CN107785245A - One kind improves conversion efficiency of solar cell diffusion method - Google Patents
One kind improves conversion efficiency of solar cell diffusion method Download PDFInfo
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- CN107785245A CN107785245A CN201610760645.4A CN201610760645A CN107785245A CN 107785245 A CN107785245 A CN 107785245A CN 201610760645 A CN201610760645 A CN 201610760645A CN 107785245 A CN107785245 A CN 107785245A
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- 238000009792 diffusion process Methods 0.000 title claims abstract description 42
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 13
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 188
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 94
- 230000003647 oxidation Effects 0.000 claims abstract description 21
- 238000007254 oxidation reaction Methods 0.000 claims abstract description 21
- 238000012545 processing Methods 0.000 claims abstract description 16
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 46
- 239000001301 oxygen Substances 0.000 claims description 46
- 229910052760 oxygen Inorganic materials 0.000 claims description 46
- XHXFXVLFKHQFAL-UHFFFAOYSA-N phosphoryl trichloride Chemical compound ClP(Cl)(Cl)=O XHXFXVLFKHQFAL-UHFFFAOYSA-N 0.000 claims description 18
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 13
- 229910052710 silicon Inorganic materials 0.000 claims description 13
- 239000010703 silicon Substances 0.000 claims description 13
- 239000007789 gas Substances 0.000 claims description 12
- 229910019213 POCl3 Inorganic materials 0.000 claims description 6
- 238000000034 method Methods 0.000 abstract description 9
- 238000005215 recombination Methods 0.000 abstract description 3
- 230000006798 recombination Effects 0.000 abstract description 3
- 150000001875 compounds Chemical class 0.000 abstract description 2
- 230000008021 deposition Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- -1 after pyrolytic Chemical compound 0.000 description 1
- 230000000747 cardiac effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000005137 deposition process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910021421 monocrystalline silicon Inorganic materials 0.000 description 1
- 125000004437 phosphorous atom Chemical group 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/04—Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer
- H01L21/18—Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer the devices having semiconductor bodies comprising elements of Group IV of the Periodic Table or AIIIBV compounds with or without impurities, e.g. doping materials
- H01L21/22—Diffusion of impurity materials, e.g. doping materials, electrode materials, into or out of a semiconductor body, or between semiconductor regions; Interactions between two or more impurities; Redistribution of impurities
- H01L21/223—Diffusion of impurity materials, e.g. doping materials, electrode materials, into or out of a semiconductor body, or between semiconductor regions; Interactions between two or more impurities; Redistribution of impurities using diffusion into or out of a solid from or into a gaseous phase
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/02104—Forming layers
- H01L21/02107—Forming insulating materials on a substrate
- H01L21/02109—Forming insulating materials on a substrate characterised by the type of layer, e.g. type of material, porous/non-porous, pre-cursors, mixtures or laminates
- H01L21/02112—Forming insulating materials on a substrate characterised by the type of layer, e.g. type of material, porous/non-porous, pre-cursors, mixtures or laminates characterised by the material of the layer
- H01L21/02123—Forming insulating materials on a substrate characterised by the type of layer, e.g. type of material, porous/non-porous, pre-cursors, mixtures or laminates characterised by the material of the layer the material containing silicon
- H01L21/02164—Forming insulating materials on a substrate characterised by the type of layer, e.g. type of material, porous/non-porous, pre-cursors, mixtures or laminates characterised by the material of the layer the material containing silicon the material being a silicon oxide, e.g. SiO2
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/02104—Forming layers
- H01L21/02107—Forming insulating materials on a substrate
- H01L21/02225—Forming insulating materials on a substrate characterised by the process for the formation of the insulating layer
- H01L21/02227—Forming insulating materials on a substrate characterised by the process for the formation of the insulating layer formation by a process other than a deposition process
- H01L21/0223—Forming insulating materials on a substrate characterised by the process for the formation of the insulating layer formation by a process other than a deposition process formation by oxidation, e.g. oxidation of the substrate
- H01L21/02233—Forming insulating materials on a substrate characterised by the process for the formation of the insulating layer formation by a process other than a deposition process formation by oxidation, e.g. oxidation of the substrate of the semiconductor substrate or a semiconductor layer
- H01L21/02236—Forming insulating materials on a substrate characterised by the process for the formation of the insulating layer formation by a process other than a deposition process formation by oxidation, e.g. oxidation of the substrate of the semiconductor substrate or a semiconductor layer group IV semiconductor
- H01L21/02238—Forming insulating materials on a substrate characterised by the process for the formation of the insulating layer formation by a process other than a deposition process formation by oxidation, e.g. oxidation of the substrate of the semiconductor substrate or a semiconductor layer group IV semiconductor silicon in uncombined form, i.e. pure silicon
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- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Manufacturing & Machinery (AREA)
- Computer Hardware Design (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Power Engineering (AREA)
- Formation Of Insulating Films (AREA)
Abstract
The present invention relates to one kind to improve conversion efficiency of solar cell diffusion method, belongs to area of solar cell.It has quartzy stove preheating, pre-oxidation treatment, prediffusion processing, continue DIFFUSION TREATMENT, whole DIFFUSION TREATMENT and rear oxidation handle 6 steps, wherein prediffusion processing, the intake for continuing small nitrogen in DIFFUSION TREATMENT and whole DIFFUSION TREATMENT taper off trend.The present invention is advantageous in that:It is a kind of with TongYuan's degression type and constant temperature incrementally compound diffusion technique, under the premise of suitable Ohmic contact is ensured, surface recombination can be reduced, improve internal doping concentration, space-charge region performance is improved, reaches good Ohmic contact and recombination-rate surface, so as to improve battery conversion efficiency.
Description
Technical field:
The present invention relates to one kind to improve conversion efficiency of solar cell diffusion method, belongs to area of solar cell.
Background technology:
Diffusing procedure is the core process of solar cell manufacturing process, and it to diffusion Quartz stove tube mainly by leading to POCL3
And oxygen, after pyrolytic, P2O5 and SI is produced, under p-type substrate, PN is formd by the diffusional deposition process of phosphorus atoms
Knot, that is, the cardiac component of solar cell, traditional diffusion technique are mainly that constant temperature Heng Yuan spreads, basic diffusing step
Or pass through:Oxidation, pre-deposition, deposition, diffusion etc..Although so sheet resistance has relatively stable, its surface recombination is dense
Spend higher, increase its recombination-rate surface(SRV), in addition, junction depth also can be partially deep, may can have been helped for open-circuit voltage Voc
Help, but can be poor for short-wave band response, influence its short circuit current(Isc), finally influence battery conversion efficiency(Eff).
The content of the invention:
For above technical problem, it is of the present invention it is a kind of improve conversion efficiency of solar cell diffusion method, have with
Lower step:
Step 1, the preheating of quartzy stove
Silicon chip is put into quartzy stove, is passed through big nitrogen, the flow of big nitrogen is 15500-16500sccm, then by the stove of quartzy stove
Temperature rise keeps 650-750s to 800-820 DEG C;
Step 2, pre-oxidation treatment
Oxygen and big nitrogen are passed through quartzy stove, wherein oxygen flow is 1800-2100sccm, and big nitrogen flow is 14700-
15000sccm, it is passed through time control and is maintained at 800-820 DEG C in 450-500s, furnace temperature, complete the pre-oxidation to silicon chip;
Step 3, prediffusion processing
The mixed gas of the small nitrogen for taking POCl3, big nitrogen and oxygen composition, the flow of its medium and small nitrogen are passed through into quartzy stove
For 850-950sccm, the flow of big nitrogen is 14000-14500sccm, and the flow of oxygen is 700-800sccm, is passed through the time and is
550-650s, furnace temperature are maintained at 800-820 DEG C, complete prediffusion processing;
Step 4, continue DIFFUSION TREATMENT
Big nitrogen is passed through flow 15500-16500sccm, while furnace temperature is gradually increased into 810-830 DEG C, keeps 300-400s, then
The mixed gas that the small nitrogen, big nitrogen and oxygen of taking POCl3 form is passed through quartzy stove, the flow of wherein its medium and small nitrogen is
750-850sccm, the flow of big nitrogen is 14500-15000sccm, and the flow of oxygen is 600-700sccm, is passed through the time and is
450-500s, furnace temperature are maintained at 810-830 DEG C, complete to continue DIFFUSION TREATMENT;
Step 5, whole DIFFUSION TREATMENT
Big nitrogen is passed through flow 15500-16500sccm, while furnace temperature is gradually increased into 817-837 DEG C, keeps 300-400s, then
The mixed gas that the small nitrogen, big nitrogen and oxygen of taking POCl3 form is passed through quartzy stove, the flow of wherein its medium and small nitrogen is
650-750sccm, the flow of big nitrogen is 14600-15100sccm, and the flow of oxygen is 500-600sccm, is passed through the time and is
350-400s, furnace temperature are maintained at 817-837 DEG C, complete to continue DIFFUSION TREATMENT;
Step 6, rear oxidation is handled
To treat that furnace temperature is down at 700-750 DEG C, oxygen and big nitrogen are passed through quartzy stove, wherein oxygen flow is 800-1500sccm,
Big nitrogen flow is 14800-15200sccm, is passed through time control in 350-400s, completes the pre-oxidation to silicon chip.
Preferably, the intake of small nitrogen tapers off in the prediffusion processing, continuation DIFFUSION TREATMENT and whole DIFFUSION TREATMENT
Trend.
Compared with prior art, usefulness of the present invention is;It is a kind of incrementally compound with constant temperature with TongYuan's degression type
Diffusion technique, under the premise of suitable Ohmic contact is ensured, surface recombination can be reduced, improve internal doping concentration, improve space
Charged region performance, reach good Ohmic contact and recombination-rate surface, so as to improve battery conversion efficiency.
Embodiment:
A kind of raising conversion efficiency of solar cell diffusion method of the present invention, has steps of:
Step 1, the preheating of quartzy stove
Silicon chip is put into quartzy stove, is passed through big nitrogen, the flow of big nitrogen is 15500-16500sccm, then by the stove of quartzy stove
Temperature rise keeps 650-750s to 800-820 DEG C;
Step 2, pre-oxidation treatment
Oxygen and big nitrogen are passed through quartzy stove, wherein oxygen flow is 1800-2100sccm, and big nitrogen flow is 14700-
15000sccm, it is passed through time control and is maintained at 800-820 DEG C in 450-500s, furnace temperature, complete the pre-oxidation to silicon chip;
Step 3, prediffusion processing
The mixed gas of the small nitrogen for taking POCl3, big nitrogen and oxygen composition, the flow of its medium and small nitrogen are passed through into quartzy stove
For 850-950sccm, the flow of big nitrogen is 14000-14500sccm, and the flow of oxygen is 700-800sccm, is passed through the time and is
550-650s, furnace temperature are maintained at 800-820 DEG C, complete prediffusion processing;
Step 4, continue DIFFUSION TREATMENT
Big nitrogen is passed through flow 15500-16500sccm, while furnace temperature is gradually increased into 810-830 DEG C, keeps 300-400s, then
The mixed gas that the small nitrogen, big nitrogen and oxygen of taking POCl3 form is passed through quartzy stove, the flow of wherein its medium and small nitrogen is
750-850sccm, the flow of big nitrogen is 14500-15000sccm, and the flow of oxygen is 600-700sccm, is passed through the time and is
450-500s, furnace temperature are maintained at 810-830 DEG C, complete to continue DIFFUSION TREATMENT;
Step 5, whole DIFFUSION TREATMENT
Big nitrogen is passed through flow 15500-16500sccm, while furnace temperature is gradually increased into 817-837 DEG C, keeps 300-400s, then
The mixed gas that the small nitrogen, big nitrogen and oxygen of taking POCl3 form is passed through quartzy stove, the flow of wherein its medium and small nitrogen is
650-750sccm, the flow of big nitrogen is 14600-15100sccm, and the flow of oxygen is 500-600sccm, is passed through the time and is
350-400s, furnace temperature are maintained at 817-837 DEG C, complete to continue DIFFUSION TREATMENT;
Step 6, rear oxidation is handled
To treat that furnace temperature is down at 700-750 DEG C, oxygen and big nitrogen are passed through quartzy stove, wherein oxygen flow is 800-1500sccm,
Big nitrogen flow is 14800-15200sccm, is passed through time control in 350-400s, completes the rear oxidation to silicon chip.
In order to further show the Spirit Essence of the present invention, it is described further with reference to embodiment:
Using raw material, thickness is 200 ± 20um, resistivity 0.5-6W.cm, by surface clean for P type monocrystalline silicon pieces
With the processing of, surface-texturing, 1-3nm positive pyramid matte is formed on surface, silicon chip is put into and expanded in quartzy stove.
Step 1, the preheating of quartzy stove
Silicon chip is put into quartzy stove, is passed through big nitrogen, the flow of big nitrogen is 16000sccm, then rises to the furnace temperature of quartzy stove
800 DEG C, keep 705s;
Step 2, pre-oxidation treatment
Oxygen and big nitrogen are passed through quartzy stove, wherein oxygen flow is 2000sccm, and big nitrogen flow is 14800sccm, when being passed through
Between control in 480s, furnace temperature is maintained at 800 DEG C, completes the pre-oxidation to silicon chip;
Step 3, prediffusion processing
The mixed gas of the small nitrogen for taking POCl3, big nitrogen and oxygen composition, the flow of its medium and small nitrogen are passed through into quartzy stove
For 900sccm, the flow of big nitrogen is 14350sccm, and the flow of oxygen is 750sccm, and it is 600s to be passed through the time, and furnace temperature is maintained at
800 DEG C, complete prediffusion processing;
Step 4, continue DIFFUSION TREATMENT
Big nitrogen is passed through flow 16000sccm, while furnace temperature is gradually increased into 820 DEG C, keeps 360s, then will take POCl3
The mixed gas of small nitrogen, big nitrogen and oxygen composition is passed through quartzy stove, and the wherein flow of its medium and small nitrogen is 800sccm, big nitrogen
Flow is 14550sccm, and the flow of oxygen is 650sccm, and it is 480s to be passed through the time, and furnace temperature is maintained at 820 DEG C, and completion continues to expand
Dissipate processing;
Step 5, whole DIFFUSION TREATMENT
Big nitrogen is passed through flow 16000sccm, while furnace temperature is gradually increased into 827 DEG C, keeps 360s, then will take POCl3
The mixed gas of small nitrogen, big nitrogen and oxygen composition is passed through quartzy stove, and the wherein flow of its medium and small nitrogen is 700sccm, big nitrogen
Flow is 14750sccm, and the flow of oxygen is 550sccm, and it is 360s to be passed through the time, and furnace temperature is maintained at 827 DEG C, and completion continues to expand
Dissipate processing;
Step 6, rear oxidation is handled
Treat that furnace temperature is down at 720 DEG C, oxygen and big nitrogen are passed through quartzy stove, wherein oxygen flow is 1000sccm, big nitrogen flow
For 15000sccm, time control is passed through in 360s, completes the rear oxidation to silicon chip.
Conventional method compares such as following table with the parameter of solar cell made of the inventive method:
Experiment condition | Open-circuit voltage (U) | Short circuit current (Isc) | Fill factor, curve factor (FF) | Series resistance (Rs) | Parallel resistance (Rsh) | Battery conversion efficiency (EFF) | Reverse current (Irev2) |
Gradient method diffusion technique | 0.635 | 8.9 | 79.31 | 0.0022 | 95 | 18.41% | 0.251 |
Normal diffusion technique | 0.635 | 8.83 | 79.53 | 0.0021 | 130.2 | 18.26% | 0.156 |
Need to be stressed that:It the above is only the introduction and description of the occupation mode of the present invention, not make any shape to the present invention
Limitation in formula, any simple modification that every technical spirit according to the present invention is made to above example, equivalent variations with
Modification, in the range of still falling within technical solution of the present invention.
Claims (3)
1. one kind improves conversion efficiency of solar cell diffusion method, it is characterised in that has steps of:
Step 1, the preheating of quartzy stove
Silicon chip is put into quartzy stove, is passed through big nitrogen, the flow of big nitrogen is 15500-16500sccm, then by the stove of quartzy stove
Temperature rise keeps 650-750s to 800-820 DEG C;
Step 2, pre-oxidation treatment
Oxygen and big nitrogen are passed through quartzy stove, wherein oxygen flow is 1800-2100sccm, and big nitrogen flow is 14700-
15000sccm, it is passed through time control and is maintained at 800-820 DEG C in 450-500s, furnace temperature, complete the pre-oxidation to silicon chip;
Step 3, prediffusion processing
The mixed gas of the small nitrogen for taking POCl3, big nitrogen and oxygen composition, the flow of its medium and small nitrogen are passed through into quartzy stove
For 850-950sccm, the flow of big nitrogen is 14000-14500sccm, and the flow of oxygen is 700-800sccm, is passed through the time and is
550-650s, furnace temperature are maintained at 800-820 DEG C, complete prediffusion processing;
Step 4, continue DIFFUSION TREATMENT
Big nitrogen is passed through flow 15500-16500sccm, while furnace temperature is gradually increased into 810-830 DEG C, keeps 300-400s, then
The mixed gas that the small nitrogen, big nitrogen and oxygen of taking POCl3 form is passed through quartzy stove, the flow of wherein its medium and small nitrogen is
750-850sccm, the flow of big nitrogen is 14500-15000sccm, and the flow of oxygen is 600-700sccm, is passed through the time and is
450-500s, furnace temperature are maintained at 810-830 DEG C, complete to continue DIFFUSION TREATMENT;
Step 5, whole DIFFUSION TREATMENT
Big nitrogen is passed through flow 15500-16500sccm, while furnace temperature is gradually increased into 817-837 DEG C, keeps 300-400s, then
The mixed gas that the small nitrogen, big nitrogen and oxygen of taking POCl3 form is passed through quartzy stove, the flow of wherein its medium and small nitrogen is
650-750sccm, the flow of big nitrogen is 14600-15100sccm, and the flow of oxygen is 500-600sccm, is passed through the time and is
350-400s, furnace temperature are maintained at 817-837 DEG C, complete to continue DIFFUSION TREATMENT;
Step 6, rear oxidation is handled
To treat that furnace temperature is down at 700-750 DEG C, oxygen and big nitrogen are passed through quartzy stove, wherein oxygen flow is 800-1500sccm,
Big nitrogen flow is 14800-15200sccm, is passed through time control in 350-400s, completes the pre-oxidation to silicon chip.
A kind of 2. raising conversion efficiency of solar cell diffusion method according to claim 1, it is characterised in that:It is described
Prediffusion processing, the intake for continuing small nitrogen in DIFFUSION TREATMENT and whole DIFFUSION TREATMENT taper off trend.
3. a kind of raising conversion efficiency of solar cell diffusion method according to claim 1, it is characterised in that each
The technological parameter of step is as follows:
Step 1, the preheating of quartzy stove
The flow of big nitrogen is 16000sccm, and the furnace temperature of quartzy stove then is risen into 800 DEG C, keeps 705s;
Step 2, pre-oxidation treatment
Oxygen flow is 2000sccm, and big nitrogen flow is 14800sccm, is passed through time control and is maintained at 800 in 480s, furnace temperature
℃;
Step 3, prediffusion processing
The flow of small nitrogen is 900sccm, and the flow of big nitrogen is 14350sccm, and the flow of oxygen is 750sccm, is passed through the time and is
600s, furnace temperature are maintained at 800-820 DEG C;
Step 4, continue DIFFUSION TREATMENT
Furnace temperature ascent stage, big nitrogen is passed through flow 16000sccm, while furnace temperature is gradually increased into 820 DEG C, keeps 360s, diffusion
In the stage, the flow of small nitrogen is 800sccm, and the flow of big nitrogen is 14550sccm, and the flow of oxygen is 650sccm, is passed through the time and is
480s, furnace temperature are maintained at 820 DEG C;
Step 5, whole DIFFUSION TREATMENT
Furnace temperature ascent stage, big nitrogen is passed through flow 16000sccm, while furnace temperature is gradually increased into 827 DEG C, keeps 360s, diffusion
In the stage, the flow of small nitrogen is 700sccm, and the flow of big nitrogen is 14750sccm, and the flow of oxygen is 550sccm, is passed through the time and is
360s, furnace temperature are maintained at 827 DEG C;
Step 6, rear oxidation is handled
Oxygen flow is 1000sccm, and big nitrogen flow is 15000sccm, is passed through time control in 360s.
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Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102723266A (en) * | 2012-06-19 | 2012-10-10 | 江苏泓源光电科技有限公司 | Solar battery diffusion method |
CN104716232A (en) * | 2015-03-13 | 2015-06-17 | 中节能太阳能科技(镇江)有限公司 | Solar cell emitter doping distribution method |
CN105280755A (en) * | 2015-09-17 | 2016-01-27 | 江西展宇新能源股份有限公司 | Thrice continuous deposition and heating diffusion technology |
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2016
- 2016-08-31 CN CN201610760645.4A patent/CN107785245A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102723266A (en) * | 2012-06-19 | 2012-10-10 | 江苏泓源光电科技有限公司 | Solar battery diffusion method |
CN104716232A (en) * | 2015-03-13 | 2015-06-17 | 中节能太阳能科技(镇江)有限公司 | Solar cell emitter doping distribution method |
CN105280755A (en) * | 2015-09-17 | 2016-01-27 | 江西展宇新能源股份有限公司 | Thrice continuous deposition and heating diffusion technology |
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Application publication date: 20180309 |