because the thermal expansion difference between green compact and stainless steel substrate 2 is too many, ensure made
Obtain the quality of stainless steel based insulation component.In some preferred embodiments, the ceramic powder includes aluminium oxide, magnesia, oxygen
Change the one or more in zirconium, silica.
In some preferred embodiments, the dielectric paste includes by weight：
As described in the text, it is preferable that glass dust makes choice according to base material, controls thermal coefficient of expansion between the two
Difference is less than 6 × 10-6/ DEG C, ceramic powder is then preferably comprising one kind in aluminium oxide, magnesia, zirconium oxide, silica
It is or several.
Preferably, the binding agent is polyacrylate or polyvinyl butyral resin or both mixture；The plasticizer
For adjacent phenyl ester class plasticizer or polyethylene glycols plasticizer or both mixture.In some preferred embodiments, the solvent
Be made of terpinol, butyl carbitol and butyl carbitol acetate, or the solvent by n-butanol, propylene glycol monomethyl ether and
Dimethyl ether forms.It is described when the solvent is made of terpinol, butyl carbitol and butyl carbitol acetate
Weight ratio between terpinol, butyl carbitol and butyl carbitol acetate is (0.5-6):(0.5-5):1；It is preferred that
Weight ratio between the terpinol, butyl carbitol and butyl carbitol acetate is (1-2):(0.8-1.8):1；It is optimal
For the weight ratio between the terpinol, butyl carbitol and butyl carbitol acetate is 1.6:1.4:1.When the solvent
When being made of n-butanol, propylene glycol monomethyl ether and dimethyl ether, the n-butanol, propylene glycol monomethyl ether and dipropylene glycol
Weight ratio between dimethyl ether is 1:(0.1-7):(0.6-9)；It is preferred that the n-butanol, propylene glycol monomethyl ether and dipropyl
Weight ratio between glycol dimethyl ether is 1:(0.5-2):(1-3)；It is optimal to be, the n-butanol, propylene glycol monomethyl ether and dipropyl
Weight ratio between glycol dimethyl ether is 1:1.2:1.8.By determining each component and proportioning, can obtain being suitably applied curtain coating
The dielectric paste of technique, ensures final product quality.
Embodiment two
As shown in Fig. 2, a kind of stainless steel based insulation component, including stainless steel substrate 2 and it is covered in 2 surface of stainless steel substrate
Insulating layer 1, the insulating layer 1 is made of by casting technique.It is appreciated that the stainless steel based insulation component in the present embodiment
It is exactly using obtained by the manufacture method of the stainless steel based insulation component provided in embodiment one.Understand from the above, this is not
Become rusty base steel insulating element, since insulating layer 1 is made of by casting technique, 1 good integrity of insulating layer that is formed and uses the longevity
Life length.Also, be not in reticulate pattern in the smooth densification in 1 surface of insulating layer due to using casting technique, and 1 side slope of insulating layer
Degree, which is less than 5 °, does not have the gradient even；The coverage rate of the insulating layer 1 can reach 85-100%.In some preferred embodiments
In, 1 thickness of insulating layer of the stainless steel based insulation component is 28-268 μm, and the breakdown voltage of insulating layer 1 can reach 1800-
4000V。
Some specific experimental groups and contrast groups are provided below
Experimental group 1
1) dielectric paste is prepared, wherein ceramic powder selects aluminium oxide；
2) green compact are made using casting technique, green compact thickness is 50 μm；
3) wet with solvent green compact and stainless steel substrate surface are used, is then bonded both, green compact covering stainless steel substrate
The 100% of surface area；
4) the primary drying sinter molding in continuous tunnel furnace, sintering temperature are 850 DEG C.
Experimental group 2
The experimental group and experimental group 1 difference lies in：Green compact thickness is 200 μm.
Experimental group 3
The experimental group and experimental group 1 difference lies in：Green compact thickness is 400 μm.
Experimental group 4
The experimental group and experimental group 1 difference lies in：Green compact thickness is 500 μm.
Experimental group 5
The experimental group and experimental group 2 difference lies in：Ceramic powder selects magnesia.
Experimental group 6
The experimental group and experimental group 2 difference lies in：Ceramic powder selects zirconium oxide.
For above-mentioned experimental group 1-6, test obtains thickness of insulating layer, the breakdown voltage (60s) of insulating layer of product, and
In micro- Microscopic observation insulating layer.As a result see the table below：
As seen from the above table, the breakdown voltage of insulating layer 1 can reach 1800-4000V, and surface is smooth without reticulate pattern.It is right
Understand that with the increase of green compact thickness, thickness of insulating layer increases therewith, and breakdown voltage also improves therewith than experimental group 1-4；Contrast
Experimental group 2,5,6 is understood, when ceramic powder selects aluminium oxide or zirconium oxide, magnesia is selected compared to ceramic powder, insulating layer
Breakdown voltage higher, and ceramic powder selects zirconium oxide more excellent.
Further it is provided that one uses the contrast groups of silk-screen printing technique：
Stainless steel substrate insulating layer is made using silk-screen printing technique, prints and is sintered, by this circulating repetition four times.
The ratio of insulating layer covering substrate surface area is 80%, and final thickness is 80 μm, and breakdown voltage 1600V, micro- Microscopic observation has
There is the gradient on reticulate pattern, border.
Knowable to experimental group and contrast groups are contrasted, the manufacturer of stainless steel based insulation component provided by the present invention
Method, can disposably complete, and production efficiency is high.And the smooth fine and close nothing of obtained stainless steel based insulation component surface of insulating layer
Reticulate pattern, border is without the gradient；Insulating layer coverage rate can reach 100%, its breakdown voltage can reach 1800-4000V.
Claims (10)
1. a kind of manufacture method of stainless steel based insulation component, including dielectric paste and stainless steel substrate, the medium slurry are provided
Material includes glass dust and ceramic powder；It is characterized in that：Green compact are made through casting technique in the dielectric paste, the green compact are pasted
The surface for overlaying on the stainless steel substrate obtains component to be sintered；To it be obtained after the component sinter molding to be sintered required
Stainless steel based insulation component, the stainless steel based insulation component include stainless steel substrate and the insulation for being covered in stainless steel substrate surface
Layer.
2. the manufacture method of stainless steel based insulation component as claimed in claim 1, it is characterised in that：The glass dust with it is described
The difference of the thermal coefficient of expansion of stainless steel substrate is less than 6 × 10-6/℃。
3. the manufacture method of stainless steel based insulation component as claimed in claim 1, it is characterised in that：The ceramic powder includes oxygen
Change the one or more in aluminium, magnesia, zirconium oxide, silica.
4. the manufacture method of stainless steel based insulation component as claimed in claim 1, it is characterised in that：The thickness of the green compact is
50-500μm。
5. the manufacture method of the stainless steel based insulation component as described in claim any one of 1-4, it is characterised in that：The burning
Knot use is once sintered, and sintering temperature is 600-1000 DEG C.
6. a kind of stainless steel based insulation component, including stainless steel substrate and the insulating layer for being covered in stainless steel substrate surface, it is special
Sign is：The insulating layer is that the green sintering formed by casting technique is made.
7. stainless steel based insulation component as claimed in claim 6, it is characterised in that：The smooth densification of surface of insulating layer, side
The face gradient is less than 5 °.
8. stainless steel based insulation component as claimed in claim 6, it is characterised in that：The coverage rate of the insulating layer is 85-
100%.
9. the stainless steel based insulation component as described in claim 6 or 7 or 8, it is characterised in that：The thickness of insulating layer is 28-
268μm。
10. stainless steel based insulation component as claimed in claim 9, it is characterised in that：The breakdown voltage of the insulating layer is
1800-4000V。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711311391.9A CN107910142A (en) | 2017-12-11 | 2017-12-11 | A kind of stainless steel based insulation component and its manufacture method |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711311391.9A CN107910142A (en) | 2017-12-11 | 2017-12-11 | A kind of stainless steel based insulation component and its manufacture method |
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| CN107910142A true CN107910142A (en) | 2018-04-13 |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1870838A (en) * | 2006-04-29 | 2006-11-29 | 吴胜红 | Electronic media material on high power stainless steel plate and its preparation method |
| CN104557100A (en) * | 2013-10-25 | 2015-04-29 | 深圳光启创新技术有限公司 | Method for pressing cast sheet on ceramic substrate and component obtained therefrom |
| CN105472791A (en) * | 2015-12-23 | 2016-04-06 | 东莞珂洛赫慕电子材料科技有限公司 | Rare earth-doped semiconductor infrared radiation thick-film electronic paste and preparation method therefor |
-
2017
- 2017-12-11 CN CN201711311391.9A patent/CN107910142A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1870838A (en) * | 2006-04-29 | 2006-11-29 | 吴胜红 | Electronic media material on high power stainless steel plate and its preparation method |
| CN104557100A (en) * | 2013-10-25 | 2015-04-29 | 深圳光启创新技术有限公司 | Method for pressing cast sheet on ceramic substrate and component obtained therefrom |
| CN105472791A (en) * | 2015-12-23 | 2016-04-06 | 东莞珂洛赫慕电子材料科技有限公司 | Rare earth-doped semiconductor infrared radiation thick-film electronic paste and preparation method therefor |
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Application publication date: 20180413 |