CN107796723A - The control characterization processes of suspension content in sewage disposal - Google Patents

The control characterization processes of suspension content in sewage disposal Download PDF

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Publication number
CN107796723A
CN107796723A CN201710950379.6A CN201710950379A CN107796723A CN 107796723 A CN107796723 A CN 107796723A CN 201710950379 A CN201710950379 A CN 201710950379A CN 107796723 A CN107796723 A CN 107796723A
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China
Prior art keywords
screen pack
conical flask
flask body
sewage
suspension
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CN201710950379.6A
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Chinese (zh)
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袁士林
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Individual
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Individual
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Priority to CN201710950379.6A priority Critical patent/CN107796723A/en
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N5/00Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The invention discloses the control characterization processes of suspension content in sewage disposal.The present invention includes (1) and pre-processed:Dried after cleaning isolating device;Second screen pack is placed into drying box and dried repeatedly, obtains the weight t1 of the second screen pack;Second screen pack is installed in isolating device;(2) sewage sample is added, the volume V of sewage is read according to the scale on conical flask body, is inverted isolating device, sewage is flowed through the second screen pack until sewage filters completely;(3) distilled water is added to concussion in conical flask body and rinses conical flask body, being then inverted makes distilled water flow out conical flask body after flowing completely through the second screen pack;(4) after repeat step (3) 2~4 times, remove the second screen pack and be placed into drying box and dry repeatedly, obtain the weight t2 of the second screen pack;(5) the content H of suspension is obtained according to calculation formula H=(t2 t1)/V.The present invention have it is simple in construction, it is easy to operate, the advantages that excellent performance.

Description

The control characterization processes of suspension content in sewage disposal
Technical field
The present invention relates to a kind of detection method of suspension content, and in particular to the control of suspension content in sewage disposal Characterization processes.
Background technology
Suspension (Suspended Solids) refers to the solid matter being suspended in water, including insoluble in water inorganic Thing, organic matter and silt particle, clay, microorganism etc..Suspension content is one of index for weighing water pollution degree in water.Suspension It is the main reason for causing water muddiness.Easy anaerobic fermentation after organic suspended matter deposition in water body, makes water quality deterioration.Chinese sewage Comprehensive discharge standard points 3 grades is, it is specified that the highest of suspension allows concentration of emission, Chinese groundwater quality mark in sewage and waste water Accurate and standards for drinking water quality dictates to suspension in water by index of turbidity.
And in the prior art, suspension refers to by the solids of filter the filter paper to constant weight can not will be claimed to be put into Bu Shi In funnel, water sample is filtered with middling speed quantitative filter paper, constant weight is dried to through 103~105 DEG C, the obtained residue that can not always filter (suspends Thing) content.Specifically detection mode is:
Suspension in water quality refers to that water sample by the filter membrane that aperture is 0.45 μm, is trapped on filter membrane and in 103~105 DEG C it is dried to the material of constant weight.The uneven solid matter of floating or submergence is not belonging to suspended material, should be removed from water sample.It is existing It is typically first to remove in water sample after the uneven solid matter of floating or submergence to have in technology, the suspension in water quality is carried out Detection, operating process is cumbersome, causes detection intensity big.
The content of the invention
The technical problems to be solved by the invention are:The detection operating process of suspension is cumbersome in the prior art, causes to examine Survey intensity it is big the problem of, and it is an object of the present invention to provide in sewage disposal suspension content control characterization processes, can effectively reduce operation Step, and testing result is effectively ensured, effect is more notable.
The present invention is achieved through the following technical solutions:
The control characterization processes of suspension content in sewage disposal, including:
(1) pre-process:Dried after cleaning isolating device;The isolating device includes the conical flask body of top end opening, screw thread The screen pack installing matrix of conical flask body upper shed opening position is connected to, is arranged on opening for screen pack installing matrix and conical flask body The first screen pack between mouthful, the pressed seat being threaded in screen pack installing matrix, and it is arranged on screen pack installation base The second screen pack between body and pressed seat;Scale is provided with the conical flask body;Wherein, the filtering accuracy of the first screen pack For 0.2um, the filtering accuracy of the second screen pack is 10nm;
Second screen pack is placed into drying box and dried repeatedly until the adjacent weight difference measured twice is less than or equal to 0.1mg, and obtain the weight t1 of the second screen pack;Second screen pack is installed in isolating device;
(2) sewage sample is added, the volume V of sewage is read according to the scale on conical flask body, isolating device is inverted, makes dirt Water flows through the second screen pack until sewage filters completely;
(3) distilled water is added to concussion in conical flask body and rinses conical flask body, being then inverted flows completely through distilled water Conical flask body is flowed out after second screen pack;
(4) after repeat step (3) 2~4 times, the second screen pack is removed, is placed into drying box and dries repeatedly until adjacent The weight difference measured twice is less than or equal to 0.1mg, and obtains the weight t2 of the second screen pack;
(5) the content H of suspension is obtained according to calculation formula, the content H of suspension calculation formula is:H=(t2- t1)/V。
By the optimization of the device of the present invention, the step of can effectively simplifying operating method, dress of the invention need to be only used Put and once filtered, then detect the weight increase situation of the second screen pack, you can effectively calculate the content of suspension, behaviour Make easier.And the mode in the present invention can be effectively isolated the uneven solid matter for floating or submerging in boiling water sample, make to hang The testing result of float is more accurate.
Further, the screen pack installing matrix top is provided with first annular protruding part, and second screen pack passes through One ring packing packing ring is fixed on first annular protruding part.The conical flask body top is provided with the second annular protruding part, should First screen pack is fixed on the second annular protruding part by the second ring packing packing ring.
By the setting of said structure, the amount of suspension adhesion in a device is reduced as far as possible, makes it viscous as far as possible It is attached on screen pack, and then effectively improves the accuracy of testing result.
Preferably, the first annular seal washer and the second ring packing packing ring are formed by quality of rubber materials, and this first The girth of ring packing packing ring under field conditions (factors) is less than or equal to the girth of first annular protruding part, the second ring packing packing ring Girth under field conditions (factors) is less than or equal to the girth of the second annular protruding part.
Further, suction filtration interface is provided with above the pressed seat, an inlet and outlet is additionally provided with the conical flask body.
By the setting, suction operation is not only easily facilitated, improves filter efficiency, and setting by the inlet and outlet Put, distilled water can be added from the opening position of the inlet and outlet, and then the suspension adhered on conical flask body is effectively flushed to filtering On the net, operating procedure is simplified, operation is easier.
Preferably, the inlet and outlet are arranged on the opening position below in the middle part of conical flask body, and inlet and outlet is opening up, should The axis of inlet and outlet and the axis of conical flask body are in 30~45 degree of angles.
The present invention compared with prior art, has the following advantages and advantages:
1st, operating procedure can effectively be simplified by the optimization of apparatus of the present invention, only the device of the present invention need to be used to carry out once Filtering, then detect the weight increase situation of the second screen pack, you can effectively calculate the content of suspension, operation is simpler Just;
2nd, the mode in the present invention can be effectively isolated the uneven solid matter for floating or submerging in boiling water sample, make suspension Testing result it is more accurate;
3rd, simple in construction, easy to operate, excellent performance of the invention, effect are very notable.
Brief description of the drawings
Accompanying drawing described herein is used for providing further understanding the embodiment of the present invention, forms one of the application Point, do not form the restriction to the embodiment of the present invention.In the accompanying drawings:
Fig. 1 is the structural representation of the present invention.
Fig. 2 is the structural representation of conical flask body opening in the present invention.
Mark and corresponding parts title in accompanying drawing:
1- conical flask bodies, 2- screen pack installing matrixes, the screen packs of 3- first, 4- pressed seats, the screen packs of 5- second, 6- are carved Degree, the first annular protruding parts of 7-, the first annular seal washers of 8-, the second annular protruding parts of 9-, 10- the second ring packing packing rings, 11- filters interface, 12- inlet and outlet.
Embodiment
For the object, technical solutions and advantages of the present invention are more clearly understood, with reference to embodiment and accompanying drawing, to this Invention is described in further detail, and exemplary embodiment of the invention and its explanation are only used for explaining the present invention, do not make For limitation of the invention.
Embodiment 1
The control characterization processes of suspension content in sewage disposal, including:
(1) pre-process:Dried after cleaning isolating device, the second screen pack is placed into drying box and dried repeatedly until phase The weight difference that neighbour measures twice is less than or equal to 0.1mg, and obtains the weight t1 of the second screen pack;By the second screen pack be installed to every From on device;
Wherein, isolating device as depicted in figs. 1 and 2, includes the conical flask body 1 of top end opening, is threaded in conical flask The screen pack installing matrix 2 of the upper shed opening position of body 1, is arranged between screen pack installing matrix 2 and the opening of conical flask body 1 First screen pack 3, the pressed seat 4 being threaded in screen pack installing matrix 2, and be arranged on screen pack installing matrix 2 with The second screen pack 5 between pressed seat 4;Scale 6 is provided with the conical flask body 1.The top of pressed seat 4 is provided with suction filtration Interface 11, an inlet and outlet 12 are additionally provided with the conical flask body 1.The filtering accuracy of first screen pack is 0.2um, and second filters The filtering accuracy of net is 10nm.
(2) sewage sample is added, the volume V of sewage is read according to the scale on conical flask body, isolating device is inverted, makes dirt Water flows through the second screen pack until sewage filters completely.
(3) distilled water is added to concussion in conical flask body and rinses conical flask body, being then inverted flows completely through distilled water Conical flask body is flowed out after second screen pack.
(4) after repeat step (3) 2~4 times, the second screen pack is removed, is placed into drying box and dries repeatedly until adjacent The weight difference measured twice is less than or equal to 0.1mg, and obtains the weight t2 of the second screen pack.
(5) the content H of suspension is obtained according to calculation formula, the content H of suspension calculation formula is:H=(t2- t1)/V。
Embodiment 2
The present embodiment and the difference of embodiment 1 are that the present embodiment is optimized at the aperture position of conical flask body 1, screen pack Installing matrix 2 and the structure of pressed seat 4, specific setting are as follows:
The top of pressed seat 4, which is provided with, filters interface 11, and an inlet and outlet 12 are additionally provided with the conical flask body 1.
The top of screen pack installing matrix 2 is provided with first annular protruding part 7, and second screen pack 5 passes through the first ring Shape seal washer 8 is fixed on first annular protruding part 7.The top of conical flask body 1 is provided with the second annular protruding part 9, should First screen pack 5 is fixed on the second annular protruding part 9 by the second ring packing packing ring 10.
The ring packing packing ring 10 of first annular seal washer 7 and second is formed by quality of rubber materials, and this is first annular The girth of seal washer 7 under field conditions (factors) is less than or equal to the girth of first annular protruding part 7, the second ring packing packing ring 10 Girth under field conditions (factors) is less than or equal to the girth of the second annular protruding part 9.
The inlet and outlet 12 are arranged on the opening position below the middle part of conical flask body 1, and inlet and outlet 12 is opening up, and this enters The axis of outlet 12 is in 30~45 degree of angles with the axis of conical flask body 1.
Above-described embodiment, the purpose of the present invention, technical scheme and beneficial effect are carried out further Describe in detail, should be understood that the embodiment that the foregoing is only the present invention, be not intended to limit the present invention Protection domain, within the spirit and principles of the invention, any modification, equivalent substitution and improvements done etc., all should include Within protection scope of the present invention.

Claims (5)

1. the control characterization processes of suspension content in sewage disposal, it is characterised in that including:
(1) pre-process:Dried after cleaning isolating device;The isolating device includes the conical flask body of top end opening, threaded connection In the screen pack installing matrix of conical flask body upper shed opening position, be arranged on screen pack installing matrix and conical flask body opening it Between the first screen pack, the pressed seat being threaded in screen pack installing matrix, and be arranged on screen pack installing matrix with The second screen pack between pressed seat;Scale is provided with the conical flask body;Wherein, the filtering accuracy of the first screen pack is 0.2um, the filtering accuracy of the second screen pack is 10nm;
By the second screen pack be placed into drying box repeatedly dry until the adjacent weight difference measured twice be less than or equal to 0.1mg, And obtain the weight t1 of the second screen pack;Second screen pack is installed in isolating device;
(2) sewage sample is added, the volume V of sewage is read according to the scale on conical flask body, isolating device is inverted, makes sewage stream The second screen pack is crossed until sewage filters completely;
(3) distilled water is added to concussion in conical flask body and rinses conical flask body, being then inverted makes distilled water flow completely through second Conical flask body is flowed out after screen pack;
(4) after repeat step (3) 2~4 times, remove the second screen pack, be placed into drying box dry repeatedly until it is adjacent twice The weight difference measured is less than or equal to 0.1mg, and obtains the weight t2 of the second screen pack;
(5) the content H of suspension is obtained according to calculation formula, the content H of suspension calculation formula is:H=(t2-t1)/ V。
2. the control characterization processes of suspension content in sewage disposal according to claim 1, it is characterised in that the pressure Suction filtration interface is provided with above tight seat, an inlet and outlet are additionally provided with the conical flask body.
3. the control characterization processes of suspension content in sewage disposal according to claim 2, it is characterised in that it is described enter Outlet is arranged on the opening position below in the middle part of conical flask body, and opening up, the axis of the inlet and outlet and the taper imported and exported The axis of bottle is in 30~45 degree of angles.
4. the control characterization processes of suspension content in sewage disposal according to claim 1, it is characterised in that the mistake Filter screen installing matrix top is provided with first annular protruding part, and second screen pack is fixed on by first annular seal washer On one annular protruding part;The conical flask body top is provided with the second annular protruding part, and first screen pack passes through the second annular Seal washer is fixed on the second annular protruding part.
5. the control characterization processes of suspension content in sewage disposal according to claim 1, it is characterised in that described One ring packing packing ring and the second ring packing packing ring are formed by quality of rubber materials, and the first annular seal washer is in natural conditions Under girth be less than or equal to the girth of first annular protruding part, the girth of the second ring packing packing ring under field conditions (factors) is less than Equal to the girth of the second annular protruding part.
CN201710950379.6A 2017-10-13 2017-10-13 The control characterization processes of suspension content in sewage disposal Withdrawn CN107796723A (en)

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Application Number Priority Date Filing Date Title
CN201710950379.6A CN107796723A (en) 2017-10-13 2017-10-13 The control characterization processes of suspension content in sewage disposal

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Application Number Priority Date Filing Date Title
CN201710950379.6A CN107796723A (en) 2017-10-13 2017-10-13 The control characterization processes of suspension content in sewage disposal

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108760560A (en) * 2018-05-21 2018-11-06 山东京博石油化工有限公司 A kind of method and device detecting the coke powder content in delayed coking acid water

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108760560A (en) * 2018-05-21 2018-11-06 山东京博石油化工有限公司 A kind of method and device detecting the coke powder content in delayed coking acid water

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Application publication date: 20180313