CN107805409A - A kind of Yellow environment-friendly disperse dye composition - Google Patents
A kind of Yellow environment-friendly disperse dye composition Download PDFInfo
- Publication number
- CN107805409A CN107805409A CN201711171712.XA CN201711171712A CN107805409A CN 107805409 A CN107805409 A CN 107805409A CN 201711171712 A CN201711171712 A CN 201711171712A CN 107805409 A CN107805409 A CN 107805409A
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- China
- Prior art keywords
- parts
- dye
- weight
- formula
- dye monomer
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 0 CC(C)C=CC=C(C*=C1C(C(c2ccccc22)=O)C2=O)C=C1OC Chemical compound CC(C)C=CC=C(C*=C1C(C(c2ccccc22)=O)C2=O)C=C1OC 0.000 description 2
- QOMLLXBOHXVMLC-UHFFFAOYSA-N COS(Oc1ccccc1)=O Chemical compound COS(Oc1ccccc1)=O QOMLLXBOHXVMLC-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0079—Azoic dyestuff preparations
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/008—Preparations of disperse dyes or solvent dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
- D06P1/18—Azo dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
- D06P3/54—Polyesters using dispersed dyestuffs
Abstract
The present invention relates to a kind of Yellow environment-friendly disperse dye mixture, the dyestuff are composed of the following components：Parts by weight are 0.01 30 parts of dye monomer A, and parts by weight are 5 70 parts of dye monomer B, and parts by weight are 0 30 parts of dye monomer C, and remaining is auxiliary agent.Dye mixture of the present invention can reduce production cost, reduce dyeing waste, as meeting the ecological ideas dyestuff of European Union's Reach laws and regulations requirements and the environmental certifications of Oeko Tex Standard 100, the compatibility of the dye mixture is good simultaneously, and the advantage in dyeing in terms of the wide adaptation range of pH value, tinctorial yield height, especially good level-dyeing property, sublimation reliability, washing fastness is more prominent, is a kind of superior Yellow environment-friendly disperse dye of properties.
Description
Technical field
The present invention relates to a kind of Yellow disperse dye, more particularly to a kind of Yellow environment-friendly disperse dye composition, this point
Dissipate the printing and dyeing that dyestuff is applied to polyester fiber.
Background technology
With the continuous improvement of environmental requirement, sensitization dyestuff has been gradually backed out market, if C.I. disperse yellows 23 are because of it
Dyeability is superior, and cheap application is relatively broad, but produces sensitization aromatic amine because it can be decomposed, and is classified as taboo by European Union
Do not used with dyestuff.Many existing Yellow environment-friendly disperse dyes of in the market, otherwise it is expensive, otherwise color fastness, carry
Liter property, compatibility can not substitute C.I. disperse yellows 23 completely.
Although has the Yellow disperse dye of some environment-friendly types in recent years, in patent CN1580133A, CN1974680A
Disclosed Yellow disperse dye is widely applied, but these Yellow disperse dyes with conventional blue 2BLN, red E-FB
Dyeing defect occurs when compatibility inconsistent situation, especially dyeing by jigger often occurring when being used as three primary colors.Cause
This, in the market is badly in need of a kind of Yellow environment-friendly disperse dye of high performance-price ratio, does not require nothing more than its compatibility and blue 2BLN, red E-FB
Matching, and dyestuff it is fast light, washing, distillation, perspiration fastness also to get well, to meet continually changing customer requirement.
The content of the invention
The technical problem that the present invention needs is to provide a kind of Yellow environment-friendly disperse dye composition.
In order to solve the above-mentioned technical problem, the present invention is achieved by the following technical solutions:
A kind of Yellow environment-friendly disperse dye composition, it is characterised in that the dye composite includes following component：
Parts by weight are 0.01~30 part of the dye monomer A as shown in formula (I) general structure,
Wherein R in formula (I)1For-C1~6Alkyl ,-CH2CH2OCOCH3Or-C2H4CN；R2For-C2H4CN or
Parts by weight are 5~70 parts of the dye monomer B as shown in formula (II) general structure,
Parts by weight are 0~30 part of the dye monomer C as shown in formula (III) general structure,
R in formula (III)3For-C1~6Alkyl, R4、R5For halogen or-H, R6For-NO2Or-H, R7For-H or
Parts by weight are 5~30 parts of auxiliary agent.
Preferably, the dye composite also includes the dye monomer D such as chemical formula (IV),
The parts by weight of the dye monomer D are 0~20 part.
Preferably, the dye composite includes：
Parts by weight are 0.01~30 part of the dye monomer A as shown in formula (I) general structure,
R in formula (I)1For-CH2CH3、-CH2CH2OCOCH3Or-C2H4CN；R2For-C2H4CN or
Parts by weight are 5~70 parts of the dye monomer B as shown in formula (II) general structure,
Parts by weight are 10~20 parts of the dye monomer C as shown in formula (III) general structure,
R in formula (III)3For-CH3Or-CH2CH3, R4、R5For-Cl or-H, R6For-NO2Or-H, R7For-H or；
Parts by weight are 5~20 parts of such as dye monomer D of chemical formula (IV),
Parts by weight are 5~30 parts of auxiliary agent.
Preferably, the dye composite is made up of following component：
Parts by weight are 0.01~30 part of dye monomer A；
Parts by weight are 10~60 parts of dye monomer B；
Parts by weight are 10~20 parts of dye monomer C；
Parts by weight are 5~20 parts of dye monomer D；
Parts by weight are 10~30 parts of auxiliary agent.
Preferably, described auxiliary agent includes one or a combination set of following thing：Lignosulfonates, the contracting of alkyl naphthalene sulfonic acid formaldehyde
Compound and naphthalene sulfonic acid-formaldehyde condensation product.
Preferably, dye monomer A be selected from the following dye monomer as shown in formula (I -1)~(I -3) any one or it is several
Kind：
Preferably, dye monomer C be selected from the following dye monomer as shown in formula (III -1)~(III -4) any one or
It is several：
Further, described auxiliary agent includes one of following or composition：Sodium lignin sulfonate (lignin 85A, 83A, S-
25th, S-28), naphthalene sulfonic acid-formaldehyde condensation product and condensation compound of methyl naphthalene sulfonic acid and formaldehyde (Dispersant MF).
Disperse dyes of the present invention can be prepared in accordance with the following methods：By the former dye monomer A of above-mentioned metering ratio, dye
Material list body B, dye monomer C and dye monomer D add auxiliary agent and warm water are dispersed with stirring dissolving, by even after pre-dispersed smash
After continuous abrasive sand is milled to terminal, then by repeating to filter, is sent by pipeline and put spray drying tower drying, while uniformly sprayed into dust-proof
Oil, end product packaging.The waste gas of output passes through dust removal by filtration for several times by cyclone dust collector in spray drying.
The dye monomer A that the present invention uses is C.I. disperse orange 25s or C.I. disperse orange 288 or C.I. disperse oranges
31；Dye monomer B be Jiangsu road win Chemical Manufacture yellow AG, dye monomer C be C.I. DISPERSE Yellow 211s, C.I. disperse yellows 114 or
Person C.I. disperse yellows 241, dye monomer D are C.I. disperse yellows 54, and commercially available prod all can be selected in several dye monomers of the above.
Color Index (C.I.) are the meanings of " Colour index number ", and it is international dyestuff title.
After adopting the above technical scheme, the beneficial effect that the present invention obtains is：It is of the invention effectively to compensate in the market Huang
The deficiency of color disperse dyes, production cost can be reduced, reduce dyeing waste, and be free of in dyestuff and disable fragrant amine component,
As the green colouring material of the environmental protection of Oeko-Tex Standard 100 and ecology is met, meet European Union's Reach laws and regulations requirements.Simultaneously
The compatibility of the dye composite is good, and in dyeing the wide adaptation range of pH value, tinctorial yield is high, enhancing is good, good level-dyeing property,
Advantage especially in terms of light fastness, washing fastness is more prominent, is that a kind of superior Yellow environment-friendly of properties disperses
Dyestuff.
Embodiment
With reference to embodiment, the present invention is further detailed explanation, but protection scope of the present invention is not limited to
This.
Embodiment 1-10
The data as shown in table 1, the former dye monomer A, dye monomer B, dye monomer C and the dye monomer D that measure ratio are passed through
It is pre-dispersed smash after, add auxiliary agent and warm water and be dispersed with stirring dissolving, by continuously grinding sand milling to terminal after, by repeating
Filter, sent by pipeline and put spray drying tower drying, while uniformly spray into dust laying oil, end product packaging.
Table 1
Disperse dyes made from above-described embodiment are subjected to composite performance test, method of testing is as follows：
Disperse dyes made from 1.0g embodiments 1-10 are respectively taken, it is the scattered of 1.0g/500ml to be configured to concentration respectively with water
Dye suspension thing, take 20ml to be mixed with 80ml water, adjust dye bath pH to 4.5-5.0 with acetic acid, be then warming up to 60 DEG C, simultaneously
It is respectively put into polyester fiber and carries out high-temperature pressure dyeing, 130 DEG C were warming up in 35 minutes, is incubated 30 minutes, is cooled to 80 DEG C
When sample.Observation cloth specimen coloured light simultaneously evaluates its dyefastness using GB/T3921, GB/T3920-1997, GB/T5718-1997.
Measurement result is shown in Table 2.
(the unit of table 2：Level)
| Embodiment title | Crock fastness | Washing fastness | Compatibility | PH scopes |
| Embodiment 1 | 4-5 | 4-5 | It is excellent | 4-9 |
| Embodiment 2 | 5 | 5 | It is excellent | 4-9 |
| Embodiment 3 | 5 | 5 | It is excellent | 4-9 |
| Embodiment 4 | 5 | 5 | It is excellent | 4-9 |
| Embodiment 5 | 5 | 5-6 | It is excellent | 4-9 |
| Embodiment 6 | 5 | 4-5 | It is excellent | 4-9 |
| Embodiment 7 | 5 | 4-5 | It is excellent | 4-9 |
| Embodiment 8 | 5 | 5 | It is excellent | 4-9 |
| Embodiment 9 | 5 | 5 | It is excellent | 4-9 |
| Embodiment 10 | 5 | 5-6 | It is excellent | 4-9 |
Particular embodiments described above simultaneously, has carried out entering one to the purpose of the present invention, technical scheme and beneficial effect
Step describes in detail, should be understood that above are only the specific embodiment of the present invention, is not intended to limit the invention,
Within the spirit and principles of the invention, any modification, equivalent substitution and improvements done etc., it should be included in the present invention's
Within protection domain.
Claims (7)
1. a kind of Yellow environment-friendly disperse dye composition, it is characterised in that the dye composite includes following component：
Parts by weight are the dye monomer A as shown in formula (I) general structure of 0.01-30 parts,
Wherein R in formula (I)1For C1~6Alkyl, CH2CH2OCOCH3Or C2H4CN；R2For C2H4CN or
Parts by weight are the dye monomer B as shown in formula (II) general structure of 5-70 parts,
Parts by weight are the dye monomer C as shown in formula (III) general structure of 0-30 parts,
R in formula (III)3For C1~6Alkyl, R4、R5Respectively halogen or H, R6For NO2Or H, R7For H or
Parts by weight are 5~30 parts of auxiliary agent.
2. Yellow environment-friendly disperse dye composition according to claim 1, it is characterised in that the dye composite also wraps
Dye monomer D containing such as chemical formula (IV),
Dye monomer D parts by weight described in composition are 0-20 parts.
A kind of 3. Yellow environment-friendly disperse dye composition according to claim 1, it is characterised in that the dye composite
It is made up of following component：
Parts by weight are the dye monomer A as shown in formula (I) general structure of 0.01-30 parts,
R in formula (I)1For CH2CH3、CH2CH2OCOCH3Or C2H4CN；R2For C2H4CN orParts by weight are
The dye monomer B as shown in formula (II) general structure of 5-70 parts,
Parts by weight are the dye monomer C as shown in formula (III) general structure of 10-20 parts,
R in formula (III)3For CH3Or CH2CH3, R4、R5Respectively Cl or H, R6For NO2Or H, R7For H or
Parts by weight are 5-20 parts such as dye monomer D of chemical formula (IV),
Parts by weight are 5~30 parts of auxiliary agent.
A kind of 4. Yellow environment-friendly disperse dye composition according to claim 1, it is characterised in that the dye composite
It is made up of following component：
Parts by weight are the dye monomer A of 0.01-30 parts；
Parts by weight are the dye monomer B of 10-60 parts；
Parts by weight are the dye monomer C of 10-20 parts；
Parts by weight are the dye monomer D of 5-20 parts；
Parts by weight are 10~30 parts of auxiliary agent.
5. according to a kind of Yellow environment-friendly disperse dye composition described in claim any one of 1-4, it is characterised in that：It is described
Auxiliary agent include one or a combination set of following thing：Lignosulfonates, alkyl naphthalene sulfonic acid formaldehyde condensation products and naphthalenesulfonateformaldehyde formaldehyde contracting
Compound.
6. according to a kind of any one of claim 1-4 Yellow environment-friendly disperse dye compositions, it is characterised in that：Such as formula
(I) the dye monomer A shown in general structure be selected from the following dye monomer as shown in formula (I -1)~(I -3) any one or
It is several：
7. according to a kind of any one of claim 1-4 Yellow environment-friendly disperse dye compositions, it is characterised in that：Such as formula
(III) the dye monomer C shown in general structure is selected from any one of the following dye monomer as shown in formula (III -1)~(III -4)
It is or several：
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711171712.XA CN107805409A (en) | 2017-11-21 | 2017-11-21 | A kind of Yellow environment-friendly disperse dye composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711171712.XA CN107805409A (en) | 2017-11-21 | 2017-11-21 | A kind of Yellow environment-friendly disperse dye composition |
Publications (1)
| Publication Number | Publication Date |
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| CN107805409A true CN107805409A (en) | 2018-03-16 |
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| CN201711171712.XA Pending CN107805409A (en) | 2017-11-21 | 2017-11-21 | A kind of Yellow environment-friendly disperse dye composition |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108410209A (en) * | 2018-02-05 | 2018-08-17 | 浙江山峪科技股份有限公司 | A kind of yellowish-brown disperse dye composition of the high fastness of environment-friendly type, dye preparations and application |
| CN109021616A (en) * | 2018-06-15 | 2018-12-18 | 浙江龙盛集团股份有限公司 | A kind of disperse yellow dye composition, its product and application |
| CN109705620A (en) * | 2019-01-08 | 2019-05-03 | 江苏道博化工有限公司 | A kind of alkali resistant yellow disperse dye composition |
| CN110776757A (en) * | 2019-12-13 | 2020-02-11 | 浙江闰土股份有限公司 | Golden yellow disperse dye composition, golden yellow disperse dye and preparation method and application thereof |
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| CN103059604A (en) * | 2013-01-10 | 2013-04-24 | 浙江山峪染料化工有限公司 | Disperse yellow dye |
| CN103740135A (en) * | 2013-12-16 | 2014-04-23 | 浙江龙盛集团股份有限公司 | Low-temperature and environment-friendly disperse yellow dye composition |
| CN104371361A (en) * | 2013-12-30 | 2015-02-25 | 阮偶娟 | Yellow disperse dye composition and disperse dye and preparation method and use thereof |
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| US4548613A (en) * | 1984-05-18 | 1985-10-22 | American Hoechst Corporation | Yellow disperse dyestuff mixtures and dyeing process |
| JPS6351466A (en) * | 1986-08-22 | 1988-03-04 | Mitsubishi Chem Ind Ltd | Dye mixture |
| GB2226826A (en) * | 1989-01-07 | 1990-07-11 | Sandoz Ltd | Disperse disazo-pyridone dyes |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108410209A (en) * | 2018-02-05 | 2018-08-17 | 浙江山峪科技股份有限公司 | A kind of yellowish-brown disperse dye composition of the high fastness of environment-friendly type, dye preparations and application |
| CN108410209B (en) * | 2018-02-05 | 2019-11-12 | 浙江山峪科技股份有限公司 | A kind of yellowish-brown disperse dye composition of the high fastness of environment-friendly type, dye preparations and application |
| CN109021616A (en) * | 2018-06-15 | 2018-12-18 | 浙江龙盛集团股份有限公司 | A kind of disperse yellow dye composition, its product and application |
| CN109021616B (en) * | 2018-06-15 | 2020-06-05 | 浙江龙盛集团股份有限公司 | Disperse yellow dye composition, and product and application thereof |
| CN109705620A (en) * | 2019-01-08 | 2019-05-03 | 江苏道博化工有限公司 | A kind of alkali resistant yellow disperse dye composition |
| CN110776757A (en) * | 2019-12-13 | 2020-02-11 | 浙江闰土股份有限公司 | Golden yellow disperse dye composition, golden yellow disperse dye and preparation method and application thereof |
| CN110776757B (en) * | 2019-12-13 | 2021-09-17 | 浙江闰土股份有限公司 | Golden yellow disperse dye composition, golden yellow disperse dye and preparation method and application thereof |
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