CN107904934A - A kind of preparation method embroidered with resistance to finishing agent of soaping - Google Patents
A kind of preparation method embroidered with resistance to finishing agent of soaping Download PDFInfo
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- CN107904934A CN107904934A CN201711239191.7A CN201711239191A CN107904934A CN 107904934 A CN107904934 A CN 107904934A CN 201711239191 A CN201711239191 A CN 201711239191A CN 107904934 A CN107904934 A CN 107904934A
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- Prior art keywords
- parts
- resistance
- soaping
- good
- finishing agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims abstract description 48
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 18
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000012153 distilled water Substances 0.000 claims abstract description 17
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 claims abstract description 16
- 229960001763 zinc sulfate Drugs 0.000 claims abstract description 16
- 229910000368 zinc sulfate Inorganic materials 0.000 claims abstract description 16
- 229940046892 lead acetate Drugs 0.000 claims abstract description 15
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 claims abstract description 14
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 claims abstract description 14
- SNRUBQQJIBEYMU-UHFFFAOYSA-N Dodecane Natural products CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 claims abstract description 12
- QNAYBMKLOCPYGJ-REOHCLBHSA-N L-alanine Chemical compound C[C@H](N)C(O)=O QNAYBMKLOCPYGJ-REOHCLBHSA-N 0.000 claims abstract description 12
- 235000004279 alanine Nutrition 0.000 claims abstract description 12
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims abstract description 12
- 229920000151 polyglycol Polymers 0.000 claims abstract description 12
- 239000010695 polyglycol Substances 0.000 claims abstract description 12
- 241001116389 Aloe Species 0.000 claims abstract description 11
- 235000011399 aloe vera Nutrition 0.000 claims abstract description 11
- 239000000945 filler Substances 0.000 claims abstract description 11
- 239000000835 fiber Substances 0.000 claims abstract description 10
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 9
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 9
- 238000002156 mixing Methods 0.000 claims description 17
- 238000010792 warming Methods 0.000 claims description 10
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 6
- NKWPZUCBCARRDP-UHFFFAOYSA-L calcium bicarbonate Chemical compound [Ca+2].OC([O-])=O.OC([O-])=O NKWPZUCBCARRDP-UHFFFAOYSA-L 0.000 claims description 5
- 229910000020 calcium bicarbonate Inorganic materials 0.000 claims description 5
- 239000012467 final product Substances 0.000 claims description 5
- 238000000227 grinding Methods 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- PQUXFUBNSYCQAL-UHFFFAOYSA-N 1-(2,3-difluorophenyl)ethanone Chemical compound CC(=O)C1=CC=CC(F)=C1F PQUXFUBNSYCQAL-UHFFFAOYSA-N 0.000 claims 3
- 229940047670 sodium acrylate Drugs 0.000 claims 3
- 230000000694 effects Effects 0.000 abstract description 8
- 239000000344 soap Substances 0.000 abstract description 7
- 239000000463 material Substances 0.000 abstract description 6
- 241000588724 Escherichia coli Species 0.000 abstract description 5
- 238000005299 abrasion Methods 0.000 abstract description 5
- 230000000845 anti-microbial effect Effects 0.000 abstract description 5
- 238000005260 corrosion Methods 0.000 abstract description 5
- 230000007797 corrosion Effects 0.000 abstract description 5
- 238000001035 drying Methods 0.000 abstract description 5
- 230000035699 permeability Effects 0.000 abstract description 5
- 231100000614 poison Toxicity 0.000 abstract description 5
- 239000003440 toxic substance Substances 0.000 abstract description 5
- 230000037303 wrinkles Effects 0.000 abstract description 5
- -1 lead acetate Chemical compound 0.000 abstract 1
- 238000009956 embroidering Methods 0.000 description 3
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 3
- 235000002991 Coptis groenlandica Nutrition 0.000 description 2
- 244000247747 Coptis groenlandica Species 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 238000005034 decoration Methods 0.000 description 2
- 150000002085 enols Chemical class 0.000 description 2
- 238000010417 needlework Methods 0.000 description 2
- 238000010422 painting Methods 0.000 description 2
- 241000272814 Anser sp. Species 0.000 description 1
- 241000271566 Aves Species 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 241000282836 Camelus dromedarius Species 0.000 description 1
- 241000282994 Cervidae Species 0.000 description 1
- 241000579895 Chlorostilbon Species 0.000 description 1
- 206010059866 Drug resistance Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- IMROMDMJAWUWLK-UHFFFAOYSA-N Ethenol Chemical compound OC=C IMROMDMJAWUWLK-UHFFFAOYSA-N 0.000 description 1
- 241000287828 Gallus gallus Species 0.000 description 1
- 241000288140 Gruiformes Species 0.000 description 1
- 240000005001 Paeonia suffruticosa Species 0.000 description 1
- 235000003889 Paeonia suffruticosa Nutrition 0.000 description 1
- 241000233805 Phoenix Species 0.000 description 1
- 235000014676 Phragmites communis Nutrition 0.000 description 1
- 235000008331 Pinus X rigitaeda Nutrition 0.000 description 1
- 235000011613 Pinus brutia Nutrition 0.000 description 1
- 241000018646 Pinus brutia Species 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 208000002173 dizziness Diseases 0.000 description 1
- 229910052876 emerald Inorganic materials 0.000 description 1
- 239000010976 emerald Substances 0.000 description 1
- 230000000855 fungicidal effect Effects 0.000 description 1
- 239000000417 fungicide Substances 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000009940 knitting Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000001937 non-anti-biotic effect Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000000306 recurrent effect Effects 0.000 description 1
- 238000009877 rendering Methods 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/51—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof
- D06M11/55—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof with sulfur trioxide; with sulfuric acid or thiosulfuric acid or their salts
- D06M11/56—Sulfates or thiosulfates other than of elements of Groups 3 or 13 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
- D06M11/76—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon oxides or carbonates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/144—Alcohols; Metal alcoholates
- D06M13/148—Polyalcohols, e.g. glycerol or glucose
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/325—Amines
- D06M13/342—Amino-carboxylic acids; Betaines; Aminosulfonic acids; Sulfo-betaines
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/327—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof
- D06M15/333—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof of vinyl acetate; Polyvinylalcohol
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/20—Treatment influencing the crease behaviour, the wrinkle resistance, the crease recovery or the ironing ease
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/30—Flame or heat resistance, fire retardancy properties
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
Abstract
This application discloses a kind of preparation method embroidered with resistance to finishing agent of soaping, distilled water, butyl acetate, filler, lead acetate, ethylene glycol, polyvinyl alcohol, seven polyglycol ether of dodecyl, alanine, Sodium Polyacrylate, zinc sulfate and aloe fibre are weighed;Preparation method is simple, and anti-mold effect is good, and 3.5 5.5MPa of tensile strength, resistance to moisture is excellent, of low cost;Removing toxic substances, bright, increase gloss, adhesion 1 grade, adhesion strength height, good corrosion resistance, abrasion resistance 400 500 times, component safety;Wrinkle resistance is good, and 65 85 acarids of water-wash resistance walk quickly and keep away rate 93.5 97.5%, and pliability 1mm, glossiness is good, good permeability;It is resistance to soap, extend embroidery service life, fast drying, fire resistance is good, and anti-microbial property is good, to Escherichia coli bacteriostasis rate 99.4 99.8%, can extensively produce and constantly replace current material.
Description
Technical field
The application belongs to embroidery material field, more particularly to a kind of preparation method embroidered with resistance to finishing agent of soaping.
Background technology
The Tang Dynasty embroidery application is very wide, and the skill of handling needles also has new development.Embroidery is typically used as the decoration of haberdashery, workmanship essence
Ingeniously, color is magnificent, has all reflected in the document and poetic prose of the Tang Dynasty.Such as li po's poem " emerald gold thread, embroider into song and dance clothing ", in vain
Easy poem " red building rich family female, gold thread thorn sieve short jacket " etc. is occupied, is all to chant song for embroidery.The embroidery of the Tang Dynasty is except as haberdashery
Outside, embroidery Buddhist sutra and the figure of buddha are additionally operable to, is religious services.The skill of handling needles of the Tang Dynasty embroidery, except having been embroidered with pigtail traditional since the Warring states
Outside, additionally use plain embroidery, get a variety of skill of handling needles such as embroidery, numerous pleat embroidery ready.Numerous pleat is embroidered and also known as moves back dizzy embroidery, i.e., the needlework in an opposite direction alleged by modern times.
It can show the different color ranges that there is the depth to change, and make the object color of description splendid, have dense decoration
Effect.
The general name of In Guangdong Province needlework.Initially originate according to legend in ethnic group-- Li nationality, previous embroidery art is wide mostly
State, Chaozhou man, are scarce.Mainly there are the embroideries such as finery, hanging panel, long, rectangular bag, the screen heart, circular fan, fan set.Artistically, Guangdong
Embroider that composition is dense lively, and color is gorgeous brilliant, it is brief to apply pin, and embroider line is relatively thick and pine, and stitch length is irregular, the overlapping dimpling of pin line.
Often using phoenix, tree peony, crane, ape, deer and chicken, goose as subject matter.The another kind of famous-object of Guangdong embroidery be with knitting golden satin or the golden lining of nail,
Namely famous nail gold is embroidered, and the golden woolen embroidery for the high camel that is especially usually coated, even more splendid, daring is simple and honest, it is multi-purpose make stage costume,
The furnishings embroidery of stage stuff and monastery temple, is suitable for the atmosphere for rendering and warmly celebrating joyously.
Nano silver belongs to non-antibiotic fungicide, and unique Antibacterial Mechanism can directly kill rapidly bacterium, makes its forfeiture numerous
Grow ability.Therefore, it is impossible to breed the next generation, can effectively avoid causing recurrent exerbation obstinate because of drug resistance.
Anglicanum develops into Tang and Song Dynasty time and has the tens of kinds of skill of handling needles, its style has also gradually formed the difference of each region
Characteristic.Embroidery be not merely to be embroidered on dress ornament, but from the flowers and plants on dress ornament developed into pure appreciating embroidered painting,
Embroidery Buddhist sutra, embroidery figure of buddha etc..During according to passing Wu Tse-tien, once ordering to embroider more than 400 width of the figure of buddha, granting monastery and neighbouring country, thus may be used
It is very prevailing to see that the Tang Dynasty embroiders the figure of buddha.
Song Dynasty is that Chinese hand embroidering prosperity was attained to the period on peak, and no matter product quality belongs to unprecedented, is particularly opening
In terms of creating pure aesthetic artistic embroidery, more it can be rated as without offspring.The prosperity of Song Dynasty hand embroidering, since event is advocated in imperial court's reward at that time.
According to《Song's history official's will》Carry, palace Chinese is embroidered institute's palm bun and embroidered.Emblem sets embroidered picture training again between ancestor's year, embroidered picture is categorized as scenery with hills and waters, building
Pavilion, personage, birds and flowers, thus name embroidery art comes forth in large number in succession, drawing is developed to tidemark, and by practicality and then be art appreciation,
Among bringing painting and calligraphy into hand embroidering, the ornamental value embroidery of uniqueness is formed.
The content of the invention
The technical problem of solution:
The application is directed to above-mentioned technical problem, there is provided a kind of preparation method embroidered with resistance to finishing agent of soaping, solves existing embroidery
Soap that finishing agent anti-mold effect is poor, glossiness is low and intolerant to the technical problem such as soap with resistance to.
Technical solution:
A kind of preparation method embroidered with resistance to finishing agent of soaping, includes the following steps:
The first step:100 parts of distilled water, 40-50 parts of butyl acetate, 20-30 parts of filler, acetic acid are weighed according to parts by weight proportioning
0.1-0.5 parts of lead, 6-10 parts of ethylene glycol, 10-30 parts of polyvinyl alcohol, 15-35 parts of seven polyglycol ether of dodecyl, alanine
4-8 parts of 14-18 parts, 6-12 parts of Sodium Polyacrylate, 5-15 parts of zinc sulfate and aloe fibre;
Second step:Lead acetate, Sodium Polyacrylate and zinc sulfate are put into grinder and grind 10-20min, input carries after grinding
Mixer mixing is opened in the reaction kettle of thermometer, mixer and heating unit, is warming up to 80-90 DEG C, mixing velocity 280-
320r/min, mixes 2-3h;
3rd step:Ethylene glycol, distilled water and butyl acetate are sequentially added, adjusts mixing velocity to 350-450 r/min, mixing
50-90min, adds surplus stock, is warming up to 125-145 DEG C, and 10-40 DEG C is cooled to after stirring 3-5h, after crossing cleaner liquid, stands
To obtain the final product after 20-24h.
As a preferred technical solution of the present invention:Embroider in the first step with the raw material of resistance to finishing agent of soaping by weight
It is as follows to measure number proportioning:100 parts of distilled water, 40 parts of butyl acetate, 20 parts of filler, 0.1 part of lead acetate, 6 parts of ethylene glycol, poly- second
10 parts of enol, 15 parts of seven polyglycol ether of dodecyl, 14 parts of alanine, 6 parts of Sodium Polyacrylate, 5 parts of zinc sulfate and aloe are fine
4 parts of dimension.
As a preferred technical solution of the present invention:Embroider in the first step with the raw material of resistance to finishing agent of soaping by weight
It is as follows to measure number proportioning:It is 100 parts of distilled water, 50 parts of butyl acetate, 30 parts of filler, 0.5 part of lead acetate, 10 parts of ethylene glycol, poly-
30 parts of vinyl alcohol, 35 parts of seven polyglycol ether of dodecyl, 18 parts of alanine, 12 parts of Sodium Polyacrylate, 15 parts of zinc sulfate and reed
8 parts of luxuriant growth fiber.
As a preferred technical solution of the present invention:Embroider in the first step with the raw material of resistance to finishing agent of soaping by weight
It is as follows to measure number proportioning:100 parts of distilled water, 45 parts of butyl acetate, 25 parts of filler, 0.3 part of lead acetate, 8 parts of ethylene glycol, poly- second
20 parts of enol, 25 parts of seven polyglycol ether of dodecyl, 16 parts of alanine, 9 parts of Sodium Polyacrylate, 10 parts of zinc sulfate and aloe are fine
6 parts of dimension.
As a preferred technical solution of the present invention:The filler uses calcium bicarbonate.
Beneficial effect:
A kind of embroider of the present invention uses above technical scheme compared with prior art with the preparation method of resistance to finishing agent of soaping,
With following technique effect:1st, preparation method is simple, and anti-mold effect is good, and tensile strength 3.5-5.5MPa, resistance to moisture is excellent, into
This is cheap;2nd, removing toxic substances, bright, increase gloss, adhesion 1 grade, adhesion strength height, good corrosion resistance, abrasion resistance 400-500
It is secondary, component safety;3rd, wrinkle resistance is good, and 65-85 acarid of water-wash resistance walks quickly and keeps away rate 93.5-97.5%, pliability 1mm, glossiness
It is good, good permeability;4th, it is resistance to soap, extend embroidery service life, fast drying, fire resistance is good, and anti-microbial property is good, to Escherichia coli
Bacteriostasis rate 99.4-99.8%, can extensively produce and constantly replace current material.
Embodiment
Embodiment 1:
100 parts of distilled water, 40 parts of butyl acetate, 20 parts of calcium bicarbonate, 0.1 part of lead acetate, second are weighed according to parts by weight proportioning
6 parts of glycol, 10 parts of polyvinyl alcohol, 15 parts of seven polyglycol ether of dodecyl, 14 parts of alanine, 6 parts of Sodium Polyacrylate, zinc sulfate
5 parts and 4 parts of aloe fibre.
Lead acetate, Sodium Polyacrylate and zinc sulfate are put into grinder and grind 10min, input carries temperature after grinding
Mixer mixing is opened in the reaction kettle of meter, mixer and heating unit, is warming up to 80 DEG C, mixing velocity 280r/min, is mixed
Close 2h.
Ethylene glycol, distilled water and butyl acetate are sequentially added, mixing velocity is adjusted to 350r/min, mixes 50min, add
Surplus stock, is warming up to 125 DEG C, and 10 DEG C are cooled to after stirring 3h, after crossing cleaner liquid, after standing 20h to obtain the final product.
Preparation method is simple, and anti-mold effect is good, and tensile strength 3.5MPa, resistance to moisture is excellent, of low cost;Removing toxic substances, light
It is bright, increase gloss, adhesion 1 grade, adhesion strength is high, good corrosion resistance, abrasion resistance 400 times, component safety;Wrinkle resistance
Good, 65 acarids of water-wash resistance walk quickly and keep away rate 93.5%, and pliability 1mm, glossiness is good, good permeability;Resistance to soap, extending embroidery makes
Good with service life, fast drying, fire resistance, anti-microbial property is good, to Escherichia coli bacteriostasis rate 99.4%, can produce extensively and continuous
Instead of current material.
Embodiment 2:
100 parts of distilled water, 50 parts of butyl acetate, 30 parts of calcium bicarbonate, 0.5 part of lead acetate, second are weighed according to parts by weight proportioning
10 parts of glycol, 30 parts of polyvinyl alcohol, 35 parts of seven polyglycol ether of dodecyl, 18 parts of alanine, 12 parts of Sodium Polyacrylate, sulfuric acid
8 parts of 15 parts of zinc and aloe fibre.
Lead acetate, Sodium Polyacrylate and zinc sulfate are put into grinder and grind 20min, input carries temperature after grinding
Mixer mixing is opened in the reaction kettle of meter, mixer and heating unit, is warming up to 90 DEG C, mixing velocity 320r/min, is mixed
Close 3h.
Ethylene glycol, distilled water and butyl acetate are sequentially added, mixing velocity is adjusted to 450 r/min, mixes 90min, add
Enter surplus stock, be warming up to 145 DEG C, 40 DEG C are cooled to after stirring 5h, after crossing cleaner liquid, after standing 24h to obtain the final product.
Preparation method is simple, and anti-mold effect is good, and tensile strength 4.5MPa, resistance to moisture is excellent, of low cost;Removing toxic substances, light
It is bright, increase gloss, adhesion 1 grade, adhesion strength is high, good corrosion resistance, abrasion resistance 450 times, component safety;Wrinkle resistance
Good, 75 acarids of water-wash resistance walk quickly and keep away rate 95.5%, and pliability 1mm, glossiness is good, good permeability;Resistance to soap, extending embroidery makes
Good with service life, fast drying, fire resistance, anti-microbial property is good, to Escherichia coli bacteriostasis rate 99.6%, can produce extensively and continuous
Instead of current material.
Embodiment 3:
100 parts of distilled water, 45 parts of butyl acetate, 25 parts of calcium bicarbonate, 0.3 part of lead acetate, second are weighed according to parts by weight proportioning
8 parts of glycol, 20 parts of polyvinyl alcohol, 25 parts of seven polyglycol ether of dodecyl, 16 parts of alanine, 9 parts of Sodium Polyacrylate, zinc sulfate
10 parts and 6 parts of aloe fibre.
Lead acetate, Sodium Polyacrylate and zinc sulfate are put into grinder and grind 15min, input carries temperature after grinding
Mixer mixing is opened in the reaction kettle of meter, mixer and heating unit, is warming up to 85 DEG C, mixing velocity 300r/min, is mixed
Close 2.5h.
Ethylene glycol, distilled water and butyl acetate are sequentially added, mixing velocity is adjusted to 400 r/min, mixes 70min, add
Enter surplus stock, be warming up to 135 DEG C, 25 DEG C are cooled to after stirring 4h, after crossing cleaner liquid, after standing 22h to obtain the final product.
Preparation method is simple, and anti-mold effect is good, and tensile strength 5.5MPa, resistance to moisture is excellent, of low cost;Removing toxic substances, light
It is bright, increase gloss, adhesion 1 grade, adhesion strength is high, good corrosion resistance, abrasion resistance 500 times, component safety;Wrinkle resistance
Good, 85 acarids of water-wash resistance walk quickly and keep away rate 97.5%, and pliability 1mm, glossiness is good, good permeability;Resistance to soap, extending embroidery makes
Good with service life, fast drying, fire resistance, anti-microbial property is good, to Escherichia coli bacteriostasis rate 99.8%, can produce extensively and continuous
Instead of current material.
Composition all components in above example can be commercially available.
The above embodiments are merely intended to illustrate the present invention rather than to limit it, therefore with the present invention's
Any change in claims suitable implication and scope, should be construed as being included in the scope of the claims.
Claims (5)
1. a kind of preparation method embroidered with resistance to finishing agent of soaping, it is characterised in that include the following steps:
The first step:100 parts of distilled water, 40-50 parts of butyl acetate, 20-30 parts of filler, acetic acid are weighed according to parts by weight proportioning
0.1-0.5 parts of lead, 6-10 parts of ethylene glycol, 10-30 parts of polyvinyl alcohol, 15-35 parts of seven polyglycol ether of dodecyl, alanine
4-8 parts of 14-18 parts, 6-12 parts of Sodium Polyacrylate, 5-15 parts of zinc sulfate and aloe fibre;
Second step:Lead acetate, Sodium Polyacrylate and zinc sulfate are put into grinder and grind 10-20min, input carries after grinding
Mixer mixing is opened in the reaction kettle of thermometer, mixer and heating unit, is warming up to 80-90 DEG C, mixing velocity 280-
320r/min, mixes 2-3h;
3rd step:Ethylene glycol, distilled water and butyl acetate are sequentially added, adjusts mixing velocity to 350-450 r/min, mixing
50-90min, adds surplus stock, is warming up to 125-145 DEG C, and 10-40 DEG C is cooled to after stirring 3-5h, after crossing cleaner liquid, stands
To obtain the final product after 20-24h.
2. the preparation method of the resistance to finishing agent of soaping of embroidery according to claim 1, it is characterised in that:In the first step
Embroidery is as follows with the raw materials by weight portion proportioning of resistance to finishing agent of soaping:100 parts of distilled water, 40 parts of butyl acetate, filler 20
It is part, 0.1 part of lead acetate, 6 parts of ethylene glycol, 10 parts of polyvinyl alcohol, 15 parts of seven polyglycol ether of dodecyl, 14 parts of alanine, poly-
4 parts of 6 parts of sodium acrylate, 5 parts of zinc sulfate and aloe fibre.
3. the preparation method of the resistance to finishing agent of soaping of embroidery according to claim 1, it is characterised in that:In the first step
Embroidery is as follows with the raw materials by weight portion proportioning of resistance to finishing agent of soaping:100 parts of distilled water, 50 parts of butyl acetate, filler 30
It is part, 0.5 part of lead acetate, 10 parts of ethylene glycol, 30 parts of polyvinyl alcohol, 35 parts of seven polyglycol ether of dodecyl, 18 parts of alanine, poly-
8 parts of 12 parts of sodium acrylate, 15 parts of zinc sulfate and aloe fibre.
4. the preparation method of the resistance to finishing agent of soaping of embroidery according to claim 1, it is characterised in that:In the first step
Embroidery is as follows with the raw materials by weight portion proportioning of resistance to finishing agent of soaping:100 parts of distilled water, 45 parts of butyl acetate, filler 25
It is part, 0.3 part of lead acetate, 8 parts of ethylene glycol, 20 parts of polyvinyl alcohol, 25 parts of seven polyglycol ether of dodecyl, 16 parts of alanine, poly-
6 parts of 9 parts of sodium acrylate, 10 parts of zinc sulfate and aloe fibre.
5. the preparation method of the resistance to finishing agent of soaping of embroidery according to claim 1, it is characterised in that:The filler is adopted
Use calcium bicarbonate.
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Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101736616A (en) * | 2009-12-30 | 2010-06-16 | 达利(中国)有限公司 | Technology for dyeing and finishing real silk/corn fabric |
CN102586038A (en) * | 2011-12-28 | 2012-07-18 | 浙江台华新材料股份有限公司 | Fabric reductive cleaning agent with high soaping-resistant color fastness and high sublimation fastness, preparation method thereof and polyester fabric treatment method |
CN103556511A (en) * | 2013-10-25 | 2014-02-05 | 华纺股份有限公司 | Color fixative and application method thereof |
-
2017
- 2017-11-30 CN CN201711239191.7A patent/CN107904934A/en not_active Withdrawn
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101736616A (en) * | 2009-12-30 | 2010-06-16 | 达利(中国)有限公司 | Technology for dyeing and finishing real silk/corn fabric |
CN102586038A (en) * | 2011-12-28 | 2012-07-18 | 浙江台华新材料股份有限公司 | Fabric reductive cleaning agent with high soaping-resistant color fastness and high sublimation fastness, preparation method thereof and polyester fabric treatment method |
CN103556511A (en) * | 2013-10-25 | 2014-02-05 | 华纺股份有限公司 | Color fixative and application method thereof |
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Application publication date: 20180413 |