CN107880767A - A kind of scrubbable ultraviolet-cured furniture coating and preparation method thereof - Google Patents
A kind of scrubbable ultraviolet-cured furniture coating and preparation method thereof Download PDFInfo
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- CN107880767A CN107880767A CN201711382403.7A CN201711382403A CN107880767A CN 107880767 A CN107880767 A CN 107880767A CN 201711382403 A CN201711382403 A CN 201711382403A CN 107880767 A CN107880767 A CN 107880767A
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- Prior art keywords
- parts
- ultraviolet
- scrubbable
- cured
- silica
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/14—Polyurethanes having carbon-to-carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses a kind of scrubbable ultraviolet-cured furniture coating, it is made up of the raw material below according to parts by weight：50 55 parts of urethane acrylate oligomer, 38 42 parts of Epoxy Phenolic Acrylates, 10 15 parts of polyvinyl alcohol, 9 13 parts of XNBR, three 25 29 parts of glycerine acrylate, 10 14 parts of trimethylolpropane trimethacrylate, 25 parts of benzoin dimethylether, 13 parts of trimethylbenzene acyl group diphenyl phosphine oxide, 23 parts of DMAA, 45 parts of polypropylene glycerol aether, 36 parts of tributyl 2-acetylcitrate, 25 parts of glyceryl tristearate, 17 21 parts of silica flatting silica, 14 18 parts of mica powder.The invention also discloses the preparation method of the scrubbable ultraviolet-cured furniture coating.The coatings for furniture has good scrub performance, is not easy peeling, comes off.
Description
Technical field
The present invention relates to coatings for furniture technical field, specifically a kind of scrubbable ultraviolet-cured furniture coating and its system
Preparation Method.
Background technology
Coatings for furniture refers to woodenware, DELICATE AND SIMPLE BAMBOO surface paint special, also known as is " woodcare paint ".Coatings for furniture can make woodenware,
DELICATE AND SIMPLE BAMBOO is more attractive beautiful, improve furniture per se with harsh hand, not only act as Preservation woodenware DELICATE AND SIMPLE BAMBOO
Effect, moreover it is possible to make whole family life become more comfortable.
Coatings for furniture species is various, and ultraviolet-curing paint is exactly one kind therein.It is purple by the development of over half a century
Outer light (UV) is coating material solidified to have become more ripe technology, in particular with the raising of people's environmental consciousness, produces and grinds
Study carefully personnel and be important to note that the coating material solidified development and application of UV.UV coating material solidified is a kind of environmental type coating, and it is accorded with completely
" 4E " principle is closed, general UV solidifications energy consumption is the 1/5 of heat cure, and UV is coating material solidified less containing volatile component, and pollution is small, most inhales
Draw researcher and developer to be that UV is coating material solidified can reduce raw materials consumption, advantageously reduce financial cost.
UV is coating material solidified to be mainly made up of oligomer, monomer, light trigger and auxiliary agent.UV solidification key reaction course be
Light trigger is caused to decompose by radiation, generation living radical triggers monomer/oligomer polymerization crosslinking.With the development in epoch,
Market proposes higher and higher performance requirement to ultraviolet-curing paint, and existing ultraviolet-curing paint is in terms of scrubbing resistance
Performance can not gradually meet the market demand, it is necessary to improve.
The content of the invention
It is an object of the invention to provide a kind of scrubbable ultraviolet-cured furniture coating and preparation method thereof, to solve
The problem of being proposed in above-mentioned background technology.
To achieve the above object, the present invention provides following technical scheme：
A kind of scrubbable ultraviolet-cured furniture coating, is made up of the raw material below according to parts by weight：Polyurethane propylene
Acid esters oligomer 50-55 parts, Epoxy Phenolic Acrylates 38-42 parts, polyvinyl alcohol 10-15 parts, XNBR 9-13 parts,
Three glycerine acrylate 25-29 parts, trimethylolpropane trimethacrylate 10-14 parts, benzoin dimethylether 2-5 parts, front three
Base benzoyl group diphenyl phosphine oxide 1-3 parts, DMAA 2-3 parts, polypropylene glycerol aether 4-5 parts, acetyl tributyl citrate
Tributyl 3-6 parts, glyceryl tristearate 2-5 parts, silica flatting silica 17-21 parts, mica powder 14-18 parts.
As the further scheme of the present invention：It is made up of the raw material below according to parts by weight：Urethane acrylate is oligomeric
Thing 51-54 parts, Epoxy Phenolic Acrylates 39-41 parts, polyvinyl alcohol 11-14 parts, XNBR 10-12 parts, 3 the third three
Alcohol acrylate 26-28 parts, trimethylolpropane trimethacrylate 11-13 parts, benzoin dimethylether 3-4 parts, trimethyl benzoyl
Base diphenyl phosphine oxide 1.3-2.5 parts, DMAA 2.2-2.8 parts, polypropylene glycerol aether 4.1-4.9 parts, acetyl
ATBC 4-5 parts, glyceryl tristearate 3-4 parts, silica flatting silica 18-20 parts, mica powder 15-17 parts.
As further scheme of the invention：It is made up of the raw material below according to parts by weight：Urethane acrylate is low
53 parts of polymers, 40 parts of Epoxy Phenolic Acrylates, 13 parts of polyvinyl alcohol, 11 parts of XNBR, three glycerine acrylate
27 parts, 12 parts of trimethylolpropane trimethacrylate, 4 parts of benzoin dimethylether, trimethylbenzene acyl group diphenyl phosphine oxide 1.8
Part, 2.5 parts of DMAA, 4.4 parts of polypropylene glycerol aether, 5 parts of tributyl 2-acetylcitrate, glyceryl tristearate
3 parts, 19 parts of silica flatting silica, 16 parts of mica powder.
As further scheme of the invention：The particle diameter of the silica flatting silica is 6.0-8.0 μm.
As further scheme of the invention：The particle diameter of the mica powder is 18-23 μm.
The preparation method of the scrubbable ultraviolet-cured furniture coating, step are as follows：
1) urethane acrylate oligomer and Epoxy Phenolic Acrylates are weighed, is put into reactor, in 80-85
DEG C, 20-30min is stirred under 300-400rpm, obtain mixture A；
2) temperature of reactor in step 1) is kept, adds XNBR, three glycerine acrylate and acetyl lemon
Lemon acid tributyl, 20-30min is stirred under 600-800rpm, obtains mixture B；
3) reactor in step 2) is cooled to 65-70 DEG C, adds XNBR, trimethylolpropane tris propylene
Acid esters, polypropylene glycerol aether and silica flatting silica, 35-40min is stirred under 600-800rpm, obtains mixture
C；
4) keep step 3) in reactor temperature, add benzoin dimethylether, trimethylbenzene acyl group diphenyl phosphine oxide,
DMAA, glyceryl tristearate and mica powder, 50-60min is stirred under 900-1100rpm, is mixed
Compound D；
5) detection is sampled to mixture D, after detection is qualified, discharging, you can.
Compared with prior art, the beneficial effects of the invention are as follows：
Coatings for furniture prepared by the present invention is formulated by improving, and has good scrub performance, is cleaning process for a long time
In, the phenomenon that be not likely to produce peeling, comes off ensure that the attractive in appearance of furniture, and good protective effect is provided for furniture, have wide
Wealthy market prospects.
Embodiment
Technical scheme is described in more detail with reference to embodiment.
Embodiment 1
A kind of scrubbable ultraviolet-cured furniture coating, is made up of the raw material below according to parts by weight：Polyurethane propylene
50 parts of acid esters oligomer, 38 parts of Epoxy Phenolic Acrylates, 10 parts of polyvinyl alcohol, 9 parts of XNBR, three glycerine propylene
25 parts of acid esters, 10 parts of trimethylolpropane trimethacrylate, 2 parts of benzoin dimethylether, trimethylbenzene acyl group diphenyl phosphine oxide 1
Part, 2 parts of DMAA, 4 parts of polypropylene glycerol aether, 3 parts of tributyl 2-acetylcitrate, 2 parts of glyceryl tristearate,
17 parts of silica flatting silica, 14 parts of mica powder.Wherein, the particle diameter of the silica flatting silica is 6.0-8.0 μm, the cloud
The particle diameter of female powder is 18-23 μm.
In the present embodiment, the preparation method of the scrubbable ultraviolet-cured furniture coating, step is as follows：
1) urethane acrylate oligomer and Epoxy Phenolic Acrylates are weighed, is put into reactor, 80 DEG C,
20min is stirred under 300rpm, obtains mixture A；
2) temperature of reactor in step 1) is kept, adds XNBR, three glycerine acrylate and acetyl lemon
Lemon acid tributyl, 20min is stirred at 600 rpm, obtain mixture B；
3) reactor in step 2) is cooled to 65 DEG C, adds XNBR, trimethylolpropane tris acrylic acid
Ester, polypropylene glycerol aether and silica flatting silica, 35min is stirred at 600 rpm, obtain mixture C；
4) keep step 3) in reactor temperature, add benzoin dimethylether, trimethylbenzene acyl group diphenyl phosphine oxide,
DMAA, glyceryl tristearate and mica powder, 50min is stirred under 900rpm, obtains mixture D；
5) detection is sampled to mixture D, after detection is qualified, discharging, you can.
Embodiment 2
A kind of scrubbable ultraviolet-cured furniture coating, is made up of the raw material below according to parts by weight：Polyurethane propylene
51 parts of acid esters oligomer, 39 parts of Epoxy Phenolic Acrylates, 11 parts of polyvinyl alcohol, 12 parts of XNBR, three glycerine third
28 parts of olefin(e) acid ester, 13 parts of trimethylolpropane trimethacrylate, 3 parts of benzoin dimethylether, the oxidation of trimethylbenzene acyl group diphenyl
1.3 parts of phosphine, 2.2 parts of DMAA, 4.9 parts of polypropylene glycerol aether, 5 parts of tributyl 2-acetylcitrate, three stearic acid
4 parts of glyceride, 18 parts of silica flatting silica, 17 parts of mica powder.Wherein, the particle diameter of the silica flatting silica is 6.0-
8.0 μm, the particle diameter of the mica powder is 18-23 μm.
In the present embodiment, the preparation method of the scrubbable ultraviolet-cured furniture coating, step is as follows：
1) urethane acrylate oligomer and Epoxy Phenolic Acrylates are weighed, is put into reactor, 80 DEG C,
23min is stirred under 300rpm, obtains mixture A；
2) temperature of reactor in step 1) is kept, adds XNBR, three glycerine acrylate and acetyl lemon
Lemon acid tributyl, 25min is stirred under 700rpm, obtains mixture B；
3) reactor in step 2) is cooled to 65 DEG C, adds XNBR, trimethylolpropane tris acrylic acid
Ester, polypropylene glycerol aether and silica flatting silica, 35min is stirred under 700rpm, obtains mixture C；
4) keep step 3) in reactor temperature, add benzoin dimethylether, trimethylbenzene acyl group diphenyl phosphine oxide,
DMAA, glyceryl tristearate and mica powder, 52min is stirred under 1000rpm, obtains mixture D；
5) detection is sampled to mixture D, after detection is qualified, discharging, you can.
Embodiment 3
A kind of scrubbable ultraviolet-cured furniture coating, is made up of the raw material below according to parts by weight：Polyurethane propylene
53 parts of acid esters oligomer, 40 parts of Epoxy Phenolic Acrylates, 13 parts of polyvinyl alcohol, 11 parts of XNBR, three glycerine third
27 parts of olefin(e) acid ester, 12 parts of trimethylolpropane trimethacrylate, 4 parts of benzoin dimethylether, the oxidation of trimethylbenzene acyl group diphenyl
1.8 parts of phosphine, 2.5 parts of DMAA, 4.4 parts of polypropylene glycerol aether, 5 parts of tributyl 2-acetylcitrate, three stearic acid
3 parts of glyceride, 19 parts of silica flatting silica, 16 parts of mica powder.Wherein, the particle diameter of the silica flatting silica is 6.0-
8.0 μm, the particle diameter of the mica powder is 18-23 μm.
In the present embodiment, the preparation method of the scrubbable ultraviolet-cured furniture coating, step is as follows：
1) urethane acrylate oligomer and Epoxy Phenolic Acrylates are weighed, is put into reactor, 82 DEG C,
25min is stirred under 400rpm, obtains mixture A；
2) temperature of reactor in step 1) is kept, adds XNBR, three glycerine acrylate and acetyl lemon
Lemon acid tributyl, 25min is stirred under 700rpm, obtains mixture B；
3) reactor in step 2) is cooled to 68 DEG C, adds XNBR, trimethylolpropane tris acrylic acid
Ester, polypropylene glycerol aether and silica flatting silica, 38min is stirred under 700rpm, obtains mixture C；
4) keep step 3) in reactor temperature, add benzoin dimethylether, trimethylbenzene acyl group diphenyl phosphine oxide,
DMAA, glyceryl tristearate and mica powder, 55min is stirred under 1000rpm, obtains mixture D；
5) detection is sampled to mixture D, after detection is qualified, discharging, you can.
Embodiment 4
A kind of scrubbable ultraviolet-cured furniture coating, is made up of the raw material below according to parts by weight：Polyurethane propylene
54 parts of acid esters oligomer, 41 parts of Epoxy Phenolic Acrylates, 14 parts of polyvinyl alcohol, 10 parts of XNBR, three glycerine third
26 parts of olefin(e) acid ester, 11 parts of trimethylolpropane trimethacrylate, 4 parts of benzoin dimethylether, the oxidation of trimethylbenzene acyl group diphenyl
2.5 parts of phosphine, 2.8 parts of DMAA, 4.1 parts of polypropylene glycerol aether, 4 parts of tributyl 2-acetylcitrate, three stearic acid
3 parts of glyceride, 20 parts of silica flatting silica, 15 parts of mica powder.Wherein, the particle diameter of the silica flatting silica is 6.0-
8.0 μm, the particle diameter of the mica powder is 18-23 μm.
In the present embodiment, the preparation method of the scrubbable ultraviolet-cured furniture coating, step is as follows：
1) urethane acrylate oligomer and Epoxy Phenolic Acrylates are weighed, is put into reactor, 85 DEG C,
25min is stirred under 300rpm, obtains mixture A；
2) temperature of reactor in step 1) is kept, adds XNBR, three glycerine acrylate and acetyl lemon
Lemon acid tributyl, 27min is stirred at 800 rpm, obtain mixture B；
3) reactor in step 2) is cooled to 70 DEG C, adds XNBR, trimethylolpropane tris acrylic acid
Ester, polypropylene glycerol aether and silica flatting silica, 38min is stirred at 800 rpm, obtain mixture C；
4) keep step 3) in reactor temperature, add benzoin dimethylether, trimethylbenzene acyl group diphenyl phosphine oxide,
DMAA, glyceryl tristearate and mica powder, 58min is stirred under 1100rpm, obtains mixture D；
5) detection is sampled to mixture D, after detection is qualified, discharging, you can.
Embodiment 5
A kind of scrubbable ultraviolet-cured furniture coating, is made up of the raw material below according to parts by weight：Polyurethane propylene
55 parts of acid esters oligomer, 42 parts of Epoxy Phenolic Acrylates, 15 parts of polyvinyl alcohol, 13 parts of XNBR, three glycerine third
29 parts of olefin(e) acid ester, 14 parts of trimethylolpropane trimethacrylate, 5 parts of benzoin dimethylether, the oxidation of trimethylbenzene acyl group diphenyl
3 parts of phosphine, 3 parts of DMAA, 5 parts of polypropylene glycerol aether, 6 parts of tributyl 2-acetylcitrate, glyceryl tristearate 5
Part, 21 parts of silica flatting silica, 18 parts of mica powder.Wherein, the particle diameter of the silica flatting silica is 6.0-8.0 μm, institute
The particle diameter for stating mica powder is 18-23 μm.
In the present embodiment, the preparation method of the scrubbable ultraviolet-cured furniture coating, step is as follows：
1) urethane acrylate oligomer and Epoxy Phenolic Acrylates are weighed, is put into reactor, 85 DEG C,
30min is stirred under 400rpm, obtains mixture A；
2) temperature of reactor in step 1) is kept, adds XNBR, three glycerine acrylate and acetyl lemon
Lemon acid tributyl, 30min is stirred at 800 rpm, obtain mixture B；
3) reactor in step 2) is cooled to 70 DEG C, adds XNBR, trimethylolpropane tris acrylic acid
Ester, polypropylene glycerol aether and silica flatting silica, 40min is stirred at 800 rpm, obtain mixture C；
4) keep step 3) in reactor temperature, add benzoin dimethylether, trimethylbenzene acyl group diphenyl phosphine oxide,
DMAA, glyceryl tristearate and mica powder, 60min is stirred under 1100rpm, obtains mixture D；
5) detection is sampled to mixture D, after detection is qualified, discharging, you can.
Coatings for furniture prepared by the present invention is formulated by improving, and has good scrub performance, is cleaning process for a long time
In, the phenomenon that be not likely to produce peeling, comes off ensure that the attractive in appearance of furniture, and good protective effect is provided for furniture, have wide
Wealthy market prospects.
The better embodiment of the present invention is explained in detail above, but the present invention is not limited to above-mentioned embodiment party
Formula, can also be on the premise of present inventive concept not be departed from one skilled in the relevant art's possessed knowledge
Various changes can be made.
Claims (6)
1. a kind of scrubbable ultraviolet-cured furniture coating, it is characterised in that be made up of the raw material below according to parts by weight：It is poly-
Urethane acrylate oligomer 50-55 parts, Epoxy Phenolic Acrylates 38-42 parts, polyvinyl alcohol 10-15 parts, carboxyl butyronitrile rubber
Glue 9-13 parts, three glycerine acrylate 25-29 parts, trimethylolpropane trimethacrylate 10-14 parts, benzoin dimethylether 2-
5 parts, trimethylbenzene acyl group diphenyl phosphine oxide 1-3 parts, DMAA 2-3 parts, polypropylene glycerol aether 4-5 parts, second
Acyl ATBC 3-6 parts, glyceryl tristearate 2-5 parts, silica flatting silica 17-21 parts, mica powder 14-18 parts.
2. scrubbable ultraviolet-cured furniture coating according to claim 1, it is characterised in that by below according to weight
The raw material composition of part：Urethane acrylate oligomer 51-54 parts, Epoxy Phenolic Acrylates 39-41 parts, polyvinyl alcohol 11-
14 parts, XNBR 10-12 parts, three glycerine acrylate 26-28 parts, trimethylolpropane trimethacrylate 11-13
Part, benzoin dimethylether 3-4 parts, trimethylbenzene acyl group diphenyl phosphine oxide 1.3-2.5 parts, DMAA 2.2-2.8
Part, polypropylene glycerol aether 4.1-4.9 parts, tributyl 2-acetylcitrate 4-5 parts, glyceryl tristearate 3-4 parts, silica
Flatting silica 18-20 parts, mica powder 15-17 parts.
3. scrubbable ultraviolet-cured furniture coating according to claim 2, it is characterised in that by below according to weight
The raw material composition of part：53 parts of urethane acrylate oligomer, 40 parts of Epoxy Phenolic Acrylates, 13 parts of polyvinyl alcohol, carboxyl
11 parts of nitrile rubber, 27 parts of three glycerine acrylate, 12 parts of trimethylolpropane trimethacrylate, 4 parts of benzoin dimethylether,
1.8 parts of trimethylbenzene acyl group diphenyl phosphine oxide, 2.5 parts of DMAA, 4.4 parts of polypropylene glycerol aether, acetyl lemon
5 parts of lemon acid tributyl, 3 parts of glyceryl tristearate, 19 parts of silica flatting silica, 16 parts of mica powder.
4. scrubbable ultraviolet-cured furniture coating according to claim 1, it is characterised in that the silica disappears
The particle diameter of light powder is 6.0-8.0 μm.
5. scrubbable ultraviolet-cured furniture coating according to claim 1, it is characterised in that the grain of the mica powder
Footpath is 18-23 μm.
6. a kind of preparation method of scrubbable ultraviolet-cured furniture coating as described in claim 1-5 is any, its feature
It is, step is as follows：
1) urethane acrylate oligomer and Epoxy Phenolic Acrylates are weighed, is put into reactor, 80-85 DEG C,
20-30min is stirred under 300-400rpm, obtains mixture A；
2) temperature of reactor in step 1) is kept, adds XNBR, three glycerine acrylate and acetyl tributyl citrate
Tributyl, 20-30min is stirred under 600-800rpm, obtains mixture B；
3) reactor in step 2) is cooled to 65-70 DEG C, adds XNBR, trimethylolpropane tris acrylic acid
Ester, polypropylene glycerol aether and silica flatting silica, 35-40min is stirred under 600-800rpm, obtains mixture C；
4) temperature of reactor in step 3) is kept, adds benzoin dimethylether, trimethylbenzene acyl group diphenyl phosphine oxide, diformazan
Base acrylamide, glyceryl tristearate and mica powder, 50-60min is stirred under 900-1100rpm, obtains mixture
D；
5) detection is sampled to mixture D, after detection is qualified, discharging, you can.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711382403.7A CN107880767A (en) | 2017-12-20 | 2017-12-20 | A kind of scrubbable ultraviolet-cured furniture coating and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711382403.7A CN107880767A (en) | 2017-12-20 | 2017-12-20 | A kind of scrubbable ultraviolet-cured furniture coating and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107880767A true CN107880767A (en) | 2018-04-06 |
Family
ID=61772034
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711382403.7A Pending CN107880767A (en) | 2017-12-20 | 2017-12-20 | A kind of scrubbable ultraviolet-cured furniture coating and preparation method thereof |
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| CN103009756A (en) * | 2012-12-10 | 2013-04-03 | 广东天安新材料股份有限公司 | Composite basement membrane with surface solidifying coating and manufacturing method of composite basement membrane |
| CN103450795A (en) * | 2013-09-17 | 2013-12-18 | 成都优品涂料有限公司 | Ultraviolet-curing fireproof flame-retardant wood paint and preparation method thereof |
| CN103627311A (en) * | 2012-08-21 | 2014-03-12 | 上海大桥化工有限公司 | Vacuum plating UV-curable priming paint |
| CN105295669A (en) * | 2015-11-19 | 2016-02-03 | 广州聚注专利研发有限公司 | UV-curing coating |
| CN107312426A (en) * | 2017-07-17 | 2017-11-03 | 广东铂年节能环保科技有限公司 | A kind of environmental protection coating material |
-
2017
- 2017-12-20 CN CN201711382403.7A patent/CN107880767A/en active Pending
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| CN103627311A (en) * | 2012-08-21 | 2014-03-12 | 上海大桥化工有限公司 | Vacuum plating UV-curable priming paint |
| CN103009756A (en) * | 2012-12-10 | 2013-04-03 | 广东天安新材料股份有限公司 | Composite basement membrane with surface solidifying coating and manufacturing method of composite basement membrane |
| CN103450795A (en) * | 2013-09-17 | 2013-12-18 | 成都优品涂料有限公司 | Ultraviolet-curing fireproof flame-retardant wood paint and preparation method thereof |
| CN105295669A (en) * | 2015-11-19 | 2016-02-03 | 广州聚注专利研发有限公司 | UV-curing coating |
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