CN107790082A - A kind of glycerine handles reactor - Google Patents

A kind of glycerine handles reactor Download PDF

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Publication number
CN107790082A
CN107790082A CN201610800293.0A CN201610800293A CN107790082A CN 107790082 A CN107790082 A CN 107790082A CN 201610800293 A CN201610800293 A CN 201610800293A CN 107790082 A CN107790082 A CN 107790082A
Authority
CN
China
Prior art keywords
glycerine
main body
separator box
inner chamber
standing groove
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610800293.0A
Other languages
Chinese (zh)
Inventor
高占友
刘长锁
马秀玲
傅丽丽
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Medicine Co Ltd Co Of Tianjin China And Sweden
Original Assignee
Medicine Co Ltd Co Of Tianjin China And Sweden
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Medicine Co Ltd Co Of Tianjin China And Sweden filed Critical Medicine Co Ltd Co Of Tianjin China And Sweden
Priority to CN201610800293.0A priority Critical patent/CN107790082A/en
Publication of CN107790082A publication Critical patent/CN107790082A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/01Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/0013Controlling the temperature of the process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00054Controlling or regulating the heat exchange system
    • B01J2219/00056Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00058Temperature measurement
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00081Tubes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)

Abstract

The invention discloses a kind of glycerine to handle reactor,Including main body,The intracavity sidewall of the main body is movably installed with activated carbon standing groove close to the lower end of charging aperture,Another side wall in inner chamber of the main body is installed with temperature detector,Bottom is installed with heater strip in the inner chamber of the main body,The outer wall side of the main body is installed with controller,The outer wall opposite side of the main body is provided with drain hole,The end of the escape pipe is installed with condensation chamber,The lower end of the condensation chamber is fixedly connected with separator box by pipeline,The side upper end of the separator box is provided with glycerine delivery hose,The end of the glycerine delivery hose is installed with hydraulic pump,The inner chamber lower end of the separator box is provided with glycerine screen pack,Glycerine processing reactor can more efficiently handle crude glycerine,And high treating effect,Sufficient purified treatment crude glycerine can be compared,It can separate and handle the glycerine of volatilization,Improve the organic efficiency of glycerine.

Description

A kind of glycerine handles reactor
Technical field
The present invention relates to technical field of food additives, specially a kind of glycerine processing reactor.
Background technology
Crude glycerine, which can isolate some when being pre-processed and float on glycerine upper strata, pigment, and can contain in crude glycerine The impurity such as a small amount of water, to ensure the smooth production of process below, it is necessary to carry out adsorption filtration to pigment and carried out to glycerine Purified treatment.But the equipment operation inconvenience for pigment adsorption filtration in the prior art, the equipment replacement of absorption is inconvenient, and It is huger for the equipment of the purified treatment of glycerine, complicated, operation inconvenience.
The content of the invention
It is an object of the invention to provide a kind of glycerine to handle reactor, is asked with solve to propose in above-mentioned background technology Topic.
To achieve the above object, the present invention provides following technical scheme:A kind of glycerine handles reactor, including main body, institute The lower end for stating main body is fixedly connected with the first supporting leg, and motor, the motor are provided with the middle part of the upper surface of the main body Both sides be respectively arranged with charging aperture and escape pipe, the intracavity sidewall of the main body is movably installed with work close to the lower end of charging aperture Property charcoal standing groove, another side wall in inner chamber of the main body are installed with temperature detector, and the output shaft end of the motor is consolidated Surely rotary shaft is connected with, the middle part and lower end of the rotary shaft are installed with puddler, and bottom is consolidated in the inner chamber of the main body Dingan County is equipped with heater strip, and the outer wall side of the main body is installed with controller, and the outer wall opposite side of the main body is provided with Drain hole, and the bottom of main body is provided with the first leakage fluid dram, the end of the escape pipe is installed with condensation chamber, the condensation The lower end of room is fixedly connected with separator box by pipeline, and the side upper end of the separator box is provided with glycerine delivery hose, described Glycerine delivery hose can be installed with hydraulic pump in separator box internal regulation height, the end of the glycerine delivery hose, The lower end both sides of the separator box are connected with the second supporting leg, and the second leakage fluid dram, institute are provided among the lower end of the separator box The inner chamber lower end for stating separator box is provided with glycerine screen pack, and the temperature detector and heater strip are electrically connected with controller.
Preferably, handle is installed with the outside of the activated carbon standing groove, and the lower end of activated carbon standing groove is set There is supporting plate, the supporting plate is fixedly connected with main body.
Preferably, the upper end of the activated carbon standing groove is set fluted.
Preferably, the lower end of the separator box is arranged to coniform.
Preferably, the port part being connected with main body of the escape pipe is provided with trapezoid-shaped openings.
Preferably, the lower end of the charging aperture is provided with extension block.
Compared with prior art, the beneficial effects of the invention are as follows:Glycerine processing reactor can be handled more efficiently Crude glycerine, and high treating effect, activated carbon can carry out preliminary treatment to crude glycerine, and activated carbon standing groove passes through bolt Connection, can be changed, and fixed than stronger, and heater strip heats to device, while has agitating device, can compare and fill The purified treatment crude glycerine divided, and escape pipe is provided with condensation chamber and separator box, further can separate and handle volatilization Glycerine, improve the organic efficiency of glycerine.
Brief description of the drawings
Fig. 1 is schematic structural view of the invention;
Fig. 2 is activated carbon standing groove front view of the present invention.
In figure:1 main body, 2 temperature detectors, 3 escape pipes, 4 motor, 5 charging apertures, 6 extension blocks, 7 activated carbon standing grooves, 71 handles, 72 supporting plates, 8 controllers, 9 rotary shafts, 10,11 first supporting legs, 12 second supporting legs, 13 second leakage fluid drams, 14 It is separator box, 15 first leakage fluid drams, 16 pipelines, 17 puddlers, 18 condensation chambers, 19,20 glycerine delivery hoses, 21 drain holes, 22 sweet Oily screen pack.
Embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.It is based on Embodiment in the present invention, those of ordinary skill in the art are obtained every other under the premise of creative work is not made Embodiment, belong to the scope of protection of the invention.
Fig. 1-2 is referred to, the present invention provides a kind of technical scheme:A kind of glycerine handles reactor, including main body 1, described The lower end of main body 1 is fixedly connected with the first supporting leg 11, and motor 4 is provided with the middle part of the upper surface of the main body 1, described electronic The both sides of machine 4 are respectively arranged with charging aperture 5 and escape pipe 3, and the port part being connected with main body 1 of the escape pipe 3 is provided with ladder Shape opening, can preferably collect steam, and the lower end of the charging aperture 5 is provided with extension block 6, activated carbon standing groove 7 is played More preferable supporting role, the intracavity sidewall of the main body 1 are movably installed with activated carbon standing groove 7, institute close to the lower end of charging aperture 5 The outside for stating activated carbon standing groove 7 is installed with handle 71, and the lower end of activated carbon standing groove 7 is provided with supporting plate 72, institute State supporting plate 72 to be fixedly connected with main body 1, the upper end setting of the activated carbon standing groove 7 is fluted, can make the liquid of entrance Preferably filtering, another side wall in inner chamber of the main body 1 are installed with temperature detector 2, the output shaft end of the motor 4 It is fixedly connected with rotary shaft 9, the middle part and lower end of the rotary shaft 9 are installed with puddler 17, in the inner chamber of the main body 1 Bottom is installed with heater strip 10, and the outer wall side of the main body 1 is installed with controller 8, and the outer wall of the main body 1 is another Side is provided with drain hole 21, and the outer wall opposite side of the main body 1 is provided with drain hole 21, and the bottom of main body 1 is provided with One leakage fluid dram 15, the end of the escape pipe 3 are installed with condensation chamber 18, and the lower end of the condensation chamber 18 is solid by pipeline 16 Surely separator box 14 is connected with,:The lower end of the separator box 14 is arranged to coniform, and the side upper end of the separator box 14 is provided with Glycerine delivery hose 20, the glycerine delivery hose 20 can be in the internal regulation of separator box 14 height, the glycerine delivery hoses 20 end is installed with hydraulic pump 19, and the lower end both sides of the separator box 14 are connected with the second supporting leg 12, the separation The second leakage fluid dram 13 is provided among the lower end of case 14, the inner chamber lower end of the separator box 14 is provided with glycerine screen pack 22, institute State temperature detector 2 and heater strip 10 is electrically connected with controller 8.
Operation principle:Crude glycerine is entered by charging aperture 5 in the inner chamber of main body 1, and activated carbon can carry out preliminary to liquid Purified treatment, then motor 4 can drive the rotation of rotary shaft 9, then the puddler 17 in rotary shaft 9 can be in main body Crude glycerine be stirred, while heater strip 10 can heat to the liquid in main body 1, and temperature detector 2 can detect Temperature in the inner chamber of main body 1, then sending instruction to controller 8 at any time, controller 8 controls the break-make of heater strip 10, so as to The temperature inside main body 1 is controlled, the heated boil-off gas of liquid enters condensation chamber 8 by escape pipe 3, by condensation chamber 8 Steam become liquid separator box 14 entered by pipeline 16, the glycerine screen pack 22 in separator box 14 can filter out glycerine and Water, glycerine delivery hose 20 can pump out glycerine in the presence of hydraulic pump 19, and drain hole 21 can purify to being put into main body 1 Material, facilitates the purification of crude glycerine.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (6)

1. a kind of glycerine handles reactor, including main body (1), it is characterised in that:The lower end of the main body (1) is fixedly connected with One supporting leg (11), the upper surface middle part of the main body (1) are provided with motor (4), and the both sides of the motor (4) are set respectively Charging aperture (5) and escape pipe (3) are equipped with, the intracavity sidewall of the main body (1) is movably installed with work close to the lower end of charging aperture (5) Property charcoal standing groove (7), another side wall in inner chamber of the main body (1) are installed with temperature detector (2), the motor (4) Output shaft end be fixedly connected with rotary shaft (9), the middle part and lower end of the rotary shaft (9) are installed with puddler (17), Bottom is installed with heater strip (10) in the inner chamber of the main body (1), and the outer wall side of the main body (1) is installed with control Device (8) processed, the outer wall opposite side of the main body (1) is provided with drain hole (21), and the bottom of main body (1) is provided with the first discharge opeing Mouth (15), the end of the escape pipe (3) are installed with condensation chamber (18), and the lower end of the condensation chamber (18) passes through pipeline (16) separator box (14) is fixedly connected with, the side upper end of the separator box (14) is provided with glycerine delivery hose (20), described Glycerine delivery hose (20) can fix peace in separator box (14) internal regulation height, the end of the glycerine delivery hose (20) Equipped with hydraulic pump (19), the lower end both sides of the separator box (14) are connected with the second supporting leg (12), the separator box (14) The second leakage fluid dram (13) is provided among lower end, the inner chamber lower end of the separator box (14) is provided with glycerine screen pack (22), institute Temperature detector (2) and heater strip (10) is stated to be electrically connected with controller (8).
A kind of 2. glycerine processing reactor according to claim 1, it is characterised in that:The activated carbon standing groove (7) Outside is installed with handle (71), and the lower end of activated carbon standing groove (7) is provided with supporting plate (72), the supporting plate (72) It is fixedly connected with main body (1).
A kind of 3. glycerine processing reactor according to claim 1, it is characterised in that:The activated carbon standing groove (7) Upper end sets fluted.
A kind of 4. glycerine processing reactor according to claim 1, it is characterised in that:The lower end of the separator box (14) is set It is set to coniform.
A kind of 5. glycerine processing reactor according to claim 1, it is characterised in that:The escape pipe (3) and main body (1) port part of connection is provided with trapezoid-shaped openings.
A kind of 6. glycerine processing reactor according to claim 1, it is characterised in that:The lower end of the charging aperture (5) is set It is equipped with extension block (6).
CN201610800293.0A 2016-08-31 2016-08-31 A kind of glycerine handles reactor Pending CN107790082A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610800293.0A CN107790082A (en) 2016-08-31 2016-08-31 A kind of glycerine handles reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610800293.0A CN107790082A (en) 2016-08-31 2016-08-31 A kind of glycerine handles reactor

Publications (1)

Publication Number Publication Date
CN107790082A true CN107790082A (en) 2018-03-13

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ID=61530586

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610800293.0A Pending CN107790082A (en) 2016-08-31 2016-08-31 A kind of glycerine handles reactor

Country Status (1)

Country Link
CN (1) CN107790082A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108469369A (en) * 2018-05-11 2018-08-31 广东产品质量监督检验研究院(国家质量技术监督局广州电气安全检验所、广东省试验认证研究院、华安实验室) Solid Phase Extraction-nitrogen blows concentration integrated device

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108469369A (en) * 2018-05-11 2018-08-31 广东产品质量监督检验研究院(国家质量技术监督局广州电气安全检验所、广东省试验认证研究院、华安实验室) Solid Phase Extraction-nitrogen blows concentration integrated device

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WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20180313

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