CN107889880B - Preservative and preservation method for preventing surface oil cells of fresh lemons from sinking - Google Patents

Preservative and preservation method for preventing surface oil cells of fresh lemons from sinking Download PDF

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Publication number
CN107889880B
CN107889880B CN201711332744.3A CN201711332744A CN107889880B CN 107889880 B CN107889880 B CN 107889880B CN 201711332744 A CN201711332744 A CN 201711332744A CN 107889880 B CN107889880 B CN 107889880B
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fresh
preservative
temperature
lemon
gibberellin
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CN107889880A (en
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曾顺德
曾小峰
商桑
高伦江
刁源
杨必祥
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Chongqing Academy of Agricultural Sciences
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23BPRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
    • A23B7/00Preservation or chemical ripening of fruit or vegetables
    • A23B7/14Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10
    • A23B7/153Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10 in the form of liquids or solids
    • A23B7/154Organic compounds; Microorganisms; Enzymes
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23BPRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
    • A23B7/00Preservation or chemical ripening of fruit or vegetables
    • A23B7/14Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10
    • A23B7/153Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10 in the form of liquids or solids
    • A23B7/154Organic compounds; Microorganisms; Enzymes
    • A23B7/155Microorganisms; Enzymes; Antibiotics
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Microbiology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Storage Of Fruits Or Vegetables (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention provides a preservative for preventing the surface oil cells of fresh lemons from sinking and a preservation method thereof. The fresh lemon has low fresh fruit decay rate and fresh fruit epidermis oil cell dent rate, and meanwhile, the commercialization treatment rate can be greatly improved due to the reduction of the pre-storage link; the fresh lemon fruits produced by the invention adopt the biological preservative, the low-dose chemical preservative and the plant growth regulator gibberellin to replace 2,4-D sodium salt, so that the edible safety is high, and the foreign exchange of exports is facilitated; the fresh lemon produced by the invention has a fresh-keeping period of 8 months.

Description

Preservative and preservation method for preventing surface oil cells of fresh lemons from sinking
Technical Field
The invention relates to the field of fruit preservation, in particular to a preservative for preventing the surface oil cells of fresh lemons from sinking and a preservation method.
Background
The lemon is the fruit of evergreen small arbor fruit tree of Citrus of Rutaceae, and the fruit is elliptical, has sharp ends and concave protrusions, and has fragrant smell. The lemon fruit is rich in VC and VB1、VB2The lemon tea can effectively improve the immunity of a human body by frequently eating essential nutrients such as saccharides, citric acid, malic acid, nicotinic acid, quinic acid, hesperidin, naringin, coumarin, Ca, P and Fe mineral substances, and has the effects of beautifying, reducing blood fat, preventing and treating cardiovascular and cerebrovascular diseases and the like.
Fresh lemon fruit is widely used in the cooking and processing industries. The traditional lemon is widely treated by chemical agents, the edible safety of the chemical agents is noticed by consumers, meanwhile, in order to keep the fresh and green fruit bases, 2,4-D sodium salt (with strong acid corrosion, low toxicity and carcinogenic action on human bodies) is frequently used, the traditional lemon is internationally forbidden, the export of the lemon in China is seriously influenced, and in addition, the traditional chemical agents often cause the oil cells on the surface of the fresh fruits to be sunken, and the commodity of the fresh fruits is seriously influenced. Therefore, the problems to be solved in the prior art are solved by screening and applying the green and safe biological preservative, reducing the use amount of the chemical preservative, preventing the surface oil cells of the fresh lemon fruits from sinking and reducing the corrosion rate of the fresh lemon fruits.
Disclosure of Invention
In view of the above disadvantages of the prior art, the present invention aims to provide an antistaling agent and a antistaling method for preventing the surface oil cells of fresh lemons, which are used for solving the problems of surface oil cells depression, corrosion damage of fresh lemons, 2,4-D sodium salt residue harming human health, etc. of the fresh lemons in the prior art.
In order to achieve the above objects and other related objects, the present invention provides, in a first aspect, an antistaling agent for preventing epidermal oil cyst depression of fresh lemons, comprising sodium bicarbonate, natamycin, nisin, imazalil, gibberellin.
In some embodiments of the invention, 0.1-0.2 wt% sodium bicarbonate, 0.20-0.40 wt% natamycin, 0.10-0.30 wt% nisin, 0.03-0.05 wt% imazalil 50% emulsion, 0.01-0.02 wt% gibberellin are included. By forming a slightly alkaline environment, combining a biological preservative with a low-dose chemical preservative, the pit of the surface oil cells of the fresh lemon fruits is reduced or even avoided, the growth regulator gibberellin is adopted to replace 2,4-D sodium salt (which is forbidden internationally, has strong acid corrosion, low toxicity and carcinogenic effect on human bodies), the fresh fruit pedicles can be fully maintained, and the gibberellin is pre-dissolved by a small amount of ethanol and then dissolved by water, so that the effect of full dissolution can be achieved.
The invention provides a method for preserving by adopting the preservative in a second aspect, which comprises the following steps:
1) adding the components into water according to the formula amount to prepare the preservative;
2) the picked lemon fruits are soaked in the preservative prepared in the step 1), after soaking is finished, the fresh lemon fruits are taken out and packaged in a single fruit plastic bag, and specifically, the fresh lemon fruits after soaking are slightly drained to be packaged in a single fruit plastic bag, so that the relative humidity in the fresh lemon plastic bag can be fully maintained, the traditional pre-storage link is reduced, and the labor and the time are saved.
In some embodiments of the invention, the soaking time in step 2) is 1-3 min.
In some embodiments of the present invention, the method further comprises the step 3) of storing and preserving: the storage and the fresh-keeping are carried out by adopting a two-stage method, the natural condition of lower air temperature in autumn, winter and early spring seasons in Chongqing areas is utilized in the last 11 months to the next 2 middle months or the last 3 months, the storage is carried out by utilizing a ventilation warehouse, the warehouse temperature can be kept at 6-10 ℃, the warehouse temperature is transferred to a high-temperature refrigeration warehouse for the second stage storage in other time periods (2 last ten days or 3 middle ten days to the current 7 months), the temperature of the warehouse is adjusted to 5-8 ℃ by utilizing mechanical refrigeration, the energy consumption can be saved, and the cost can be reduced. In some embodiments of the present invention, the method further comprises step 4) ex-warehouse fresh sales: and after the refrigerator is taken out, the temperature is raised to the same outside temperature in stages.
In some embodiments of the invention, after the fresh lemon fruits are taken out of the refrigeration house, the temperature is raised to the same outside temperature in stages at the speed of 0.1 ℃/h, so that the pits, the oily spots and the browning of the surface oil cells of the fresh lemon fruits can be reduced.
In some embodiments of the present invention, in step 2), the relative humidity of the fresh lemon fruit single fruit packaging bag is 95-100%.
In some embodiments of the present invention, in step 1), ethanol is used to pre-dissolve gibberellin, and after complete dissolution, the pre-dissolved gibberellin is added to the mixed solution of the antistaling agent.
In some embodiments of the invention, in step 1), the mass of ethanol is 3-5 times the mass of gibberellin.
In a third aspect, the invention provides fresh lemon fruit treated by the above method.
As mentioned above, the preservative and the preservation method for preventing the surface oil cells of the fresh lemon fruits have the following beneficial effects: the fresh-keeping fresh fruit of the invention has low rotten rate and pit rate of the surface oil cells of the fresh fruit, reduces the pre-storage link, can greatly improve the commercialized treatment rate of the lemon, saves the energy consumption, and can achieve the fresh-keeping period of the fresh lemon up to 8 months. Because the biological preservative (natamycin and nisin), the low-dose chemical preservative (imazalil) and the plant growth regulator gibberellin are adopted to replace the 2,4-D sodium salt, the edible safety is high, and the export and the foreign exchange are facilitated.
Detailed Description
The embodiments of the present invention are described below with reference to specific embodiments, and other advantages and effects of the present invention will be easily understood by those skilled in the art from the disclosure of the present specification. The invention is capable of other and different embodiments and of being practiced or of being carried out in various ways, and its several details are capable of modification in various respects, all without departing from the spirit and scope of the present invention.
It should be understood that the processing equipment or devices not specifically mentioned in the following examples are conventional in the art; all pressure values and ranges refer to absolute pressures.
Furthermore, it is to be understood that one or more method steps mentioned in the present invention does not exclude that other method steps may also be present before or after the combined steps or that other method steps may also be inserted between these explicitly mentioned steps, unless otherwise indicated; it is also to be understood that a combined connection between one or more devices/apparatus as referred to in the present application does not exclude that further devices/apparatus may be present before or after the combined device/apparatus or that further devices/apparatus may be interposed between two devices/apparatus explicitly referred to, unless otherwise indicated. Moreover, unless otherwise indicated, the numbering of the various method steps is merely a convenient tool for identifying the various method steps, and is not intended to limit the order in which the method steps are arranged or the scope of the invention in which the invention may be practiced, and changes or modifications in the relative relationship may be made without substantially changing the technical content.
Example 1
A fresh-keeping method for preventing epidermal oil cells of fresh lemons from sinking comprises the following steps:
1) fresh-keeping treatment: selecting fresh, non-mildew, non-rot, non-damage and inherent-color lemon variety as raw material, adding the above-mentioned raw materials into water to prepare a mixture containing 0.2 wt% of NaHCO3The preservative solution comprises 0.20 wt% of natamycin, 0.20 wt% of nisin, 0.05 wt% of imazalil 50% emulsion and 0.01 wt% of gibberellin (firstly ethanol with the mass 5 times that of the gibberellin is adopted to pre-dissolve the gibberellin, and then the dissolved solution is added into water), fresh lemon fruits are completely submerged in the preservative solution, the soaking time is 3min, and the agent can play a good role in preserving, so that the oil cell depression, the green rot and the brown rot of the surface of the fresh lemon fruits can be effectively prevented.
2) And (3) instant packaging: the soaked fresh lemons are slightly drained, and then single-fruit plastic bag packaging can be carried out, so that the relative humidity of the surfaces of the fresh lemons can be fully maintained, the traditional pre-storage link is reduced, the labor and the time are saved, and the relative humidity of the fresh lemons is 95%.
3) Storage and preservation: the storage and preservation adopt a two-stage method, and an economical and efficient storage and transportation mode is selected according to the local air temperature and the appropriate temperature for preserving the lemons. Ventilating the warehouse for storage (the first section) from 11 months of the last year to 2 months of the next year, and keeping the warehouse temperature at 6-10 ℃; storing in a refrigerator at high temperature from 2 last ten days to 7 months in the current year (the second stage), and adjusting the temperature of the refrigerator to 5-8 ℃.
4) Ex-warehouse and fresh sale: after the fresh lemons are taken out of the refrigeration house, the temperature is gradually raised in stages at the heating rate of 0.1 ℃/h to reach the same temperature as the outside, so that the superficial oil cell depression, the oil stain disease browning and the like of the fresh lemons are reduced.
Example 2
A fresh-keeping method for preventing epidermal oil cells of fresh lemons from sinking comprises the following steps:
1) fresh-keeping treatment: selecting fresh, non-mildew, non-rot, non-damage and inherent color and luster lemon variety as raw material, adding the above-mentioned raw materials into water to prepare a mixture containing 0.15 wt% of NaHCO3The preservative solution comprises 0.30 wt% of natamycin, 0.10 wt% of nisin, 0.03 wt% of imazalil 50% emulsion and 0.015 wt% of gibberellin (firstly, ethanol with the mass being 3 times of that of the gibberellin is adopted to pre-dissolve the gibberellin, and then the dissolved solution is added into water), wherein fresh lemon fruits are completely submerged in the preservative solution, the soaking time is 2min, and the preservative solution can play a good role in preserving, so that the oil cell depression, green rot and brown rot of the surface of the fresh lemon fruits can be effectively prevented.
2) And (3) instant packaging: the soaked fresh lemons are slightly drained, and then single-fruit plastic bag packaging can be carried out, so that the relative humidity of the surfaces of the fresh lemons can be fully maintained, the traditional pre-storage link is reduced, the labor and the time are saved, and the relative humidity of the fresh lemons is 100%.
3) Storage and preservation: the storage and preservation adopt a two-stage method, and an economical and efficient storage and transportation mode is selected according to the local air temperature and the appropriate temperature for preserving the lemons. Ventilating the warehouse for storage (the first section) from 11 months of the last year to 2 months of the next year, and keeping the warehouse temperature at 6-10 ℃; storing in a refrigerator at high temperature from 2 last ten days to 7 months in the current year (the second stage), and adjusting the temperature of the refrigerator to 5-8 ℃.
4) Ex-warehouse and fresh sale: after the fresh lemons are taken out of the refrigeration house, the temperature is gradually raised in stages at the heating rate of 0.1 ℃/h to reach the same temperature as the outside, so that the superficial oil cell depression, the oil stain disease browning and the like of the fresh lemons are reduced.
Example 3
A preservation method for preventing the surface oil cells of fresh lemons from sinking comprises the following steps:
1) fresh-keeping treatment: selecting fresh, non-mildew, non-rot, non-damage and inherent-color lemon variety as raw material, adding all the components into water, and preparing into the invented product containing 0.1 wt% of NaHCO3The preservative solution comprises 0.40 wt% of natamycin, 0.30 wt% of nisin, 0.04 wt% of imazalil 50% emulsion and 0.02 wt% of gibberellin (firstly ethanol with the mass 5 times that of the gibberellin is adopted to pre-dissolve the gibberellin, and then the dissolved solution is added into water), fresh lemon fruits are completely submerged in the preservative solution, the soaking time is 1min, and the agent can play a good role in preserving, so that the oil cell depression, the green rot and the brown rot of the surface of the fresh lemon fruits can be effectively prevented.
2) And (3) instant packaging: the soaked fresh lemons are slightly drained, and then single-fruit plastic bag packaging can be carried out, so that the relative humidity of the surfaces of the fresh lemons can be fully maintained, the traditional pre-storage link is reduced, the labor and the time are saved, and the relative humidity of the fresh lemons is 98%.
3) Storage and preservation: the storage and preservation adopt a two-stage method, and an economical and efficient storage and transportation mode is selected according to the local air temperature and the appropriate temperature for preserving the lemons. Ventilating the warehouse for storage (the first section) from 11 months of the last year to 3 months of the next year, and keeping the warehouse temperature at 7-10 ℃; storing in a high-temperature refrigerator from 3 middle ten days to 7 months in the current year (the second stage), and adjusting the temperature of the refrigerator to 6-8 ℃.
4) Ex-warehouse and fresh sale: before the fresh lemon fruits are taken out of the refrigeration house, the temperature is gradually raised in stages at the heating rate of 0.1 ℃/h to reach the same temperature as the outside, so that the pits of oil cells on the surface of the fresh lemon fruits, the brown stain and the like are reduced.
Example 4
A preservation method for preventing the surface oil cells of fresh lemons from sinking comprises the following steps:
1) fresh-keeping treatment: selecting fresh, non-mildew, non-rot, non-damage and inherent color and luster lemon variety as raw material, adding the above-mentioned raw materials into water to prepare a mixture containing 0.2 wt% of NaHCO3The preservative solution comprises 0.40 wt% of natamycin, 0.20 wt% of nisin, 0.05 wt% of imazalil 50% emulsion and 0.01 wt% of gibberellin (firstly, ethanol with the mass 4 times that of the gibberellin is adopted to pre-dissolve the gibberellin, and then the dissolved solution is added into water), fresh lemon fruits are completely submerged in the preservative solution, the soaking time is 3min, and the preservative solution can play a good role in preserving, so that the oil cell depression, green rot and brown rot of the surface of the fresh lemon fruits can be effectively prevented.
2) And (3) instant packaging: the soaked fresh lemons are slightly drained, and then single-fruit plastic bag packaging can be carried out, so that the relative humidity of the surfaces of the fresh lemons can be fully maintained, the traditional pre-storage link is reduced, the labor and the time are saved, and the relative humidity of the fresh lemons is 100%.
3) Storage and preservation: the storage and preservation adopt a two-stage method, and an economical and efficient storage and transportation mode is selected according to the local air temperature and the appropriate temperature for preserving the lemons. Ventilating the warehouse for storage (the first section) from 11 months of the last year to 3 months of the next year, and keeping the warehouse temperature at 7-10 ℃; storing in a high-temperature refrigerator from 3 middle ten days to 7 months in the current year (the second stage), and adjusting the temperature of the refrigerator to 6-8 ℃.
4) Ex-warehouse and fresh sale: before the fresh lemon fruits are taken out of the refrigeration house, the temperature is gradually raised in stages at the heating rate of 0.1 ℃/h to reach the same temperature as the outside, so that the pits of oil cells on the surface of the fresh lemon fruits, the brown stain and the like are reduced.
The average decay rate and the pit of the surface oil cells of the fresh lemons obtained in examples 1 to 4 were analyzed, and the results were as follows:
the control group preservative formula comprises 250ppm of 2,4-D sodium salt, 0.10 wt% of imazalil 50% emulsion and 0.10 wt% of thiophanate methyl.
TABLE 1 sensory evaluation results Table
Figure BDA0001506955800000051
In conclusion, compared with the traditional chemical agent preservation, the fresh lemon fruit preserved by the invention has the following effective effects: 1. the fresh lemon has low fresh fruit decay rate and fresh fruit epidermis oil cell dent rate, and meanwhile, the commercialization treatment rate can be greatly improved due to the reduction of the pre-storage link; 2. the invention adopts a two-section storage mode, thus saving energy consumption and reducing cost; 3. the fresh lemon fruits produced by the invention adopt the biological preservative, the low-dose chemical preservative and the plant growth regulator gibberellin to replace 2,4-D sodium salt, so that the edible safety is high, and the foreign exchange of exports is facilitated; 4. the fresh lemon produced by the invention has a fresh-keeping period of 8 months.
The foregoing embodiments are merely illustrative of the principles and utilities of the present invention and are not intended to limit the invention. Any person skilled in the art can modify or change the above-mentioned embodiments without departing from the spirit and scope of the present invention. Accordingly, it is intended that all equivalent modifications or changes which can be made by those skilled in the art without departing from the spirit and technical spirit of the present invention be covered by the claims of the present invention.

Claims (8)

1. The preservative for preventing the surface oil cells of the fresh lemons from sinking is characterized by comprising the following components in percentage by weight: 0.1-0.2 wt% of sodium bicarbonate, 0.20-0.40 wt% of natamycin, 0.10-0.30 wt% of nisin, 0.03-0.05 wt% of imazalil, 50% of emulsion and 0.01-0.02 wt% of gibberellin; the preservative is prepared by adding all components into water, wherein gibberellin is pre-dissolved by adopting ethanol, and then the dissolved solution is added into the water.
2. The preservative according to claim 1, characterized in that: the mass of the ethanol is 3-5 times of that of the gibberellin.
3. A method for retaining freshness by using the freshness keeping agent of claim 1, characterized by comprising the steps of:
1) adding the components into water according to the formula amount to prepare the preservative;
2) and (3) soaking the picked lemon fruits in the preservative prepared in the step 1), taking out the fresh lemon fruits after soaking, and packaging the fresh lemon fruits in single-fruit plastic bags.
4. The method of claim 3, wherein: in the step 2), the soaking time is 1-3 min.
5. The method of claim 3, further comprising the step of 3) storing and refreshing: storing and refreshing by a two-section method, wherein the temperature in a ventilated warehouse is kept at 6-10 ℃ from 11 months to 2 middle or 3 last days of the next year, and the temperature in the warehouse is kept at 5-8 ℃ in a high-temperature cold storage warehouse in other time periods.
6. The method of claim 5, wherein: further comprises the step 4) of ex-warehouse fresh selling: after the material is taken out of the refrigeration house, the temperature is increased to the same outside temperature in stages at the speed of 0.1 ℃/h.
7. The method of claim 3, wherein: in the step 2), the relative humidity in the single-fruit plastic bag of the fresh lemon fruits is 95-100%.
8. Fresh lemon fruit treated according to the method of any one of claims 3 to 7.
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