CN107904814B - Linen yarn and sizing process thereof, warping sizing process and fabric - Google Patents

Linen yarn and sizing process thereof, warping sizing process and fabric Download PDF

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Publication number
CN107904814B
CN107904814B CN201711366724.8A CN201711366724A CN107904814B CN 107904814 B CN107904814 B CN 107904814B CN 201711366724 A CN201711366724 A CN 201711366724A CN 107904814 B CN107904814 B CN 107904814B
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linen
yarn
warping
yarns
sizing
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CN107904814A (en
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刘建波
田柱安
王允
夏为雄
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Guangdong Esquel Textiles Co Ltd
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Guangdong Esquel Textiles Co Ltd
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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06BTREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B3/00Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
    • D06B3/04Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of yarns, threads or filaments
    • DTEXTILES; PAPER
    • D02YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02HWARPING, BEAMING OR LEASING
    • D02H3/00Warping machines
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06BTREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B23/00Component parts, details, or accessories of apparatus or machines, specially adapted for the treating of textile materials, not restricted to a particular kind of apparatus, provided for in groups D06B1/00 - D06B21/00
    • D06B23/04Carriers or supports for textile materials to be treated
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/144Alcohols; Metal alcoholates
    • D06M13/148Polyalcohols, e.g. glycerol or glucose
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03Polysaccharides or derivatives thereof
    • D06M15/11Starch or derivatives thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/285Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acid amides or imides
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/327Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof
    • D06M15/333Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof of vinyl acetate; Polyvinylalcohol
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02Natural fibres, other than mineral fibres
    • D06M2101/04Vegetal fibres
    • D06M2101/06Vegetal fibres cellulosic
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/40Reduced friction resistance, lubricant properties; Sizing compositions

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Warping, Beaming, Or Leasing (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention relates to a linen yarn and a sizing process, a warping sizing process and a fabric thereof. The sizing process of the linen yarn comprises the following steps: pre-wetting linen yarns wound on a warp beam in water at 65-75 ℃; controlling the moisture regain of the linen yarns to be 35% -45%; sizing treatment and wet leasing treatment are carried out on the flax yarns in sequence; drying the linen yarns to ensure that the moisture regain of the linen yarns is 13-15%; sequentially carrying out waxing treatment and coiling treatment on the linen yarns. The linen yarn obtained by the sizing process of the linen yarn can improve the weaving efficiency.

Description

Linen yarn and sizing process thereof, warping sizing process and fabric
Technical Field
The invention relates to the technical field of spinning, in particular to a linen yarn, a sizing process of the linen yarn, a warping sizing process of the linen yarn and a fabric.
Background
The flax yarn is spun by flax fiber, the flax fiber is the only fasciculate plant fiber in natural fiber, has natural fusiform structure and unique pectic substance bevel edge hole, and the excellent characteristics of moisture absorption, ventilation, corrosion prevention, bacteriostasis, low static electricity and the like are generated, so that the flax fabric becomes a fabric capable of breathing naturally, and is known as 'fiber queen'. Then, because the length of the flax bundle fiber is short, only 10 mm-26 mm, the splitting degree is large, the surface hairiness of the flax yarn is large and long and hard, and the hairiness is difficult to stick to the surface, the flax yarn is generally required to be subjected to warping slashing treatment before weaving, however, the flax yarn subjected to the existing warping slashing treatment still has the problems of poor wear resistance, easy brittle fracture and low weaving efficiency.
Disclosure of Invention
Accordingly, there is a need for a sizing process for linen yarns, which can improve the weaving efficiency of linen yarns obtained by the sizing process for linen yarns.
In addition, a warping slashing process of the linen yarn, the linen yarn and the fabric are also provided.
A sizing process of linen yarns comprises the following steps:
pre-wetting linen yarns wound on a warp beam in water at 65-75 ℃;
controlling the moisture regain of the linen yarns to be 35% -45%;
sequentially sizing and wet leasing the linen yarns;
drying the linen yarns to enable the moisture regain of the linen yarns to be 13% -15%; and
and sequentially carrying out waxing treatment and reeling treatment on the linen yarns.
The sizing process of the linen yarn is characterized in that the linen yarn is placed in hot water at 65-75 ℃ for pre-wetting treatment before sizing treatment, the moisture regain of the linen yarn is controlled to be 35-45% before sizing, the surface tension of the linen yarn can be reduced, the size absorption condition of the linen yarn is improved, the penetration of size in the subsequent sizing treatment process is facilitated, the wear resistance of the linen yarn is improved, the hairiness on the linen yarn is better attached, the hairiness amount is reduced, the surface friction coefficient of the linen yarn is reduced, and the wet leasing treatment is adopted before drying treatment, so that the hairiness of the linen yarn is further reduced; the moisture regain of the linen yarn is controlled to be 13% -15% through drying treatment, so that the linen yarn has a proper moisture regain in the subsequent weaving process, and the weaving efficiency is improved; and the surface of the linen yarn is coated with the wax film by waxing treatment, so that the surface friction coefficient of the linen yarn is reduced, and the linen yarn obtained by the slashing process of the linen yarn can improve the weaving efficiency.
In one embodiment, the unwinding tension of the warp beam is 2.0 Bar-3.0 Bar, the tension of the linen yarn in the sizing treatment is 240N-300N, the tension of the linen yarn in the drying treatment is 240N-300N, and the tension of the linen yarn in the waxing treatment is 1760N-1980N; the winding tension during the winding process is 2160N-2430N, the flax yarn is wound on the reel by using a reel and a yarn pressing shaft which are matched, and the pressure of the yarn pressing shaft during the winding process is 1900N-2250N.
In one embodiment, the device used in the sizing process of the linen yarn is a sizing machine, the warp beam is installed on the sizing machine, the speed of the sizing machine is 55-65 m/min, and the drying temperature during the drying treatment is 100-105 ℃.
In one embodiment, the linen yarn has a waxing amount of 0.4 kg/km to 0.6 kg/km.
In one embodiment, the slurry used in the step of sizing treatment comprises the following components in percentage by mass: 40 to 45 percent of starch, 20 to 25 percent of polyacrylamide, 12 to 16 percent of polyvinyl alcohol, 12 to 16 percent of glycerol and 5 to 7 percent of emulsifying wax.
A warping slashing process of linen yarns comprises the following steps:
warping the linen yarns to enable the linen yarns to be wound on a warp beam; and
and carrying out sizing treatment on the linen yarns according to the sizing process of the linen yarns.
In one embodiment, before the step of warping the linen yarn, the step of humidifying the linen yarn so that the moisture regain of the linen yarn is 9-11% is further included.
In one embodiment, the step of humidifying the linen yarns specifically comprises: and placing the linen yarns in an environment with the temperature of 26-28 ℃ and the relative humidity of 65-75% RH for spray humidification.
In one embodiment, in the step of warping the linen yarns, the warping number is 300 to 400 per beam.
In one embodiment, in the step of warping the linen yarns, the distance between two adjacent linen yarns is 0.4 cm to 0.5 cm.
In one embodiment, in the step of warping the linen yarns, the warping reed adopts a mode of 1 reed empty and 1 reed.
In one embodiment, in the step of warping the linen yarn, the linen yarn is warped by a warping machine, a creel of the warping machine is in a V shape, and the tension of the pre-tension bar is zero when the yarn gripper is closed during the warping process.
The linen yarn is prepared by a slashing process of the linen yarn or a warping slashing process of the linen yarn.
A fabric woven by the linen yarns.
Drawings
FIG. 1 is a flow diagram of a warping slashing process for a linen yarn according to an embodiment;
FIG. 2 is a flow diagram of a sizing process in the warping sizing process of the linen yarn shown in FIG. 1;
FIG. 3 is a schematic structural diagram of a simulated loom used for abrasion resistance tests of the linen yarns of examples 1-3 and comparative examples 1-4.
Detailed Description
To facilitate an understanding of the invention, the invention will now be described more fully with reference to the accompanying drawings. Preferred embodiments of the present invention are shown in the drawings. This invention may, however, be embodied in many different forms and should not be construed as limited to the embodiments set forth herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete.
Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terminology used in the description of the invention herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. As used herein, the term "and/or" includes any and all combinations of one or more of the associated listed items.
As shown in fig. 1, a warping slashing process of a linen yarn according to an embodiment includes the steps of:
step S110: the linen yarns are humidified to ensure that the moisture regain of the linen yarns is 9-11%.
Wherein, the linen yarn in the step S110 is the yarn spun by the linen fiber.
Specifically, the steps of humidifying the linen yarns are as follows: the linen yarn is put into an environment with the temperature of 26-28 ℃ and the relative humidity of 65-75% RH for spray humidification, so that the moisture regain of the linen yarn is 9-11%. The flax yarn is humidified to reduce the warping breakage rate of the flax yarn, improve the production efficiency and improve the warping quality.
Step S120: the linen yarn is subjected to a warping process so that the linen yarn is wound on a beam.
Specifically, the apparatus used in step S120 is a warping machine.
Specifically, in the step of warping the linen yarns, the warping parts are 300 to 400 per beam so as to reduce the warping breakage rate of the linen yarns.
Furthermore, in the step of warping the linen yarns, the distance between two adjacent linen yarns is 0.4-0.5 cm, so that the adhesion condition of long hairiness between the adjacent yarns can be reduced, and the warping efficiency is improved.
Furthermore, in the step of warping the linen yarns, the warping reed adopts a mode of 1 reed empty and 1 reed. Through setting up warping row reed according to this mode for the yarn when appearing jumping the reed, it can jump to adjacent empty dent with it in, continues to carry out the warping and handles, thereby avoids the yarn to jump the reed to adjacent flax yarn corresponding dent in and the reed that leads to on have two yarns and slashing to form hank, the end of meeting, improves the warping quality.
In the present embodiment, in the step of warping the linen yarn, the linen yarn is warped using a warping machine, a creel of the warping machine is V-shaped, and the tension of the pre-tension lever is zero by closing the yarn gripper during the warping process. The pre-tension rod is used for providing certain tension for the yarn when the yarn feeder is opened so as to prevent the yarn from loosening. The V-shaped creel is not adopted for warping treatment of the linen yarns generally, the linen yarns are easy to loosen due to the fact that the linen yarns are heavy in weight in the production process due to the fact that the V-shaped creel is a tension-free creel, and the tension of the pre-tension rod is controlled by closing the yarn clamping device during warping treatment, so that warping treatment of the linen yarns by the warping machine directly adopting the V-shaped creel can be achieved, and the application range of the warping machine of the V-shaped creel is expanded.
Step S130: sizing the linen yarns.
Referring to fig. 2, the sizing process for the linen yarn comprises the following steps:
step S132: the linen yarn wound on the beam is pre-wet treated in water with the temperature of 65-75 ℃.
Specifically, the device used for sizing the linen yarn is a sizing machine. When sizing the linen yarn, a warp beam wound with the linen yarn is mounted on a sizing machine.
Specifically, the linen yarn wound on a beam is passed through a water tank filled with water at 65-75 ℃ to be subjected to pre-wetting treatment.
Step S134: the moisture regain of the linen yarn is controlled to be 35-45%.
Specifically, 30000N-50000N pressure is applied to the linen yarn so as to control the moisture regain of the linen yarn to be 35-45%. Wherein, the higher the pressure, the more water is pressed out, and the lower the moisture regain is.
Step S135: sizing treatment and wet leasing treatment are carried out on the linen yarns in sequence.
Before sizing treatment, the linen yarn is placed in hot water at the temperature for pre-wetting treatment in the step S132, the moisture regain of the linen yarn is controlled to be 35% -45% in the step S134, air in the yarn is extruded out through pressurization in the process, and water permeates into the linen yarn, so that the linen yarn capillary effect is promoted to be carried out in the subsequent sizing process, the contact area ratio of the serous fluid and the fiber is enlarged, the penetration depth of the serous fluid in the linen yarn is improved, the serous fluid is distributed in the linen yarn more uniformly, the sizing quality is better, and the weaving efficiency of the linen fiber is improved.
The sizing treatment is directly carried out on the sized linen yarns without drying, and the wet splitting treatment is beneficial to reducing the hairiness of the linen yarns.
Specifically, the sizing treatment comprises the following steps: the linen yarn is sized in the size and then pressure is applied to the linen yarn out of the size to press the size into the linen yarn and control the sizing amount. Wherein, the pressure applied by the pressure roller to the linen yarns in the pulp outlet groove is 15000N-25000N, and the sizing amount is controlled by controlling the pressure of the pressure roller.
Specifically, the slurry used in the sizing treatment step comprises the following components in percentage by mass: 40 to 45 percent of starch, 20 to 25 percent of polyacrylamide, 12 to 16 percent of polyvinyl alcohol, 12 to 16 percent of glycerol and 5 to 7 percent of emulsifying wax.
Wherein the starch is modified starch, such AS AS-1 modified starch from emollient assistant, Inc. of Changzhou city. The emulsifying WAX is WAX-1 emulsifying WAX from Changzhou lubricating aid Co.
Specifically, the wet leasing treatment is realized by adopting a wet leasing device.
Step S136: drying the linen yarns to ensure that the moisture regain of the linen yarns is 13-15%.
The moisture regain of the linen yarns is controlled to be 13% -15% through drying, so that the linen yarns have a proper moisture regain in the subsequent weaving process, and the weaving efficiency is improved. The wet strength of the linen yarn is usually higher than the dry strength, and within the moisture regain range, the linen yarn can be ensured to be always in an optimal state in the weaving process.
Specifically, the device used in the sizing treatment process of the linen yarns is a sizing machine, the speed of the sizing machine is 55-65 m/min in the sizing treatment process, and the drying temperature in the drying treatment is 100-105 ℃.
The speed of the whole sizing treatment process is controlled to be 55-65 m/min, so that 13-15% of moisture regain can be obtained at the drying temperature of 100-105 ℃ when the linen yarn passes through the drying zone (namely when the speed of the sizing treatment process is constant, a plurality of drying temperatures are too high, the moisture regain is low, and a plurality of drying temperatures are too low, the moisture regain is high).
Step S137: sequentially carrying out waxing treatment and coiling treatment on the linen yarns.
The surface of the linen yarn is coated with the wax film through waxing treatment, so that the surface friction coefficient of the linen yarn is reduced, and the weaving efficiency is improved.
Specifically, the device used in the waxing process is a double-sided waxing device. In the step of waxing, the waxing amount of the linen yarns is 0.4 kg/km to 0.6 kg/km. The surface friction coefficient of the linen yarns is smaller by controlling the waxing amount of the linen yarns. More specifically, in the step of waxing treatment, the temperature of wax liquid is 70-80 ℃; the rotating speed of the wax roller is 0.2 m/min to 0.4 m/min.
Further, in the step of sizing the linen yarns, the unwinding tension of the warp beam is 2.0 Bar-3.0 Bar; the tension of the linen yarn in the sizing treatment is 240N-300N; the tension of the linen yarn during drying treatment is 240N-300N; the tension of the linen yarn in the waxing process is 1760N-1980N; the winding tension during winding treatment is 2160N-2430N, the flax yarn is wound on the reel by using the reel and the yarn pressing shaft, and the pressure of the yarn pressing shaft during winding treatment is 1900N-2250N. The unwinding tension of the warp beam, the sizing tension of the linen yarn, the drying tension, the waxing tension, the winding tension and the pressure of the yarn pressing shaft are controlled according to the parameters, so that the linen yarn has a certain elongation after sizing treatment, the brittle fracture property of the linen yarn is improved, and the weaving efficiency is improved.
The warping slashing process of the linen yarns has at least the following advantages:
(1) in the warping slashing process of the linen yarns, the linen yarns are placed in hot water at the temperature for prewetting treatment before slashing treatment, and the moisture regain of the linen yarns is controlled to be 40%, so that the surface tension of the linen yarns can be reduced, the size absorption condition of the linen yarns can be improved, the penetration of size in the subsequent slashing treatment process is facilitated, the wear resistance of the linen yarns is improved, the hairiness on the linen yarns is better attached, and the hairiness amount is reduced; wet leasing treatment is adopted before drying treatment, so that the hairiness of the linen yarns can be further reduced; the linen yarns can have a proper moisture regain in the subsequent weaving process through the subsequent drying treatment; and the surface of the linen yarn is coated with the wax film by waxing treatment, so that the surface friction coefficient of the linen yarn is reduced, and the linen yarn obtained by the slashing process of the linen yarn can improve the weaving efficiency.
(2) The moisture regain of the linen yarns is controlled to be 9% -11% by humidifying the linen yarns before warping, warping ends are 300/shaft-400/shaft, the distance between two adjacent linen yarns is 0.4-0.5 cm, warping breakage rate can be effectively improved, warping breakage rate can be reduced to 3.2 times/million meters from 10.8 times/million meters before, and warping efficiency is improved.
(3) Because the linen yarns may jump to the reed corresponding to the adjacent linen yarns due to yarn jumping during the warping treatment process, two yarns are arranged on one reed, and when the warping arrangement reed adopts a mode of 1 reed empty 1 reed, the yarns can jump to the empty reed dent adjacent to the beaming arrangement reed and continue the warping treatment.
The flax yarn of an embodiment is produced by the sizing process of the flax yarn described above. The linen yarn has less hairiness, better wear resistance and difficult brittle fracture, can effectively improve the weaving speed and the weaving efficiency, and improves the unit yield by more than 38 percent.
Another embodiment of the linen yarn is prepared by the warping slashing process of the linen yarn. The linen yarn has less hairiness, better wear resistance and difficult brittle fracture, can effectively improve the weaving speed and the weaving efficiency, and improves the unit yield by more than 38 percent.
An embodiment fabric is woven from the linen yarn. The linen yarns have less hairiness and better wear resistance, so that the fabric woven by the linen yarns has less cloth cover defects.
The following are examples (the following examples, unless otherwise specified, contain no other components not specifically indicated except for unavoidable impurities in the examples, and in the following examples, a batch warping machine of beneger is used for the warping process, and a prewet slasher of karmeyer is used for the slashing process):
example 1
The warping slashing process of the linen yarn in the embodiment specifically comprises the following steps:
(1) the moisture regain of the linen yarn was measured to be 9% by spray-humidifying the linen yarn at 26 ℃ under an atmosphere of 65% RH for 48 hours.
(2) Warping the linen yarn obtained in the step (1) by using a warping machine so as to enable the linen yarn to be wound on a warp beam: the V-shaped creel is adopted, the warping head is 300 pieces/minute, the warping and reed arrangement adopts a mode of 1 reed empty 1 reed, the distance between two adjacent linen yarns is 0.5 cm, the yarn clamping device is closed, and the tension of the pre-tension rod is 0.
(3) Installing a warp beam wound with the linen yarns on a sizing machine, and sizing the linen yarns obtained in the step (2):
pre-wetting the linen yarns in a pre-wetting water tank filled with 65 ℃ water; then, 30000N pressure is applied to the linen yarns to control the moisture regain of the linen yarns to be 45%; and then the linen yarns pass through a size tank filled with size, and then 25000N of pressure is applied to the linen yarns discharged from the size tank through a sizing roller, wherein the size comprises the following components in percentage by mass: 44% starch, 22% polyacrylamide, 14% polyvinyl alcohol, 14% glycerol and 6% emulsifying wax; then, the linen yarns are subjected to wet leasing treatment through a wet leasing device and then enter a drying cylinder for drying treatment until the moisture regain of the linen yarns is 13%; after the flax yarn is taken out of the drying cylinder, the flax yarn is waxed by a double-sided waxing device, wherein the temperature of the wax liquid is 70 ℃, the waxing amount of the flax yarn is 0.4 kg/km, and the rotating speed of a wax roller is 0.2 m/min; and finally, winding the waxed linen yarn by a winding device.
Wherein, in the sizing treatment process: the speed of the sizing machine was 55 m/min, the unwinding tension of the warp beam was 2.0Bar, the tension of the linen yarn during sizing was 240N, the tension of the linen yarn during drying was 240N, the drying temperature was 100 ℃, the tension of the linen yarn during waxing was 1760N, the winding tension of the linen yarn during winding was 2160N, and the pressure of the yarn pressing shaft used during winding was 2000N.
Example 2
The warping slashing process of the linen yarn in the embodiment specifically comprises the following steps:
(1) the moisture regain of the linen yarn was 11% when the linen yarn was spray-humidified for 48 hours in an environment of 28 ℃ and a relative humidity of 75% RH.
(2) Warping the linen yarns obtained in the step (1) to enable the linen yarns to be wound on a warp beam: the V-shaped creel is adopted, the warping head is 400 pieces/minute, the warping and reed arrangement adopts a mode of 1 reed empty 1 reed, the distance between two adjacent linen yarns is 0.4 cm, the yarn clamping device is closed, and the tension of the pre-tension rod is 0.
(3) Installing a warp beam wound with the linen yarns on a sizing machine, and sizing the linen yarns obtained in the step (2):
pre-wetting the linen yarn in a pre-wetting water tank filled with water at 75 ℃; applying 50000N pressure on the linen yarns to control the moisture regain of the linen yarns to be 35%; and then the linen yarns pass through a size tank filled with size, and then 25000N of pressure is applied to the linen yarns discharged from the size tank through a sizing roller, wherein the size comprises the following components in percentage by mass: 44% starch, 22% polyacrylamide, 14% polyvinyl alcohol, 14% glycerol and 6% emulsifying wax; then, the linen yarns are subjected to wet leasing treatment through a wet leasing device and then enter a drying cylinder for drying treatment until the moisture regain of the linen yarns is 15%; after the flax yarn is taken out of the drying cylinder, the flax yarn is waxed by a double-sided waxing device, wherein the temperature of the wax liquid is 80 ℃, the waxing amount of the flax yarn is 0.6 kg/km, and the rotating speed of a wax roller is 0.4 m/min; and finally, winding the waxed linen yarn by a winding device.
Wherein, in the sizing treatment process: the speed of the sizing machine was 65 m/min, the unwinding tension of the warp beam was 3.0Bar, the tension of the linen yarn during sizing was 300N, the tension of the linen yarn during drying was 300N, the drying temperature was 105 ℃, the tension of the linen yarn during waxing was 1980N, the winding tension of the linen yarn during winding was 2430N, and the pressure of the yarn presser shaft used during winding was 2250N.
Example 3
The warping slashing process of the linen yarn in the embodiment specifically comprises the following steps:
(1) the moisture regain of the linen yarn was measured to be 10% by spray-humidifying the linen yarn at 27 ℃ under an environment of 70% RH for 48 hours.
(2) Warping the linen yarns obtained in the step (1) to enable the linen yarns to be wound on a warp beam: the V-shaped creel is adopted, the warping head is 350 pieces/minute, the warping and reed arrangement adopts a mode of 1 reed empty 1 reed, the distance between two adjacent linen yarns is 0.45 cm, the yarn clamping device is closed, and the tension of the pre-tension rod is 0.
(3) Installing a warp beam wound with the linen yarns on a sizing machine, and sizing the linen yarns obtained in the step (2):
pre-wetting flax yarn in a pre-wetting water tank filled with water at 70 ℃; applying 40000N pressure on the linen yarns to control the moisture regain of the linen yarns to be 40%; and then the linen yarns pass through a size tank filled with size, and then the pressure of 20000N is applied to the linen yarns discharged with the size through a sizing roller, wherein the size comprises the following components in percentage by mass: 44% starch, 22% polyacrylamide, 14% polyvinyl alcohol, 14% glycerol and 6% emulsifying wax; then, the linen yarns are subjected to wet leasing treatment through a wet leasing device and then enter a drying cylinder for drying treatment until the moisture regain of the linen yarns is 14%; after the flax yarn is taken out of the drying cylinder, the flax yarn is waxed by a double-sided waxing device, wherein the temperature of the wax liquid is 75 ℃, the waxing amount of the flax yarn is 0.5 kg/km, and the rotating speed of a wax roller is 0.3 m/min; and finally, winding the waxed linen yarn by a winding device.
Wherein, in the sizing treatment process: the speed of the sizing machine was 60 m/min, the unwinding tension of the warp beam was 2.5Bar, the tension of the linen yarn during sizing was 270N, the tension of the linen yarn during drying was 270N, the drying temperature was 102 ℃, the tension of the linen yarn during waxing was 1870N, the winding tension of the linen yarn during winding was 2295N, and the pressure of the yarn presser shaft used during winding was 2125N.
Comparative example 1
The procedure of the warping slashing process of the linen yarn of comparative example 1 was substantially the same as that of example 3 except that, in the slashing treatment, the drying cylinder was dried until the moisture regain of the linen yarn was 12%.
Comparative example 2
The procedure of the warping slashing process of the linen yarn of comparative example 2 was substantially the same as that of example 3 except that, in the slashing treatment, the drying cylinder was dried until the moisture regain of the linen yarn was 16%.
Comparative example 3
The warping slashing process step of the linen yarn of comparative example 3 was substantially the same as that of example 3, except that in the step of slashing the linen yarn in step (3) of comparative example 3, the linen yarn obtained in step (2) was directly passed through a slashing tank filled with a size and then a pressure of 20000N was applied to the sized linen yarn by a slashing roller without previously subjecting the linen yarn to pre-wetting treatment and moisture regain control.
Comparative example 4
The warping slashing process of the linen yarn of comparative example 4 was substantially the same as that of example 3, except that comparative example 4 pre-wets the linen slashing with steam boiled by heating water during slashing treatment and controls the moisture regain of the linen yarn to be 40%.
And (3) testing:
(1) wear resistance tests were carried out on the linen yarns obtained after the warping slashing treatment in examples 1 to 3 and the linen yarns obtained after the warping slashing treatment in comparative examples 1 to 4 by using a method simulating loom production: as shown in fig. 3, the simulated loom is provided with four pins 210, and the linen yarns 20 obtained by warping slashing treatment in examples 1 to 3 and comparative examples 1 to 4 are installed on the simulated loom and pass through the four pins 210, and friction occurs between the yarns due to friction between the linen yarns when passing through the pins.
The strength before and after the testing of the linen yarns of the examples 1-3 and the comparative examples 1-4 is tested by a method GB/T3916-97 'determination of single yarn breaking strength and breaking elongation' see Table 1, and the strength loss rate of the linen yarns is calculated and is shown in Table 1. Wherein the strength loss rate is (strength before test-strength after test) × 100%/strength before test.
The amounts of the hairiness before and after the testing of the linen yarns of the examples 1 to 3 and the comparative examples 1 to 4 are tested by adopting an FZ/T01086-2000 textile yarn hairiness measuring method through a projection counting method and are shown in a table 2, and the hairiness increase rate of the linen yarns is calculated and is shown in the table 2, wherein the hairiness increase rate is (the amount of the hairiness before the testing-the amount of the hairiness after the testing) multiplied by 100% per the amount of the hairiness before the testing.
TABLE 1
Figure BDA0001513047000000111
As can be seen from table 1, the strength of the linen yarns of examples 1 to 3 before test is at least 588CN, and the strength loss after test is at most 8.3%, while the strength of the linen yarns of comparative examples 1 to 4 before test is only 562CN at most, and the strength loss after test is at least 14.6%, which is far inferior to that of examples 1 to 3.
TABLE 2
Figure BDA0001513047000000121
As can be seen from Table 2, the amount of the hairiness of the linen yarns of the examples 1 to 3 before the test is only 21 hairiness/m at most, and after the test, the hairiness increase rate is 76.5% at most, while the amount of the hairiness of the linen yarns of the comparative examples 1 to 4 before the test is at least 29 hairiness/m, and the hairiness increase rate after the test is at least 106.7% which is far higher than that of the examples 1 to 3.
Obviously, the linen yarns obtained by the warping slashing process of the linen yarns of the embodiments 1-3 not only have better strength and less hairiness, but also have better wear resistance.
(2) The linen yarns obtained after the warping slashing treatment of examples 1 to 3 and the linen yarns obtained after the warping slashing treatment of comparative examples 1 to 4 were both woven into fabrics (the variety of the fabric is PM2121-1Q6749, the fabric specification is 58 x 52/21 x 21, the fabric texture 1/1; the number of warp shafts is 10), and the weaving efficiency, the weaving speed and the weaving unit yield of the linen yarns obtained after the warping slashing treatment of examples 1 to 3 and the warping slashing of comparative examples 1 to 4 were respectively obtained, as shown in Table 3.
TABLE 3
Figure BDA0001513047000000122
Figure BDA0001513047000000131
As can be seen from table 3, the weaving efficiency of the linen yarns obtained in examples 1 to 3 is at least 90.2%, the weaving speed can reach 350 r/min, the number of shifts is at least 75.7 yards/shift, while the highest weaving efficiency of the linen yarns obtained after the warping slashing treatment in comparative examples 1 to 4 is only 85.4%, the weaving speed can only reach 250 r/min, and the specific yield is only 54.6 yards/shift, and obviously, the weaving efficiency of examples 1 to 3 is improved by at least 9.0%, the weaving speed is improved by 40%, the specific yield is improved by 38.6%, and the weaving efficiency, the weaving speed and the specific yield are far higher than those of comparative examples 1 to 4.
The technical features of the embodiments described above may be arbitrarily combined, and for the sake of brevity, all possible combinations of the technical features in the embodiments described above are not described, but should be considered as being within the scope of the present specification as long as there is no contradiction between the combinations of the technical features.
The above-mentioned embodiments only express several embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present patent shall be subject to the appended claims.

Claims (13)

1. The sizing process of the linen yarn is characterized by comprising the following steps:
pre-wetting linen yarns wound on a warp beam in water at 65-75 ℃;
controlling the moisture regain of the linen yarns to be 40% -45%;
sequentially sizing and wet leasing the linen yarns;
drying the linen yarns to enable the moisture regain of the linen yarns to be 13% -15%; and
sequentially carrying out waxing treatment and coiling treatment on the linen yarns; the waxing amount of the flax yarn is 0.4 kg/kilometer to 0.6 kg/kilometer.
2. The sizing process for linen yarns as claimed in claim 1, wherein the unwinding tension of said warp beam is 2.0 Bar-3.0 Bar, the tension of said linen yarns during said sizing treatment is 240N-300N, the tension of said linen yarns during said drying treatment is 240N-300N, the tension of said linen yarns during said waxing treatment is 1760N-1980N; the winding tension during the winding process is 2160N-2430N, the flax yarn is wound on the reel by using a reel and a yarn pressing shaft which are matched, and the pressure of the yarn pressing shaft during the winding process is 1900N-2250N.
3. The sizing process for linen yarns according to claim 1, characterized in that the device used in the sizing process for linen yarns is a sizing machine, the warp beam is mounted on the sizing machine, the speed of the sizing machine is 55-65 m/min, and the drying temperature during the drying treatment is 100-105 ℃.
4. The sizing process for linen yarns as claimed in claim 1, wherein the size used in said sizing step comprises, in mass%: 40 to 45 percent of starch, 20 to 25 percent of polyacrylamide, 12 to 16 percent of polyvinyl alcohol, 12 to 16 percent of glycerol and 5 to 7 percent of emulsifying wax.
5. The warping slashing process of the linen yarns is characterized by comprising the following steps:
warping the linen yarns to enable the linen yarns to be wound on a warp beam; and
the sizing process for the linen yarn according to any one of claims 1 to 4, wherein the linen yarn is subjected to sizing treatment.
6. The linen yarn warping slashing process according to claim 5, further comprising a step of humidifying the linen yarn so that the moisture regain of the linen yarn is 9% -11% before the step of warping the linen yarn.
7. The linen yarn warping slashing process according to claim 6, wherein the step of humidifying the linen yarn comprises: and placing the linen yarns in an environment with the temperature of 26-28 ℃ and the relative humidity of 65-75% RH for spray humidification.
8. The linen yarn warping slashing process according to claim 5, wherein in the step of warping the linen yarn, the warping number is 300 to 400 per beam.
9. The linen yarn warping slashing process according to claim 8, wherein in the step of warping the linen yarns, the distance between two adjacent linen yarns is 0.4 cm to 0.5 cm.
10. The linen yarn warping slashing process according to claim 8, wherein in the step of warping the linen yarn, a warping reed is adopted in a manner of 1 reed empty and 1 reed.
11. The linen yarn warping slashing process according to claim 5, wherein in the step of warping the linen yarn, the linen yarn is warped by a warping machine, a creel of the warping machine is V-shaped, and during the warping process, the yarn gripper is closed, and the tension of the pre-tension bar is zero.
12. A linen yarn produced by the slashing process of the linen yarn according to any one of claims 1 to 4 or the warping slashing process of the linen yarn according to any one of claims 5 to 11.
13. A fabric woven from the linen yarn of claim 12.
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CN114369953B (en) * 2021-12-21 2023-09-19 东华大学 Desizing-free linen yarn sizing treatment method and desizing-free linen fabric
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