CN107899518A - A kind of efficiently chemical industry solid-liquid security reaction device - Google Patents
A kind of efficiently chemical industry solid-liquid security reaction device Download PDFInfo
- Publication number
- CN107899518A CN107899518A CN201711335308.1A CN201711335308A CN107899518A CN 107899518 A CN107899518 A CN 107899518A CN 201711335308 A CN201711335308 A CN 201711335308A CN 107899518 A CN107899518 A CN 107899518A
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- babinet
- chemical industry
- reaction
- reaction device
- liquid
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/08—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
- B01J8/082—Controlling processes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/08—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
- B01J8/10—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles moved by stirrers or by rotary drums or rotary receptacles or endless belts
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Toys (AREA)
- Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
Abstract
The invention discloses a kind of efficiently chemical industry solid-liquid security reaction device, including guide wheel, shaft, babinet, drain pipe, heater, water inlet pipe, fluid flowmeter, camera, air bag, gauze pocket, gas cleaning plant and overflow pipe, the tank floor is equipped with guide wheel, heater is equipped with babinet, wall box is equipped with thermometer and PH detectors, water inlet pipe is connected with babinet top, fluid flowmeter is installed on water inlet pipe, babinet top is equipped with liquid level gauge and timer, air bag is equipped with babinet, it is connected below air bag by lifting rope with gauze pocket, shaft is equipped with babinet, impeller is installed in shaft, babinet top inner wall is equipped with camera, babinet top is connected with appendix, the appendix other end is connected with gas cleaning plant, babinet bottom is equipped with drain pipe.Present invention increase reaction contact area, improves reaction rate, while avoids unreacted solid residue from entering in reaction solution, is convenient to clean at the same time, simple in structure, easy to use, beneficial to popularization.
Description
Technical field
The present invention relates to a kind of chemical industry equipment, is specifically a kind of efficiently chemical industry solid-liquid security reaction device.
Background technology
The relation of the mankind and chemical industry is very close, spreads to the every aspect of life.In the modern life, almost at any time with
Ground all be unable to do without chemical products, from material lifes such as food, clothing, housing and transportation to culture and arts, the cultural life such as amusement, being required for
Chemical product services for it.Some chemical products play epoch-making important function in human development history.Their production and
Using, or even represent certain historical stage of human civilization.The mankind constantly make to try to achieve survival and development with the Nature
Struggle, deepened the understanding to world around step by step so that grasped conquer nature, the ability of reforming world.By very long
Historical practice, the mankind excel at leveraging all the more natural conditions, and oneself to create the abundant material world.Due to natural goods
The proper property of matter can not meet people's needs, and just generates various processing technologies, natural materials are transformed into a variety of
The novel substance of performance, and progressively put into effect in industrial scale.Solid-liquid reaction is wherein important in chemical industry equipment
A part.Residue can be usually produced during solid-liquid reaction, influences the quality of reactant, while easily blocks pipeline, cleaning is difficult.
Solid is generally deposited in bottom at the same time, and few with the contact area of liquid, reaction efficiency is low.
The content of the invention
It is an object of the invention to provide a kind of efficiently chemical industry solid-liquid security reaction device, to solve in above-mentioned background technology
The problem of proposition.
To achieve the above object, the present invention provides following technical solution：
A kind of efficiently chemical industry solid-liquid security reaction device, including guide wheel, shaft, babinet, drain pipe, heater, water inlet pipe, liquid
Flowmeter, camera, air bag, gauze pocket, gas cleaning plant and overflow pipe, the tank floor are equipped with guide wheel, in babinet
Equipped with heater, wall box is equipped with thermometer and PH detectors, is equipped with stirring motor in babinet, stirring motor is externally provided with
Anti- sump, stirring motor output shaft and stirring axis connection, the winding of agitating shaft outer wall set helical blade, stirring are installed on agitating shaft
Impeller, agitator arm are equipped with auxiliary agitating plate, spine, water inlet pipe and babinet are designed with agitator arm edge and cabinet wall
Top connects, and fluid flowmeter is installed on water inlet pipe, and babinet top is equipped with liquid level gauge and timer, air bag, gas are equipped with babinet
It is connected below capsule by lifting rope with gauze pocket, air bag is connected by appendix with inflation means of deflation, and wall box is equipped with medicament
Adding tube, medicament adding tube are equipped with scale, are equipped with runner in babinet, runner outer wall is equipped with returning face plate, runner and external electrical
Machine connects, and is equipped with water board in babinet, water board is equipped with trapezoidal limbers, detachably catalyst tank, babinet are equipped with babinet
Interior installation headlamp, babinet top inner wall are equipped with camera, and babinet top is connected with appendix, the appendix other end and gas
Purifier connects, and babinet bottom is equipped with drain pipe, and overflow pipe one end is connected with babinet top, the overflow pipe other end and drain pipe
Connection.
As the further scheme of the present invention：The guide wheel is equipped with parking brake.
As further scheme of the invention：It is flat where plane and agitator arm where the auxiliary agitating plate
Face is mutually perpendicular to.
As further scheme of the invention：The gauze pocket beginning is equipped with bungee, and gauze pocket is internally provided with more
Layer interlayer net.
As further scheme of the invention：Through hole is uniformly provided with the catalyst tank side wall.
As further scheme of the invention：The camera is connected with external display device.
As further scheme of the invention：The water board is detachably connected with babinet.
As further scheme of the invention：The drain pipe is equipped with strainer with babinet junction.
Compared with prior art, the beneficial effects of the invention are as follows：Guide wheel of the present invention facilitates device to move, time saving and energy saving, adds
Hot device ensures the most desirable temperature of reaction, and thermometer measures case body temperature at any time, and PH detectors measure reaction solution in babinet
Acid-base property, ensures suitable reaction environment, and fluid flowmeter record enters the amount of reaction liquid in babinet, and liquid level gauge measures at any time
The amount of reaction solution, is conveniently replenished in time in babinet, and timer record simultaneously is used for controlling the reaction time, ensures the accurate of the extent of reaction
Property, convenient operation carries out reaction by stirring motor being stirred up and down, there is provided reaction solution and solid reactant
Contact and impact, there is provided reaction efficiency and effect, while the bubble of generation is punctured by spine, beneficial to its reaction, pass through runner
Drive returning face plate to rotate, improve the speed of current, facilitate liquid reactants and solid reactant comes into full contact with impact, improves instead
The speed and effect answered, are entered by water from trapezoidal limbers big opening end, and the outflow of osculum end, improves water velocity, improve reaction
Speed and effect, by medicament adding tube physical examination suitable excipients, ensure the progress of reaction, catalyst be housed in catalyst tank,
Facilitate the progress of chemical reaction, headlamp provides illumination for some special reactions, while conveniently checks the reaction feelings in babinet
Condition, reaction solid is placed in gauze pocket, by being inflated to air bag, changes the overall buoyancy of reaction solid and air bag,
Reaction solid is suspended in reaction solution rolling, increase reaction contact area, improve reaction rate, while avoid unreacted solid
Body residue enters in reaction solution, is convenient to clean at the same time, sees the response situation in babinet, gas purification dress clearly in time by camera
The gas for collecting that simultaneously purification reaction produces is put, avoids it from being directly discharged in air, causes environmental pollution, strainer avoids impurity from hindering
Pipeline is filled in, overflow pipe avoids reaction solution from excessively influencing to react, simple in structure, easy to use, beneficial to popularization.
Brief description of the drawings
Fig. 1 is a kind of structure diagram of efficiently chemical industry solid-liquid security reaction device.
Fig. 2 is a kind of structure diagram of agitator arm in efficiently chemical industry solid-liquid security reaction device.
Fig. 3 is a kind of structure diagram of gauze pocket in efficiently chemical industry solid-liquid security reaction device.
In figure：1st, guide wheel, 2, anti-sump, 3, stirring motor, 4, babinet, 5, drain pipe, 6, strainer, 7, heater, 8, temperature
Degree meter, 9, PH detectors, 10, water inlet pipe, 11, fluid flowmeter, 12, liquid level gauge, 13, timer, 14, camera, 15, gas
Capsule, 16, gauze pocket, 17, appendix, 18, gas cleaning plant, 19, overflow pipe, 20, agitating shaft, 21, helical blade, 22, stir
Mix impeller, 23, auxiliary agitating plate, 24, spine, 25, medicament adding tube, 26, appendix, 27, inflation means of deflation, 28, catalysis
Agent tank, 29, headlamp, 30, bungee, 31, interlayer net, 32, runner, 33, returning face plate, 34, water board, 35, limbers.
Embodiment
The technical solution of this patent is described in more detail with reference to embodiment.
- 3 are please referred to Fig.1, a kind of efficiently chemical industry solid-liquid security reaction device, including guide wheel 1, shaft 2, babinet 4, drain pipe
5th, heater 7, water inlet pipe 10, fluid flowmeter 11, camera 14, air bag 15, gauze pocket 16, gas cleaning plant 18 and overflow
Pipe 19,4 bottom surface of babinet are equipped with guide wheel 1, and guide wheel 1 is equipped with parking brake, and guide wheel 1 facilitates device to move, time saving and energy saving, babinet
Heater 7 is equipped with 4,4 side wall of babinet is equipped with thermometer 8 and PH detectors 9, and heater 7 ensures the most suitable temperature of reaction
Degree, thermometer 8 measure temperature in babinet 4 at any time, and PH detectors 9 measure the acid-base property of reaction solution in babinet 4, ensure suitable anti-
Environment is answered, is equipped with stirring motor 3 in babinet 4, stirring motor 3 is externally provided with anti-sump 2, and anti-sump 2 avoids external reaction liquid to stirring
The influence of motor 3 is mixed, 3 output shaft of stirring motor is connected with agitating shaft 20, and the winding of 20 outer wall of agitating shaft sets helical blade 21,
Agitator arm 22 is installed, agitator arm 22 is equipped with auxiliary agitating plate 23, the plane where auxiliary agitating plate 23 on agitating shaft 20
It is mutually perpendicular to the plane where agitator arm 22, spine 24 is designed with 4 inner wall of 22 edge of agitator arm and babinet, by stirring
Mix motor 3 and being stirred up and down is carried out to reaction, there is provided contact and impact of the reaction solution with solid reactant, there is provided is anti-
Efficiency and effect are answered, while the bubble of generation is punctured by spine 24, beneficial to its reaction, water inlet pipe 10 is connected with 4 top of babinet,
Fluid flowmeter 11 is installed, the record of fluid flowmeter 11 enters the amount of reaction liquid in babinet 4,4 top of babinet on water inlet pipe 10
Equipped with liquid level gauge 12 and timer 13, liquid level gauge 12 measures the amount of reaction solution in babinet 4 at any time, is conveniently replenished in time, timer
13 record and for controlling the reaction time, ensure the accuracy of the extent of reaction, convenient operation, babinet 4 is interior to be equipped with air bag 15, air bag
15 lower sections are connected by lifting rope with gauze pocket 16, and air bag 15 is connected by appendix 26 with inflation means of deflation 27, gauze pocket 16
Beginning is equipped with bungee 30, and gauze pocket 16 is internally provided with multilayer interlayer net 31, and reaction solid is placed layering respectively is placed on gauze
In on interlayer net 31 in pocket 16, by being inflated to air bag 15, change the overall buoyancy of reaction solid and air bag 15, make anti-
Answer solid to suspend in reaction solution rolling, increase reaction contact area, improve reaction rate, 4 side wall of babinet is equipped with medicament addition
Pipe 25, medicament adding tube 25 are equipped with scale, by 25 physical examination suitable excipients of medicament adding tube, ensure the progress of reaction, babinet 4
Interior to be equipped with runner 32,32 outer wall of runner is equipped with returning face plate 33, and runner 32 is connected with external motor, is driven and overturn by runner 32
Plate 33 rotates, and improves the speed of current, facilitates the speed for coming into full contact with impact, improving reaction of liquid reactants and solid reactant
Degree and effect, babinet 4 is interior to be equipped with water board 34, and water board 34 is equipped with trapezoidal limbers 35, and water board 34 and babinet 4 are detachable
Connection, is entered by water from trapezoidal 35 big opening end of limbers, and the outflow of osculum end, improves water velocity, improve the speed of reaction with
Effect, is detachably equipped with catalyst tank 28 on babinet 4, is uniformly provided with through hole on 28 side wall of catalyst tank, catalyst tank 28 is built-in
There is catalyst, facilitate the progress of chemical reaction, install 29. headlamp 29 of headlamp in babinet 4 provides photograph for some special reactions
It is bright, while conveniently check the response situation in babinet 4,4 top inner wall of babinet is equipped with camera 14, and camera 14 is shown with exterior
Equipment connects, and sees the response situation in babinet 4 clearly in time by camera 14,4 top of babinet is connected with appendix 17, appendix
17 other ends are connected with gas cleaning plant 18, and the gas that gas cleaning plant 18 is collected and purification reaction produces, avoids its straight
Run in and be put into air, cause environmental pollution, 4 bottom of babinet is equipped with drain pipe 5, and drain pipe 5 is equipped with strainer with 4 junction of babinet
6, strainer 6 avoids impurity from blocking pipeline, and 19 one end of overflow pipe is connected with 4 top of babinet, and 19 other end of overflow pipe connects with drain pipe 5
Logical, overflow pipe 19 avoids reaction solution from excessively influencing to react.
The present invention operation principle be：Guide wheel of the present invention facilitates device to move, time saving and energy saving, and heater ensures reaction most
Suitable temperature, thermometer measure case body temperature at any time, and PH detectors measure the acid-base property of reaction solution in babinet, and it is suitable to ensure
Reaction environment, fluid flowmeter record enter the amount of reaction liquid in babinet, and liquid level gauge measures the amount of reaction solution in babinet at any time,
Conveniently it is replenished in time, timer record simultaneously is used for controlling the reaction time, ensures the accuracy of the extent of reaction, convenient operation, passes through
Stirring motor carries out being stirred up and down to reaction, there is provided contact and impact of the reaction solution with solid reactant, there is provided
Reaction efficiency and effect, while the bubble of generation is punctured by spine, beneficial to its reaction, rotated by driven by rotating wheel returning face plate,
The speed of current is improved, facilitates the speed and effect that come into full contact with impact, improve reaction of liquid reactants and solid reactant,
Entered by water from trapezoidal limbers big opening end, the outflow of osculum end, improves water velocity, improve the speed and effect of reaction, lead to
Cross medicament adding tube physical examination suitable excipients, ensure the progress of reaction, catalyst is housed in catalyst tank, facilitate chemical reaction into
OK, headlamp provides illumination for some special reactions, while conveniently checks the response situation in babinet, and reaction solid is placed
In gauze pocket, by being inflated to air bag, change the overall buoyancy of reaction solid and air bag, make reaction solid in reaction solution
The middle rolling that suspends, increases reaction contact area, improves reaction rate, while avoid unreacted solid residue from entering reaction solution
It is interior, it is convenient to clean at the same time, sees the response situation in babinet clearly in time by camera, gas cleaning plant is collected and purification reaction
The gas of generation, avoids it from being directly discharged in air, causes environmental pollution, and strainer avoids impurity from blocking pipeline, and overflow pipe is kept away
Exempting from reaction solution excessively influences to react.
The better embodiment of this patent is explained in detail above, but this patent is not limited to above-mentioned embodiment party
Formula, can also be on the premise of this patent objective not be departed from the knowledge that one skilled in the relevant art possesses
Make a variety of changes.
Claims (8)
- A kind of 1. efficiently chemical industry solid-liquid security reaction device, including guide wheel, shaft, babinet, drain pipe, heater, water inlet pipe, liquid Flowmeter body, camera, air bag, gauze pocket, gas cleaning plant and overflow pipe, it is characterised in that the tank floor is set There is guide wheel, heater is equipped with babinet, wall box is equipped with thermometer and PH detectors, stirring motor is equipped with babinet, Stirring motor is externally provided with anti-sump, and stirring motor output shaft and stirring axis connection, the winding of agitating shaft outer wall set helical blade, stir Mix and agitator arm is installed on axis, agitator arm is equipped with auxiliary agitating plate, and point is designed with agitator arm edge and cabinet wall Thorn, water inlet pipe are connected with babinet top, fluid flowmeter are installed on water inlet pipe, babinet top is equipped with liquid level gauge and timer, case Air bag is equipped with vivo, is connected below air bag by lifting rope with gauze pocket, and air bag is connected by appendix with inflation means of deflation, case Body sidewall is equipped with medicament adding tube, and medicament adding tube is equipped with scale, and runner is equipped with babinet, and runner outer wall is equipped with upset Plate, runner are connected with external motor, are equipped with water board in babinet, water board is equipped with trapezoidal limbers, is detachably set on babinet There is catalyst tank, headlamp is installed in babinet, babinet top inner wall is equipped with camera, and babinet top is connected with appendix, gas transmission The pipe other end is connected with gas cleaning plant, and babinet bottom is equipped with drain pipe, and overflow pipe one end is connected with babinet top, overflow pipe The other end is connected with drain pipe.
- 2. a kind of efficiently chemical industry solid-liquid security reaction device according to claim 1, it is characterised in that on the guide wheel Equipped with parking brake.
- 3. a kind of efficiently chemical industry solid-liquid security reaction device according to claim 1, it is characterised in that the auxiliary is stirred Mix the plane where plate and the plane where agitator arm is mutually perpendicular to.
- A kind of 4. efficiently chemical industry solid-liquid security reaction device according to claim 1, it is characterised in that the gauze pocket Beginning is equipped with bungee, and gauze pocket is internally provided with multilayer interlayer net.
- A kind of 5. efficiently chemical industry solid-liquid security reaction device according to claim 1, it is characterised in that the catalyst Through hole is uniformly provided with pot sidewall.
- A kind of 6. efficiently chemical industry solid-liquid security reaction device according to claim 1, it is characterised in that the camera It is connected with external display device.
- A kind of 7. efficiently chemical industry solid-liquid security reaction device according to claim 1, it is characterised in that the water board It is detachably connected with babinet.
- A kind of 8. efficiently chemical industry solid-liquid security reaction device according to claim 1, it is characterised in that the drain pipe Strainer is equipped with babinet junction.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711335308.1A CN107899518A (en) | 2017-12-14 | 2017-12-14 | A kind of efficiently chemical industry solid-liquid security reaction device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711335308.1A CN107899518A (en) | 2017-12-14 | 2017-12-14 | A kind of efficiently chemical industry solid-liquid security reaction device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107899518A true CN107899518A (en) | 2018-04-13 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711335308.1A Pending CN107899518A (en) | 2017-12-14 | 2017-12-14 | A kind of efficiently chemical industry solid-liquid security reaction device |
Country Status (1)
| Country | Link |
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| CN (1) | CN107899518A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111821932A (en) * | 2020-07-15 | 2020-10-27 | 中国科学院上海有机化学研究所 | Continuous preparation device and preparation method of trialkyl phosphine oxide |
-
2017
- 2017-12-14 CN CN201711335308.1A patent/CN107899518A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111821932A (en) * | 2020-07-15 | 2020-10-27 | 中国科学院上海有机化学研究所 | Continuous preparation device and preparation method of trialkyl phosphine oxide |
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180413 |