CN107904018A - A kind of preparation method of composite essential oil - Google Patents
A kind of preparation method of composite essential oil Download PDFInfo
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- CN107904018A CN107904018A CN201711175888.2A CN201711175888A CN107904018A CN 107904018 A CN107904018 A CN 107904018A CN 201711175888 A CN201711175888 A CN 201711175888A CN 107904018 A CN107904018 A CN 107904018A
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- essential oil
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- grandis
- limonene
- terpinene
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention relates to a kind of preparation method of composite essential oil, it includes following preparation process：Following raw material for standby is taken to include Eucalyptus urophylla-grandis essential oil, containing 1,8 Cineole 30% 50%, 4 alcohol type narrow leaved tea tree essential oil tea tree ethereal oil of terpinene, containing 4 terpinols 30% 40%（Mass fraction）；The preparation method of composite essential oil of the present invention, the characteristics of less toxic, efficient, degradable and environmental pollution is small, excellent actual fungistatic effect, composite essential oil has pleasant fragrance and good health protection and therapeutic action, it can be largely used to produce various spices, essence, soap, cosmetics, food additives, chemical industry and biological pesticide etc., the articles for daily use of the suitable house travelling such as similar essential wind oil, cooling ointment, white flower oil, 10 drops, mosquitofugal oil are equally can be developed into, there is good application effect and prospect.
Description
Technical field
The present invention relates to a kind of preparation method of composite essential oil.
Background technology
The natural some components reformed essential oil and refer to be enriched with natural essential oil using specific method, while removing unit is grouped
Point, other natural constituents are incorporated, it is reached certain requirement in component, quality and bioactivity.Natural essential oil is with it
Naturally, environmental protection and it is paid more and more attention with antibacterial insecticidal action, can makes full use of resource by reforming compounding, make natural essential oil
Keep its original characteristic and produce synergy, so as to improve the bioactivity of composite essential oil.What alpine ash and Eucalyptus urophylla hybridized
The quick growing species of trees, resource is quite abundant, and the seeds are with luxuriant foliage and spreading branches in leafy profusion, and the essential oil of considerable amount is can obtain after steam distillation,
Eucalyptus urophylla-grandis leaf volatile oil oil-phase component yield 0.67%, water soluble ingredient yield 0.87%.Research shows Eucalyptus urophylla-grandis leaf volatile oil oil
Property component has plant certain bioactivity, available for industries such as medicine, spices, food additives.Eucalyptus urophylla-grandis volatile oil
There is allelopathy to fungi and insect, thus it is speculated that terpenoid is main allelopathy material.But, Eucalyptus urophylla-grandis leaf for a long time
And its essential oil fails to be develop and useedd well.Terpinene-4-alcohol type narrow leaved tea tree essential oil, is commonly called as " tea tree
Oil ", has the characteristics that has a broad antifungal spectrum, antibacterial activity are strong, to staphylococcus aureus, staphylococcus epidermis, Escherichia coli
There is good antibacterial action.Discovery, different types of narrow leaved tea tree essential oil are studied to the antibacterial action of different type tea oil
There is bacteriostasis, each principal component has different antimicrobial mechanisms, plays and cooperates with antibacterial effect.Titrol is curved to jejunum
Curved bar bacterium also has very strong bacteriostasis, its fragrance is pleasant, nonirritant to human skin, has sterilization and removes the work of acarid
With can be as the active ingredient of the preparations such as skin care, washing, dissipation.Narrow leaved tea tree essential oil has nontoxic, fragrant and broad-spectrum antibacterial
The characteristics such as sterilization, widely use in industries such as daily use chemicals, medicine, spices, are rare natural health medical materials.Eucalyptus urophylla-grandis
Essential oil and narrow leaved tea tree essential oil, which reform compounding, can give full play to the synergistic effect of active component, can significantly improve antibacterial desinsection effect
Fruit.Using Eucalyptus urophylla-grandis essential oil and terpinene alcohol type narrow leaved tea tree essential oil as raw material, composite precision is made by rectifying, reformation, compounding
Oil, controls main component and content, method is accurate, can effectively control the product quality of composite essential oil using gas-chromatography.In vitro
Experiment proves that Cineole-pine tar alcohol type reforms compounding composite essential oil to staphylococcus aureus, staphylococcus epidermis, beta hemolysis
It is different degrees of that property 6 kinds of streptococcus, Escherichia coli, Pseudomonas aeruginosa and Candida albicans can cause the pathogen of skin infection to have
Fungistatic effect, there is antibacterial, desinsection isoreactivity to act on.This product preparation method is simple, stable and controllable for quality, is adapted to industry metaplasia
Production.Antibacterial insecticide of the compounding composite essential oil as natural environmental protection is reformed, there are good market prospects.Eucalyptus urophylla-grandis aboundresources,
Substantial amounts of essential oil can be obtained using a large amount of branches and leaves after felling, narrow leaved tea tree growth cycle is short, and raw material sources enrich, rationally profit
With resource, give full play to the advantage in resources exploitation new product, can produce the social and economic benefit of higher.
The content of the invention
The present invention proposes a kind of preparation method of composite essential oil.
A kind of preparation method of composite essential oil of the present invention, including following preparation process：
（1）Following raw material for standby is taken to include Eucalyptus urophylla-grandis essential oil, 30%-50% containing 1, 8-Cineole, the mutual leaf of terpinene-4-alcohol type white thousand
Layer essential oil tea tree ethereal oil, the 30%-40% of terpinol containing 4-（Mass fraction）；
（2）Eucalyptus urophylla-grandis essential oil is subjected to distillation processing, wherein limonene 12%-25%, 1, 8-Cineole 7%-20%, p-cymene
7%-15%, terpinene-4-alcohol 25%-35%,α- terpinol 5%-15%；
（3）Eucalyptus urophylla-grandis essential oil is taken to carry out rectifying, 115-117 DEG C of front-end volatiles kettle temperature degree, 85-88 DEG C of tower top temperature, reflux ratio 4: 1-5
: 1, wherein containingα- firpene 20%-30%, 1,8- Cineole 30%-40%, limonene 15%-30%；2 kettle temperature degree 117-125 of front-end volatiles
DEG C, 88-92 DEG C of tower top temperature, reflux ratio 1: 1-4: 1,30%-40% containing limonene, p-cymene 10%-20%, 1, 8-Cineole
15%-30%；3 147-153 DEG C of kettle temperature degree of tails, 120-125 DEG C of tower top temperature, full receipts are closed in reflux, containing terpinene-4-alcohol
10%-20%、α- terpinol 20%-30%；
（4）3 cuts that above-mentioned Eucalyptus urophylla-grandis essential oil is fractionated are taken, as the constituent for reforming compounding, Eucalyptus urophylla-grandis essential oil warp
Undue cut does not weigh 3 different fractions and tea oil of Eucalyptus urophylla-grandis essential oil in proportion, adds in container, is sufficiently mixed
It is even,
Composite essential oil is made.
Preferably, the limonene 12%, 1, 8-Cineole 7%, p-cymene 7%, terpinene-4-alcohol 25%,α- terpinol
15%。
Preferably, the step（3）Middle 115 DEG C of front-end volatiles kettle temperature degree, 85 DEG C of tower top temperature, reflux ratio 4: 1, wherein containingα-
Firpene 20%, 1,8- Cineoles 30%, limonene 15%；125 DEG C of 2 kettle temperature degree of front-end volatiles, 92 DEG C of tower top temperature, reflux ratio 4: 1, contains
Limonene 40%, p-cymene 20%, 1,8- Cineoles 15%；147 DEG C of 3 kettle temperature degree of tails, 120 DEG C of tower top temperature, reflux are closed
It is complete to receive, containing terpinene-4-alcohol 10%,α- terpinol 20%.
It is the characteristics of preparation method of composite essential oil of the present invention, less toxic, efficient, degradable and environmental pollution is small, excellent
Different actual fungistatic effect, composite essential oil have pleasant fragrance and good health protection and therapeutic action, can be largely used to produce
Various spices, essence, soap, cosmetics, food additives, chemical industry and biological pesticide etc., equally can be developed into similar essential wind oil,
The articles for daily use of the suitable house travelling such as cooling ointment, white flower oil, 10 drops, mosquitofugal oil, have good application effect and prospect.
Embodiment
A kind of preparation method of composite essential oil of the present invention, including following preparation process：
（1）Following raw material for standby is taken to include Eucalyptus urophylla-grandis essential oil, 30%-50% containing 1, 8-Cineole, the mutual leaf of terpinene-4-alcohol type white thousand
Layer essential oil tea tree ethereal oil, the 30%-40% of terpinol containing 4-（Mass fraction）；
（2）Eucalyptus urophylla-grandis essential oil is subjected to distillation processing, wherein limonene 12%-25%, 1, 8-Cineole 7%-20%, p-cymene
7%-15%, terpinene-4-alcohol 25%-35%,α- terpinol 5%-15%；
（3）Eucalyptus urophylla-grandis essential oil is taken to carry out rectifying, 115-117 DEG C of front-end volatiles kettle temperature degree, 85-88 DEG C of tower top temperature, reflux ratio 4: 1-5
: 1, wherein containingα- firpene 20%-30%, 1,8- Cineole 30%-40%, limonene 15%-30%；2 kettle temperature degree 117-125 of front-end volatiles
DEG C, 88-92 DEG C of tower top temperature, reflux ratio 1: 1-4: 1,30%-40% containing limonene, p-cymene 10%-20%, 1, 8-Cineole
15%-30%；3 147-153 DEG C of kettle temperature degree of tails, 120-125 DEG C of tower top temperature, full receipts are closed in reflux, containing terpinene-4-alcohol
10%-20%、α- terpinol 20%-30%；
（4）3 cuts that above-mentioned Eucalyptus urophylla-grandis essential oil is fractionated are taken, as the constituent for reforming compounding, Eucalyptus urophylla-grandis essential oil warp
Undue cut does not weigh 3 different fractions and tea oil of Eucalyptus urophylla-grandis essential oil in proportion, adds in container, is sufficiently mixed
It is even,
Composite essential oil is made.
The limonene 12%, 1,8- Cineoles 7%, p-cymene 7%, terpinene-4-alcohol 25%,α- terpinol 15%.
The step（3）Middle 115 DEG C of front-end volatiles kettle temperature degree, 85 DEG C of tower top temperature, reflux ratio 4: 1, wherein containingα- firpene
20%th, 1,8- Cineoles 30%, limonene 15%；125 DEG C of 2 kettle temperature degree of front-end volatiles, 92 DEG C of tower top temperature, reflux ratio 4: 1, containing lemon
Alkene 40%, p-cymene 20%, 1,8- Cineoles 15%；147 DEG C of 3 kettle temperature degree of tails, 120 DEG C of tower top temperature, reflux are closed complete
Receive, containing terpinene-4-alcohol 10%,α- terpinol 20%.
Claims (3)
1. a kind of preparation method of composite essential oil, it is characterised in that including following preparation process：
（1）Following raw material for standby is taken to include Eucalyptus urophylla-grandis essential oil, 30%-50% containing 1, 8-Cineole, the mutual leaf of terpinene-4-alcohol type white thousand
Layer essential oil tea tree ethereal oil, the 30%-40% of terpinol containing 4-（Mass fraction）；
（2）Eucalyptus urophylla-grandis essential oil is subjected to distillation processing, wherein limonene 12%-25%, 1, 8-Cineole 7%-20%, p-cymene
7%-15%, terpinene-4-alcohol 25%-35%,α- terpinol 5%-15%；
（3）Eucalyptus urophylla-grandis essential oil is taken to carry out rectifying, 115-117 DEG C of front-end volatiles kettle temperature degree, 85-88 DEG C of tower top temperature, reflux ratio 4: 1-5
: 1, wherein containingα- firpene 20%-30%, 1,8- Cineole 30%-40%, limonene 15%-30%；2 kettle temperature degree 117-125 of front-end volatiles
DEG C, 88-92 DEG C of tower top temperature, reflux ratio 1: 1-4: 1,30%-40% containing limonene, p-cymene 10%-20%, 1, 8-Cineole
15%-30%；3 147-153 DEG C of kettle temperature degree of tails, 120-125 DEG C of tower top temperature, full receipts are closed in reflux, containing terpinene-4-alcohol
10%-20%、α- terpinol 20%-30%；
（4）3 cuts that above-mentioned Eucalyptus urophylla-grandis essential oil is fractionated are taken, as the constituent for reforming compounding, Eucalyptus urophylla-grandis essential oil warp
Undue cut does not weigh 3 different fractions and tea oil of Eucalyptus urophylla-grandis essential oil in proportion, adds in container, is sufficiently mixed
It is even,
Composite essential oil is made.
2. a kind of preparation method of composite essential oil as claimed in claim 1, it is characterised in that the limonene 12%, 1,8- folium eucalyptis
Element 7%, p-cymene 7%, terpinene-4-alcohol 25%,α- terpinol 15%.
A kind of 3. preparation method of composite essential oil as claimed in claim 1, it is characterised in that the step（3）Middle front-end volatiles kettle temperature
115 DEG C of degree, 85 DEG C of tower top temperature, reflux ratio 4: 1, wherein containingα- firpene 20%, 1,8- Cineoles 30%, limonene 15%；Front-end volatiles
2 125 DEG C of kettle temperature degree, 92 DEG C of tower top temperature, reflux ratio 4: 1, containing limonene 40%, p-cymene 20%, 1, 8-Cineole 15%；Afterwards
147 DEG C of 3 kettle temperature degree of cut, 120 DEG C of tower top temperature, reflux close it is complete receive, containing terpinene-4-alcohol 10%,α- terpinol 20%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711175888.2A CN107904018A (en) | 2017-11-22 | 2017-11-22 | A kind of preparation method of composite essential oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711175888.2A CN107904018A (en) | 2017-11-22 | 2017-11-22 | A kind of preparation method of composite essential oil |
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| Publication Number | Publication Date |
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| CN107904018A true CN107904018A (en) | 2018-04-13 |
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ID=61847048
Family Applications (1)
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| CN201711175888.2A Withdrawn CN107904018A (en) | 2017-11-22 | 2017-11-22 | A kind of preparation method of composite essential oil |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108902140A (en) * | 2018-06-27 | 2018-11-30 | 魔范（中山）科技有限公司 | A method of mentioning antibacterial liquid from tea tree hydrosol |
| CN109042748A (en) * | 2018-11-06 | 2018-12-21 | 上海澳克林新材料科技有限公司 | A kind of sterilizing and anti-virus plants essential oil and preparation method thereof |
| CN112920906A (en) * | 2021-03-16 | 2021-06-08 | 南京林业大学 | Preparation method of flavoring-grade fir essential oil |
-
2017
- 2017-11-22 CN CN201711175888.2A patent/CN107904018A/en not_active Withdrawn
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108902140A (en) * | 2018-06-27 | 2018-11-30 | 魔范（中山）科技有限公司 | A method of mentioning antibacterial liquid from tea tree hydrosol |
| CN109042748A (en) * | 2018-11-06 | 2018-12-21 | 上海澳克林新材料科技有限公司 | A kind of sterilizing and anti-virus plants essential oil and preparation method thereof |
| CN112920906A (en) * | 2021-03-16 | 2021-06-08 | 南京林业大学 | Preparation method of flavoring-grade fir essential oil |
| CN112920906B (en) * | 2021-03-16 | 2021-10-08 | 南京林业大学 | Preparation method of flavoring-grade fir essential oil |
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Application publication date: 20180413 |