CN106378075A - Floating ball positioning bubble removing reaction kettle - Google Patents

Floating ball positioning bubble removing reaction kettle Download PDF

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Publication number
CN106378075A
CN106378075A CN201611016949.6A CN201611016949A CN106378075A CN 106378075 A CN106378075 A CN 106378075A CN 201611016949 A CN201611016949 A CN 201611016949A CN 106378075 A CN106378075 A CN 106378075A
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CN
China
Prior art keywords
shaft
fixed
froth breaking
shell
net
Prior art date
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Granted
Application number
CN201611016949.6A
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Chinese (zh)
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CN106378075B (en
Inventor
孟祥宇
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
XINGTAI MAOXIN CHEMICAL PRODUCT CO., LTD.
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Guangxi University
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Priority to CN201611016949.6A priority Critical patent/CN106378075B/en
Publication of CN106378075A publication Critical patent/CN106378075A/en
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Publication of CN106378075B publication Critical patent/CN106378075B/en
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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D19/00Degasification of liquids
    • B01D19/02Foam dispersion or prevention
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/0013Controlling the temperature of the process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/006Baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00083Coils
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00765Baffles attached to the reactor wall
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00779Baffles attached to the stirring means
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18Details relating to the spatial orientation of the reactor
    • B01J2219/185Details relating to the spatial orientation of the reactor vertical

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Degasification And Air Bubble Elimination (AREA)

Abstract

The invention discloses a floating ball positioning bubble removing reaction kettle, which comprises a base, a case, a motor and a feeding opening, wherein stirring blades are fixed between two stirring transverse rods; a heat exchange coil pipe is fixedly arranged in the case; wave-shaped bulges are arranged on the inner side wall of the case; a horizontal defoaming net is arranged right above the stirring transverse rod at the upper side; a support position limiting device is arranged under the defoaming net; the support position limiting device consists of a positioning limiting block, steel balls and a rotating groove; a plurality of floating balls are fixed at the lower surface of the defoaming net; a vertical rod in vertical arrangement is fixed at the upper surface of the defoaming net; scale lines are drawn on the vertical rod. A stirring rotator is driven by a motor to rotate; inside liquid is stirred through the stirring blades; meanwhile, the wave-shaped bulges arranged on the side wall of the case are matched, so that reaction liquid generates turbulent flow; the reaction speed is effectively accelerated; the defoaming net is positioned through the floating balls; the defoaming net is maintained on the surface of the liquid for removing bubbles; the normal implementation of defoaming is ensured.

Description

A kind of ball float positions the reactor of de-bubble
Technical field
The present invention relates to a kind of chemical industry equipment, specifically a kind of reactor of ball float positioning de-bubble.
Background technology
Reactor is the most commonly used reaction vessel of chemical field, and substantial amounts of material can react in reactor, obtain To corresponding chemical industry product.Material is in a kettle., it usually needs stirring, to reach the abundant thoroughly purpose of reaction, along with The stirring of agitating device, makes liquid surface easily form bubble, what aeration reacted is normally carried out, in prior art, by being Froth breaking net is fixed on shaft, makes froth breaking net reduce foam and produce, but its position is fixed, the liquid levels in reactor are solid Fixed, thus the liquid volume of reaction is restricted, when liquid is more, still can not realize defoaming function, be unfavorable for reacting Kettle uses.
Content of the invention
It is an object of the invention to provide a kind of ball float positions the reactor of de-bubble, to solve to propose in above-mentioned background technology Problem.
For achieving the above object, the present invention provides following technical scheme:
A kind of ball float positions the reactor of de-bubble, including base, shell, motor and charging aperture;Described shell is fixed on base, Motor is fixedly mounted on the top of shell, and the output shaft of motor extend into inside the shell straight down, in the output shaft lower end of motor It is fixedly connected vertical shaft, the lower end of shaft is arranged on the bottom of shell by bearing, is fixed with two on shaft The individual stirring cross bar being parallel to each other, fixes paddle between two stirring cross bars, and paddle is platy structure;Described inside the shell is solid Equipped with heat exchange coil, heat exchange coil is located at the outside of paddle slewing area for Dingan County, and the lower end of heat exchange coil connects water inlet pipe, on End connection outlet pipe;The medial wall of described shell is provided with wavy projection;The surface of stirring cross bar up sets There is the froth breaking net of level, shaft passes through froth breaking net, shaft is provided with sleeve with the junction of froth breaking net, and sleeve is fixed on and disappears On indulging in serfing the Net, its internal diameter is more than shaft, the lower section of froth breaking net is provided with supporting and limiting device, supporting and limiting device is by spacing Block, steel ball and rotation slot are constituted, and limited block is fixed on shaft, and is looped around the outside of shaft, the upper surface of limited block Offer the semi-circular recesses of concave downward, several steel balls are set in groove, rotation slot is fixed on sleeve, and corresponding steel ball Position on be also equipped with semi-circular recesses, rotation slot is buckled on limited block, so that limited block is relatively rotated with rotation slot, to froth breaking Net supports, and keeps it from moving;The lower surface of described froth breaking net is fixed with several ball floats;The upper surface of described froth breaking net is solid Surely there is vertical montant, froth breaking net passes shell straight up, is decorated with graduation mark on montant, and its end is fixed with handle; The top of described shell opens up charging aperture, and bottom connects discharge nozzle.
Further:Described base is damping base.
Further:At least provided with four, the height of paddle is the 1/3~1/2 of stirring shaft length to described paddle.
Further:The material of described montant is plastics.
Compared with prior art, the invention has the beneficial effects as follows:The present invention drives stirring to walk around dynamic, paddle by motor Agitation internal liquid, coordinates the wavy bulge on side wall of outer shell so that reactant liquor produces sinuous flow simultaneously, is effectively increased anti- Answer speed, while reaction, the temperature of reactant liquor is changed so as to reaction condition is in the temperature adapting to by heat exchange coil, protect Card quick and high efficient reaction is carried out;Ball float positioning is crossed by froth breaking Netcom, keeps froth breaking net on the surface of liquid, bubble is removed it is ensured that Froth breaking is normally carried out, and liquid body will not increase and affect froth breaking, froth breaking net can also indicate the surplus of internal liquid, is easy to grasp The amount of reactant, is easy to enterprise and produces, reduce energy waste.
Brief description
Fig. 1 is a kind of structural representation of the reactor that ball float positions de-bubble.
In figure:1- base, 2- shell, 3- motor, 4- charging aperture, 5- shaft, 6- stirs cross bar, 7- paddle, and 8- is convex Rise, 9- heat exchange coil, 10- water inlet pipe, 11- outlet pipe, 12- discharge nozzle, 13- froth breaking net, 14- ball float, 15- limited block, 16- steel Pearl, 17- rotation slot, 18- montant, 19- graduation mark, 20- handle, 21- sleeve.
Specific embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete Site preparation description is it is clear that described embodiment is only a part of embodiment of the present invention, rather than whole embodiments.It is based on Embodiment in the present invention, it is every other that those of ordinary skill in the art are obtained under the premise of not making creative work Embodiment, broadly falls into the scope of protection of the invention.
Refer to figure, in the embodiment of the present invention, a kind of ball float positions the reactor of de-bubble, including base 1, shell 2, motor 3 and charging aperture 4;Described shell 2 is fixed on base 1, and base 1 is damping base, weakens the vibration producing when reactor runs, Reduce noise, protection equipment, motor 3 is fixedly mounted on the top of shell 2, and the output shaft of motor 3 extend into shell 2 straight down Interior, it is fixedly connected vertical shaft 5 in the output shaft lower end of motor 3, the lower end of shaft 5 is arranged on shell 2 by bearing Bottom, two stirring cross bars 6 being parallel to each other are fixed with shaft 5, between two stirring cross bars 6, fix paddle 7, Paddle 7 is platy structure, and at least provided with four, the height of paddle 7 is the 1/3~1/2 of shaft 5 length to paddle 7; It is installed with heat exchange coil 9, heat exchange coil 9 is located at the outside of paddle 7 slewing area, heat exchange coil 9 will in described shell 2 The heat producing during reaction is taken away, or provides heat for reaction, adjusts reaction temperature, the lower end connection water inlet pipe of heat exchange coil 9 10, upper end connects outlet pipe 11, so that the water circulation in heat exchange coil 9 is flowed, and constantly adjusts internal temperature;Described shell 2 Medial wall is provided with has certain obstruction to reactant liquor so that reactant liquor produces sinuous flow, effectively in wavy raised 8, raised 8 Increased response speed;The surface of stirring cross bar 6 up is provided with the froth breaking net 13 of level, and shaft 5 passes through froth breaking Net 13, shaft 5 is provided with sleeve 21 with the junction of froth breaking net 13, and sleeve 21 is fixed on froth breaking net 13, and its internal diameter is more than Shaft 5, when so that shaft 5 is rotated, froth breaking net 13 will not follow rotation, and the lower section of froth breaking net 13 is provided with support limit dress Put, supporting and limiting device is made up of limited block 15, steel ball 16 and rotation slot 17, and limited block 15 is fixed on shaft 5, and cincture In the outside of shaft 5, the upper surface of limited block 15 offers the semi-circular recesses of concave downward, arranges several steel in groove Pearl 16, rotation slot 17 is fixed on sleeve 21, and is also equipped with semi-circular recesses on the position of corresponding steel ball 16, and rotation slot 17 is detained On limited block 15, so that limited block 15 is relatively rotated with rotation slot 17, offset 13 supports of indulging in serfing the Net, and keep it from moving;Described The lower surface of froth breaking net 13 is fixed with several ball floats 14, and ball float 14 is contacted with the page, and froth breaking net 13 is supported on liquid level;Institute The upper surface stating froth breaking net 13 is fixed with vertical montant 18, and the material of montant 18 is plastics, and froth breaking net 13 passes straight up Shell 2, is decorated with graduation mark 19 on montant 18, and its end is fixed with handle 20, be can indicate that by floating of froth breaking net 13 The height of liquid level, is easy to grasp internal liquid surplus;The top of described shell 2 opens up charging aperture 4, and bottom connects discharge nozzle 12.
Liquid reacts in reactor, drives stirring to turn 5 rotations by motor 3, paddle 7 stirs internal liquid, simultaneously Wavy bulge 8 on cooperation shell 2 side wall, so that reactant liquor produces sinuous flow, is effectively increased response speed, in reaction Simultaneously by heat exchange coil 9 change reactant liquor temperature so as to reaction condition in the temperature adapting to it is ensured that quick and high efficient reaction Carry out;Froth breaking net 13 is positioned by ball float 14, keeps froth breaking net 13 on the surface of liquid, bubble is removed it is ensured that froth breaking is normal Carry out, liquid body will not increase and affect froth breaking, froth breaking net 13 can also indicate the surplus of internal liquid, be easy to grasp reactant Amount, be easy to enterprise produce, reduce energy waste.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie In the case of the spirit or essential attributes of the present invention, the present invention can be realized in other specific forms.Therefore, no matter From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power Profit requires rather than described above limits, it is intended that all in the implication and scope of the equivalency of claim by falling Change is included in the present invention.Any reference in claim should not be considered as limiting involved claim.
Moreover, it will be appreciated that although this specification is been described by according to embodiment, not each embodiment only wraps Containing an independent technical scheme, only for clarity, those skilled in the art should for this narrating mode of description Using description as an entirety, the technical scheme in each embodiment can also form those skilled in the art through appropriately combined Understandable other embodiment.

Claims (4)

1. a kind of ball float positions the reactor of de-bubble, including base(1), shell(2), motor(3)And charging aperture(4);Its feature It is:Described shell(2)It is fixed on base(1)On, motor(3)It is fixedly mounted on shell(2)Top, motor(3)Output Axle extend into shell straight down(2)Interior, in motor(3)Output shaft lower end be fixedly connected vertical shaft(5), shaft (5)Lower end shell is arranged on by bearing(2)Bottom, in shaft(5)On to be fixed with two stirrings of being parallel to each other horizontal Bar(6), two stirring cross bars(6)Between fix paddle(7), paddle(7)For platy structure;Described shell(2)Interior fixation Heat exchange coil is installed(9), heat exchange coil(9)Positioned at paddle(7)The outside of slewing area, heat exchange coil(9)Lower end even Logical water inlet pipe(10), upper end connects outlet pipe(11);Described shell(2)Medial wall be provided with wavy projection(8);? The stirring cross bar of top(6)Surface be provided with the froth breaking net of level(13), shaft(5)Through froth breaking net(13), shaft (5)With froth breaking net(13)Junction be provided with sleeve(21), sleeve(21)It is fixed on froth breaking net(13)On, its internal diameter be more than stir Mix axle(5), in froth breaking net(13)Lower section be provided with supporting and limiting device, supporting and limiting device is by limited block(15), steel ball (16)And rotation slot(17)Constitute, limited block(15)It is fixed on shaft(5)On, and it is looped around shaft(5)Outside, spacing Block(15)Upper surface offer several steel balls be set in the semi-circular recesses of concave downward, groove(16), rotation slot(17) It is fixed on sleeve(21)On, and corresponding steel ball(16)Position on be also equipped with semi-circular recesses, rotation slot(17)It is buckled in spacing Block(15)On, make limited block(15)With rotation slot(17)Relatively rotate, offset and indulge in serfing the Net(13)Support, and keep it from moving;Institute State froth breaking net(13)Lower surface be fixed with several ball floats(14);Described froth breaking net(13)Upper surface be fixed with vertical perpendicular Bar(18), froth breaking net(13)Pass shell straight up(2), in montant(18)On be decorated with graduation mark(19), fixing on its end There is handle(20);Described shell(2)Top open up charging aperture(4), bottom connects discharge nozzle(12).
2. a kind of ball float according to claim 1 position de-bubble reactor it is characterised in that:Described base(1)For subtracting Shake base.
3. a kind of ball float according to claim 1 position de-bubble reactor it is characterised in that:Described paddle(7)Extremely It is provided with four less, paddle(7)Height be shaft(5)The 1/3~1/2 of length.
4. a kind of ball float according to claim 1 position de-bubble reactor it is characterised in that:Described montant(18)Material Matter is plastics.
CN201611016949.6A 2016-11-18 2016-11-18 A kind of reaction kettle of floating ball positioning de-bubble Active CN106378075B (en)

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CN106378075B CN106378075B (en) 2019-04-05

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108261998A (en) * 2018-04-10 2018-07-10 湖南铭煌科技发展有限公司 A kind of defoaming device applied to polycarboxylic acid water reducer macromer
CN108542262A (en) * 2018-05-11 2018-09-18 朱柏艳 One kind is convenient for milk-powder brewing uniformly and the good cup of cooling
CN112140694A (en) * 2020-09-11 2020-12-29 杭州伟成印刷有限公司 Gravure ink tank device integrating safety, environmental protection and energy saving and control method thereof
CN113856570A (en) * 2021-09-30 2021-12-31 池州方达科技有限公司 Reaction device for condensation of hydroxyethyl acrylate

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1996024397A2 (en) * 1995-02-08 1996-08-15 Medtronic, Inc. Perfusion system
CN104549104A (en) * 2014-12-29 2015-04-29 常州市龙道电子商务有限公司 Reaction kettle provided with built-in defomaing device
CN204768687U (en) * 2015-06-24 2015-11-18 建德市聚合新材料有限公司 Two heat transfer reation kettle
CN205495586U (en) * 2016-04-01 2016-08-24 西北民族大学 Be provided with fire fighting equipment's reation kettle
CN205586990U (en) * 2016-05-04 2016-09-21 绍兴市宇洲化工有限公司 Reaction kettle

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1996024397A2 (en) * 1995-02-08 1996-08-15 Medtronic, Inc. Perfusion system
CN104549104A (en) * 2014-12-29 2015-04-29 常州市龙道电子商务有限公司 Reaction kettle provided with built-in defomaing device
CN204768687U (en) * 2015-06-24 2015-11-18 建德市聚合新材料有限公司 Two heat transfer reation kettle
CN205495586U (en) * 2016-04-01 2016-08-24 西北民族大学 Be provided with fire fighting equipment's reation kettle
CN205586990U (en) * 2016-05-04 2016-09-21 绍兴市宇洲化工有限公司 Reaction kettle

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108261998A (en) * 2018-04-10 2018-07-10 湖南铭煌科技发展有限公司 A kind of defoaming device applied to polycarboxylic acid water reducer macromer
CN108542262A (en) * 2018-05-11 2018-09-18 朱柏艳 One kind is convenient for milk-powder brewing uniformly and the good cup of cooling
CN112140694A (en) * 2020-09-11 2020-12-29 杭州伟成印刷有限公司 Gravure ink tank device integrating safety, environmental protection and energy saving and control method thereof
CN112140694B (en) * 2020-09-11 2022-06-03 杭州伟成印刷有限公司 Gravure ink tank device integrating safety, environmental protection and energy saving and control method thereof
CN113856570A (en) * 2021-09-30 2021-12-31 池州方达科技有限公司 Reaction device for condensation of hydroxyethyl acrylate
CN113856570B (en) * 2021-09-30 2022-06-10 池州方达科技有限公司 Reaction device for condensation of hydroxyethyl acrylate

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