CN107898556A - Magnetic far-infrared negative-ion energy eye-mask - Google Patents
Magnetic far-infrared negative-ion energy eye-mask Download PDFInfo
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- CN107898556A CN107898556A CN201711242922.3A CN201711242922A CN107898556A CN 107898556 A CN107898556 A CN 107898556A CN 201711242922 A CN201711242922 A CN 201711242922A CN 107898556 A CN107898556 A CN 107898556A
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- infrared
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- ion energy
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- 239000000654 additive Substances 0.000 claims abstract description 46
- 230000000996 additive effect Effects 0.000 claims abstract description 45
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- 229920000728 polyester Polymers 0.000 claims abstract description 27
- 239000002270 dispersing agent Substances 0.000 claims abstract description 13
- 125000000129 anionic group Chemical group 0.000 claims abstract description 11
- 239000006249 magnetic particle Substances 0.000 claims abstract description 11
- 239000004744 fabric Substances 0.000 claims abstract description 10
- 229920000742 Cotton Polymers 0.000 claims abstract description 4
- 239000002657 fibrous material Substances 0.000 claims abstract description 4
- 239000000945 filler Substances 0.000 claims abstract description 4
- 238000002844 melting Methods 0.000 claims abstract description 4
- 230000008018 melting Effects 0.000 claims abstract description 4
- 239000000758 substrate Substances 0.000 claims abstract description 4
- 239000002245 particle Substances 0.000 claims description 20
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 15
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 15
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 14
- 239000004575 stone Substances 0.000 claims description 11
- XOLBLPGZBRYERU-UHFFFAOYSA-N SnO2 Inorganic materials O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 claims description 10
- GEYXPJBPASPPLI-UHFFFAOYSA-N manganese(III) oxide Inorganic materials O=[Mn]O[Mn]=O GEYXPJBPASPPLI-UHFFFAOYSA-N 0.000 claims description 10
- 239000004005 microsphere Substances 0.000 claims description 10
- 239000002105 nanoparticle Substances 0.000 claims description 10
- 239000000843 powder Substances 0.000 claims description 10
- 150000001450 anions Chemical class 0.000 claims description 9
- 238000005245 sintering Methods 0.000 claims description 9
- 229910052613 tourmaline Inorganic materials 0.000 claims description 9
- 229940070527 tourmaline Drugs 0.000 claims description 9
- 239000011032 tourmaline Substances 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 7
- 238000002360 preparation method Methods 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 6
- 238000009987 spinning Methods 0.000 claims description 6
- 230000032050 esterification Effects 0.000 claims description 4
- 238000005886 esterification reaction Methods 0.000 claims description 4
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- 238000006068 polycondensation reaction Methods 0.000 claims description 4
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- -1 Polyethylene Polymers 0.000 claims description 3
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- 239000004202 carbamide Substances 0.000 claims description 3
- 238000005119 centrifugation Methods 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 238000001027 hydrothermal synthesis Methods 0.000 claims description 3
- 239000011656 manganese carbonate Substances 0.000 claims description 3
- 229910000016 manganese(II) carbonate Inorganic materials 0.000 claims description 3
- 229920000573 polyethylene Polymers 0.000 claims description 3
- 229910001220 stainless steel Inorganic materials 0.000 claims description 3
- 239000010935 stainless steel Substances 0.000 claims description 3
- 238000005406 washing Methods 0.000 claims description 3
- NGWKGSCSHDHHAJ-YPFQVHCOSA-N Liquoric acid Chemical compound C1C[C@H](O)C(C)(C)C2CC[C@@]3(C)[C@]4(C)C[C@H]5O[C@@H]([C@](C6)(C)C(O)=O)C[C@@]5(C)[C@@H]6C4=CC(=O)C3[C@]21C NGWKGSCSHDHHAJ-YPFQVHCOSA-N 0.000 claims description 2
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 claims description 2
- 229910010967 Ti—Sn Inorganic materials 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 claims description 2
- 238000009833 condensation Methods 0.000 claims description 2
- 230000005494 condensation Effects 0.000 claims description 2
- 238000003837 high-temperature calcination Methods 0.000 claims description 2
- 230000005389 magnetism Effects 0.000 claims description 2
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- 238000006116 polymerization reaction Methods 0.000 claims description 2
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- 230000005855 radiation Effects 0.000 description 6
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- 150000002500 ions Chemical class 0.000 description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 230000017531 blood circulation Effects 0.000 description 2
- 235000013339 cereals Nutrition 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 230000008092 positive effect Effects 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- 208000019901 Anxiety disease Diseases 0.000 description 1
- 229920002955 Art silk Polymers 0.000 description 1
- 239000004594 Masterbatch (MB) Substances 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 239000004113 Sepiolite Substances 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 230000036506 anxiety Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
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- 239000003054 catalyst Substances 0.000 description 1
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- 230000006872 improvement Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
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- 238000002074 melt spinning Methods 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 230000004089 microcirculation Effects 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F9/00—Methods or devices for treatment of the eyes; Devices for putting-in contact lenses; Devices to correct squinting; Apparatus to guide the blind; Protective devices for the eyes, carried on the body or in the hand
- A61F9/04—Eye-masks ; Devices to be worn on the face, not intended for looking through; Eye-pads for sunbathing
- A61F9/045—Eye-shades or visors; Shields beside, between or below the eyes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61N—ELECTROTHERAPY; MAGNETOTHERAPY; RADIATION THERAPY; ULTRASOUND THERAPY
- A61N2/00—Magnetotherapy
- A61N2/002—Magnetotherapy in combination with another treatment
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61N—ELECTROTHERAPY; MAGNETOTHERAPY; RADIATION THERAPY; ULTRASOUND THERAPY
- A61N2/00—Magnetotherapy
- A61N2/004—Magnetotherapy specially adapted for a specific therapy
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61N—ELECTROTHERAPY; MAGNETOTHERAPY; RADIATION THERAPY; ULTRASOUND THERAPY
- A61N2/00—Magnetotherapy
- A61N2/06—Magnetotherapy using magnetic fields produced by permanent magnets
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61N—ELECTROTHERAPY; MAGNETOTHERAPY; RADIATION THERAPY; ULTRASOUND THERAPY
- A61N5/00—Radiation therapy
- A61N5/06—Radiation therapy using light
- A61N5/0613—Apparatus adapted for a specific treatment
- A61N5/0625—Warming the body, e.g. hyperthermia treatment
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
- C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
- C08G63/16—Dicarboxylic acids and dihydroxy compounds
- C08G63/18—Dicarboxylic acids and dihydroxy compounds the acids or hydroxy compounds containing carbocyclic rings
- C08G63/181—Acids containing aromatic rings
- C08G63/183—Terephthalic acids
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/92—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61N—ELECTROTHERAPY; MAGNETOTHERAPY; RADIATION THERAPY; ULTRASOUND THERAPY
- A61N5/00—Radiation therapy
- A61N5/06—Radiation therapy using light
- A61N2005/0635—Radiation therapy using light characterised by the body area to be irradiated
- A61N2005/0643—Applicators, probes irradiating specific body areas in close proximity
- A61N2005/0645—Applicators worn by the patient
- A61N2005/0647—Applicators worn by the patient the applicator adapted to be worn on the head
- A61N2005/0648—Applicators worn by the patient the applicator adapted to be worn on the head the light being directed to the eyes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61N—ELECTROTHERAPY; MAGNETOTHERAPY; RADIATION THERAPY; ULTRASOUND THERAPY
- A61N5/00—Radiation therapy
- A61N5/06—Radiation therapy using light
- A61N2005/0658—Radiation therapy using light characterised by the wavelength of light used
- A61N2005/0659—Radiation therapy using light characterised by the wavelength of light used infrared
- A61N2005/066—Radiation therapy using light characterised by the wavelength of light used infrared far infrared
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61N—ELECTROTHERAPY; MAGNETOTHERAPY; RADIATION THERAPY; ULTRASOUND THERAPY
- A61N5/00—Radiation therapy
- A61N5/06—Radiation therapy using light
- A61N2005/0664—Details
Abstract
This application involves a kind of magnetic far-infrared negative-ion energy eye-mask, from outside to inside, include shading layer of cloth, magnetic far-infrared fiber chip layer, elastic sponge layer and pure cotton cloth layer successively, the magnetic far-infrared fiber chip layer is made of magnetic far-infrared fibrous material, the magnetic far-infrared fiber is using polyester as substrate, it is blended by melting using magnetic particle, far infrared additive, anionic additive, additive dispersant as filler, it is prepared.
Description
Technical field
This application involves a kind of energy eye-mask, more particularly to a kind of magnetic far-infrared negative-ion energy eye-mask.
Background technology
As social competition aggravates, the pressure that people bear is increasing, nervous, and mood is uneasy, then triggers each
The disease of kind various kinds, particularly cybraian, student race and working clan, before being sitting in computer for a long time, easily there is spirit in excess eye-using
Anxiety, glasses fatigue, forms myopia, and severe patient also results in Other diseases.
It is well known that infrared ray can be stimulated directly, massaging skin, make around to produce fuel factor, promote capillary blood stream
Dynamic active, microcirculation is accelerated, and has preferable health-care efficacy.
The content of the invention
The present invention is intended to provide a kind of magnetic far-infrared negative-ion energy eye-mask, set forth above to solve the problems, such as.
A kind of magnetic far-infrared negative-ion energy eye-mask is provided in the embodiment of the present invention, from outside to inside, is included successively
There are shading layer of cloth, magnetic far-infrared fiber chip layer, elastic sponge layer and pure cotton cloth layer, the magnetic far-infrared fiber chip
Layer is made of magnetic far-infrared fibrous material, and the magnetic far-infrared fiber is using polyester as substrate, with magnetic particle, far infrared
Additive, anionic additive, additive dispersant are filler, blended by melting, and are prepared.
The technical solution that the embodiment of the present invention provides can include the following benefits：
The magnetic far-infrared negative-ion energy eye-mask of the present invention, health-care effect is good, sweat-absorbing breathable, without side-effects, can releive
Ocular nerve and blood vessel, make blood circulation more unimpeded, dispelling fatigue.
The aspect and advantage that the application adds will be set forth in part in the description, and will partly become from the following description
Obtain substantially, or recognized by the practice of the application.It should be appreciated that the general description and following detailed description of the above are only
It is exemplary and explanatory, the application can not be limited.
Brief description of the drawings
Using attached drawing, the invention will be further described, but the embodiment in attached drawing does not form any limit to the present invention
System, for those of ordinary skill in the art, without creative efforts, can also obtain according to the following drawings
Other attached drawings.
Fig. 1 is the structure diagram of eyeshade of the present invention；
Embodiment
Here exemplary embodiment will be illustrated in detail, its example is illustrated in the accompanying drawings.Following description is related to
During attached drawing, unless otherwise indicated, the same numbers in different attached drawings represent the same or similar key element.Following exemplary embodiment
Described in embodiment do not represent and the consistent all embodiments of the present invention.On the contrary, they be only with it is such as appended
The example of the consistent apparatus and method of some aspects being described in detail in claims, of the invention.
The embodiment of the present invention is related to a kind of magnetic far-infrared negative-ion energy eye-mask, with reference to Fig. 1, from outside to inside, successively
Include shading layer of cloth 1, magnetic far-infrared fiber chip layer 2, elastic sponge layer 3 and pure cotton cloth layer 4, wherein, the magnetism
Far IR fibre chip layer 2 is made of magnetic far-infrared fibrous material, the magnetic far-infrared fiber using polyester as substrate, with
Magnetic particle, far infrared additive, anionic additive are filler, blended by melting, and are prepared.
Far-infrared negative-ion energy eye-mask of the present invention, by the magnetic launched in its magnetic far-infrared fiber chip layer
The line of force, far infrared etc. act synergistically, and generate positive effect, eye health protection positive effect.
In magnetic far-infrared fiber described above, its raw material includes according to percentage by weight：2% magnetic particle, 5%
Anionic additive, 8% far infrared additive, surplus be polyester.For the functionalization of fiber, industrial circle usual way
It is inorganic powder of the addition with far-infrared transmitting function, anion emission function etc.；For example patent application 2011110289921
In, tourmaline powder, sepiolite, pearl powder are added in polyester fondant by it carries out melt spinning, is made with healthcare function
Polyester fiber, in technical solution of the present invention, is added by adding magnetic particle, anionic additive and far infrared in the polyester
Agent so that the magnetic far-infrared fiber is provided with the magnetic line of force, anion and far-infrared transmitting function, has expanded answering for polyester fiber
Use scope.
Wherein, in magnetic far-infrared fiber of the invention, the anionic additive is tourmaline anion powder, its
In, particle diameter is that the content of 500nm accounts for the 98% of gross weight in tourmaline anion powder, is preferably 99%, more preferably
99.6%.Currently, the common natural crystal that can discharge anion is two kinds, diatomite and tourmaline, it is diatomaceous mainly into
It is divided into the oxide containing silicon, aluminium and iron etc., its aperture is 50nm, and surface area reaches 37.8m2/ g, can be discharged negative using diatomite
The characteristic of ion, is exploring and is being applied in fiber-like articles for use；Tourmaline has the natural electrode similar to magnet poles,
It is widely used in many fields such as environmental protection, daily life, and tourmaline mineral ultra-fine grinding is added in fiber, because
The powder has positive and negative electrode, and fabric is processed into the artificial silk containing the powder, can be in skin after the fabric and human contact
Surface produces countless weak currents, stimulates blood circulation, and form the negative ion effect in air；At present, tourmaline radiation is negative
The characteristic of ion has been confirmed, it is mixed with other additives, so that it is one that fiber, which has multiple combination functions,
The emphasis of research；In technical scheme, in addition to using anionic additive, also by itself and magnetic particle, far infrared
Additive is used in combination, and by controlling the proportioning of each material, on the premise of keeping each material to give full play to function, has reached negative
The maximization of emission of ions, generates unexpected technique effect.
Wherein, in magnetic far-infrared fiber of the invention, the far infrared additive is a kind of polynary sintered body nanometer
Powder, is specially Si-Zr-Ti-Sn sintered body nanopowders, and particle diameter is less than 1 μm, it is by Tai Ji stone nano particle, ZrO2、
TiO2、SnO2According to what is formed after certain quality proportioning mixed pressuring plate, high temperature sintering, crushing, grinding.As a kind of natural ore deposit
Stone, the main component of Tai Ji stone are silica, and the metalliferous mineral element of lot of trace, its resonance frequency with human body cell
Rate is fairly close, can promote absorption of human body and aggregation positive energy.Currently, natural crystal raw material is applied to functional textile product
Research carrying out, such as, present invention applicant is noticed in prior art, by Tai Ji stone master batch be added to polyester fibre
In dimension, to improve its infrared emission performance, but its function is more single, stability and bad.In addition, in order to increase polyester fiber
Feature, and Multimetal oxide is subjected to simple mechanical mixture, it can not improve the microcosmic phase structure of material,
So that the multi-functional performance of stuff and other stuff is affected.In technical solution of the present invention, carried out using multi-element metal oxide
High temperature sintering, is then added to after then being crushed in magnetic far-infrared fiber, can change microcosmic particle using high temperature sintering
Phase structure, and reconfigure it, form substitutional type solid, the anharmonicity of lattice polarity vibrations is enhanced, so that greatly
Radiance is improved greatly, achieves unexpected beneficial effect.
In the far infrared additive, Tai Ji stone nano particle, ZrO2、TiO2、SnO2Quality proportioning is 9:7:3:3.Matter
Amount proportioning is to influence a kind of important parameter that polynary sintered body nanopowder infrared property plays, and in above-mentioned substance, Tai Ji stone is received
Rice grain has the function of infrared emission, ZrO in itself2、TiO2Also there is certain infra-red radiation ability, and SnO2Itself do not possess
Infra red radiation function, in technical solution of the present invention, by above-mentioned substance mixed sintering, in the case of above-mentioned quality proportioning, SnO2This
Body enables to remaining substance ion fully to merge, the generation for substitutional type solid plays great work as a kind of reinforcing agent
With.
Specifically, which is 500nm, the ZrO2Particle diameter is 300nm, the TiO2Particle diameter is
400nm, the SnO2Particle diameter is 500nm.Performance of the particle diameter of nano particle for nano-particle function produces significant impact, is based on
Different materials, the grain size needed in sintering process is also different, and the present inventor passes through experimental verification, in said ratio feelings
Under condition, under the limitation of above-mentioned particle diameter, said mixture can fully merge in sintering process, so as to fully react, produce
Substitutional type solid, so as to greatly improve the output of infra-red radiation material, improves radiation efficiency in infrared band, plays expectation not
The technique effect arrived.
In addition, the far infrared additive, in sintering process, technical solution of the present invention preferably sinters at 1250 DEG C
3h, when temperature is higher or lower than the sintering temperature, the yield of substitutional type solid declines.
Preferably, additive dispersant is further included in magnetic far-infrared fiber of the present invention, at this time, the polyester
In functional fibre, its raw material includes according to percentage by weight：2% magnetic particle, 5% anionic additive, 8% it is remote red
External additive, 4% additive dispersant, surplus are polyester.Also, the additive dispersant is Mn2O3Porous microsphere, its
In, Mn2O3The preparation process of porous microsphere is：First, by the Mn (CH of 15mmol3COO)2·6H2O, the urea and 2g of 45mmol
Polyethylene glycol-2000 is placed in 40ml ethylene glycol solutions, is stirred, and dissolving finishes, and is then transferred to resulting solution
In stainless steel cauldron, hydro-thermal reaction 30h is sealed at 220 DEG C, natural cooling, centrifugation, collection, washing, drying, obtain
MnCO3, it is finally calcined into 10h at 650 DEG C in Muffle furnace, obtains Mn2O3Porous microsphere；Mn2O3A diameter of 1 μ of porous microsphere
m.The additive dispersant can be uniformly dispersed in polyester fiber, be effectively improved anionic additive and far infrared addition bolus
The generation of poly- phenomenon.
Embodiment 1
The preparation process of magnetic far-infrared fiber described above is：
Step 1, prepare far infrared additive：By Tai Ji stone nano particle, ZrO2、TiO2、SnO2According to 9:7:3:3 mass
Proportioning is uniformly mixed, and is put into mixing bottle and is sufficiently mixed, disc-shaped is pressed on hydraulic press, the high-temperature calcination 3h at 1250 DEG C,
After being cooled to room temperature, take out, crush, grinding is uniform, filters out the sintered body nano particle that particle diameter is less than 1 μm；
Step 2, prepare additive dispersant：First, by the Mn (CH of 15mmol3COO)2·6H2O, the urea of 45mmol and
2g Polyethylene glycol-2000s are placed in 40ml ethylene glycol solutions, are stirred, and dissolving finishes, and then shift resulting solution
Into stainless steel cauldron, hydro-thermal reaction 30h is sealed at 220 DEG C, natural cooling, centrifugation, collection, washing, drying, obtain
MnCO3, it is finally calcined into 10h at 650 DEG C in Muffle furnace, obtains Mn2O3Porous microsphere；Mn2O3A diameter of 1 μ of porous microsphere
m；
Step 3, prepare polyester master particle：First, magnetic particle, far infrared additive, additive dispersant, anion are added
Agent and ethylene glycol is added to mix, ultrasound 5h at room temperature after stirring, obtains mixed liquor；Then by mixed liquor and p-phthalic acid,
Catalyst aid is esterified, and polymerization, obtains polyester master particle, wherein, esterification temperature is 260 DEG C, and pressure 280KPa, esterification yield reaches
Polycondensation reaction is carried out during more than 96.5%, condensation temperature is 290 DEG C, is evacuated to 20Mpa, and polycondensation to inherent viscosity is 0.72
When, discharging, blank；
Step 4, prepare polyester preoriented yarn：Polyester master particle is melted, filter is then fed into and is filtered, through metering
Afterwards, into spinning pack, the tow of ejection is being cooled down, is being oiled, preoriented yarn is wound into after deflector roll, wherein, spinning
Temperature is 285 DEG C, spinning speed 3400m/min；
Step 5, prepare magnetic far-infrared fiber：Polyester preoriented yarn can after a roller, hot tank, two rollers, scroll tube, winding
Compound polyester functional fibre is prepared into, wherein, draft speed 500m/min, draw ratio 3.1, a roll temperature is 90 DEG C,
Two roll temperatures are 140 DEG C.
The far-infrared radiation of fiber is characterized by measuring the normal emittance of magnetic far-infrared fiber in the present embodiment
Can, inspection result shows that its normal emittance is 0.95, is shown in Table 1, accurate on the assessment of bids of far infrared performance according to this area, normal direction hair
Far-infrared textiles can be assessed as more than or equal to 0.8 by penetrating rate, and the composite fibre in the present embodiment meets standard requirement.
Embodiment 2
In the present embodiment, the preparation process of the magnetic far-infrared fiber is similar to Example 1, and difference is：Magnetic
Far infrared additive is not included in property far IR fibre.
Embodiment 3
In the present embodiment, the preparation process of the magnetic far-infrared fiber is similar to Example 1, and difference is：Magnetic
Additive dispersant is not included in property far IR fibre.
Embodiment 4
In the present embodiment, the preparation process of the magnetic far-infrared fiber is similar to Example 1, and difference is：Magnetic
SnO is not included in far infrared additive in property far IR fibre2。
Table 1, the normal emittance of composite fibre in embodiment 1-4
The foregoing is merely the preferred mode of the present invention, it is not intended to limit the invention, it is all in the spiritual and former of the present invention
Within then, any modification, equivalent replacement, improvement and so on, should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of magnetic far-infrared negative-ion energy eye-mask, from outside to inside, includes shading layer of cloth, magnetic far-infrared fiber successively
Chip layer, elastic sponge layer and pure cotton cloth layer, it is characterised in that the magnetic far-infrared fiber chip layer is by magnetic far-infrared
Fibrous material is formed, and the magnetic far-infrared fiber is using polyester as substrate, with magnetic particle, far infrared additive, anion
Additive, additive dispersant are filler, blended by melting, and are prepared.
2. a kind of magnetic far-infrared negative-ion energy eye-mask according to claim 1, it is characterised in that the magnetism is remote
In infrared fibre, its raw material includes according to percentage by weight：2% magnetic particle, 5% anionic additive, 8% it is remote red
External additive, 4% additive dispersant, surplus are polyester.
A kind of 3. magnetic far-infrared negative-ion energy eye-mask according to claim 2, it is characterised in that the anion
Additive is tourmaline anion powder.
A kind of 4. magnetic far-infrared negative-ion energy eye-mask according to claim 3, it is characterised in that the tourmaline bear from
Sub- powder footpath is 500nm.
A kind of 5. magnetic far-infrared negative-ion energy eye-mask according to claim 2, it is characterised in that the additive
Dispersant is Mn2O3Porous microsphere, the Mn2O3The preparation process of porous microsphere is：First, by the Mn (CH of 15mmol3COO)2·
6H2O, the urea of 45mmol and 2g Polyethylene glycol-2000s are placed in 40ml ethylene glycol solutions, are stirred, and dissolving finishes,
Then resulting solution is transferred in stainless steel cauldron, hydro-thermal reaction 30h, natural cooling, centrifugation, receipts is sealed at 220 DEG C
Collection, washing, drying, obtain MnCO3, it is finally calcined into 10h at 650 DEG C in Muffle furnace, obtains Mn2O3Porous microsphere；Mn2O3
A diameter of 1 μm of porous microsphere.
A kind of 6. magnetic far-infrared negative-ion energy eye-mask according to claim 2, it is characterised in that the far infrared
Additive is a kind of polynary sintered body nanopowder, is specially Si-Zr-Ti-Sn sintered body nanopowders, and particle diameter is less than 1 μm,
It is by Tai Ji stone nano particle, ZrO2、TiO2、SnO2According to certain quality proportioning mixed pressuring plate, high temperature sintering, crush, grind
Formed after mill.
A kind of 7. magnetic far-infrared negative-ion energy eye-mask according to claim 6, it is characterised in that the far infrared
In additive, Tai Ji stone nano particle, ZrO2、TiO2、SnO2Quality proportioning is 9:7:3:3.
A kind of 8. magnetic far-infrared negative-ion energy eye-mask according to claim 7, it is characterised in that the Tai Ji stone nanometer
Grain diameter is 500nm, the ZrO2Particle diameter is 300nm, the TiO2Particle diameter is 400nm, the SnO2Particle diameter is 500nm.
9. a kind of magnetic far-infrared negative-ion energy eye-mask according to claim 5, it is characterised in that described magnetic remote red
The preparation process of outer fiber is：
Step 1, prepare far infrared additive：By Tai Ji stone nano particle, ZrO2、TiO2、SnO2According to 9:7:3:3 quality proportionings
It is uniformly mixed, is put into mixing bottle and is sufficiently mixed, disc-shaped is pressed on hydraulic press, high-temperature calcination, after being cooled to room temperature, takes
Go out, crush, grinding is uniform, filters out the sintered body nano particle that particle diameter is less than 1 μm；
Step 2, prepare polyester master particle：First, by magnetic particle, far infrared additive, additive dispersant, anionic additive
Mixed with ethylene glycol, ultrasound 5h at room temperature after stirring, obtains mixed liquor；Then by mixed liquor and p-phthalic acid, catalysis
Auxiliary agent is esterified, and polymerization, obtains polyester master particle, wherein, esterification temperature is 260 DEG C, pressure 280KPa, and esterification yield, which reaches, to be more than
Polycondensation reaction is carried out when 96.5%, condensation temperature is 290 DEG C, is evacuated to 20Mpa, when polycondensation to inherent viscosity is 0.72, goes out
Material, blank；
Step 3, prepare polyester preoriented yarn：Polyester master particle is melted, filter is then fed into and is filtered, after metering, into
Enter spinning pack, the tow of ejection is being cooled down, is being oiled, preoriented yarn is wound into after deflector roll, wherein, spinning temperature is
285 DEG C, spinning speed 3400m/min；
Step 4, prepare magnetic far-infrared fiber：Polyester preoriented yarn can be prepared after a roller, hot tank, two rollers, scroll tube, winding
Into compound polyester functional fibre, wherein, draft speed 500m/min, draw ratio 3.1, a roll temperature is 90 DEG C, two rollers
Temperature is 140 DEG C.
A kind of 10. magnetic far-infrared negative-ion energy eye-mask according to claim 9, it is characterised in that the step 1
In, the high-temperature burning process is to sinter 3h at 1250 DEG C.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108720092A (en) * | 2018-06-27 | 2018-11-02 | 佛山市南海区佳妍内衣有限公司 | A kind of pearl anion antibacterial underwear trousers |
| CN108842217A (en) * | 2018-06-11 | 2018-11-20 | 佛山市南海区佳妍内衣有限公司 | It is a kind of with magnetism, far infrared, antibacterial functions composite fibre |
| CN108995327A (en) * | 2018-06-27 | 2018-12-14 | 佛山市南海区佳妍内衣有限公司 | A kind of composite polar fleece fabric |
| CN108992244A (en) * | 2018-06-08 | 2018-12-14 | 佛山市南海区佳妍内衣有限公司 | Magnetic far-infrared energy eye-mask |
| CN109130411A (en) * | 2018-07-17 | 2019-01-04 | 佛山市南海区佳妍内衣有限公司 | Underwear based on healthcare function |
| CN113476294A (en) * | 2021-08-06 | 2021-10-08 | 上海康怡德量子科技有限公司 | Acupuncture point pressure stimulation patch with quantum micro-energy effect |
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| CN108995327A (en) * | 2018-06-27 | 2018-12-14 | 佛山市南海区佳妍内衣有限公司 | A kind of composite polar fleece fabric |
| CN109130411A (en) * | 2018-07-17 | 2019-01-04 | 佛山市南海区佳妍内衣有限公司 | Underwear based on healthcare function |
| CN113476294A (en) * | 2021-08-06 | 2021-10-08 | 上海康怡德量子科技有限公司 | Acupuncture point pressure stimulation patch with quantum micro-energy effect |
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