CN107789224A - A kind of tea oil for being used to take care of hair - Google Patents

A kind of tea oil for being used to take care of hair Download PDF

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Publication number
CN107789224A
CN107789224A CN201711018527.7A CN201711018527A CN107789224A CN 107789224 A CN107789224 A CN 107789224A CN 201711018527 A CN201711018527 A CN 201711018527A CN 107789224 A CN107789224 A CN 107789224A
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China
Prior art keywords
tea oil
tea
hair
oil
refined
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CN201711018527.7A
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Chinese (zh)
Inventor
刘健华
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Zhejiang Shengtai Oil Technology Co Ltd
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Zhejiang Shengtai Oil Technology Co Ltd
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Priority to CN201711018527.7A priority Critical patent/CN107789224A/en
Publication of CN107789224A publication Critical patent/CN107789224A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/006Antidandruff preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/02Pretreatment
    • C11B1/04Pretreatment of vegetable raw material
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/06Production of fats or fatty oils from raw materials by pressing
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/001Refining fats or fatty oils by a combination of two or more of the means hereafter
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/008Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Microbiology (AREA)
  • Dermatology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Cosmetics (AREA)

Abstract

The present invention provides a kind of refined tea oil for being used to take care of hair, and comprises the following steps:(1) preparation of tea oil is refined:Using the pressing method of low temperature, refine and obtain tea oil;(2) preparation of tea oil leaves shampoo:Citric acid 10g, dodecyl polyoxy ethylene sulfate 100g, neopelex 50g are fitted into container, 1 hour is stirred at 50 DEG C to thawing;The refined tea oil of 10g steps (1) is added, is sufficiently stirred, obtains viscous liquid;Cool down 24 hours, get product at room temperature;(3) optionally, after natural cooling, 2 3g essence, preferably vanillic aldehyde can be added.The leaves shampoo made of the tea oil, there is dandruff-removing itching-relieve, moisten the effect of hair care.The tea oil directly can also be acted on into hair, hair can be made pitch-black beautiful, high resilience.

Description

A kind of tea oil for being used to take care of hair
Technical field
The invention belongs to filed of daily-use chemical industry, and in particular to a kind of tea oil for hair-washing hair-care.
Background technology
Tea oil is the vegetable oil obtained in a kind of seed from tea oil tree, rich in multiple nutritional components, is preventing high blood Pressure, angiocardiopathy, the health-care effect that suppresses atherosclerosis etc. are recognized by more and more people so that its into For the high-grade edible health products praised highly extensively.However, tea oil need further to develop in terms of external application value.Modern study Show, the oleic acid in tea oil is easily absorbed by the skin, salubrious oiliness after and to cell Yellow Gentian Extract, contained dimension in tea oil Raw plain E, squalene, Tea Polyphenols isoreactivity material have the effect of sterilization, moisturizing, skin care.Its Tea Saponin contained, smell are fragrant Virtue, with effects such as moistening, sterilizations.Therefore, develop the tea oil product of a variety of external applications, for widen tea oil application, It is significant to improve its economic value.
Traditional milling process is typically extracted oil using wooden crusher, and tea seed is crushed before squeezing, shells, steam at stir-fry Reason.Crushing process includes, by shelling camellia seeds, then crushing by pulverizer.Traditional steaming, which is fried, is divided into wet steaming stir-fry and dry blowing stir-fry, Typically fried preferably with wet steam, moisture and temperature are also because different and otherwise varied using mechanical type when steaming stir-fry.Traditional wooden crusher Although temperature requirement is relatively low, Tea Polyphenols in tea oil, squalene, general flavone, vitamin E isoreactivity material can be ensured not It is destroyed, but the oil yield of the technique is low, is not suitable for industrialization production.
CN102517141 discloses a kind of method for producing camellia oil, including drying and processing, heat treatment, squeezing hair Oil, filtering, washing, dry and cooling step, low temperature growing the grain, refined filtration.Wherein drying and processing is entered under the conditions of 75 DEG C of highest OK, the oil outlet temperature of crude oil is also controlled at 75 DEG C, 80-90 DEG C has been heated in deodorising step, in 90-95 after deodorization processing 1-2 hours are continued drying out at DEG C.Above-mentioned multistep high-temperature operation, most of active material of tea oil can be all caused to be destroyed, separately Outside, harmful substance can be also produced in deodorising process, such as trans acids and polymer, adverse effect is brought to human body.
A kind of method that CN103305334 discloses cold press and extraction technology stage extraction tea oil, this method use Organic solvent makes it remain grease and is extracted out to grouts powder contact, immersion or spray after crushing.But use Poisonous chemical reagent causes follow-up food and commodity potential potential safety hazard to be all present as solvent.
CN104277906 discloses low-temperature cold pressing camellia oil process for refining, is walked including depickling, decolouring, deodorization etc. Suddenly.Added in depickling step concentration be 10-12% sodium hydroxide, 1-3% decolorising agents are added in decolorization process, The use of these chemical reagent has not only broken up active material in tea oil, and generates chemical residue.
In summary, existing tea oil extraction process can all use a large amount of chemicals or by high-temperature process, no Active material in tea oil is only destroyed, and generates chemical residue.Therefore it is unfavorable for using it for external nursing, such as For hair-washing hair-care.
The content of the invention
In view of the shortcomings of the prior art, it is an object of the invention to provide the tea oil that a kind of low temperature is produced, it can retain Active material and natural plants delicate fragrance, quickly absorb and adjust secretion and male sex hormone releveling in vivo, the hair washing being made from it Breast can reach dandruff-removing itching-relieve, moisten the effect of hair care.
Specifically, the present invention provides a kind of method of tea oil leaves shampoo, comprise the steps of:
(1) preparation of tea oil is refined:Using the pressing method of low temperature, refine and obtain tea oil;
(2) preparation of tea oil leaves shampoo:By citric acid 10g, dodecyl polyoxy ethylene sulfate 100g, dodecyl Benzene sulfonic acid sodium salt 50g is fitted into container, and 1 hour is stirred at 50 DEG C to thawing;The refined tea oil of 10g steps (1) is added, fully Stirring, obtains viscous liquid;Cool down 24 hours, get product at room temperature.
(3) optionally, after natural cooling, 2-3g essence can be added, preferably is selected from vanillic aldehyde.
Preferably, the present invention provides a kind of preparation method of above-mentioned refined tea oil, comprises the steps of:
(1) cultivate:The tea seed kind of oil content more than 35% is filtered out, carries out scale organic farming, is tea oil Prepare and Organic Ingredients is provided;
(2) store:After tea seed naturally dry, low tempertaure storage is carried out under the conditions of 0-10 DEG C, prevents raw material from going bad;
(3) clear up:The first step removes the impurity in tea seed using manual method, and control impurity content is less than 5%;The Two steps continue to remove residual impurity using mechanical means, control the impurity content of raw material to be less than 1%;
(4) shelling is broken:Tea seed is obtained into tea seed kernel by mechanical exfoliation, then tea seed kernel carried out using disintegrating machine It is broken, control particle diameter 30-50 mesh;
(5) it is quenched:The pure water of 2-3% mass ratioes is added in above-mentioned oil plant;
(6) squeeze:Tea seed kernel is squeezed under the conditions of 35-40 DEG C, obtains just squeezing tea oil;
(7) filter:Tea oil filtering will be just squeezed, insoluble impurity is removed, obtains tea oil;
(8) wash:Pure water according to 1-2% mass ratioes is added in above-mentioned tea oil, and 5-10 is stirred at 25-30 DEG C Minute, remove impurity after staticly settling 1 hour;Repeat the step 2-3 times;
(9) crystallize:Crystal is cultivated under the conditions of 0-5 DEG C 48 hours, then raise temperature to 20-25 DEG C, produced after filtering The refined tea oil of finished product.
Embodiment
Below by way of specific embodiment, the above of the present invention is described in further details, but should not be by this It is interpreted as any restrictions to subject matter of the present invention.All technical schemes realized based on the above of the present invention are belonged to The scope of the present invention.
Embodiment 1 refines tea oil
The tea seed kind of oil content more than 35% is filtered out, the cultivation that organic farming base carries out scale is established, is The preparation of tea oil provides Organic Ingredients.By after the tea seed naturally dry for cultivating harvest, low tempertaure storage is carried out under the conditions of 5 DEG C, Prevent raw material from going bad.Before use, first removing most of impurity in tea seed using manual method, control impurity content is less than 5%;Then continue to remove residual impurity using mechanical means, control the impurity content of raw material to be less than 1%.Then, by tea seed Tea seed kernel is obtained by mechanical exfoliation, then tea seed kernel crushed using disintegrating machine, controls the mesh of particle diameter 40.According to mass ratio, 2% pure water is added in above-mentioned oil plant, squeezed under the conditions of 35 DEG C, obtains just squeezing tea oil.Tea oil mistake will just be squeezed Filter, removes insoluble impurity.Then wash:2% pure water is added according to mass ratio, is stirred 10 minutes at 30 DEG C, is stood Precipitation removes impurity after 1 hour;The water-washing step repeats 2 times.Crystal is finally cultivated under the conditions of 0 DEG C 48 hours, then heated up To 25 DEG C, the refined tea oil that is got product after filtering.
The refined tea oil of the present embodiment, there is fixed tea perfume, after testing, wherein moisture and volatile matter content content 0.01%, Insoluble impurity content≤0.01%, acid number (KOH)≤0.05mg/g, peroxide value≤0.5mmol/Kg.
The tea oil leaves shampoo of embodiment 2
According to following weight proportion:
The refined tea oil of embodiment 1:10g;
Citric acid:10g;
Dodecyl polyoxy ethylene sulfate:100g;
Neopelex:50g.
Citric acid, dodecyl polyoxy ethylene sulfate, neopelex are fitted into container, at 50 DEG C Stirring is extremely melted for 1 hour;Then the refined tea oil of embodiment 1 is added, is sufficiently stirred, obtains viscous liquid;Cool down at room temperature After 24 hours, 2g vanillic aldehydes are added, are got product.
Control group 1
Using commercially available leaves shampoo.
Control group 2
Using the tea oil of CN102517141 embodiments 1, according to the Recipe of the embodiment of the present invention 2, obtained tea oil is washed Hair-cream.
The tea oil leaves shampoo of the present invention and control group are compared, as a result shown:The tea oil leaves shampoo of the present invention, it is right Hair has the effect of anti-inflammation, dandruff-removing itching-relieve, nutrition are moistened, and also retains natural plants delicate fragrance.
The tea perfume degree of table 1 and moisture retention
Explanation:In above-mentioned table 1, +++ it is very good to represent effect;++ representative works well;+ representative has general effect;Zero generation Table does not have effect.Wherein what the time of table 1 represented is the interval time after each use.
Further, since tea oil of the present invention has the effect of dandruff-removing itching-relieve, nutrition moisten, thus can also directly act on Hair.Specific operation process is:After hair washing, take the refined tea oil of appropriate embodiment 1 to be applied on wet hair, wet give out a contract for a project is wrapped in 20-30 minutes, fully absorb it in hot towel, then naturally dry, without cleaning again.Adhere to using more than 1 year, as a result It has been shown that, hair is pitch-black beautiful, high resilience.

Claims (4)

1. a kind of preparation method of tea oil leaves shampoo for hair-washing hair-care, is comprised the following steps:
(1) preparation of tea oil is refined:Using the pressing method of low temperature, refine and obtain tea oil;
(2) preparation of tea oil leaves shampoo:By citric acid 10g, dodecyl polyoxy ethylene sulfate 100g, DBSA Sodium 50g is fitted into container, and 1 hour is stirred at 50 DEG C to thawing;The refined tea oil of 10g steps (1) is added, is sufficiently stirred, obtains To viscous liquid;Cool down 24 hours, get product at room temperature.
(3) optionally, after natural cooling, 2-3g essence, preferably vanillic aldehyde can be added.
2. producing the method for tea oil according to claim 1 low temperature, wherein the refined tea oil described in step (1) includes following preparation step Suddenly:
(1) cultivate:The tea seed kind of oil content more than 35% is filtered out, carries out scale organic farming, is the preparation of tea oil Organic Ingredients is provided;
(2) store:After tea seed naturally dry, low tempertaure storage is carried out under the conditions of 0-10 DEG C, prevents raw material from going bad;
(3) clear up:The first step removes the impurity in tea seed using manual method, and control impurity content is less than 5%;Second step is adopted Mechanically continue to remove residual impurity, control the impurity content of raw material to be less than 1%;
(4) shelling is broken:Tea seed is obtained into tea seed kernel by mechanical exfoliation, then tea seed kernel crushed using disintegrating machine, Control particle diameter 30-50 mesh;
(5) it is quenched:The pure water of 2-3% mass ratioes is added in above-mentioned oil plant;
(6) squeeze:Tea seed kernel is squeezed under the conditions of 35-40 DEG C, obtains just squeezing tea oil;
(7) filter:Tea oil filtering will be just squeezed, insoluble impurity is removed, obtains tea oil;
(8) wash:Pure water according to 1-2% mass ratioes is added in above-mentioned tea oil, and 5-10 minutes are stirred at 25-30 DEG C, Impurity is removed after staticly settling 1 hour;Repeat the step 2-3 times;
(9) crystallize:Crystal is cultivated under the conditions of 0-5 DEG C 48 hours, then raise temperature to 20-25 DEG C, got product after filtering Refined tea oil.
3. a kind of method for being used to defend the doctrine by tea oil, comprises the following steps:After hair washing, appropriate refined tea oil is taken to be applied to wet hair On, by 20-30 minutes in the wet excessively hot towel of hair, fully absorb it, then naturally dry, without cleaning again.
4. method according to claim 3, it is characterised in that:Described refined tea oil is preparation side according to claim 2 Method is prepared.
CN201711018527.7A 2017-10-27 2017-10-27 A kind of tea oil for being used to take care of hair Pending CN107789224A (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102517141A (en) * 2011-12-16 2012-06-27 湖北四季春茶油有限公司 Method for purely physically preparing camellia oil at low temperature
CN102952626A (en) * 2012-11-06 2013-03-06 安徽新世界绿洲茶油有限公司 Preparation process of cold-pressed tea seed oil
CN103305334A (en) * 2012-03-14 2013-09-18 湖南湘纯农业科技有限公司 Method for extracting tea oil by cold pressing and solvent leaching technique in stages
CN103860428A (en) * 2014-03-11 2014-06-18 安徽亿宏生物科技有限公司 Tea oil shampoo and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102517141A (en) * 2011-12-16 2012-06-27 湖北四季春茶油有限公司 Method for purely physically preparing camellia oil at low temperature
CN103305334A (en) * 2012-03-14 2013-09-18 湖南湘纯农业科技有限公司 Method for extracting tea oil by cold pressing and solvent leaching technique in stages
CN102952626A (en) * 2012-11-06 2013-03-06 安徽新世界绿洲茶油有限公司 Preparation process of cold-pressed tea seed oil
CN103860428A (en) * 2014-03-11 2014-06-18 安徽亿宏生物科技有限公司 Tea oil shampoo and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
松田有利子: "《天然食物治百病》", 30 September 2000 *

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