CN107904997A - A kind of levelling agent and preparation method thereof - Google Patents
A kind of levelling agent and preparation method thereof Download PDFInfo
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- CN107904997A CN107904997A CN201711320162.3A CN201711320162A CN107904997A CN 107904997 A CN107904997 A CN 107904997A CN 201711320162 A CN201711320162 A CN 201711320162A CN 107904997 A CN107904997 A CN 107904997A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
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- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
- D06P1/5207—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
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- D06P1/5228—Polyalkenyl alcohols, e.g. PVA
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- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/62—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
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- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
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- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
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- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
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- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
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- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
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- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67391—Salts or oxidising-compounds mixtures
Abstract
The present invention provides a kind of levelling agent and preparation method thereof.It is made of following steps：（1）By hydromica, galapectite, talcum powder, sodium bentonite and isopropanol mixed grinding；（2）It is eluted with water, is dried after filtering；（3）200 mesh sieves are crossed, remove bulky grain；（4）With prodan, Sodium Caseinate, sodium selenate, sodium ferulate, xylitol, deionized water mixing, heating stirring reaction；（5）It is put into centrifuge and is centrifuged, abandoning supernatant；（6）Add spherical nano TiO 2, NaLS, polyvinyl alcohol, N methyl pyrrolidones, stearoyl lactate, diacetyl tartarate monoglyceride, fatty alcohol polyoxyethylene ether, Java Cananga Oil and remaining deionized water, high-speed stirred to obtain the final product.The levelling agent of the present invention is uniform for textile dyeing, and even dyeing effect is good, does, fastness to wet rubbing grade height, while washes and be basically unchanged color, not staining, and washing fastness is also very high.
Description
Technical field
The present invention relates to textile material field, and in particular to a kind of levelling agent and preparation method thereof.
Background technology
Textile auxiliary is most important to the surcharge for improving textile, can not only make functions of textile fabrics, Er Qieke
Make that its is superior, more sense of the times, but to have the advantages that these premise is that the dyeing of fabric wants even, generally all can be by even
Stain is realized.Most of levelling agent is water miscible surfactant, according to levelling agent to dyestuff diffusion and the shadow of concentration class
Ring, be broadly divided into two types：One kind is close fibroid levelling agent, its concentration class to dyestuff has little to no effect, but to fibre
The affinity of dimension is greater than affinity of the dyestuff to fiber, therefore such levelling agent can be combined first with fiber in dyeing course,
Dyestuff dyeing rate is reduced, this kind of levelling agent only has the function that slow dye；Another kind is the dye levelling agent of parent, it can be notable
Dye aggregation degree is improved, affinity of the dyestuff to fiber is more than to the affinity of dyestuff, such dyestuff, which has slow dye and moves dye, to be made
With.But the shortcomings that this two classes levelling agent is poor to different types of dyestuff applicability, is had to the light fastness of dyeing
Harmful effect, and price is also higher.Thus develop with function admirable new levelling agent to improve textile dyeing quality,
Dyeing cost is reduced to be of great significance.
The content of the invention
Technical problems to be solved：It is uniform for textile dyeing the object of the present invention is to provide a kind of levelling agent, level dyeing effect
Fruit is good, does, fastness to wet rubbing grade height, while washes and be basically unchanged color, not staining, and washing fastness is also very high.
Technical solution：A kind of levelling agent, is prepared by following component with parts by weight：2-5 parts of hydromica, ball shaped nano two
1-2 parts of titanium oxide, 2-5 parts of galapectite, 2-5 parts of sodium bentonite, 2-5 parts of prodan, 2-5 parts of Sodium Caseinate, sodium selenate 2-4
Part, 1-2 parts of sodium ferulate, 2-4 parts of NaLS, 1-2 parts of talcum powder, 3-6 parts of polyvinyl alcohol, 2-4 parts of xylitol, N- first
1-2 parts of base pyrrolidones, 3-7 parts of diacetyl tartarate monoglyceride, 2-5 parts of stearoyl lactate, 3-6 parts of Java Cananga Oil, isopropyl
4-8 parts of alcohol, 150-250 parts of deionized water.
It is further preferred that a kind of levelling agent, is prepared by following component with parts by weight：3.5 parts of hydromica,
1.5 parts of spherical nano TiO 2,3.5 parts of galapectite, 3.5 parts of sodium bentonite, 3.5 parts of prodan, Sodium Caseinate 3.5
Part, 3 parts of sodium selenate, 1.5 parts of sodium ferulate, 3 parts of NaLS, 1.5 parts of talcum powder, 4.5 parts of polyvinyl alcohol, xylitol 3
Part, 1.5 parts of 1-methyl-2-pyrrolidinone, 5 parts of diacetyl tartarate monoglyceride, 3.5 parts of stearoyl lactate, 4.5 parts of Java Cananga Oil,
6 parts of isopropanol, 200 parts of deionized water.
The preparation method of above-mentioned levelling agent comprises the following steps：
（1）By hydromica, galapectite, talcum powder, sodium bentonite and isopropanol mix, with grinder grinding 10-12 it is small when；
（2）It is eluted with water, is put into after filtering in baking oven and is dried at 90-100 DEG C of temperature；
（3）200 mesh sieves are crossed, remove bulky grain；
（4）With prodan, Sodium Caseinate, sodium selenate, sodium ferulate, xylitol, 100-150 parts of deionized water mixing, heating
To 70-80 DEG C stirring reaction 2-3 it is small when；
（5）It is put into centrifuge and is centrifuged, abandoning supernatant；
（6）Add spherical nano TiO 2, NaLS, polyvinyl alcohol, 1-methyl-2-pyrrolidinone, stearoyl lactylates
Sodium, diacetyl tartarate monoglyceride, fatty alcohol polyoxyethylene ether, Java Cananga Oil and remaining deionized water, 20-30 points of high-speed stirred
Clock to obtain the final product.
It is further preferred that step（1）When middle milling time is 11 small.
It is further preferred that step（4）In be heated to 75 DEG C, the reaction time for 2.5 it is small when.
It is further preferred that step（6）High speed mixing time is 25 minutes.
Beneficial effect：The levelling agent of the present invention is uniform for textile dyeing, and even dyeing effect is good, dry fastness grade highest
Up to 5 grades, fastness to wet rubbing is also at 5 grades, while washing is basically unchanged color, not staining, and washing fastness highest is also all up to 5
Level.
Embodiment
Embodiment 1
A kind of levelling agent, is prepared by following component with parts by weight：2 parts of hydromica, 1 part of spherical nano TiO 2, Ai Luo
2 parts of stone, 2 parts of sodium bentonite, 2 parts of prodan, 2 parts of Sodium Caseinate, 2 parts of sodium selenate, 1 part of sodium ferulate, lauryl sulfate
2 parts of sodium, 1 part of talcum powder, 3 parts of polyvinyl alcohol, 2 parts of xylitol, 1 part of 1-methyl-2-pyrrolidinone, diacetyl tartarate monoglyceride 3
Part, 2 parts of stearoyl lactate, 3 parts of Java Cananga Oil, 4 parts of isopropanol, 150 parts of deionized water.
The preparation method of above-mentioned levelling agent is：
（1）By hydromica, galapectite, talcum powder, sodium bentonite and isopropanol mix, with grinder grinding 10 it is small when；
（2）It is eluted with water, is put into after filtering in baking oven and is dried at 90 DEG C of temperature；
（3）200 mesh sieves are crossed, remove bulky grain；
（4）With prodan, Sodium Caseinate, sodium selenate, sodium ferulate, xylitol, 100 parts of deionized water mixing, 70 are heated to
DEG C stirring reaction 2 it is small when；
（5）It is put into centrifuge and is centrifuged, abandoning supernatant；
（6）Add spherical nano TiO 2, NaLS, polyvinyl alcohol, 1-methyl-2-pyrrolidinone, stearoyl lactylates
Sodium, diacetyl tartarate monoglyceride, fatty alcohol polyoxyethylene ether, Java Cananga Oil and remaining deionized water, high-speed stirred 20 minutes
To obtain the final product.
Embodiment 2
A kind of levelling agent, is prepared by following component with parts by weight：3 parts of hydromica, spherical nano TiO 2 1.2 part, angstrom
3 parts of Lip river stone, 3 parts of sodium bentonite, 3 parts of prodan, 3 parts of Sodium Caseinate, 2.5 parts of sodium selenate, 1.5 parts of sodium ferulate, bay
3 parts of base sodium sulphate, 1.5 parts of talcum powder, 4 parts of polyvinyl alcohol, 2.5 parts of xylitol, 1.5 parts of 1-methyl-2-pyrrolidinone, biacetyl wine
4 parts of stone acid monoglyceride, 3 parts of stearoyl lactate, 4 parts of Java Cananga Oil, 5 parts of isopropanol, 200 parts of deionized water.
The preparation method of above-mentioned levelling agent is：
（1）By hydromica, galapectite, talcum powder, sodium bentonite and isopropanol mix, with grinder grinding 11 it is small when；
（2）It is eluted with water, is put into after filtering in baking oven and is dried at 95 DEG C of temperature；
（3）200 mesh sieves are crossed, remove bulky grain；
（4）With prodan, Sodium Caseinate, sodium selenate, sodium ferulate, xylitol, 120 parts of deionized water mixing, 75 are heated to
DEG C stirring reaction 2-3 it is small when；
（5）It is put into centrifuge and is centrifuged, abandoning supernatant；
（6）Add spherical nano TiO 2, NaLS, polyvinyl alcohol, 1-methyl-2-pyrrolidinone, stearoyl lactylates
Sodium, diacetyl tartarate monoglyceride, fatty alcohol polyoxyethylene ether, Java Cananga Oil and remaining deionized water, high-speed stirred 25 minutes
To obtain the final product.
Embodiment 3
A kind of levelling agent, is prepared by following component with parts by weight：3.5 parts of hydromica, 1.5 parts of spherical nano TiO 2,
3.5 parts of galapectite, 3.5 parts of sodium bentonite, 3.5 parts of prodan, 3.5 parts of Sodium Caseinate, 3 parts of sodium selenate, sodium ferulate 1.5
It is part, 3 parts of NaLS, 1.5 parts of talcum powder, 4.5 parts of polyvinyl alcohol, 3 parts of xylitol, 1.5 parts of 1-methyl-2-pyrrolidinone, double
5 parts of acetyltartaric acid monoglyceride, 3.5 parts of stearoyl lactate, 4.5 parts of Java Cananga Oil, 6 parts of isopropanol, 200 parts of deionized water.
The preparation method of above-mentioned levelling agent is：
（1）By hydromica, galapectite, talcum powder, sodium bentonite and isopropanol mix, with grinder grinding 11 it is small when；
（2）It is eluted with water, is put into after filtering in baking oven and is dried at 95 DEG C of temperature；
（3）200 mesh sieves are crossed, remove bulky grain；
（4）With prodan, Sodium Caseinate, sodium selenate, sodium ferulate, xylitol, 120 parts of deionized water mixing, 75 are heated to
DEG C stirring reaction 2.5 it is small when；
（5）It is put into centrifuge and is centrifuged, abandoning supernatant；
（6）Add spherical nano TiO 2, NaLS, polyvinyl alcohol, 1-methyl-2-pyrrolidinone, stearoyl lactylates
Sodium, diacetyl tartarate monoglyceride, fatty alcohol polyoxyethylene ether, Java Cananga Oil and remaining deionized water, high-speed stirred 25 minutes
To obtain the final product.
Embodiment 4
A kind of levelling agent, is prepared by following component with parts by weight：4 parts of hydromica, spherical nano TiO 2 1.5 part, angstrom
4 parts of Lip river stone, 4 parts of sodium bentonite, 4 parts of prodan, 4 parts of Sodium Caseinate, 3.5 parts of sodium selenate, 1.5 parts of sodium ferulate, bay
3.5 parts of base sodium sulphate, 1.5 parts of talcum powder, 5 parts of polyvinyl alcohol, 3.5 parts of xylitol, 1.5 parts of 1-methyl-2-pyrrolidinone, biacetyl
6 parts of tartaric esters of monoglycerides, 4 parts of stearoyl lactate, 5 parts of Java Cananga Oil, 7 parts of isopropanol, 200 parts of deionized water.
The preparation method of above-mentioned levelling agent is：
（1）By hydromica, galapectite, talcum powder, sodium bentonite and isopropanol mix, with grinder grinding 11 it is small when；
（2）It is eluted with water, is put into after filtering in baking oven and is dried at 95 DEG C of temperature；
（3）200 mesh sieves are crossed, remove bulky grain；
（4）With prodan, Sodium Caseinate, sodium selenate, sodium ferulate, xylitol, 140 parts of deionized water mixing, 75 are heated to
DEG C stirring reaction 2.5 it is small when；
（5）It is put into centrifuge and is centrifuged, abandoning supernatant；
（6）Add spherical nano TiO 2, NaLS, polyvinyl alcohol, 1-methyl-2-pyrrolidinone, stearoyl lactylates
Sodium, diacetyl tartarate monoglyceride, fatty alcohol polyoxyethylene ether, Java Cananga Oil and remaining deionized water, high-speed stirred 25 minutes
To obtain the final product.
Embodiment 5
A kind of levelling agent, is prepared by following component with parts by weight：5 parts of hydromica, 2 parts of spherical nano TiO 2, Ai Luo
5 parts of stone, 5 parts of sodium bentonite, 5 parts of prodan, 5 parts of Sodium Caseinate, 4 parts of sodium selenate, 2 parts of sodium ferulate, lauryl sulfate
4 parts of sodium, 2 parts of talcum powder, 6 parts of polyvinyl alcohol, 4 parts of xylitol, 2 parts of 1-methyl-2-pyrrolidinone, diacetyl tartarate monoglyceride 7
Part, 5 parts of stearoyl lactate, 6 parts of Java Cananga Oil, 8 parts of isopropanol, 250 parts of deionized water.
The preparation method of above-mentioned levelling agent is：
（1）By hydromica, galapectite, talcum powder, sodium bentonite and isopropanol mix, with grinder grinding 12 it is small when；
（2）It is eluted with water, is put into after filtering in baking oven and is dried at 100 DEG C of temperature；
（3）200 mesh sieves are crossed, remove bulky grain；
（4）With prodan, Sodium Caseinate, sodium selenate, sodium ferulate, xylitol, 150 parts of deionized water mixing, 80 are heated to
DEG C stirring reaction 3 it is small when；
（5）It is put into centrifuge and is centrifuged, abandoning supernatant；
（6）Add spherical nano TiO 2, NaLS, polyvinyl alcohol, 1-methyl-2-pyrrolidinone, stearoyl lactylates
Sodium, diacetyl tartarate monoglyceride, fatty alcohol polyoxyethylene ether, Java Cananga Oil and remaining deionized water, high-speed stirred 30 minutes
To obtain the final product.
Comparative example 1
Difference lies in do not contain hydromica and galapectite with embodiment 1 for the present embodiment.Specifically：
A kind of levelling agent, is prepared by following component with parts by weight：1 part of spherical nano TiO 2,2 parts of sodium bentonite,
2 parts of prodan, 2 parts of Sodium Caseinate, 2 parts of sodium selenate, 1 part of sodium ferulate, 2 parts of NaLS, 1 part of talcum powder, poly- second
3 parts of enol, 2 parts of xylitol, 1 part of 1-methyl-2-pyrrolidinone, 3 parts of diacetyl tartarate monoglyceride, 2 parts of stearoyl lactate,
3 parts of Java Cananga Oil, 4 parts of isopropanol, 150 parts of deionized water.
The preparation method of above-mentioned levelling agent is：
（1）By talcum powder, sodium bentonite and isopropanol mix, with grinder grinding 10 it is small when；
（2）It is eluted with water, is put into after filtering in baking oven and is dried at 90 DEG C of temperature；
（3）200 mesh sieves are crossed, remove bulky grain；
（4）With prodan, Sodium Caseinate, sodium selenate, sodium ferulate, xylitol, 100 parts of deionized water mixing, 70 are heated to
DEG C stirring reaction 2 it is small when；
（5）It is put into centrifuge and is centrifuged, abandoning supernatant；
（6）Add spherical nano TiO 2, NaLS, polyvinyl alcohol, 1-methyl-2-pyrrolidinone, stearoyl lactylates
Sodium, diacetyl tartarate monoglyceride, fatty alcohol polyoxyethylene ether, Java Cananga Oil and remaining deionized water, high-speed stirred 20 minutes
To obtain the final product.
Comparative example 2
Difference lies in do not contain diacetyl tartarate monoglyceride and stearoyl lactate with embodiment 5 for the present embodiment.Specifically
Ground, which is said, is：
A kind of levelling agent, is prepared by following component with parts by weight：2 parts of hydromica, 1 part of spherical nano TiO 2, Ai Luo
2 parts of stone, 2 parts of sodium bentonite, 2 parts of prodan, 2 parts of Sodium Caseinate, 2 parts of sodium selenate, 1 part of sodium ferulate, lauryl sulfate
2 parts of sodium, 1 part of talcum powder, 3 parts of polyvinyl alcohol, 2 parts of xylitol, 1 part of 1-methyl-2-pyrrolidinone, 3 parts of Java Cananga Oil, 4 parts of isopropanol,
150 parts of deionized water.
The preparation method of above-mentioned levelling agent is：
（1）By hydromica, galapectite, talcum powder, sodium bentonite and isopropanol mix, with grinder grinding 10 it is small when；
（2）It is eluted with water, is put into after filtering in baking oven and is dried at 90 DEG C of temperature；
（3）200 mesh sieves are crossed, remove bulky grain；
（4）With prodan, Sodium Caseinate, sodium selenate, sodium ferulate, xylitol, 100 parts of deionized water mixing, 70 are heated to
DEG C stirring reaction 2 it is small when；
（5）It is put into centrifuge and is centrifuged, abandoning supernatant；
（6）Add spherical nano TiO 2, NaLS, polyvinyl alcohol, 1-methyl-2-pyrrolidinone, fatty alcohol polyoxy second
Alkene ether, Java Cananga Oil and remaining deionized water, high-speed stirred 20 minutes to obtain the final product.
The embodiment of material of the present invention and the partial properties index of comparative example see the table below, it will be seen that material of the present invention
Material is uniform for textile dyeing, and even dyeing effect is good, and dry fastness grade reaches as high as 5 grades, and fastness to wet rubbing is also at 5 grades, together
Shi Shuixi is basically unchanged color, not staining, and washing fastness highest is also all up to 5 grades.
The partial properties index of 1 levelling agent of table
Note：Above-mentioned performance indicator measures after carrying out normal dyeing technique to fabric for this product.
Claims (6)
- A kind of 1. levelling agent, it is characterised in that：It is prepared by following component with parts by weight：2-5 parts of hydromica, ball shaped nano two 1-2 parts of titanium oxide, 2-5 parts of galapectite, 2-5 parts of sodium bentonite, 2-5 parts of prodan, 2-5 parts of Sodium Caseinate, sodium selenate 2-4 Part, 1-2 parts of sodium ferulate, 2-4 parts of NaLS, 1-2 parts of talcum powder, 3-6 parts of polyvinyl alcohol, 2-4 parts of xylitol, N- first 1-2 parts of base pyrrolidones, 3-7 parts of diacetyl tartarate monoglyceride, 2-5 parts of stearoyl lactate, 3-6 parts of Java Cananga Oil, isopropyl 4-8 parts of alcohol, 150-250 parts of deionized water.
- A kind of 2. levelling agent according to claim 1, it is characterised in that：It is prepared by following component with parts by weight：Water 3.5 parts of mica, 1.5 parts of spherical nano TiO 2,3.5 parts of galapectite, 3.5 parts of sodium bentonite, 3.5 parts of prodan, junket 3.5 parts of protein acid sodium, 3 parts of sodium selenate, 1.5 parts of sodium ferulate, 3 parts of NaLS, 1.5 parts of talcum powder, polyvinyl alcohol 4.5 Part, 3 parts of xylitol, 1.5 parts of 1-methyl-2-pyrrolidinone, 5 parts of diacetyl tartarate monoglyceride, 3.5 parts of stearoyl lactate, according to Blue 4.5 parts of oil, 6 parts of isopropanol, 200 parts of deionized water.
- A kind of 3. preparation method of levelling agent of claim 1 to 2 any one of them, it is characterised in that：Comprise the following steps：（1）By hydromica, galapectite, talcum powder, sodium bentonite and isopropanol mix, with grinder grinding 10-12 it is small when；（2）It is eluted with water, is put into after filtering in baking oven and is dried at 90-100 DEG C of temperature；（3）200 mesh sieves are crossed, remove bulky grain；（4）With prodan, Sodium Caseinate, sodium selenate, sodium ferulate, xylitol, 100-150 parts of deionized water mixing, heating To 70-80 DEG C stirring reaction 2-3 it is small when；（5）It is put into centrifuge and is centrifuged, abandoning supernatant；（6）Add spherical nano TiO 2, NaLS, polyvinyl alcohol, 1-methyl-2-pyrrolidinone, stearoyl lactylates Sodium, diacetyl tartarate monoglyceride, fatty alcohol polyoxyethylene ether, Java Cananga Oil and remaining deionized water, 20-30 points of high-speed stirred Clock to obtain the final product.
- A kind of 4. preparation method of levelling agent according to claim 3, it is characterised in that：The step（1）During middle grinding Between for 11 it is small when.
- A kind of 5. preparation method of levelling agent according to claim 3, it is characterised in that：The step（4）In be heated to 75 DEG C, when the reaction time is 2.5 small.
- A kind of 6. preparation method of levelling agent according to claim 3, it is characterised in that：The step（6）High speed is stirred The time is mixed as 25 minutes.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108842479A (en) * | 2018-06-02 | 2018-11-20 | 叶建民 | A kind of preparation method of environmental protection type crucian seed levelling agent |
| CN112012027A (en) * | 2020-09-09 | 2020-12-01 | 吴江德伊时装面料有限公司 | Method for dyeing cellulose acetate fiber fabric |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106049106A (en) * | 2016-07-01 | 2016-10-26 | 潘明华 | Montmorillonite uniform-dyeing agent and preparation method thereof |
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Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106049106A (en) * | 2016-07-01 | 2016-10-26 | 潘明华 | Montmorillonite uniform-dyeing agent and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108842479A (en) * | 2018-06-02 | 2018-11-20 | 叶建民 | A kind of preparation method of environmental protection type crucian seed levelling agent |
| CN112012027A (en) * | 2020-09-09 | 2020-12-01 | 吴江德伊时装面料有限公司 | Method for dyeing cellulose acetate fiber fabric |
| CN112012027B (en) * | 2020-09-09 | 2023-10-24 | 吴江德伊时装面料有限公司 | Dyeing method of acetate cellulose fiber fabric |
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Application publication date: 20180413 |