CN107904934A - A kind of preparation method embroidered with resistance to finishing agent of soaping - Google Patents

A kind of preparation method embroidered with resistance to finishing agent of soaping Download PDF

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Publication number
CN107904934A
CN107904934A CN201711239191.7A CN201711239191A CN107904934A CN 107904934 A CN107904934 A CN 107904934A CN 201711239191 A CN201711239191 A CN 201711239191A CN 107904934 A CN107904934 A CN 107904934A
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Prior art keywords
parts
resistance
soaping
good
finishing agent
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Application number
CN201711239191.7A
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王学珍
王丽佳
王月忠
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Suzhou Embroidery Art World Embroidery Technology Co Ltd
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Suzhou Embroidery Art World Embroidery Technology Co Ltd
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Priority to CN201711239191.7A priority Critical patent/CN107904934A/en
Publication of CN107904934A publication Critical patent/CN107904934A/en
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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/224Esters of carboxylic acids; Esters of carbonic acid
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/51Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof
    • D06M11/55Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof with sulfur trioxide; with sulfuric acid or thiosulfuric acid or their salts
    • D06M11/56Sulfates or thiosulfates other than of elements of Groups 3 or 13 of the Periodic Table
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/73Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
    • D06M11/76Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon oxides or carbonates
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/144Alcohols; Metal alcoholates
    • D06M13/148Polyalcohols, e.g. glycerol or glucose
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/188Monocarboxylic acids; Anhydrides, halides or salts thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/325Amines
    • D06M13/342Amino-carboxylic acids; Betaines; Aminosulfonic acids; Sulfo-betaines
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    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/263Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/327Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof
    • D06M15/333Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof of vinyl acetate; Polyvinylalcohol
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    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/53Polyethers
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    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/20Treatment influencing the crease behaviour, the wrinkle resistance, the crease recovery or the ironing ease
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/30Flame or heat resistance, fire retardancy properties

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
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Abstract

This application discloses a kind of preparation method embroidered with resistance to finishing agent of soaping, distilled water, butyl acetate, filler, lead acetate, ethylene glycol, polyvinyl alcohol, seven polyglycol ether of dodecyl, alanine, Sodium Polyacrylate, zinc sulfate and aloe fibre are weighed;Preparation method is simple, and anti-mold effect is good, and 3.5 5.5MPa of tensile strength, resistance to moisture is excellent, of low cost;Removing toxic substances, bright, increase gloss, adhesion 1 grade, adhesion strength height, good corrosion resistance, abrasion resistance 400 500 times, component safety;Wrinkle resistance is good, and 65 85 acarids of water-wash resistance walk quickly and keep away rate 93.5 97.5%, and pliability 1mm, glossiness is good, good permeability;It is resistance to soap, extend embroidery service life, fast drying, fire resistance is good, and anti-microbial property is good, to Escherichia coli bacteriostasis rate 99.4 99.8%, can extensively produce and constantly replace current material.

Description

A kind of preparation method embroidered with resistance to finishing agent of soaping
Technical field
The application belongs to embroidery material field, more particularly to a kind of preparation method embroidered with resistance to finishing agent of soaping.
Background technology
The Tang Dynasty embroidery application is very wide, and the skill of handling needles also has new development.Embroidery is typically used as the decoration of haberdashery, workmanship essence Ingeniously, color is magnificent, has all reflected in the document and poetic prose of the Tang Dynasty.Such as li po's poem " emerald gold thread, embroider into song and dance clothing ", in vain Easy poem " red building rich family female, gold thread thorn sieve short jacket " etc. is occupied, is all to chant song for embroidery.The embroidery of the Tang Dynasty is except as haberdashery Outside, embroidery Buddhist sutra and the figure of buddha are additionally operable to, is religious services.The skill of handling needles of the Tang Dynasty embroidery, except having been embroidered with pigtail traditional since the Warring states Outside, additionally use plain embroidery, get a variety of skill of handling needles such as embroidery, numerous pleat embroidery ready.Numerous pleat is embroidered and also known as moves back dizzy embroidery, i.e., the needlework in an opposite direction alleged by modern times. It can show the different color ranges that there is the depth to change, and make the object color of description splendid, have dense decoration Effect.
The general name of In Guangdong Province needlework.Initially originate according to legend in ethnic group-- Li nationality, previous embroidery art is wide mostly State, Chaozhou man, are scarce.Mainly there are the embroideries such as finery, hanging panel, long, rectangular bag, the screen heart, circular fan, fan set.Artistically, Guangdong Embroider that composition is dense lively, and color is gorgeous brilliant, it is brief to apply pin, and embroider line is relatively thick and pine, and stitch length is irregular, the overlapping dimpling of pin line. Often using phoenix, tree peony, crane, ape, deer and chicken, goose as subject matter.The another kind of famous-object of Guangdong embroidery be with knitting golden satin or the golden lining of nail, Namely famous nail gold is embroidered, and the golden woolen embroidery for the high camel that is especially usually coated, even more splendid, daring is simple and honest, it is multi-purpose make stage costume, The furnishings embroidery of stage stuff and monastery temple, is suitable for the atmosphere for rendering and warmly celebrating joyously.
Nano silver belongs to non-antibiotic fungicide, and unique Antibacterial Mechanism can directly kill rapidly bacterium, makes its forfeiture numerous Grow ability.Therefore, it is impossible to breed the next generation, can effectively avoid causing recurrent exerbation obstinate because of drug resistance.
Anglicanum develops into Tang and Song Dynasty time and has the tens of kinds of skill of handling needles, its style has also gradually formed the difference of each region Characteristic.Embroidery be not merely to be embroidered on dress ornament, but from the flowers and plants on dress ornament developed into pure appreciating embroidered painting, Embroidery Buddhist sutra, embroidery figure of buddha etc..During according to passing Wu Tse-tien, once ordering to embroider more than 400 width of the figure of buddha, granting monastery and neighbouring country, thus may be used It is very prevailing to see that the Tang Dynasty embroiders the figure of buddha.
Song Dynasty is that Chinese hand embroidering prosperity was attained to the period on peak, and no matter product quality belongs to unprecedented, is particularly opening In terms of creating pure aesthetic artistic embroidery, more it can be rated as without offspring.The prosperity of Song Dynasty hand embroidering, since event is advocated in imperial court's reward at that time. According to《Song's history official's will》Carry, palace Chinese is embroidered institute's palm bun and embroidered.Emblem sets embroidered picture training again between ancestor's year, embroidered picture is categorized as scenery with hills and waters, building Pavilion, personage, birds and flowers, thus name embroidery art comes forth in large number in succession, drawing is developed to tidemark, and by practicality and then be art appreciation, Among bringing painting and calligraphy into hand embroidering, the ornamental value embroidery of uniqueness is formed.
The content of the invention
The technical problem of solution:
The application is directed to above-mentioned technical problem, there is provided a kind of preparation method embroidered with resistance to finishing agent of soaping, solves existing embroidery Soap that finishing agent anti-mold effect is poor, glossiness is low and intolerant to the technical problem such as soap with resistance to.
Technical solution:
A kind of preparation method embroidered with resistance to finishing agent of soaping, includes the following steps:
The first step:100 parts of distilled water, 40-50 parts of butyl acetate, 20-30 parts of filler, acetic acid are weighed according to parts by weight proportioning 0.1-0.5 parts of lead, 6-10 parts of ethylene glycol, 10-30 parts of polyvinyl alcohol, 15-35 parts of seven polyglycol ether of dodecyl, alanine 4-8 parts of 14-18 parts, 6-12 parts of Sodium Polyacrylate, 5-15 parts of zinc sulfate and aloe fibre;
Second step:Lead acetate, Sodium Polyacrylate and zinc sulfate are put into grinder and grind 10-20min, input carries after grinding Mixer mixing is opened in the reaction kettle of thermometer, mixer and heating unit, is warming up to 80-90 DEG C, mixing velocity 280- 320r/min, mixes 2-3h;
3rd step:Ethylene glycol, distilled water and butyl acetate are sequentially added, adjusts mixing velocity to 350-450 r/min, mixing 50-90min, adds surplus stock, is warming up to 125-145 DEG C, and 10-40 DEG C is cooled to after stirring 3-5h, after crossing cleaner liquid, stands To obtain the final product after 20-24h.
As a preferred technical solution of the present invention:Embroider in the first step with the raw material of resistance to finishing agent of soaping by weight It is as follows to measure number proportioning:100 parts of distilled water, 40 parts of butyl acetate, 20 parts of filler, 0.1 part of lead acetate, 6 parts of ethylene glycol, poly- second 10 parts of enol, 15 parts of seven polyglycol ether of dodecyl, 14 parts of alanine, 6 parts of Sodium Polyacrylate, 5 parts of zinc sulfate and aloe are fine 4 parts of dimension.
As a preferred technical solution of the present invention:Embroider in the first step with the raw material of resistance to finishing agent of soaping by weight It is as follows to measure number proportioning:It is 100 parts of distilled water, 50 parts of butyl acetate, 30 parts of filler, 0.5 part of lead acetate, 10 parts of ethylene glycol, poly- 30 parts of vinyl alcohol, 35 parts of seven polyglycol ether of dodecyl, 18 parts of alanine, 12 parts of Sodium Polyacrylate, 15 parts of zinc sulfate and reed 8 parts of luxuriant growth fiber.
As a preferred technical solution of the present invention:Embroider in the first step with the raw material of resistance to finishing agent of soaping by weight It is as follows to measure number proportioning:100 parts of distilled water, 45 parts of butyl acetate, 25 parts of filler, 0.3 part of lead acetate, 8 parts of ethylene glycol, poly- second 20 parts of enol, 25 parts of seven polyglycol ether of dodecyl, 16 parts of alanine, 9 parts of Sodium Polyacrylate, 10 parts of zinc sulfate and aloe are fine 6 parts of dimension.
As a preferred technical solution of the present invention:The filler uses calcium bicarbonate.
Beneficial effect:
A kind of embroider of the present invention uses above technical scheme compared with prior art with the preparation method of resistance to finishing agent of soaping, With following technique effect:1st, preparation method is simple, and anti-mold effect is good, and tensile strength 3.5-5.5MPa, resistance to moisture is excellent, into This is cheap;2nd, removing toxic substances, bright, increase gloss, adhesion 1 grade, adhesion strength height, good corrosion resistance, abrasion resistance 400-500 It is secondary, component safety;3rd, wrinkle resistance is good, and 65-85 acarid of water-wash resistance walks quickly and keeps away rate 93.5-97.5%, pliability 1mm, glossiness It is good, good permeability;4th, it is resistance to soap, extend embroidery service life, fast drying, fire resistance is good, and anti-microbial property is good, to Escherichia coli Bacteriostasis rate 99.4-99.8%, can extensively produce and constantly replace current material.
Embodiment
Embodiment 1:
100 parts of distilled water, 40 parts of butyl acetate, 20 parts of calcium bicarbonate, 0.1 part of lead acetate, second are weighed according to parts by weight proportioning 6 parts of glycol, 10 parts of polyvinyl alcohol, 15 parts of seven polyglycol ether of dodecyl, 14 parts of alanine, 6 parts of Sodium Polyacrylate, zinc sulfate 5 parts and 4 parts of aloe fibre.
Lead acetate, Sodium Polyacrylate and zinc sulfate are put into grinder and grind 10min, input carries temperature after grinding Mixer mixing is opened in the reaction kettle of meter, mixer and heating unit, is warming up to 80 DEG C, mixing velocity 280r/min, is mixed Close 2h.
Ethylene glycol, distilled water and butyl acetate are sequentially added, mixing velocity is adjusted to 350r/min, mixes 50min, add Surplus stock, is warming up to 125 DEG C, and 10 DEG C are cooled to after stirring 3h, after crossing cleaner liquid, after standing 20h to obtain the final product.
Preparation method is simple, and anti-mold effect is good, and tensile strength 3.5MPa, resistance to moisture is excellent, of low cost;Removing toxic substances, light It is bright, increase gloss, adhesion 1 grade, adhesion strength is high, good corrosion resistance, abrasion resistance 400 times, component safety;Wrinkle resistance Good, 65 acarids of water-wash resistance walk quickly and keep away rate 93.5%, and pliability 1mm, glossiness is good, good permeability;Resistance to soap, extending embroidery makes Good with service life, fast drying, fire resistance, anti-microbial property is good, to Escherichia coli bacteriostasis rate 99.4%, can produce extensively and continuous Instead of current material.
Embodiment 2:
100 parts of distilled water, 50 parts of butyl acetate, 30 parts of calcium bicarbonate, 0.5 part of lead acetate, second are weighed according to parts by weight proportioning 10 parts of glycol, 30 parts of polyvinyl alcohol, 35 parts of seven polyglycol ether of dodecyl, 18 parts of alanine, 12 parts of Sodium Polyacrylate, sulfuric acid 8 parts of 15 parts of zinc and aloe fibre.
Lead acetate, Sodium Polyacrylate and zinc sulfate are put into grinder and grind 20min, input carries temperature after grinding Mixer mixing is opened in the reaction kettle of meter, mixer and heating unit, is warming up to 90 DEG C, mixing velocity 320r/min, is mixed Close 3h.
Ethylene glycol, distilled water and butyl acetate are sequentially added, mixing velocity is adjusted to 450 r/min, mixes 90min, add Enter surplus stock, be warming up to 145 DEG C, 40 DEG C are cooled to after stirring 5h, after crossing cleaner liquid, after standing 24h to obtain the final product.
Preparation method is simple, and anti-mold effect is good, and tensile strength 4.5MPa, resistance to moisture is excellent, of low cost;Removing toxic substances, light It is bright, increase gloss, adhesion 1 grade, adhesion strength is high, good corrosion resistance, abrasion resistance 450 times, component safety;Wrinkle resistance Good, 75 acarids of water-wash resistance walk quickly and keep away rate 95.5%, and pliability 1mm, glossiness is good, good permeability;Resistance to soap, extending embroidery makes Good with service life, fast drying, fire resistance, anti-microbial property is good, to Escherichia coli bacteriostasis rate 99.6%, can produce extensively and continuous Instead of current material.
Embodiment 3:
100 parts of distilled water, 45 parts of butyl acetate, 25 parts of calcium bicarbonate, 0.3 part of lead acetate, second are weighed according to parts by weight proportioning 8 parts of glycol, 20 parts of polyvinyl alcohol, 25 parts of seven polyglycol ether of dodecyl, 16 parts of alanine, 9 parts of Sodium Polyacrylate, zinc sulfate 10 parts and 6 parts of aloe fibre.
Lead acetate, Sodium Polyacrylate and zinc sulfate are put into grinder and grind 15min, input carries temperature after grinding Mixer mixing is opened in the reaction kettle of meter, mixer and heating unit, is warming up to 85 DEG C, mixing velocity 300r/min, is mixed Close 2.5h.
Ethylene glycol, distilled water and butyl acetate are sequentially added, mixing velocity is adjusted to 400 r/min, mixes 70min, add Enter surplus stock, be warming up to 135 DEG C, 25 DEG C are cooled to after stirring 4h, after crossing cleaner liquid, after standing 22h to obtain the final product.
Preparation method is simple, and anti-mold effect is good, and tensile strength 5.5MPa, resistance to moisture is excellent, of low cost;Removing toxic substances, light It is bright, increase gloss, adhesion 1 grade, adhesion strength is high, good corrosion resistance, abrasion resistance 500 times, component safety;Wrinkle resistance Good, 85 acarids of water-wash resistance walk quickly and keep away rate 97.5%, and pliability 1mm, glossiness is good, good permeability;Resistance to soap, extending embroidery makes Good with service life, fast drying, fire resistance, anti-microbial property is good, to Escherichia coli bacteriostasis rate 99.8%, can produce extensively and continuous Instead of current material.
Composition all components in above example can be commercially available.
The above embodiments are merely intended to illustrate the present invention rather than to limit it, therefore with the present invention's Any change in claims suitable implication and scope, should be construed as being included in the scope of the claims.

Claims (5)

1. a kind of preparation method embroidered with resistance to finishing agent of soaping, it is characterised in that include the following steps:
The first step:100 parts of distilled water, 40-50 parts of butyl acetate, 20-30 parts of filler, acetic acid are weighed according to parts by weight proportioning 0.1-0.5 parts of lead, 6-10 parts of ethylene glycol, 10-30 parts of polyvinyl alcohol, 15-35 parts of seven polyglycol ether of dodecyl, alanine 4-8 parts of 14-18 parts, 6-12 parts of Sodium Polyacrylate, 5-15 parts of zinc sulfate and aloe fibre;
Second step:Lead acetate, Sodium Polyacrylate and zinc sulfate are put into grinder and grind 10-20min, input carries after grinding Mixer mixing is opened in the reaction kettle of thermometer, mixer and heating unit, is warming up to 80-90 DEG C, mixing velocity 280- 320r/min, mixes 2-3h;
3rd step:Ethylene glycol, distilled water and butyl acetate are sequentially added, adjusts mixing velocity to 350-450 r/min, mixing 50-90min, adds surplus stock, is warming up to 125-145 DEG C, and 10-40 DEG C is cooled to after stirring 3-5h, after crossing cleaner liquid, stands To obtain the final product after 20-24h.
2. the preparation method of the resistance to finishing agent of soaping of embroidery according to claim 1, it is characterised in that:In the first step Embroidery is as follows with the raw materials by weight portion proportioning of resistance to finishing agent of soaping:100 parts of distilled water, 40 parts of butyl acetate, filler 20 It is part, 0.1 part of lead acetate, 6 parts of ethylene glycol, 10 parts of polyvinyl alcohol, 15 parts of seven polyglycol ether of dodecyl, 14 parts of alanine, poly- 4 parts of 6 parts of sodium acrylate, 5 parts of zinc sulfate and aloe fibre.
3. the preparation method of the resistance to finishing agent of soaping of embroidery according to claim 1, it is characterised in that:In the first step Embroidery is as follows with the raw materials by weight portion proportioning of resistance to finishing agent of soaping:100 parts of distilled water, 50 parts of butyl acetate, filler 30 It is part, 0.5 part of lead acetate, 10 parts of ethylene glycol, 30 parts of polyvinyl alcohol, 35 parts of seven polyglycol ether of dodecyl, 18 parts of alanine, poly- 8 parts of 12 parts of sodium acrylate, 15 parts of zinc sulfate and aloe fibre.
4. the preparation method of the resistance to finishing agent of soaping of embroidery according to claim 1, it is characterised in that:In the first step Embroidery is as follows with the raw materials by weight portion proportioning of resistance to finishing agent of soaping:100 parts of distilled water, 45 parts of butyl acetate, filler 25 It is part, 0.3 part of lead acetate, 8 parts of ethylene glycol, 20 parts of polyvinyl alcohol, 25 parts of seven polyglycol ether of dodecyl, 16 parts of alanine, poly- 6 parts of 9 parts of sodium acrylate, 10 parts of zinc sulfate and aloe fibre.
5. the preparation method of the resistance to finishing agent of soaping of embroidery according to claim 1, it is characterised in that:The filler is adopted Use calcium bicarbonate.
CN201711239191.7A 2017-11-30 2017-11-30 A kind of preparation method embroidered with resistance to finishing agent of soaping Withdrawn CN107904934A (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101736616A (en) * 2009-12-30 2010-06-16 达利(中国)有限公司 Technology for dyeing and finishing real silk/corn fabric
CN102586038A (en) * 2011-12-28 2012-07-18 浙江台华新材料股份有限公司 Fabric reductive cleaning agent with high soaping-resistant color fastness and high sublimation fastness, preparation method thereof and polyester fabric treatment method
CN103556511A (en) * 2013-10-25 2014-02-05 华纺股份有限公司 Color fixative and application method thereof

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Application publication date: 20180413