CN107828560B - A kind of production method of soap rice - Google Patents
A kind of production method of soap rice Download PDFInfo
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- CN107828560B CN107828560B CN201711258951.9A CN201711258951A CN107828560B CN 107828560 B CN107828560 B CN 107828560B CN 201711258951 A CN201711258951 A CN 201711258951A CN 107828560 B CN107828560 B CN 107828560B
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- Prior art keywords
- grinding
- soap
- binder
- blade
- discharge barrel
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/14—Shaping
- C11D13/18—Shaping by extrusion or pressing
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/14—Shaping
- C11D13/20—Shaping in the form of small particles, e.g. powder or flakes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/005—Synthetic soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
Abstract
The present invention relates to a kind of production methods of soap rice, it is characterized in that: being carried out saponification using natural ox or suet, coconut oil, palm-kernel oil as raw material and soap base being made, and soap base are made to the neat soap of 8~12 ㎜ of partial size；Neat soap, essence are added in crutcher, the pot temperature that reconciles is maintained at 60~80 DEG C, with blender that material stirring in crutcher is uniform, in which: essence dosage is 1~1.5 wt%；The material stirred evenly is continued through three-roll mill to mill, is milled into laminar material, in which: three-roll mill controls in 0.2~0.4mm clearance between roll, and the revolving speed of roller is 15~25r/min；Laminar material is continuously introduced into grinding pelletizer to be granulated；Vibrating screen is set in the lower section of grinding pelletizer, after shaker vibration is sieved, obtains the soap rice grain that partial size is less than or equal to 0.5 ㎜.Its advantage is that: equipment is at low, low energy consumption, high production efficiency, and soap grain of rice diameter is small, and dissolving power is very strong, and the machine washing that is more suitable uses.
Description
Technical field
The present invention relates to a kind of production methods of soap rice, belong to articles for washing technical field.
Background technique
Clothes washing has two kinds of washing and dry-cleaning, dry-cleans and laundry is suitble to use, and is not suitable for home laundry；Everyday home is washed
It washs clothing and takes washing, there are two types of modes again for washing: first is that hand-washing, second is that washing machine is machine-washed.Washing clothing have to using
Detergent, existing detergent mainly have: washing powder, liquid detergent, soap, soap powder, every kind of detergent have advantage and disadvantage, washing powder
The advantages of be: facilitate machine washing, dirt-removing power is strong, the disadvantage is that: course of dissolution heat release is hurt hand wound body, is not readily dissolved, easily deposit,
It is easy injury clothes fiber and color, is not easy to rinse；The advantages of liquid detergent is: clothing not fugitive color, solution rate is fast, easily floats
It washes, the disadvantage is that: it is not easy to determine dosage, cannot place for a long time, it is perishable；The advantages of soap is: dirt-removing power is strong, does not burn skin,
The disadvantage is that: it cannot machine-wash, turn to be yellow, harden after clothes washing, be not easy to rinse；Soap powder is common by soap component and a variety of chemical components
It constitutes, wherein soap component accounting is less than 70%, its advantage is that: containing extraordinary lime soap dispersant, strong detergency, low bubble is easily rinsed,
Water-saving saves time in washing process, the disadvantage is that: containing chemical addition agent, not environmentally, clothing easily remains calcium soap.As people are strong
The enhancing of health, environmental consciousness, to washing class Product Safety and it is functional require it is higher and higher, just above-mentioned four kinds of detergent and
Speech, soap is the safest and environmental protection, but soap cannot be used for machine-washing, so that its use is extremely limited, Er Qieqi
In use Yi Fahuang after existing clothes washing, harden, being not easy the shortcomings that rinsing more limits the use of soap.It is practical
On, soap Yi Fahuang after washing clothing, harden, be not easy to rinse main cause be make soap base raw material it is impure, and in order to
Reduce soap cost and increase washing effect and added with caused by additive (such as talcum powder) in soap.In order to overcome laundry
Powder, liquid detergent, soap powder not environmentally the shortcomings that and soap the shortcomings that cannot machine-washing, the present inventor invented " a kind of soap rice and its system
Make method " and patent application is proposed by Hongwei Daily Chemical Co., Ltd., Baotou, application number: 2016104551017, after more
Entitled " a kind of soap rice ".Although the shortcomings that overcoming washing powder, liquid detergent, soap powder in the disclosure in this patent not environmentally, also solves
The problem of soap cannot machine-wash, but since the manufacturing process of use is straight line extrusion process, manufacture difficulty is high.Extruder goes out
Material end is equipped with plate face and is uniformly provided with aperture in the porous bushing of 0.5~1mm discharge hole, and for pressure-bearing, the thickness of bushing is not small
In 4cm, hole of the aperture diameter between 0.5~1mm on such thick steel plate also only has military enterprise that can accomplish in China,
And want to output the hole that aperture is less than 0.5mm, it can accomplish currently without enterprise.It is very high to make such bushing cost, and
Bushing in this way, which squeezes out soap base, needs high pressure that discharge end is done tapered (loudspeaker in order to increase the pressure-bearing of bushing
Mouth), while groined type reinforcing rib is set at the back side of bushing, it just can guarantee that soap rice normally produces.Production efficiency is lower, and
The column soap rice diameter produced is not less than 0.5mm, and solvability is not good enough in actual use.
Summary of the invention
The object of the present invention is to provide one kind, and diameter can will be processed into using pure natural raw material soap base less than or equal to 0.5
㎜, equipment cost are low, low energy consumption, soap rice is more soluble, are more suitable for the production method for the soap rice that machine washing uses.
Technical scheme is as follows:
It 1) is original with the palm-kernel oil of the natural ox of 75~85wt% or suet, the coconut oil of 15~25 wt%, 0~5 wt%
Material carries out saponification and soap base is made, and soap base is made to the neat soap of 8~12 ㎜ of partial size；
2) neat soap, essence are added in crutcher, the pot temperature that reconciles is maintained at 60~80 DEG C, will be in crutcher with blender
Material stirring is uniform, in which: essence dosage is 1~1.5 wt%；
3) material stirred evenly is continued through three-roll mill to mill, is milled into laminar material, in which: three
Roller grinding mill controls in 0.2~0.4mm clearance between roll, and the revolving speed of roller is 15~25r/min；
4) by laminar material be continuously introduced into grinding pelletizer be granulated, grinding pelletizer include feed hopper, discharge barrel,
Binder impeller, grinding break bar, feed hopper is the infundibulate of opening upwards, and discharge barrel is the cylindrical shape surrounded by side wall and bottom surface,
Side wall is uniformly densely covered with discharge hole, and the diameter of discharge hole is less than or equal to 0.5 mm, and discharge barrel is connected to lower end of hopper；Binder
Impeller is formed by binder wheel hub and by the equally spaced binder blade being arranged on binder wheel hub of circumference, every binder blade and water
Plane grinds break bar by grinding wheel hub and by the equally spaced grinding being arranged on grinding wheel hub of circumference at 30~52 ° of inclinations angle
Blade composition, the knife face for grinding blade is arc surface, grinds the knife face and horizontal plane of blade, binder impeller and grinding break bar
It is driven using concentric shafts, concentric shafts pass perpendicularly through discharge barrel bottom center, and are connect by bearing with discharge barrel bottom surface, binder leaf
Wheel is located on grinding break bar, binder wheel hub and grinding wheel hub clearance fit, grinding knife sheet head and discharge barrel side wall at 0~
15 degree of angles, and cooperate with discharge barrel sidewall spacers, binder impeller rotates horizontally direction along binder blade pitch angle institute, grinding
Break bar is rotated horizontally along grinding blade protrusion direction, and binder impeller is opposite with grinding break bar direction of rotation；Material is sent into grinding
After pelletizer, fallen into the gap between the grinding blade in discharge barrel by the interlobate gap of binder, binder wheel rotation is to object
Expect downward pressure, the rotation of grinding knife wheel grinds and forms abrasive power between blade and discharge barrel side wall, by material by discharge barrel side
The discharge hole of wall is ground away, and is fallen naturally according to gravity；
5) it obtains partial size after shaker vibration is sieved in the lower section setting vibrating screen of grinding pelletizer and is less than or equal to
The soap rice grain of 0.5 ㎜.
The discharging bore dia of the discharge barrel is 0.3~0.5 mm；
It is wrapped with circular ring shape protective cover in the side wall of the discharge barrel, it is several that rule is uniformly provided on the side wall of protective cover
The eyelet of what shape；
The wall thickness of the protective cover is not less than 0.3 centimetre；
The quantity of binder blade on the binder impeller is 3~9 (blade quantity is determined by the size of equipment), and is
Odd number piece；
The quantity for grinding the grinding blade on break bar is 3~12；
By the speed of control grinding pelletizer, binder impeller and the revolving speed for grinding break bar in step 4), make grinding knife
The temperature of piece is maintained between 30~50 degrees Celsius.
The invention has the advantages that using pure natural grease as raw material, being free of any chemical addition agent, safety and environmental protection has
The functions such as potent decontamination, sterilization, skin care；The process reform of the invention straight line of original rotary-type Squeezinggranulator
The production method that " squash type " is granulated, changes into the production method of " extruding+grinding ", so that equipment cost is greatly reduced, energy consumption
Also it is greatly reduced, substantially improves the yield of soap rice, production efficiency is greatly improved, and it is also bright to produce soap grain of rice diameter
Aobvious to become smaller, dissolving power is very strong, and the machine washing that is more suitable uses.
Detailed description of the invention
Fig. 1 is the structure principle chart for grinding pelletizer；
Fig. 2 is the top view of Fig. 1；
Fig. 3 is the cooperation schematic diagram of binder impeller and grinding break bar；
Fig. 4 is the cooperation schematic diagram of discharge barrel and protective cover.
Specific embodiment
Referring to attached drawing, the present invention is with the natural ox of 75~85wt% or suet, the coconut oil of 15~25 wt%, 0~5 wt%
Palm-kernel oil be that raw material carries out saponification soap base is made, and soap base is made to the neat soap of 8~12 ㎜ of partial size；By neat soap, perfume (or spice)
Finishing enters in crutcher, and the pot temperature that reconciles is maintained at 60~80 DEG C, and with blender that material stirring in crutcher is uniform, stirring is big
About 10 minutes, in which: essence dosage is 1~1.5 wt%；The material stirred evenly is continued through three-roll mill to grind
Mill, is milled into laminar material, in which: three-roll mill controls in 0.2~0.4mm clearance between roll, and the revolving speed of roller is
15~25r/min；Laminar material is continuously introduced into grinding pelletizer to be granulated, grinding pelletizer includes feed hopper 1, discharging
Cylinder 3, binder impeller 2, grinding break bar 4, feed hopper is the infundibulate of opening upwards, and discharge barrel is the circle surrounded by side wall and bottom surface
Tubular, side wall are uniformly densely covered with discharge hole 7, and the diameter of discharge hole is 0.3 mm, and discharge barrel is connected to lower end of hopper；Binder leaf
Wheel is formed by binder wheel hub and by the equally spaced three pieces binder blade being arranged on binder wheel hub of circumference, every binder blade with
Horizontal plane inclination angle at 45 °, grinding break bar are ground by grinding wheel hub and by equally spaced six be arranged on grinding wheel hub of circumference
Sharpening sheet composition, the knife face for grinding blade is arc surface, grinds the knife face and horizontal plane of blade, binder impeller and grinding knife
Wheel is driven using concentric shafts, and concentric shafts pass perpendicularly through discharge barrel bottom center, and are connect by bearing with discharge barrel bottom surface, with one heart
The outer shaft 5 of axis is connect with grinding wheel hub, and inner shaft 6 is connect with binder wheel hub.Binder impeller is located on grinding break bar, pressure wheel
Hub and grinding wheel hub clearance fit, grinding knife sheet head and discharge barrel side wall at 0~15 degree of angle, and with discharge barrel sidewall spacers
Cooperation, is wrapped with 0.3 centimetre of wall thickness of stainless steel circular ring shape protective cover 8 in the side wall of discharge barrel, on the side wall of protective cover
Uniformly it is provided with the eyelet 9 of regular hexagon；Binder impeller rotates horizontally direction along binder blade pitch angle institute, and grinding break bar edge is ground
Sharpening sheet protrusion direction rotates horizontally, and binder impeller is opposite with grinding break bar direction of rotation；After material is sent into grinding pelletizer,
It is fallen into the gap between the grinding blade in discharge barrel by the interlobate gap of binder, the binder wheel rotation pressure downward to material
Power, the rotation of grinding knife wheel grind and form abrasive power between blade and discharge barrel side wall, by material by the discharge hole of discharge barrel side wall
Grinding is gone out, and is fallen naturally according to gravity, by the binder impeller of control grinding pelletizer and the revolving speed of grinding break bar, makes to grind
The temperature of blade is maintained between 30~50 degrees Celsius；In the vibrating screen of the lower section setting three-layer screen of grinding pelletizer, pass through
After shaker vibration screening, the soap rice grain that partial size is 0.3 ㎜ is obtained.
Embodiment 1:
The soap base composition of raw materials component of soap rice are as follows: ox or suet 85wt%, refined coconut 15 wt % of oil are added in soap base
The edible essence of 1.5 wt %, manufactured soap rice grain are the cylinder of 1~5 ㎜ of length, 0.3 ㎜ of diameter.For washing machine machine
Washed, dissolution is fast, strong detergency, low bubble, and easily rinsing, dirt-removing power is strong, non-sclerous after clothes washing, not static electrification.
Embodiment 2:
The soap base composition of raw materials component of soap rice are as follows: ox or suet 80wt%, 15 wt % of refined coconut oil, 5 wt of palm-kernel oil
%, is added the edible essence of 1.2wt % in soap base, and manufactured soap rice grain is the cylinder of 1~5 ㎜ of length, 0.3 ㎜ of diameter.
For washing machine machine washing of clothes, fast, strong detergency, low bubble are dissolved, easily rinsing, dirt-removing power is strong, and it is non-sclerous after clothes washing, no
Static electrification.
Embodiment 3:
The soap base composition of raw materials component of soap rice are as follows: ox or suet 75wt%, refined coconut oil 22 wt %, palm-kernel oil 3wt
%, is added the edible essence of 1 wt % in soap base, and manufactured soap rice grain is the cylinder of 1~5 ㎜ of length, 0.3 ㎜ of diameter.
For washing machine machine washing of clothes, fast, strong detergency, low bubble are dissolved, easily rinsing, dirt-removing power is strong, and it is non-sclerous after clothes washing, no
Static electrification.
Claims (6)
1. a kind of production method of soap rice, it is characterized in that:
1) using the natural ox of 75~85wt% or suet, the coconut oil of 15~25 wt%, 0~5 wt% palm-kernel oil as raw material into
Soap base is made in row saponification, and soap base is made to the neat soap of 8~12 ㎜ of partial size；
2) neat soap, essence are added in crutcher, the pot temperature that reconciles is maintained at 60~80 DEG C, with blender by material in crutcher
It stirs evenly, in which: essence dosage is 1~1.5 wt%；
3) material stirred evenly is continued through three-roll mill to mill, is milled into laminar material, in which: three rollers are ground
Grinding machine controls in 0.2~0.4mm clearance between roll, and the revolving speed of roller is 15~25r/min；
4) laminar material is continuously introduced into grinding pelletizer to be granulated, grinding pelletizer includes feed hopper, discharge barrel, binder
Impeller, grinding break bar, feed hopper is the infundibulate of opening upwards, and discharge barrel is the cylindrical shape surrounded by side wall and bottom surface, side wall
It is uniformly densely covered with discharge hole, the diameter of discharge hole is less than or equal to 0.5 mm, and discharge barrel is connected to lower end of hopper；Binder impeller
It is formed by binder wheel hub and by the equally spaced binder blade being arranged on binder wheel hub of circumference, every binder blade and horizontal plane
At 30~52 ° of inclinations angle, break bar is ground by grinding wheel hub and by the equally spaced grinding blade being arranged on grinding wheel hub of circumference
Composition, the knife face for grinding blade is arc surface, grinds the knife face and horizontal plane of blade, and binder impeller and grinding break bar use
Concentric shafts driving, concentric shafts pass perpendicularly through discharge barrel bottom center, and are connect by bearing with discharge barrel bottom surface, binder impeller position
On grinding break bar, binder wheel hub and grinding wheel hub clearance fit, grinding knife sheet head and discharge barrel side wall are at 0~15 degree
Angle, and cooperate with discharge barrel sidewall spacers, binder impeller rotates horizontally direction along binder blade pitch angle institute, grinds break bar
It is rotated horizontally along grinding blade protrusion direction, and binder impeller is opposite with grinding break bar direction of rotation；Material is sent into grinding and is granulated
After machine, by the interlobate gap of binder fall into discharge barrel grinding blade between gap in, binder wheel rotation to material to
Under pressure, the rotation of grinding knife wheel grinds and forms abrasive power between blade and discharge barrel side wall, by material by discharge barrel side wall
Discharge hole is ground away, and is fallen naturally according to gravity；
5) vibrating screen is set in the lower section of grinding pelletizer, after shaker vibration is sieved, obtains partial size less than or equal to 0.5 ㎜
Soap rice grain.
2. the production method of soap rice according to claim 1, it is characterized in that: the discharging bore dia of the discharge barrel is 0.3
~0.5 mm.
3. the production method of soap rice according to claim 1, it is characterized in that: the side wall in the discharge barrel is wrapped with circle
Ring protection cover is uniformly provided with the eyelet of regular geometric shapes on the side wall of protective cover.
4. the production method of soap rice according to claim 1, it is characterized in that: the number of the binder blade on the binder impeller
Amount is 3~9, and is odd number piece.
5. the production method of soap rice according to claim 1, it is characterized in that: the quantity of the grinding blade on grinding break bar is
3~12.
6. the production method of soap rice according to claim 1, it is characterized in that: passing through control grinding pelletizer in step 4)
Binder impeller and grind break bar revolving speed, make grind blade temperature be maintained between 30~50 degrees Celsius.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711258951.9A CN107828560B (en) | 2017-12-04 | 2017-12-04 | A kind of production method of soap rice |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711258951.9A CN107828560B (en) | 2017-12-04 | 2017-12-04 | A kind of production method of soap rice |
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| Publication Number | Publication Date |
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| CN107828560A CN107828560A (en) | 2018-03-23 |
| CN107828560B true CN107828560B (en) | 2019-11-22 |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2935595T3 (en) | 2015-09-16 | 2023-03-08 | Apeel Tech Inc | Method of forming a protective coating by applying fatty acid glyceride compounds to a surface |
| ES2939007T3 (en) | 2015-12-10 | 2023-04-18 | Apeel Tech Inc | Compositions of plant extracts to form protective coatings |
| EP3541192A4 (en) | 2016-11-17 | 2020-07-01 | Apeel Technology, Inc. | Compositions formed from plant extracts and methods of preparation thereof |
| JP2023516406A (en) | 2020-03-04 | 2023-04-19 | アピール テクノロジー，インコーポレイテッド | Coated produce and corresponding methods |
| CN116457332A (en) * | 2020-10-30 | 2023-07-18 | 阿比尔技术公司 | Composition and method for preparing same |
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| CN106118921B (en) * | 2016-06-22 | 2018-03-16 | 包头市红卫日用化工有限公司 | A kind of soap rice |
| CN205838956U (en) * | 2016-06-22 | 2016-12-28 | 包头市红卫日用化工有限公司 | A kind of soap rice produces equipment |
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